Crystallography Open Database

Information card for entry 1571731

Preview

Coordinates	1571731.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H73 Os4 Th
Calculated formula	C46 H73 Os4 Th
Title of publication	Photolysis-driven bond activation by thorium and uranium tetraosmate polyhydride complexes.
Authors of publication	Ye, Christopher Z.; Del Rosal, Iker; Kelly, Sheridon N.; Brackbill, I. Joseph; Maron, Laurent; Camp, Clément; Arnold, John
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	25
Pages of publication	9784 - 9792
a	18.6052 ± 0.0005 Å
b	9.9998 ± 0.0003 Å
c	13.383 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	2489.88 ± 0.12 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	4
Space group number	31
Hermann-Mauguin space group symbol	P m n 21
Hall space group symbol	P 2ac -2
Residual factor for all reflections	0.0247
Residual factor for significantly intense reflections	0.0216
Weighted residual factors for significantly intense reflections	0.0463
Weighted residual factors for all reflections included in the refinement	0.047
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
292895 (current)	2024-07-05	cif/ Updating files of 1571730, 1571731, 1571732, 1571733, 1571734 Original log message: Adding full bibliography for 1571730--1571734.cif.	1571731.cif
292131	2024-06-01	cif/ Adding structures of 1571730, 1571731, 1571732, 1571733, 1571734 via cif-deposit CGI script.	1571731.cif