Crystallography Open Database

Information card for entry 1571730

Preview

Coordinates	1571730.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H60 Os4 Th
Calculated formula	C40 H60 Os4 Th
Title of publication	Photolysis-driven bond activation by thorium and uranium tetraosmate polyhydride complexes.
Authors of publication	Ye, Christopher Z.; Del Rosal, Iker; Kelly, Sheridon N.; Brackbill, I. Joseph; Maron, Laurent; Camp, Clément; Arnold, John
Journal of publication	Chemical science
Year of publication	2024
Journal volume	15
Journal issue	25
Pages of publication	9784 - 9792
a	23.163 ± 0.002 Å
b	12.6413 ± 0.0011 Å
c	15.781 ± 0.0013 Å
α	90°
β	91.796 ± 0.003°
γ	90°
Cell volume	4618.6 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0521
Residual factor for significantly intense reflections	0.0387
Weighted residual factors for significantly intense reflections	0.0801
Weighted residual factors for all reflections included in the refinement	0.0862
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.7288 Å
Diffraction radiation type	synchrotron
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
292895 (current)	2024-07-05	cif/ Updating files of 1571730, 1571731, 1571732, 1571733, 1571734 Original log message: Adding full bibliography for 1571730--1571734.cif.	1571730.cif
292131	2024-06-01	cif/ Adding structures of 1571730, 1571731, 1571732, 1571733, 1571734 via cif-deposit CGI script.	1571730.cif