Crystallography Open Database

Information card for entry 7716707

Preview

Coordinates	7716707.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C88 H148 K2 O12 S2 U2
Calculated formula	C88 H148 K2 O12 S2 U2
Title of publication	Synthesis, structure and redox properties of single-atom bridged diuranium complexes supported by aryloxides.
Authors of publication	Hsueh, Fang-Che; Barluzzi, Luciano; Rajeshkumar, Thayalan; Scopelliti, Rosario; Zivkovic, Ivica; Maron, Laurent; Mazzanti, Marinella
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2024
Journal volume	53
Journal issue	32
Pages of publication	13416 - 13426
a	13.70485 ± 0.00013 Å
b	14.20424 ± 0.00013 Å
c	15.06289 ± 0.00017 Å
α	93.7454 ± 0.0009°
β	113.924 ± 0.001°
γ	98.2448 ± 0.0008°
Cell volume	2627.79 ± 0.05 Å³
Cell temperature	139.99 ± 0.1 K
Ambient diffraction temperature	139.99 ± 0.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0258
Residual factor for significantly intense reflections	0.0236
Weighted residual factors for significantly intense reflections	0.0605
Weighted residual factors for all reflections included in the refinement	0.0631
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
294536 (current)	2024-09-06	cif/ Updating files of 7716706, 7716707, 7716708, 7716709, 7716710 Original log message: Adding full bibliography for 7716706--7716710.cif.	7716707.cif
293513	2024-07-24	cif/ Adding structures of 7716706, 7716707, 7716708, 7716709, 7716710 via cif-deposit CGI script.	7716707.cif