#------------------------------------------------------------------------------ #$Date: 2025-06-14 02:42:54 +0300 (Sat, 14 Jun 2025) $ #$Revision: 300082 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/25/05/7250559.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7250559 loop_ _publ_author_name 'Gu, Jiayi' 'Xin, Meixiu' 'Cheng, Zhuo' 'Zou, Zhiru' 'Du, Zhibo' 'Cheng, Xinyi' 'Wang, Yan' 'Zou, Yong' _publ_section_title ; Anti-Markovnikov Hydrosulfenylation of Unactivated Alkenes/Alkynes via Visible Light Organic Photocatalysis ; _journal_name_full 'Green Chemistry' _journal_paper_doi 10.1039/D5GC02604K _journal_year 2025 _chemical_formula_moiety 'C15 H15 Cl O S' _chemical_formula_sum 'C15 H15 Cl O S' _chemical_formula_weight 278.78 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-12-31 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _audit_update_record ; 2025-01-14 deposited with the CCDC. 2025-06-11 downloaded from the CCDC. ; _cell_angle_alpha 76.4892(19) _cell_angle_beta 82.2856(18) _cell_angle_gamma 71.4025(19) _cell_formula_units_Z 4 _cell_length_a 9.2974(2) _cell_length_b 10.0625(2) _cell_length_c 15.8641(4) _cell_measurement_reflns_used 12123 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 75.2610 _cell_measurement_theta_min 2.8380 _cell_volume 1364.86(6) _computing_cell_refinement 'CrysAlisPro 1.171.43.136a (Rigaku OD, 2024)' _computing_data_collection 'CrysAlisPro 1.171.43.136a (Rigaku OD, 2024)' _computing_data_reduction 'CrysAlisPro 1.171.43.136a (Rigaku OD, 2024)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.961 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -69.00 -27.00 0.50 0.05 -- -100.00 61.00 120.00 84 2 \w -67.00 -29.00 0.50 0.05 -- -100.00 61.00 90.00 76 3 \w -62.00 -33.00 0.50 0.05 -- -100.00 61.00 60.00 58 4 \w -68.00 -28.00 0.50 0.05 -- -100.00 61.00 30.00 80 5 \w -28.00 25.00 0.50 0.05 -- -45.64 19.00 60.00 106 6 \w -28.00 32.00 0.50 0.05 -- -45.64 19.00-120.00 120 7 \w 55.00 80.00 0.50 0.05 -- 45.64-162.00-142.00 50 8 \w 102.00 137.00 0.50 0.05 -- 105.05-162.00-142.00 70 9 \w 82.00 112.00 0.50 0.05 -- 105.05-125.00 -90.00 60 10 \w 43.00 73.00 0.50 0.05 -- 105.05-125.00 -90.00 60 11 \w 60.00 112.00 0.50 0.05 -- 105.05-125.00 -30.00 104 12 \w 70.00 109.00 0.50 0.05 -- 105.05-117.00 7.00 78 13 \w 68.00 108.00 0.50 0.05 -- 105.05-106.00 34.70 80 14 \w 32.00 76.00 0.50 0.05 -- 105.05 -94.00 -90.00 88 15 \w 46.00 80.00 0.50 0.05 -- 105.05 -94.00-150.00 68 16 \w 13.00 58.00 0.50 0.05 -- 45.64-117.00 7.00 90 17 \w 39.00 65.00 0.50 0.05 -- 105.05 -77.00 120.00 52 18 \w 32.00 70.00 0.50 0.05 -- 105.05 -61.00 120.00 76 19 \w 36.00 61.00 0.50 0.05 -- 105.05 -61.00 150.00 50 20 \w 68.00 93.00 0.50 0.05 -- 105.05 -77.00 120.00 50 21 \w 32.00 72.00 0.50 0.05 -- 105.05 -61.00 -30.00 80 22 \w 48.00 81.00 0.50 0.05 -- 105.05 -77.00-150.00 66 23 \w 107.00 141.00 0.50 0.05 -- 105.05 117.00 94.00 68 24 \w 89.00 174.00 0.50 0.05 -- 105.05 45.00 90.00 170 25 \w 55.00 118.00 0.50 0.05 -- 45.64 162.00-115.00 126 26 \w 81.00 106.00 0.50 0.05 -- 105.05 162.00-115.00 50 27 \w 96.00 169.00 0.50 0.05 -- 105.05 30.00-180.00 146 28 \w 58.00 119.00 0.50 0.05 -- 45.64 57.00-120.00 122 29 \w -117.00 -23.00 0.50 0.05 -- -45.64 -77.00 -60.00 188 30 \w -112.00 -80.00 0.50 0.05 -- -100.00 -15.00-180.00 64 31 \w -175.00-128.00 0.50 0.05 -- -100.00 -15.00-180.00 94 32 \w -148.00 -84.00 0.50 0.05 -- -100.00 -45.00 -90.00 128 33 \w -135.00-109.00 0.50 0.05 -- -100.00 -30.00 60.00 52 34 \w -175.00-138.00 0.50 0.05 -- -100.00 -30.00 60.00 74 35 \w -152.00-108.00 0.50 0.05 -- -100.00-117.00 7.00 88 36 \w -105.00 -75.00 0.50 0.05 -- -45.64-162.00-142.00 60 37 \w -127.00-102.00 0.50 0.05 -- -100.00-162.00-142.00 50 38 \w -114.00 -76.00 0.50 0.05 -- -100.00-125.00 60.00 76 39 \w -169.00-126.00 0.50 0.05 -- -100.00-125.00 60.00 86 40 \w -81.00 -15.00 0.50 0.05 -- -45.64 117.00 94.00 132 41 \w -86.00 -61.00 0.50 0.05 -- -100.00 117.00 94.00 50 42 \w -111.00 -70.00 0.50 0.05 -- -100.00 125.00 30.00 82 43 \w -102.00 -74.00 0.50 0.05 -- -45.64 162.00-115.00 56 44 \w -104.00 -50.00 0.50 0.05 -- -100.00 162.00-115.00 108 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0848716000 _diffrn_orient_matrix_UB_12 0.0411935000 _diffrn_orient_matrix_UB_13 0.0621051000 _diffrn_orient_matrix_UB_21 -0.0563942000 _diffrn_orient_matrix_UB_22 -0.0999577000 _diffrn_orient_matrix_UB_23 0.0771464000 _diffrn_orient_matrix_UB_31 0.1425142000 _diffrn_orient_matrix_UB_32 -0.1246130000 _diffrn_orient_matrix_UB_33 -0.0144319000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0416 _diffrn_reflns_av_unetI/netI 0.0368 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.961 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 17258 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.961 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 75.481 _diffrn_reflns_theta_min 2.871 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 3.773 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.75955 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.43.136a (Rigaku Oxford Diffraction, 2024) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.357 _exptl_crystal_description block _exptl_crystal_F_000 584 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.433 _refine_diff_density_min -0.479 _refine_diff_density_rms 0.070 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.085 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 325 _refine_ls_number_reflns 5444 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.085 _refine_ls_R_factor_all 0.0438 _refine_ls_R_factor_gt 0.0417 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0806P)^2^+0.2139P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1215 _refine_ls_wR_factor_ref 0.1235 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4993 _reflns_number_total 5444 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d5gc02604k2.cif _cod_data_source_block gujy_a_241224_auto _cod_original_cell_volume 1364.85(5) _cod_database_code 7250559 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula CHOSCl _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.660 _shelx_estimated_absorpt_t_min 0.519 _reflns_odcompleteness_completeness 99.90 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2.a Secondary CH2 refined with riding coordinates: C22(H22A,H22B), C23(H23A,H23B), C24(H24A,H24B), C8(H8A,H8B), C9(H9A,H9B), C7(H7A,H7B) 2.b Aromatic/amide H refined with riding coordinates: C16(H16), C20(H20), C30(H30), C5(H5), C15(H15), C19(H19), C26(H26), C17(H17), C4(H4), C27(H27), C29(H29), C14(H14), C1(H1), C3(H3), C18(H18), C2(H2), C11(H11), C12(H12) ; _shelx_res_file ; TITL gujy_a_241224_auto_a.res in P-1 gujy_a_241224_auto.res created by SHELXL-2018/3 at 14:51:16 on 31-Dec-2024 REM Old TITL gujy_a_241224_auto in P-1 REM SHELXT solution in P-1: R1 0.124, Rweak 0.004, Alpha 0.044 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C6 O1 Cl4 CELL 1.54184 9.297357 10.062488 15.864079 76.4892 82.2856 71.4025 ZERR 4 0.000204 0.000214 0.000352 0.0019 0.0018 0.0019 LATT 1 SFAC C H Cl O S UNIT 60 60 4 4 4 L.S. 4 PLAN 7 SIZE 0.12 0.15 0.2 TEMP -173 CONF BOND MORE -1 BOND $H fmap 2 acta htab REM REM REM WGHT 0.080600 0.213900 FVAR 0.61540 S2 5 0.458950 0.927269 0.387100 11.00000 0.01765 0.01891 = 0.01856 -0.00732 -0.00365 -0.00333 S1 5 0.958981 0.393958 0.406224 11.00000 0.02500 0.02078 = 0.01864 -0.00727 -0.00241 -0.00493 CL2 3 0.395993 0.865095 0.010975 11.00000 0.04702 0.03850 = 0.01568 -0.00387 -0.00695 -0.01855 CL1 3 0.902012 0.362566 0.022112 11.00000 0.05027 0.04283 = 0.01749 -0.00406 -0.00822 -0.02166 O2 4 0.303806 1.009229 0.418198 11.00000 0.02033 0.02253 = 0.02453 -0.01031 -0.00136 -0.00025 O1 4 0.811768 0.492249 0.434089 11.00000 0.04066 0.02418 = 0.02514 -0.00901 0.00049 0.00712 C25 1 0.439866 0.896151 0.282816 11.00000 0.01694 0.01759 = 0.01898 -0.00356 -0.00396 -0.00492 C16 1 0.629814 0.472929 0.752718 11.00000 0.02032 0.01972 = 0.02729 -0.00481 -0.00318 -0.00311 AFIX 43 H16 2 0.666108 0.386776 0.731213 11.00000 -1.20000 AFIX 0 C20 1 0.516267 0.727347 0.730029 11.00000 0.01998 0.02012 = 0.01937 -0.00270 -0.00208 -0.00132 AFIX 43 H20 2 0.473845 0.816789 0.692774 11.00000 -1.20000 AFIX 0 C30 1 0.568633 0.831507 0.234302 11.00000 0.01652 0.02533 = 0.02304 -0.00717 -0.00346 -0.00447 AFIX 43 H30 2 0.665044 0.795280 0.258515 11.00000 -1.20000 AFIX 0 C22 1 0.557267 0.603595 0.601156 11.00000 0.02738 0.01845 = 0.02133 -0.00507 -0.00028 -0.00569 AFIX 23 H22A 2 0.481922 0.554781 0.597374 11.00000 -1.20000 H22B 2 0.657143 0.547507 0.578567 11.00000 -1.20000 AFIX 0 C10 1 0.943733 0.384890 0.296168 11.00000 0.01917 0.01752 = 0.01854 -0.00339 -0.00228 -0.00469 C5 1 1.026922 0.256836 0.728507 11.00000 0.01880 0.02290 = 0.02249 -0.00566 -0.00385 -0.00339 AFIX 43 H5 2 0.985631 0.350062 0.694958 11.00000 -1.20000 AFIX 0 C23 1 0.512556 0.751848 0.543203 11.00000 0.02365 0.01976 = 0.02038 -0.00494 -0.00380 -0.00425 AFIX 23 H23A 2 0.589821 0.799844 0.544567 11.00000 -1.20000 H23B 2 0.414034 0.809573 0.566252 11.00000 -1.20000 AFIX 0 C15 1 1.073683 0.326408 0.246581 11.00000 0.01700 0.02580 = 0.02307 -0.00582 -0.00376 -0.00302 AFIX 43 H15 2 1.170168 0.291359 0.270678 11.00000 -1.20000 AFIX 0 C21 1 0.567522 0.602583 0.695882 11.00000 0.01679 0.02128 = 0.02012 -0.00371 -0.00081 -0.00393 C19 1 0.526289 0.722784 0.817349 11.00000 0.02113 0.02551 = 0.02152 -0.00695 -0.00182 -0.00333 AFIX 43 H19 2 0.491356 0.808736 0.839082 11.00000 -1.20000 AFIX 0 C26 1 0.298153 0.950434 0.248502 11.00000 0.01727 0.02140 = 0.02060 -0.00368 -0.00235 -0.00355 AFIX 43 H26 2 0.211284 0.994888 0.282137 11.00000 -1.20000 AFIX 0 C24 1 0.498678 0.746420 0.449352 11.00000 0.02196 0.01834 = 0.02079 -0.00607 -0.00410 -0.00275 AFIX 23 H24A 2 0.415367 0.706683 0.446141 11.00000 -1.20000 H24B 2 0.594618 0.684805 0.426243 11.00000 -1.20000 AFIX 0 C17 1 0.639424 0.468179 0.839977 11.00000 0.02077 0.02450 = 0.02573 0.00149 -0.00588 -0.00530 AFIX 43 H17 2 0.681963 0.379078 0.877517 11.00000 -1.20000 AFIX 0 C4 1 1.024152 0.238022 0.818024 11.00000 0.01955 0.02910 = 0.02291 -0.00959 -0.00243 -0.00449 AFIX 43 H4 2 0.983179 0.318262 0.845046 11.00000 -1.20000 AFIX 0 C6 1 1.089203 0.141502 0.686560 11.00000 0.01544 0.02760 = 0.02333 -0.00834 -0.00419 -0.00313 C28 1 0.413246 0.875158 0.116987 11.00000 0.03082 0.02191 = 0.01585 -0.00170 -0.00494 -0.01152 C27 1 0.284503 0.939194 0.164650 11.00000 0.02119 0.02611 = 0.02395 -0.00043 -0.00926 -0.00829 AFIX 43 H27 2 0.188196 0.974934 0.140326 11.00000 -1.20000 AFIX 0 C8 1 0.944754 0.188508 0.553941 11.00000 0.02036 0.02309 = 0.02158 -0.00423 -0.00222 -0.00650 AFIX 23 H8A 2 0.910731 0.102868 0.578868 11.00000 -1.20000 H8B 2 0.868732 0.271466 0.573623 11.00000 -1.20000 AFIX 0 C29 1 0.555286 0.820421 0.150866 11.00000 0.02216 0.02481 = 0.02297 -0.00690 0.00126 -0.00576 AFIX 43 H29 2 0.641999 0.775997 0.117118 11.00000 -1.20000 AFIX 0 C14 1 1.061321 0.319690 0.161948 11.00000 0.02252 0.02703 = 0.02305 -0.00875 0.00204 -0.00536 AFIX 43 H14 2 1.148904 0.279550 0.127278 11.00000 -1.20000 AFIX 0 C1 1 1.143105 0.005074 0.738028 11.00000 0.02053 0.02366 = 0.03180 -0.00939 -0.00731 -0.00093 AFIX 43 H1 2 1.182972 -0.075516 0.711246 11.00000 -1.20000 AFIX 0 C3 1 1.081101 0.102223 0.868270 11.00000 0.01895 0.03722 = 0.01993 -0.00496 -0.00199 -0.00884 AFIX 43 H3 2 1.080337 0.089207 0.929582 11.00000 -1.20000 AFIX 0 C18 1 0.587126 0.593142 0.872843 11.00000 0.01941 0.03043 = 0.01753 -0.00302 -0.00225 -0.00709 AFIX 43 H18 2 0.593051 0.589650 0.932677 11.00000 -1.20000 AFIX 0 C13 1 0.919037 0.372468 0.128393 11.00000 0.02998 0.02387 = 0.01713 -0.00160 -0.00568 -0.01208 C2 1 1.139249 -0.014543 0.828116 11.00000 0.02230 0.02533 = 0.03113 0.00050 -0.00871 -0.00634 AFIX 43 H2 2 1.176502 -0.108065 0.862196 11.00000 -1.20000 AFIX 0 C9 1 0.950135 0.214273 0.454941 11.00000 0.02434 0.02072 = 0.02172 -0.00478 -0.00447 -0.00515 AFIX 23 H9A 2 0.858429 0.200956 0.437123 11.00000 -1.20000 H9B 2 1.040459 0.143426 0.433806 11.00000 -1.20000 AFIX 0 C11 1 0.802249 0.440075 0.261435 11.00000 0.01742 0.02703 = 0.02610 -0.00617 -0.00079 -0.00308 AFIX 43 H11 2 0.714890 0.482379 0.295527 11.00000 -1.20000 AFIX 0 C7 1 1.098050 0.166583 0.588718 11.00000 0.01977 0.03218 = 0.02326 -0.00876 -0.00305 -0.00371 AFIX 23 H7A 2 1.174327 0.083386 0.569435 11.00000 -1.20000 H7B 2 1.132334 0.252162 0.564123 11.00000 -1.20000 AFIX 0 C12 1 0.789414 0.433006 0.176789 11.00000 0.02091 0.03108 = 0.02584 -0.00134 -0.00844 -0.00776 AFIX 43 H12 2 0.693224 0.469111 0.152323 11.00000 -1.20000 AFIX 0 HKLF 4 REM gujy_a_241224_auto_a.res in P-1 REM wR2 = 0.1235, GooF = S = 1.085, Restrained GooF = 1.085 for all data REM R1 = 0.0417 for 4993 Fo > 4sig(Fo) and 0.0438 for all 5444 data REM 325 parameters refined using 0 restraints END WGHT 0.0806 0.2139 REM Instructions for potential hydrogen bonds EQIV $1 -x+1, -y+2, -z+1 HTAB C23 O2_$1 HTAB C24 O1 EQIV $2 -x+1, -y+1, -z+1 HTAB C8 O2_$2 EQIV $3 x+1, y-1, z HTAB C9 O2_$3 REM Highest difference peak 0.433, deepest hole -0.479, 1-sigma level 0.070 Q1 1 0.4501 0.8533 0.4179 11.00000 0.05 0.43 Q2 1 1.0110 0.2558 0.5424 11.00000 0.05 0.40 Q3 1 1.0031 0.2675 0.4530 11.00000 0.05 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1.76 1.15 1 -8 -1 2.26 0.82 1 -8 -1 1.20 1.05 1 -8 -1 1.02 1.88 1 -8 -1 1.25 1.13 1 -8 0 198.52 10.31 1 -8 0 195.96 9.09 1 -8 0 200.20 10.61 1 -8 0 189.62 11.11 1 -8 0 192.84 11.40 1 -8 0 166.25 10.80 1 -8 1 67.87 4.80 1 -8 1 72.87 5.09 1 -8 1 75.07 5.38 1 -8 1 61.59 5.38 1 -8 1 70.36 5.72 1 -8 2 19.27 2.22 1 -8 2 14.68 2.33 1 -8 2 16.59 2.53 1 -8 2 15.02 2.60 1 -8 3 66.85 4.69 1 -8 3 71.20 5.66 1 -8 3 83.78 5.75 1 -8 3 88.01 5.96 1 -8 4 216.29 11.99 1 -8 4 222.78 12.14 1 -8 4 200.05 11.75 1 -8 5 12.16 2.25 -1 8 -5 13.75 1.63 1 -8 6 8.17 2.72 1 -8 6 4.41 1.65 -1 8 -6 4.63 1.03 1 -8 7 0.94 1.23 1 -8 7 1.60 1.18 -1 8 -7 1.62 0.76 1 -8 8 10.86 1.94 1 -8 8 10.84 1.87 -1 8 -8 9.85 1.27 1 -8 9 143.93 7.33 -1 8 -9 126.17 6.48 -1 8 -10 38.38 2.40 1 -7 -17 0.39 0.35 1 -7 -17 0.47 0.36 1 -7 -16 6.99 1.06 1 -7 -16 8.27 1.16 1 -7 -15 353.58 16.20 1 -7 -15 365.99 16.30 1 -7 -15 328.30 17.20 1 -7 -14 44.28 3.55 1 -7 -14 46.63 4.50 1 -7 -14 45.52 3.73 1 -7 -13 15.76 2.76 1 -7 -13 15.27 2.33 1 -7 -13 16.00 1.79 1 -7 -12 71.98 5.51 1 -7 -12 72.26 4.59 1 -7 -12 69.02 6.27 1 -7 -11 46.27 4.42 1 -7 -11 49.01 5.19 1 -7 -11 57.39 3.87 1 -7 -11 54.74 3.67 1 -7 -10 922.80 42.84 1 -7 -10 982.92 40.16 1 -7 -10 928.92 39.89 1 -7 -10 905.94 39.94 1 -7 -9 751.52 33.34 1 -7 -9 772.13 32.83 1 -7 -9 764.32 34.64 1 -7 -9 731.15 31.58 1 -7 -9 710.99 31.70 1 -7 -9 710.79 31.65 1 -7 -8 138.81 8.59 1 -7 -8 122.04 7.99 1 -7 -8 144.75 8.47 1 -7 -8 132.68 7.20 1 -7 -8 142.13 9.40 1 -7 -8 146.24 7.24 1 -7 -7 61.69 4.85 1 -7 -7 69.84 5.65 1 -7 -7 59.55 4.93 1 -7 -7 56.80 4.72 1 -7 -7 58.92 4.96 1 -7 -7 58.38 3.84 1 -7 -7 59.98 3.80 1 -7 -7 64.88 5.06 1 -7 -6 146.80 8.63 1 -7 -6 140.86 8.41 1 -7 -6 151.21 9.12 1 -7 -6 136.52 8.44 1 -7 -6 124.33 8.15 1 -7 -6 138.32 8.12 1 -7 -6 134.19 7.12 1 -7 -6 129.07 6.98 1 -7 -6 129.60 8.16 1 -7 -6 147.16 7.06 1 -7 -5 160.50 9.94 1 -7 -5 197.95 11.00 1 -7 -5 181.38 10.23 1 -7 -5 174.33 8.69 1 -7 -5 180.27 9.45 1 -7 -5 169.60 8.76 1 -7 -5 192.58 10.32 1 -7 -5 172.98 10.06 1 -7 -5 205.32 10.71 1 -7 -4 152.16 9.14 1 -7 -4 147.83 9.16 1 -7 -4 166.54 9.89 1 -7 -4 165.00 9.37 1 -7 -4 147.46 7.68 1 -7 -4 167.33 9.00 1 -7 -4 154.63 7.87 1 -7 -4 172.23 8.48 1 -7 -4 142.99 8.97 1 -7 -4 168.22 9.87 1 -7 -3 1063.97 49.68 1 -7 -3 1238.43 50.99 1 -7 -3 1126.98 48.87 1 -7 -3 1200.79 49.61 1 -7 -3 1142.03 48.33 1 -7 -3 1131.36 48.14 1 -7 -3 1122.87 49.97 1 -7 -3 1263.46 50.71 1 -7 -2 459.10 23.55 1 -7 -2 489.54 23.38 1 -7 -2 499.37 23.82 1 -7 -2 517.92 22.91 1 -7 -2 515.04 23.16 1 -7 -2 501.28 23.67 1 -7 -2 556.93 24.23 1 -7 -1 765.37 34.47 1 -7 -1 811.62 33.81 1 -7 -1 776.43 33.68 1 -7 -1 776.33 34.37 1 -7 -1 720.41 34.28 1 -7 -1 730.61 33.83 1 -7 0 68.65 5.48 1 -7 0 80.26 5.36 1 -7 0 71.82 4.95 1 -7 0 77.31 5.62 1 -7 0 67.04 5.41 1 -7 1 8.05 1.97 1 -7 1 9.18 1.81 1 -7 1 7.90 1.48 1 -7 1 8.17 1.72 1 -7 1 6.67 1.69 1 -7 2 67.07 5.46 1 -7 2 77.13 4.98 1 -7 2 74.34 5.45 1 -7 2 77.18 5.55 1 -7 2 65.89 5.41 1 -7 2 78.61 5.89 1 -7 3 369.27 16.95 1 -7 3 347.84 16.99 1 -7 3 334.02 15.73 1 -7 4 247.58 13.03 1 -7 4 240.81 11.80 1 -7 5 66.51 4.67 1 -7 5 61.06 5.10 1 -7 6 83.00 6.16 1 -7 7 93.11 6.53 1 -7 8 11.95 2.94 1 -7 9 34.03 3.73 1 -7 9 36.87 3.50 -1 7 -10 111.48 5.92 -1 7 -10 125.30 6.46 1 -7 10 126.41 7.00 1 -7 10 121.95 7.30 -1 7 -11 312.67 14.19 -1 7 -11 337.52 14.70 1 -7 11 351.37 15.65 -1 7 -12 45.62 2.80 1 -7 12 48.14 3.30 1 -6 -18 49.90 2.76 1 -6 -18 49.07 3.31 1 -6 -17 16.39 1.53 1 -6 -17 15.55 2.15 1 -6 -16 6.89 1.18 1 -6 -16 5.72 1.67 1 -6 -15 1.89 0.90 1 -6 -15 4.22 1.70 1 -6 -15 3.26 1.12 1 -6 -14 19.79 2.51 1 -6 -14 21.99 2.57 1 -6 -13 17.34 3.20 1 -6 -13 20.65 2.31 1 -6 -13 24.61 2.54 1 -6 -13 17.93 2.52 1 -6 -12 0.13 0.75 1 -6 -12 0.21 1.08 1 -6 -12 -0.36 1.39 1 -6 -11 1.85 0.80 1 -6 -11 2.83 0.97 1 -6 -11 2.49 1.79 1 -6 -11 2.95 1.48 1 -6 -10 0.86 0.66 1 -6 -10 0.95 0.74 1 -6 -10 0.75 0.77 1 -6 -10 1.03 1.28 1 -6 -10 0.84 1.18 1 -6 -9 0.17 0.93 1 -6 -9 0.16 0.75 1 -6 -9 0.65 1.27 1 -6 -9 -0.12 0.66 1 -6 -9 0.33 0.56 1 -6 -9 0.93 0.75 1 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146.41 7.71 1 -6 -2 130.51 7.85 1 -6 -2 142.66 7.73 1 -6 -2 148.48 8.53 1 -6 -1 291.61 14.87 1 -6 -1 331.23 15.02 1 -6 -1 315.76 14.49 1 -6 -1 282.24 14.58 1 -6 -1 282.19 14.88 1 -6 -1 326.41 15.66 1 -6 0 166.54 9.58 1 -6 0 182.56 9.34 1 -6 0 192.08 9.26 1 -6 0 197.51 9.75 1 -6 0 179.86 9.62 1 -6 0 154.91 9.19 1 -6 0 161.71 9.55 1 -6 1 3.13 1.21 1 -6 1 1.79 1.17 1 -6 1 5.89 1.37 1 -6 1 4.71 1.19 1 -6 1 3.66 1.18 1 -6 1 3.23 1.13 1 -6 2 25.39 2.92 1 -6 2 30.50 3.02 1 -6 2 30.59 2.94 1 -6 2 26.20 2.49 1 -6 2 27.50 2.86 1 -6 2 22.37 2.71 1 -6 3 123.09 7.98 1 -6 3 150.40 8.31 1 -6 3 157.02 8.38 1 -6 3 139.85 7.47 1 -6 3 127.68 8.00 1 -6 4 2.05 0.84 1 -6 4 0.74 0.81 1 -6 4 1.72 1.21 1 -6 4 1.47 1.19 1 -6 5 0.81 1.21 1 -6 6 14.90 2.38 1 -6 7 1.53 1.39 1 -6 8 117.11 7.61 1 -6 9 1.24 1.39 1 -6 10 0.22 2.36 1 -6 10 0.74 2.23 -1 6 -11 205.59 10.21 1 -6 11 208.44 11.02 -1 6 -12 83.54 4.68 -1 6 -12 92.92 5.12 1 -6 12 88.88 5.74 -1 6 -13 33.98 2.22 -1 6 -13 35.77 2.52 1 -6 13 36.27 2.88 1 -5 -18 60.99 4.46 1 -5 -18 67.18 3.68 1 -5 -17 141.47 7.08 1 -5 -17 141.20 8.64 1 -5 -16 66.19 4.23 1 -5 -16 55.94 5.35 1 -5 -15 570.44 25.91 1 -5 -15 540.27 28.04 1 -5 -15 605.62 25.89 1 -5 -14 23.92 3.81 1 -5 -14 27.67 2.89 1 -5 -13 85.87 5.90 1 -5 -13 80.97 7.41 1 -5 -13 96.23 5.40 1 -5 -13 82.29 4.88 1 -5 -12 69.02 5.26 1 -5 -12 65.71 6.62 1 -5 -12 75.81 4.68 1 -5 -12 75.39 4.69 1 -5 -12 71.09 4.34 1 -5 -11 147.79 8.65 1 -5 -11 140.16 10.24 1 -5 -11 143.89 7.69 1 -5 -11 150.32 7.77 1 -5 -11 145.76 7.44 1 -5 -10 1783.92 73.52 1 -5 -10 1687.40 71.96 1 -5 -10 1914.59 76.30 1 -5 -10 1702.60 72.28 1 -5 -9 11.30 1.64 1 -5 -9 18.13 2.35 1 -5 -9 14.29 1.64 1 -5 -9 14.06 1.37 1 -5 -9 14.97 2.83 1 -5 -9 14.94 1.68 1 -5 -9 13.95 1.58 1 -5 -8 101.79 6.53 1 -5 -8 105.59 6.16 1 -5 -8 111.64 6.43 1 -5 -8 106.50 5.31 1 -5 -8 103.58 5.67 1 -5 -8 101.02 5.59 1 -5 -8 109.76 7.84 1 -5 -7 482.06 21.80 1 -5 -7 533.38 23.14 1 -5 -7 488.17 21.81 1 -5 -7 489.79 21.86 1 -5 -7 467.13 20.99 1 -5 -7 462.94 21.01 1 -5 -7 466.50 21.68 1 -5 -7 556.35 24.13 1 -5 -6 60.12 4.10 1 -5 -6 67.64 4.52 1 -5 -6 58.76 4.14 1 -5 -6 57.39 4.17 1 -5 -5 868.85 38.58 1 -5 -5 908.14 38.76 1 -5 -5 891.10 38.83 1 -5 -5 930.95 38.79 1 -5 -4 156.40 8.40 1 -5 -4 162.22 8.48 1 -5 -4 156.77 8.27 1 -5 -4 152.90 8.03 1 -5 -4 161.81 8.41 1 -5 -3 764.62 32.54 1 -5 -3 711.22 31.98 1 -5 -3 767.38 32.35 1 -5 -2 1412.43 59.34 1 -5 -2 1417.50 59.62 1 -5 -1 9.03 1.86 1 -5 0 323.10 15.90 1 -5 0 335.08 15.72 1 -5 1 28.66 2.91 1 -5 1 25.78 2.44 1 -5 1 23.54 2.20 1 -5 1 22.38 2.40 1 -5 2 353.37 15.43 1 -5 2 335.34 15.21 1 -5 3 326.99 16.47 1 -5 3 334.21 16.53 1 -5 4 4.52 1.23 1 -5 4 5.58 1.43 1 -5 4 4.49 1.11 1 -5 4 4.50 1.27 1 -5 5 46.20 3.49 1 -5 5 41.00 3.48 1 -5 5 49.47 3.99 1 -5 6 43.79 3.90 1 -5 6 43.96 3.58 1 -5 7 21.12 2.81 1 -5 7 23.95 2.69 1 -5 8 26.81 3.21 1 -5 8 32.57 3.25 1 -5 9 -0.21 1.22 1 -5 9 0.40 1.31 1 -5 10 19.10 2.66 1 -5 10 17.11 2.52 1 -5 11 23.56 2.74 1 -5 11 21.94 3.03 -1 5 -11 18.81 2.05 1 -5 12 300.44 15.22 -1 5 -12 301.51 13.97 1 -5 13 1.80 1.06 -1 5 -13 2.32 0.72 -1 5 -14 10.35 1.33 1 -5 14 9.69 1.49 -1 5 -14 9.46 1.14 -1 5 -15 3.27 0.69 1 -4 -19 24.24 2.20 1 -4 -18 182.52 8.52 1 -4 -18 171.73 9.80 1 -4 -17 4.20 0.86 1 -4 -16 13.87 2.00 1 -4 -16 13.29 1.69 -1 4 16 10.64 1.33 -1 4 15 177.49 9.47 1 -4 -15 200.27 10.33 1 -4 -15 206.64 10.15 1 -4 -15 210.95 9.59 -1 4 14 5.33 1.08 1 -4 -14 6.11 1.09 1 -4 -14 5.15 1.36 -1 4 13 11.70 1.54 1 -4 -13 12.56 1.47 -1 4 13 13.65 1.79 1 -4 -13 13.23 2.02 1 -4 -13 16.10 1.71 -1 4 12 0.45 0.59 1 -4 -12 -0.21 0.55 1 -4 -12 0.25 0.61 1 -4 -12 -0.25 0.62 1 -4 -12 0.29 0.45 1 -4 -11 87.56 4.98 1 -4 -11 89.61 5.23 1 -4 -11 86.97 5.19 1 -4 -11 87.63 4.83 1 -4 -10 104.18 5.52 1 -4 -10 103.73 5.73 1 -4 -10 99.64 5.69 1 -4 -10 103.36 5.34 1 -4 -9 2.97 0.69 1 -4 -9 3.93 0.88 1 -4 -9 3.42 0.65 1 -4 -8 31.36 2.56 1 -4 -8 35.81 2.49 1 -4 -8 31.15 2.11 1 -4 -7 0.10 0.49 1 -4 -7 0.43 0.60 1 -4 -7 0.60 0.33 1 -4 -6 10.55 1.36 1 -4 -6 11.27 1.50 1 -4 -6 11.26 1.00 1 -4 -5 0.43 0.69 1 -4 -5 0.60 0.59 1 -4 -5 0.44 0.55 1 -4 -5 0.04 0.24 1 -4 -4 74.85 4.68 1 -4 -4 78.03 4.50 1 -4 -3 108.76 6.14 1 -4 -3 115.81 5.94 1 -4 -3 120.09 6.14 1 -4 -2 31.68 2.29 1 -4 -2 25.59 2.25 1 -4 -1 32.34 2.62 1 -4 -1 37.20 2.69 1 -4 -1 30.24 2.37 1 -4 0 74.00 4.19 1 -4 0 61.61 2.83 1 -4 1 163.71 8.52 1 -4 1 172.44 8.26 1 -4 1 172.70 8.45 1 -4 2 317.97 15.69 1 -4 2 353.23 15.54 1 -4 2 368.31 15.79 1 -4 3 39.11 3.01 1 -4 3 41.29 2.98 1 -4 4 131.93 7.25 1 -4 4 119.20 6.96 1 -4 5 46.17 3.34 1 -4 5 48.10 3.65 1 -4 6 44.79 3.67 1 -4 6 46.01 3.49 1 -4 7 13.43 2.01 1 -4 7 12.59 1.93 1 -4 8 10.81 2.04 1 -4 8 11.79 1.94 1 -4 9 11.69 2.11 1 -4 9 9.18 1.98 1 -4 10 55.60 4.73 1 -4 10 73.89 5.39 1 -4 11 556.55 25.37 1 -4 11 550.16 25.90 1 -4 12 15.82 2.18 1 -4 12 18.59 2.77 1 -4 12 17.28 2.70 -1 4 -12 20.50 2.13 1 -4 13 6.90 1.72 1 -4 13 8.01 1.19 -1 4 -13 8.80 1.92 1 -4 14 147.58 8.38 -1 4 -14 162.39 7.95 -1 4 -15 54.22 3.36 -1 4 -15 55.21 3.44 -1 4 -16 134.82 6.35 1 -3 -19 106.91 6.11 -1 3 18 317.21 13.81 1 -3 -18 303.30 15.62 1 -3 -18 316.51 14.00 -1 3 17 25.00 2.08 1 -3 -17 25.93 3.40 -1 3 16 381.94 17.42 1 -3 -16 365.90 17.36 1 -3 -16 404.82 17.17 -1 3 15 59.16 4.05 1 -3 -15 59.77 4.22 1 -3 -15 58.02 3.78 -1 3 14 8.62 1.45 -1 3 14 8.15 1.41 1 -3 -14 7.23 1.42 1 -3 -14 8.52 1.32 -1 3 13 293.36 15.05 1 -3 -13 327.54 14.91 -1 3 13 340.63 15.45 1 -3 -13 342.69 15.06 -1 3 12 175.36 8.87 1 -3 -12 163.64 8.45 1 -3 -12 171.48 8.41 1 -3 -11 1306.00 54.34 1 -3 -11 1279.41 54.32 1 -3 -11 1289.07 54.14 1 -3 -11 1297.99 54.06 1 -3 -10 99.99 5.44 1 -3 -10 95.38 5.39 1 -3 -10 99.29 5.30 1 -3 -10 101.65 5.23 1 -3 -9 19.10 1.71 1 -3 -9 17.36 1.52 1 -3 -9 18.48 1.60 1 -3 -8 245.32 10.46 1 -3 -8 236.49 10.16 1 -3 -7 19.44 1.72 -1 3 7 14.95 1.40 1 -3 -6 247.81 10.31 1 -3 -6 255.42 10.89 1 -3 -6 272.54 11.03 -1 3 5 90.78 4.08 1 -3 -5 105.77 4.80 1 -3 -5 101.05 4.81 -1 3 5 76.94 3.83 1 -3 -5 89.19 4.07 1 -3 -4 0.62 0.54 1 -3 -4 0.72 0.52 1 -3 -4 1.01 0.46 1 -3 -4 0.96 0.29 1 -3 -3 146.45 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1.66 2 -5 -5 7.17 1.61 2 -5 -5 4.55 1.32 2 -5 -5 3.76 1.52 2 -5 -4 26.90 2.07 2 -5 -4 27.63 2.58 2 -5 -4 24.32 2.70 2 -5 -4 29.29 2.97 2 -5 -4 25.86 2.77 2 -5 -4 27.59 3.32 2 -5 -4 26.85 2.78 2 -5 -4 31.10 2.95 2 -5 -3 2.74 1.06 2 -5 -3 2.09 1.13 2 -5 -3 0.78 0.77 2 -5 -3 1.86 1.14 2 -5 -3 1.46 0.95 2 -5 -3 1.32 1.08 2 -5 -3 1.96 0.82 2 -5 -2 2.82 0.98 2 -5 -2 0.80 0.93 2 -5 -1 46.84 3.90 2 -5 -1 50.78 3.95 2 -5 -1 44.93 3.39 2 -5 0 41.65 3.67 2 -5 0 48.04 3.44 2 -5 0 50.61 3.82 2 -5 0 46.90 3.84 2 -5 0 38.58 3.50 2 -5 1 56.01 4.45 2 -5 1 62.81 4.30 2 -5 1 65.22 4.50 2 -5 1 62.81 5.02 2 -5 1 62.87 4.59 2 -5 1 59.65 4.62 2 -5 1 64.04 4.21 2 -5 2 85.98 5.34 2 -5 2 87.13 6.13 2 -5 2 80.75 5.24 2 -5 2 83.34 6.11 2 -5 2 70.85 5.23 2 -5 2 73.63 5.43 2 -5 2 86.08 5.08 2 -5 3 39.98 3.44 2 -5 3 39.50 3.29 2 -5 3 38.47 3.46 2 -5 3 36.64 3.63 2 -5 3 36.70 3.04 2 -5 4 25.77 2.91 2 -5 4 25.84 2.81 2 -5 4 29.80 2.60 2 -5 4 28.90 2.73 2 -5 5 45.22 4.02 2 -5 5 53.81 3.83 2 -5 5 42.82 3.35 2 -5 5 41.46 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3 -7 -5 389.47 18.14 3 -7 -5 363.54 16.90 3 -7 -4 42.18 4.78 3 -7 -4 43.58 3.94 3 -7 -4 38.17 4.35 3 -7 -4 42.85 4.36 3 -7 -4 44.65 4.26 3 -7 -4 31.45 3.75 3 -7 -4 45.79 5.03 3 -7 -4 40.80 3.70 3 -7 -4 41.57 3.30 3 -7 -4 41.59 4.07 3 -7 -3 224.56 12.98 3 -7 -3 237.64 11.40 3 -7 -3 265.97 14.59 3 -7 -3 258.60 14.03 3 -7 -3 258.65 14.36 3 -7 -3 244.10 12.94 3 -7 -2 535.84 25.41 3 -7 -2 528.61 23.46 3 -7 -2 552.87 24.88 3 -7 -2 551.98 26.36 3 -7 -2 564.84 25.36 3 -7 -2 572.32 26.73 3 -7 -2 552.56 25.98 3 -7 -2 486.28 25.39 3 -7 -2 563.20 27.00 3 -7 -1 6.85 1.05 3 -7 -1 5.46 1.60 3 -7 -1 7.28 1.51 3 -7 -1 7.34 1.98 3 -7 -1 6.57 2.00 3 -7 -1 8.16 2.25 3 -7 -1 4.28 2.07 3 -7 -1 4.82 1.63 3 -7 0 98.02 5.22 3 -7 0 100.97 6.84 3 -7 0 94.95 6.30 3 -7 0 100.98 6.27 3 -7 0 102.82 6.79 3 -7 0 91.32 6.93 3 -7 0 104.95 8.08 3 -7 0 103.93 7.33 3 -7 1 39.64 3.94 3 -7 1 47.58 3.89 3 -7 1 39.45 3.67 3 -7 1 46.48 3.73 3 -7 1 50.39 4.25 3 -7 1 35.62 3.99 3 -7 1 42.38 4.43 3 -7 1 48.46 5.29 3 -7 2 12.56 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30.49 2.67 3 -6 -9 28.39 2.76 3 -6 -8 12.79 2.03 3 -6 -8 11.26 2.21 3 -6 -8 11.30 2.30 3 -6 -8 8.10 1.56 3 -6 -8 12.95 1.69 3 -6 -8 11.33 1.67 3 -6 -7 35.77 3.74 3 -6 -7 34.33 3.71 3 -6 -7 35.27 4.36 3 -6 -7 41.64 4.17 3 -6 -7 35.47 3.33 3 -6 -7 33.16 2.94 3 -6 -7 36.74 2.89 3 -6 -7 35.11 2.66 3 -6 -7 36.96 3.34 3 -6 -7 33.73 3.29 3 -6 -7 37.91 3.67 3 -6 -6 1.96 1.23 3 -6 -6 1.22 1.53 3 -6 -6 4.62 1.56 3 -6 -6 1.73 0.94 3 -6 -6 2.53 1.23 3 -6 -6 2.29 0.70 3 -6 -6 3.16 1.15 3 -6 -6 3.08 1.53 3 -6 -6 3.51 1.39 3 -6 -6 2.53 0.82 3 -6 -6 3.20 0.77 3 -6 -6 2.84 0.85 3 -6 -5 0.67 1.27 3 -6 -5 0.35 0.57 3 -6 -5 0.85 0.97 3 -6 -5 0.65 0.84 3 -6 -5 1.53 1.61 3 -6 -5 0.68 1.24 3 -6 -5 1.78 1.17 3 -6 -5 1.04 1.24 3 -6 -5 0.19 0.71 3 -6 -5 -0.21 1.03 3 -6 -4 25.37 2.22 3 -6 -4 23.08 2.53 3 -6 -4 25.91 2.86 3 -6 -4 26.59 3.35 3 -6 -4 28.71 3.28 3 -6 -4 24.36 3.05 3 -6 -4 30.58 3.98 3 -6 -4 27.00 3.92 3 -6 -4 27.35 3.24 3 -6 -4 31.34 3.76 3 -6 -4 28.46 3.03 3 -6 -3 31.21 3.09 3 -6 -3 27.39 2.67 3 -6 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3 -6 3 47.05 4.66 3 -6 4 1.57 1.01 3 -6 4 1.42 1.21 3 -6 4 1.88 1.26 3 -6 4 2.16 1.13 3 -6 4 1.86 1.05 3 -6 4 1.77 1.32 3 -6 5 10.33 1.73 3 -6 5 5.94 1.40 3 -6 5 9.85 2.08 3 -6 5 8.29 1.94 3 -6 6 54.34 3.97 3 -6 6 62.73 5.05 3 -6 7 131.26 7.68 3 -6 7 120.29 7.68 3 -6 8 333.77 16.60 3 -6 9 4.58 1.56 3 -6 10 4.79 1.53 3 -6 11 221.63 10.89 3 -6 11 203.00 10.85 3 -6 12 17.52 1.92 3 -6 12 16.35 1.96 -3 6 -12 16.48 1.51 -3 6 -13 80.24 3.96 3 -5 -17 19.75 1.47 3 -5 -16 39.94 3.61 3 -5 -16 40.09 2.74 3 -5 -16 43.82 2.72 3 -5 -15 0.72 1.20 3 -5 -15 0.44 0.55 3 -5 -14 18.36 2.11 3 -5 -13 323.75 14.93 3 -5 -13 312.53 14.61 3 -5 -13 315.81 14.66 3 -5 -12 0.63 0.99 3 -5 -12 0.35 1.54 3 -5 -12 -0.69 0.91 3 -5 -11 38.24 3.92 3 -5 -11 42.32 3.91 3 -5 -10 17.69 2.37 3 -5 -10 13.63 2.31 3 -5 -10 16.63 2.44 3 -5 -10 18.53 2.62 3 -5 -10 16.46 1.95 3 -5 -9 24.94 2.98 3 -5 -9 26.10 3.19 3 -5 -9 20.14 3.66 3 -5 -9 22.84 2.28 3 -5 -9 24.37 3.11 3 -5 -8 194.44 11.14 3 -5 -8 221.73 11.90 3 -5 -8 197.82 12.95 3 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51.80 3.57 3 -5 -4 52.48 3.37 3 -5 -4 56.18 4.42 3 -5 -4 51.98 3.21 3 -5 -4 53.40 4.00 3 -5 -4 58.37 4.08 3 -5 -3 178.98 8.90 3 -5 -3 186.34 10.19 3 -5 -3 184.93 9.78 3 -5 -3 194.27 9.73 3 -5 -3 193.72 10.44 3 -5 -3 197.15 10.61 3 -5 -3 175.57 10.22 3 -5 -3 192.14 11.36 3 -5 -3 208.31 11.09 3 -5 -3 200.17 10.46 3 -5 -2 1399.58 59.77 3 -5 -2 1377.28 58.68 3 -5 -2 1393.44 59.44 3 -5 -2 1509.08 62.22 3 -5 -2 1505.81 61.31 3 -5 -2 1333.08 60.30 3 -5 -2 1565.19 62.08 3 -5 -1 10.74 2.03 3 -5 -1 11.96 1.28 3 -5 -1 20.18 2.07 3 -5 -1 10.26 2.33 3 -5 -1 14.47 2.15 3 -5 -1 12.77 2.11 3 -5 -1 13.49 2.31 3 -5 -1 13.33 2.63 3 -5 0 412.18 19.78 3 -5 0 435.87 19.74 3 -5 0 446.99 19.79 3 -5 0 459.89 21.84 3 -5 0 441.78 21.17 3 -5 0 451.13 20.48 3 -5 0 397.56 20.35 3 -5 0 430.89 20.67 3 -5 1 11.45 1.74 3 -5 1 8.40 1.62 3 -5 1 11.15 1.77 3 -5 1 8.73 1.72 3 -5 1 6.62 1.83 3 -5 1 9.00 2.08 3 -5 1 7.99 1.93 3 -5 1 6.62 1.61 3 -5 2 5.99 1.38 3 -5 2 7.65 1.63 3 -5 2 6.52 1.53 3 -5 2 6.68 1.64 3 -5 2 6.61 1.82 3 -5 2 7.53 2.02 3 -5 2 6.77 1.88 3 -5 2 8.05 1.61 3 -5 2 5.43 1.43 3 -5 3 823.73 35.80 3 -5 3 819.68 35.70 3 -5 3 791.58 36.11 3 -5 3 726.59 35.77 3 -5 3 902.04 35.90 3 -5 3 793.34 35.58 3 -5 4 3.38 1.48 3 -5 4 4.72 1.64 3 -5 4 4.17 1.26 3 -5 4 4.85 1.34 3 -5 4 2.05 1.29 3 -5 5 221.40 11.62 3 -5 5 225.36 12.30 3 -5 5 207.26 11.98 3 -5 6 70.92 5.54 3 -5 6 70.93 4.73 3 -5 7 71.65 5.37 3 -5 7 58.42 4.17 3 -5 8 92.96 6.51 3 -5 9 44.16 4.41 3 -5 9 52.55 4.51 3 -5 10 385.16 18.93 3 -5 11 396.22 19.09 3 -5 12 11.95 1.95 3 -5 13 19.24 2.14 -3 5 -14 72.39 3.85 3 -4 -17 5.75 1.31 3 -4 -17 8.29 1.01 3 -4 -16 18.04 1.70 3 -4 -16 21.85 2.84 3 -4 -16 21.75 1.97 3 -4 -15 13.98 2.06 3 -4 -15 16.11 1.83 3 -4 -15 15.38 2.69 3 -4 -15 15.49 1.86 3 -4 -14 21.03 2.77 3 -4 -14 24.47 2.50 3 -4 -14 23.35 2.50 3 -4 -14 20.06 3.34 3 -4 -13 1.19 1.14 3 -4 -13 1.01 1.62 3 -4 -13 1.07 2.67 3 -4 -13 2.84 1.06 3 -4 -12 4.15 1.36 3 -4 -12 5.08 1.67 3 -4 -12 3.02 1.90 3 -4 -12 4.87 1.35 3 -4 -11 8.53 2.04 3 -4 -11 9.26 1.75 3 -4 -11 7.64 2.49 -3 4 11 7.84 1.33 3 -4 -11 8.88 1.78 3 -4 -10 23.12 3.18 3 -4 -10 25.19 2.80 3 -4 -10 26.96 3.22 3 -4 -10 19.11 3.50 3 -4 -10 23.42 2.73 3 -4 -9 1.25 0.96 3 -4 -9 0.49 1.02 3 -4 -9 1.61 1.12 3 -4 -9 1.80 1.51 3 -4 -9 1.34 1.23 3 -4 -9 0.74 0.62 3 -4 -8 3.92 1.20 3 -4 -8 4.62 1.48 3 -4 -8 5.81 1.43 3 -4 -8 6.01 1.70 3 -4 -8 5.15 1.01 3 -4 -8 4.88 1.07 3 -4 -7 3.08 1.72 3 -4 -7 3.12 1.20 3 -4 -7 3.51 0.98 3 -4 -7 2.60 1.17 3 -4 -7 2.23 1.19 3 -4 -7 3.27 1.39 3 -4 -7 2.17 0.92 3 -4 -7 1.88 0.61 3 -4 -7 2.81 0.82 3 -4 -6 6.07 1.97 3 -4 -6 5.46 1.46 3 -4 -6 5.49 1.49 3 -4 -6 5.30 1.22 3 -4 -6 3.86 0.81 3 -4 -6 4.13 1.04 3 -4 -6 6.03 1.46 3 -4 -6 7.12 1.40 3 -4 -6 4.46 1.11 3 -4 -6 6.35 1.59 3 -4 -6 4.15 0.81 3 -4 -6 5.42 0.97 3 -4 -5 5.89 1.40 3 -4 -5 6.41 1.25 3 -4 -5 6.50 1.43 3 -4 -5 7.59 1.79 3 -4 -5 5.67 1.79 3 -4 -5 7.26 1.64 3 -4 -5 6.04 1.93 3 -4 -5 5.30 1.34 3 -4 -5 5.95 1.21 3 -4 -5 6.38 1.25 3 -4 -4 58.00 4.36 3 -4 -4 52.80 4.16 3 -4 -4 57.24 5.04 3 -4 -4 58.52 4.25 3 -4 -4 57.19 5.20 3 -4 -3 30.25 2.99 3 -4 -3 29.43 2.90 3 -4 -3 28.50 3.42 3 -4 -2 1.90 1.04 3 -4 -2 1.81 1.32 3 -4 -1 39.58 3.43 3 -4 -1 39.25 3.48 3 -4 -1 44.53 3.62 3 -4 0 181.95 10.18 3 -4 0 187.40 10.31 3 -4 1 147.10 8.54 3 -4 1 162.83 8.67 3 -4 1 149.45 8.07 3 -4 1 154.96 8.04 3 -4 2 153.32 9.16 3 -4 2 133.16 8.33 3 -4 2 123.18 7.86 3 -4 2 162.91 8.34 3 -4 2 141.51 7.76 3 -4 2 139.07 7.64 3 -4 3 38.54 3.63 3 -4 3 42.49 3.65 3 -4 3 41.42 3.95 3 -4 3 42.79 3.45 3 -4 3 47.69 3.58 3 -4 3 42.09 3.25 3 -4 3 48.75 3.77 3 -4 3 38.33 3.36 3 -4 4 29.43 3.09 3 -4 4 25.18 2.84 3 -4 4 31.45 2.81 3 -4 4 33.55 2.94 3 -4 4 26.42 2.57 3 -4 4 25.87 2.82 3 -4 4 28.87 2.97 3 -4 5 51.92 3.93 3 -4 5 52.80 4.38 3 -4 5 48.45 4.21 3 -4 6 20.93 2.37 3 -4 6 20.87 2.68 3 -4 7 104.52 6.19 3 -4 7 88.35 6.27 3 -4 7 89.86 6.51 3 -4 8 5.22 1.64 3 -4 8 5.02 1.88 3 -4 9 9.15 2.10 3 -4 9 7.69 1.92 -3 4 -10 361.11 17.18 3 -4 10 420.87 19.44 3 -4 10 423.75 19.18 -3 4 -11 13.71 1.53 3 -4 11 16.85 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15.66 5 -6 1 81.64 6.08 5 -6 1 103.01 7.02 5 -6 1 103.00 6.55 5 -6 1 85.99 7.48 5 -6 2 1.17 1.05 5 -6 2 0.20 1.91 5 -6 2 3.03 1.55 5 -6 2 5.56 2.32 5 -6 3 7.26 1.63 5 -6 3 4.76 2.37 5 -6 3 3.12 1.35 5 -6 3 4.76 1.38 5 -6 3 4.07 1.37 5 -6 4 19.03 2.45 5 -6 4 24.52 2.59 5 -6 4 26.15 5.22 5 -6 4 29.26 2.87 5 -6 4 25.95 2.81 5 -6 5 78.04 5.12 5 -6 5 97.93 7.14 5 -6 5 82.63 5.26 5 -6 5 83.28 5.60 5 -6 6 74.34 4.68 5 -6 6 66.10 5.86 5 -6 7 179.64 9.05 5 -6 7 172.97 10.58 5 -6 8 0.51 0.49 5 -6 8 0.42 0.95 5 -6 8 0.39 1.08 5 -6 9 59.73 4.31 5 -5 -14 83.10 5.23 5 -5 -14 82.79 4.29 5 -5 -13 134.56 8.31 5 -5 -13 147.33 7.11 5 -5 -12 0.35 0.61 5 -5 -12 0.41 0.59 5 -5 -11 35.64 3.38 5 -5 -11 41.78 3.28 5 -5 -11 43.83 3.15 5 -5 -10 18.82 2.54 5 -5 -10 17.28 2.44 5 -5 -10 16.19 2.10 5 -5 -10 16.82 1.95 5 -5 -9 153.97 8.97 5 -5 -9 137.85 8.53 5 -5 -9 131.62 7.47 5 -5 -8 276.66 14.43 5 -5 -8 257.59 12.77 5 -5 -8 270.63 14.04 5 -5 -8 271.68 12.99 5 -5 -8 247.69 13.03 5 -5 -8 254.77 12.65 5 -5 -7 22.97 3.27 5 -5 -7 18.61 3.60 5 -5 -7 18.33 2.28 5 -5 -7 21.69 2.56 5 -5 -7 19.65 2.10 5 -5 -7 17.23 2.74 5 -5 -7 17.06 2.29 5 -5 -7 14.75 1.94 5 -5 -6 61.01 5.12 5 -5 -6 50.06 3.88 5 -5 -6 53.44 4.23 5 -5 -6 53.30 5.84 5 -5 -6 66.67 6.45 5 -5 -6 66.22 5.74 5 -5 -6 51.50 4.26 5 -5 -6 56.72 4.59 5 -5 -6 58.37 3.62 5 -5 -6 54.13 3.91 5 -5 -5 140.75 8.99 5 -5 -5 135.75 7.77 5 -5 -5 145.84 8.15 5 -5 -5 142.08 10.19 5 -5 -5 160.03 9.94 5 -5 -5 141.58 8.36 5 -5 -5 152.99 8.81 5 -5 -5 140.78 7.13 5 -5 -5 131.01 7.51 5 -5 -4 27.32 3.75 5 -5 -4 29.38 3.12 5 -5 -4 28.02 3.26 5 -5 -4 25.63 2.67 5 -5 -4 26.87 2.14 5 -5 -4 22.90 2.32 5 -5 -3 339.32 17.43 5 -5 -3 381.46 18.10 5 -5 -3 358.90 17.04 5 -5 -2 77.81 6.47 5 -5 -2 75.79 5.53 5 -5 -2 68.25 5.00 5 -5 -2 79.19 7.04 5 -5 -1 87.12 6.92 5 -5 -1 83.35 6.00 5 -5 -1 87.83 6.28 5 -5 -1 85.46 5.67 5 -5 -1 80.25 7.16 5 -5 0 6.83 2.41 5 -5 0 6.06 1.82 5 -5 0 7.22 2.31 5 -5 0 6.42 2.21 5 -5 1 215.04 12.93 5 -5 1 188.24 12.07 5 -5 1 218.79 13.37 5 -5 1 208.49 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5 -4 -3 0.60 0.82 5 -4 -3 1.56 1.24 5 -4 -3 -0.34 1.81 -5 4 3 1.13 0.75 5 -4 -3 0.21 1.06 5 -4 -3 0.19 1.00 5 -4 -3 1.41 1.59 5 -4 -3 1.84 0.85 5 -4 -2 19.66 2.29 5 -4 -2 20.78 3.53 5 -4 -2 13.86 2.22 5 -4 -2 20.57 3.53 5 -4 -2 21.71 3.30 5 -4 -2 20.64 2.69 5 -4 -2 15.89 1.87 5 -4 -1 93.94 7.90 5 -4 -1 99.88 7.38 5 -4 -1 92.62 6.38 5 -4 -1 106.71 6.27 5 -4 -1 97.38 7.82 5 -4 0 106.79 6.76 5 -4 0 101.26 8.28 5 -4 0 110.00 7.85 5 -4 0 112.78 7.21 5 -4 0 111.13 6.25 5 -4 0 107.62 8.24 5 -4 1 3.67 1.35 5 -4 1 6.04 1.59 5 -4 1 3.34 1.41 5 -4 1 5.54 1.53 5 -4 1 4.04 1.69 5 -4 1 3.47 1.08 5 -4 1 3.78 1.94 5 -4 2 11.29 1.99 5 -4 2 11.64 2.10 5 -4 2 12.13 2.07 5 -4 2 11.10 1.99 5 -4 2 8.56 2.19 5 -4 2 8.92 1.62 5 -4 2 11.90 2.59 5 -4 3 89.08 6.19 5 -4 3 79.06 5.52 5 -4 3 82.07 5.89 5 -4 3 77.11 6.37 5 -4 3 89.12 5.97 5 -4 3 85.13 5.91 5 -4 3 95.23 5.66 5 -4 3 69.28 6.54 5 -4 4 70.06 5.19 5 -4 4 82.66 5.79 5 -4 4 69.50 5.63 5 -4 4 75.40 6.19 5 -4 4 82.29 5.57 5 -4 4 71.25 5.34 5 -4 4 82.47 5.30 5 -4 4 65.42 6.19 5 -4 5 106.64 6.88 5 -4 5 121.21 7.51 5 -4 5 98.29 7.20 5 -4 5 124.41 7.13 5 -4 5 100.32 6.69 5 -4 5 112.69 6.80 5 -4 5 100.85 7.99 5 -4 6 20.09 2.95 5 -4 6 19.77 2.59 5 -4 6 22.34 3.01 5 -4 6 21.59 2.52 5 -4 6 17.37 2.30 5 -4 6 23.76 2.69 5 -4 6 16.24 3.01 5 -4 7 3.92 1.68 5 -4 7 3.79 1.44 5 -4 8 251.60 13.19 5 -4 8 275.21 14.15 5 -4 8 245.05 14.16 5 -4 9 88.95 6.24 5 -4 9 97.68 6.99 5 -4 9 90.52 6.94 5 -4 10 122.11 7.32 5 -4 10 130.64 8.15 5 -4 10 112.10 6.47 5 -4 10 118.73 7.82 5 -4 11 2.89 1.30 5 -4 11 2.34 1.28 5 -4 12 9.83 1.73 5 -3 -15 11.05 1.20 5 -3 -15 8.61 1.38 5 -3 -14 283.66 12.52 5 -3 -14 245.46 13.15 5 -3 -13 39.58 3.00 5 -3 -13 37.84 3.71 5 -3 -12 41.07 3.77 5 -3 -12 37.74 4.40 5 -3 -12 44.25 3.45 5 -3 -12 43.56 4.29 5 -3 -12 40.65 3.32 5 -3 -11 69.44 5.78 5 -3 -11 78.25 7.40 5 -3 -11 87.58 5.46 5 -3 -11 69.48 6.07 5 -3 -11 92.90 5.59 5 -3 -10 16.65 2.80 5 -3 -10 19.21 3.60 5 -3 -10 17.39 2.35 5 -3 -10 16.16 2.82 5 -3 -9 551.79 24.70 5 -3 -9 471.64 25.13 5 -3 -9 491.03 22.57 5 -3 -9 480.13 24.35 5 -3 -9 495.03 22.91 5 -3 -8 195.63 10.15 5 -3 -8 211.87 11.87 5 -3 -8 176.36 11.99 5 -3 -8 183.95 10.00 5 -3 -8 189.14 11.50 5 -3 -8 182.02 10.15 5 -3 -7 23.27 2.71 5 -3 -7 31.34 3.95 5 -3 -7 23.68 2.52 5 -3 -7 20.83 3.51 5 -3 -7 25.17 2.72 5 -3 -7 22.35 2.54 5 -3 -7 23.07 3.35 5 -3 -7 22.32 2.61 5 -3 -6 177.14 9.63 5 -3 -6 157.23 10.45 5 -3 -6 189.13 11.05 5 -3 -6 171.58 9.36 5 -3 -6 193.39 9.86 5 -3 -6 162.16 9.14 5 -3 -5 765.74 31.68 -5 3 5 614.47 30.66 5 -3 -5 689.55 30.06 5 -3 -5 695.68 30.87 5 -3 -5 782.43 33.26 5 -3 -5 695.72 31.21 5 -3 -5 773.48 31.76 5 -3 -5 699.75 32.64 5 -3 -5 711.08 30.51 5 -3 -4 2.10 0.93 5 -3 -4 2.00 0.86 5 -3 -4 2.59 1.39 5 -3 -4 2.87 2.18 -5 3 4 1.71 0.89 5 -3 -4 1.69 1.08 5 -3 -4 1.18 0.87 5 -3 -4 2.50 0.87 5 -3 -4 1.58 0.57 5 -3 -3 134.47 7.35 5 -3 -3 144.05 8.95 5 -3 -3 129.44 7.62 5 -3 -3 170.56 9.27 5 -3 -3 143.94 9.66 -5 3 3 130.35 7.65 5 -3 -3 131.00 9.41 5 -3 -3 144.35 9.19 5 -3 -3 132.87 7.81 5 -3 -3 130.02 7.34 5 -3 -2 72.26 4.78 5 -3 -2 73.40 5.83 5 -3 -2 72.01 5.74 5 -3 -2 66.64 5.47 5 -3 -2 84.97 6.79 5 -3 -2 80.45 6.71 5 -3 -2 76.66 6.07 5 -3 -2 72.57 5.09 5 -3 -2 75.94 4.73 5 -3 -1 24.62 2.54 5 -3 -1 29.55 3.44 5 -3 -1 28.45 3.88 5 -3 -1 31.51 3.57 5 -3 -1 24.82 2.73 5 -3 -1 25.70 2.38 5 -3 -1 27.03 3.27 5 -3 -1 24.02 3.02 5 -3 -1 28.43 3.82 5 -3 0 1892.45 78.02 5 -3 0 1746.25 77.34 5 -3 0 1943.70 80.32 5 -3 0 1874.29 79.06 5 -3 0 1833.87 76.98 5 -3 0 1918.26 79.75 5 -3 1 1.15 1.07 5 -3 1 0.56 0.96 5 -3 1 12.04 1.79 5 -3 1 13.25 1.90 5 -3 1 3.44 1.76 5 -3 1 2.87 1.48 5 -3 1 6.06 1.22 5 -3 1 1.89 1.22 5 -3 1 3.14 1.21 5 -3 1 2.22 1.63 5 -3 2 159.79 9.30 5 -3 2 145.69 8.73 5 -3 2 167.14 9.10 5 -3 2 138.41 9.38 5 -3 2 170.65 9.15 5 -3 2 180.70 11.03 5 -3 2 167.42 8.56 5 -3 2 176.04 9.95 5 -3 2 156.90 10.11 5 -3 3 5.14 1.50 5 -3 3 5.39 1.64 5 -3 3 5.46 1.37 5 -3 3 6.04 1.55 5 -3 3 3.98 1.21 5 -3 3 3.75 1.50 5 -3 3 3.90 1.18 5 -3 3 4.14 1.82 5 -3 4 49.53 4.11 5 -3 4 43.88 4.04 5 -3 4 43.88 4.23 5 -3 4 48.54 4.51 5 -3 4 47.21 4.00 5 -3 4 52.65 4.11 5 -3 4 50.77 3.80 5 -3 4 36.92 4.32 5 -3 5 655.37 29.12 5 -3 5 661.04 29.90 5 -3 5 677.95 30.26 5 -3 5 612.37 30.01 5 -3 5 581.37 29.07 5 -3 6 0.72 1.41 5 -3 6 1.34 0.92 5 -3 6 0.70 0.74 5 -3 7 401.55 20.07 5 -3 8 140.00 8.29 5 -3 8 157.02 9.18 5 -3 8 139.72 9.20 5 -3 9 3.50 1.38 5 -3 9 2.04 1.53 5 -3 10 195.48 10.50 5 -3 10 200.30 11.21 5 -3 11 34.71 3.99 5 -3 12 63.78 4.82 5 -3 12 66.67 5.22 5 -3 13 11.15 2.02 5 -3 14 45.19 3.55 5 -3 14 44.07 3.20 5 -2 -16 1.47 0.43 5 -2 -16 1.07 0.63 5 -2 -15 2.89 0.71 5 -2 -15 3.44 1.16 5 -2 -14 5.42 1.56 5 -2 -14 3.55 0.97 5 -2 -14 5.11 1.42 5 -2 -13 51.86 4.89 5 -2 -13 51.76 3.76 5 -2 -13 54.59 4.81 5 -2 -12 19.15 2.68 5 -2 -12 25.21 3.61 5 -2 -12 26.37 2.58 5 -2 -12 21.34 3.13 5 -2 -12 17.96 2.11 5 -2 -11 1.46 1.26 5 -2 -11 2.25 2.61 5 -2 -11 2.53 1.57 5 -2 -11 2.32 0.92 5 -2 -11 1.15 1.33 5 -2 -10 63.99 5.57 5 -2 -10 50.99 5.52 5 -2 -10 59.43 4.42 5 -2 -10 58.16 5.55 5 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1.12 5 -2 -2 5.69 1.27 5 -2 -2 5.80 1.92 5 -2 -2 4.31 1.58 5 -2 -2 6.19 1.13 5 -2 -1 3.61 1.33 5 -2 -1 4.85 1.43 5 -2 -1 2.81 1.18 5 -2 -1 4.80 1.91 5 -2 -1 4.43 1.12 5 -2 -1 3.02 0.99 5 -2 -1 7.63 2.08 5 -2 -1 4.40 1.59 5 -2 -1 4.36 0.98 5 -2 0 6.14 1.49 5 -2 0 6.39 1.33 5 -2 0 3.57 1.33 5 -2 0 4.80 1.36 5 -2 0 7.56 2.10 5 -2 0 6.41 1.35 5 -2 0 6.26 1.85 5 -2 0 6.20 1.63 5 -2 0 4.50 1.53 5 -2 1 1.77 1.09 5 -2 1 2.43 1.10 5 -2 1 4.25 1.19 5 -2 1 5.20 1.71 5 -2 1 2.29 1.18 5 -2 1 2.61 1.42 5 -2 2 99.31 6.65 5 -2 2 88.63 6.31 5 -2 2 86.98 6.12 5 -2 2 83.65 6.49 5 -2 2 109.69 6.51 5 -2 2 88.23 5.90 5 -2 2 90.37 5.86 5 -2 2 94.75 7.15 5 -2 2 97.38 6.49 5 -2 2 95.09 5.89 5 -2 2 93.37 5.47 5 -2 3 17.79 2.54 5 -2 3 17.23 2.42 5 -2 3 14.73 2.21 5 -2 3 13.52 2.50 5 -2 3 15.13 2.16 5 -2 3 17.55 2.34 5 -2 3 16.79 2.40 5 -2 3 14.83 2.85 5 -2 3 17.70 2.45 5 -2 3 20.82 2.32 5 -2 3 15.98 1.92 5 -2 4 24.95 3.04 5 -2 4 24.89 2.83 5 -2 4 21.09 3.07 5 -2 4 25.96 3.03 5 -2 4 26.44 2.16 5 -2 4 22.58 2.75 5 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5 -1 -9 243.31 14.22 5 -1 -9 254.51 12.38 -5 1 8 578.42 27.49 5 -1 -8 650.22 27.73 5 -1 -8 651.74 29.99 5 -1 -8 621.61 27.63 -5 1 7 50.41 4.00 5 -1 -7 53.15 5.01 5 -1 -7 54.99 4.06 5 -1 -7 58.38 5.38 5 -1 -7 60.13 4.16 5 -1 -6 1066.56 50.68 5 -1 -6 1248.56 52.43 5 -1 -6 1222.24 50.70 -5 1 6 1162.77 50.72 5 -1 -6 1219.77 52.76 5 -1 -6 1247.98 50.63 5 -1 -5 3.17 1.14 5 -1 -5 2.39 0.87 5 -1 -5 2.64 1.24 5 -1 -5 2.78 0.92 -5 1 5 2.89 0.99 5 -1 -5 3.93 1.48 5 -1 -5 2.59 1.05 5 -1 -5 2.48 1.00 5 -1 -4 349.27 18.31 5 -1 -4 394.56 17.64 5 -1 -4 386.64 18.93 5 -1 -4 385.19 17.66 -5 1 4 434.79 18.11 5 -1 -4 386.73 19.26 5 -1 -4 347.98 18.18 5 -1 -4 374.68 18.18 5 -1 -3 16.11 2.29 5 -1 -3 23.28 2.59 5 -1 -3 21.17 3.02 5 -1 -3 17.30 2.40 5 -1 -3 19.62 2.13 5 -1 -3 18.88 2.66 5 -1 -3 19.09 2.08 -5 1 3 25.78 2.47 5 -1 -3 21.87 2.35 5 -1 -3 19.71 2.04 5 -1 -2 2.41 1.06 5 -1 -2 0.67 0.77 -5 1 2 2.01 0.99 5 -1 -2 2.09 1.09 5 -1 -2 4.56 1.58 5 -1 -2 2.01 1.05 5 -1 -2 1.66 0.91 5 -1 -1 2935.47 124.47 5 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101.90 5.95 6 6 8 563.90 24.25 -6 -6 -8 510.57 24.51 6 6 8 562.07 24.60 -6 -6 -9 3.95 1.13 6 6 9 4.04 1.05 -6 -6 -9 4.83 1.47 6 6 9 4.23 1.26 -6 -6 -10 921.40 40.03 6 6 10 907.86 39.59 -6 -6 -11 45.91 4.01 6 6 11 46.13 3.68 -6 -6 -12 11.08 2.03 6 6 12 9.99 1.70 6 6 13 293.65 14.10 -6 -6 -13 308.57 14.89 6 6 13 290.56 14.23 -6 -6 -14 75.29 5.04 6 6 14 70.67 4.55 6 6 15 154.26 7.89 -6 -6 -15 153.16 8.39 6 6 15 154.09 8.04 6 6 16 76.33 4.46 -6 -6 -16 76.48 4.84 6 6 16 81.70 4.65 6 6 17 567.67 24.20 6 6 17 568.14 24.34 6 7 -11 92.39 4.75 -6 -7 11 107.68 5.14 6 7 -10 138.23 6.98 -6 -7 10 149.08 7.31 6 7 -9 14.33 1.66 -6 -7 9 14.77 1.80 6 7 -8 7.21 1.38 -6 -7 8 9.32 1.57 -6 -7 7 10.08 1.72 -6 -7 6 11.83 1.86 6 7 -5 76.72 5.16 -6 -7 5 58.40 4.48 6 7 -4 14.39 2.10 -6 -7 4 10.78 1.87 -6 -7 3 12.59 1.92 6 7 -3 11.57 1.85 -6 -7 3 11.07 1.84 -6 -7 3 10.19 1.92 -6 -7 2 222.71 11.08 -6 -7 2 210.90 11.53 6 7 -2 219.06 11.25 -6 -7 2 214.84 11.64 -6 -7 1 144.90 8.86 6 7 -1 160.13 8.63 -6 -7 1 153.13 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3.21 8 2 -5 43.72 3.65 8 2 -4 24.10 3.12 8 2 -4 25.74 3.27 8 2 -4 23.40 3.17 8 2 -4 35.56 2.89 8 2 -4 28.77 3.11 8 2 -3 116.97 8.17 8 2 -3 106.81 7.89 8 2 -3 121.89 8.39 8 2 -3 127.19 8.26 8 2 -3 121.02 7.51 -8 -2 3 130.26 8.04 8 2 -3 132.76 7.22 8 2 -3 131.18 7.99 8 2 -2 8.24 1.69 8 2 -2 6.69 1.84 -8 -2 2 7.04 1.82 8 2 -2 9.18 2.21 8 2 -2 8.75 2.04 8 2 -2 9.14 1.66 8 2 -2 7.55 1.90 8 2 -1 2440.32 106.35 8 2 -1 2250.34 106.39 8 2 -1 2522.27 105.83 8 2 -1 2510.54 105.22 8 2 -1 2547.06 104.52 8 2 -1 2708.73 105.86 8 2 0 8.36 2.19 8 2 0 8.80 2.21 8 2 0 5.60 1.52 -8 -2 0 11.55 2.11 8 2 0 6.53 1.80 8 2 0 8.30 1.65 8 2 0 6.59 1.89 8 2 1 73.16 5.39 8 2 1 56.06 5.47 8 2 1 62.55 5.89 -8 -2 -1 59.18 4.95 8 2 1 66.34 4.73 8 2 1 55.61 5.12 8 2 2 1.53 1.38 8 2 2 2.00 1.36 8 2 2 5.05 1.49 -8 -2 -2 4.52 1.49 8 2 2 4.49 1.60 8 2 2 3.83 1.50 8 2 3 3.00 1.51 8 2 3 6.14 1.61 -8 -2 -3 6.57 1.61 8 2 3 4.60 1.67 8 2 3 8.10 1.88 8 2 4 417.17 20.56 8 2 4 399.40 20.77 8 2 4 351.77 18.87 -8 -2 -4 406.08 19.11 8 2 4 425.90 19.75 8 2 4 376.59 19.30 8 2 5 109.82 7.75 8 2 5 105.54 7.85 8 2 5 79.58 6.16 -8 -2 -5 97.61 6.49 8 2 5 96.33 6.88 8 2 5 94.75 6.69 8 2 6 1347.32 53.47 8 2 6 1223.63 52.96 8 2 6 1360.23 53.74 8 2 6 1274.18 53.70 8 2 6 1009.91 51.25 -8 -2 -6 1211.03 51.72 8 2 6 1216.59 52.44 8 2 6 1113.31 51.81 8 2 7 135.99 8.58 8 2 7 122.55 8.13 8 2 7 108.83 7.48 8 2 7 132.98 8.70 8 2 8 1.92 1.21 8 2 8 7.05 1.86 8 2 8 2.63 1.19 8 2 8 7.14 1.71 8 2 8 5.63 1.71 8 2 9 348.69 17.35 8 2 9 374.69 17.36 8 2 9 326.80 17.68 8 2 9 366.02 17.67 8 2 10 35.28 3.20 8 2 10 40.16 4.35 8 2 10 27.29 2.27 8 2 11 85.01 5.51 8 2 11 85.35 4.79 8 2 12 46.48 4.10 8 2 12 52.16 3.67 8 2 13 12.61 1.96 8 2 13 12.87 1.54 8 2 14 45.05 3.44 8 2 15 1.30 0.59 -8 -2 -15 1.54 0.67 -8 -3 11 -0.39 0.59 -8 -3 10 6.24 1.09 8 3 -10 3.59 1.02 -8 -3 9 133.53 6.80 8 3 -9 115.38 7.00 -8 -3 8 166.82 8.02 8 3 -8 122.98 7.98 8 3 -7 36.31 2.93 8 3 -7 40.52 3.78 8 3 -6 6.29 1.23 8 3 -6 5.01 1.52 8 3 -5 23.71 2.80 8 3 -5 22.77 2.93 8 3 -5 23.90 2.43 8 3 -5 24.61 2.66 8 3 -4 15.02 2.48 8 3 -4 19.53 2.85 8 3 -4 20.07 2.74 8 3 -4 23.58 2.45 8 3 -4 26.17 2.84 8 3 -3 13.70 2.49 8 3 -3 15.56 2.18 8 3 -3 9.27 1.97 -8 -3 3 12.73 2.21 8 3 -3 12.28 2.30 8 3 -3 12.31 1.91 8 3 -3 17.38 2.41 8 3 -2 30.08 3.72 8 3 -2 25.10 3.55 8 3 -2 29.07 3.30 8 3 -2 32.39 3.31 8 3 -2 31.90 3.04 8 3 -2 35.79 3.63 8 3 -1 62.39 5.74 8 3 -1 59.91 5.79 8 3 -1 62.11 4.98 -8 -3 1 69.68 5.26 8 3 -1 61.59 4.62 8 3 -1 66.05 5.32 8 3 0 24.21 3.49 8 3 0 24.07 3.55 8 3 0 22.87 2.87 -8 -3 0 23.21 2.90 8 3 0 23.16 2.65 8 3 0 25.92 3.19 8 3 1 105.72 8.21 8 3 1 105.96 8.46 8 3 1 120.92 6.59 -8 -3 -1 122.07 7.60 8 3 1 119.21 7.21 8 3 1 131.41 7.81 8 3 2 77.79 5.76 8 3 2 70.69 6.33 8 3 2 72.66 6.52 8 3 2 76.11 4.80 -8 -3 -2 78.05 5.68 8 3 2 80.42 5.86 8 3 2 87.82 5.69 8 3 2 78.92 6.04 8 3 3 19.39 2.80 8 3 3 18.18 2.59 8 3 3 17.87 2.05 -8 -3 -3 21.09 2.67 8 3 3 19.65 2.56 8 3 3 23.79 2.92 8 3 4 7.68 2.22 8 3 4 10.28 2.41 8 3 4 11.48 2.06 -8 -3 -4 11.03 1.94 8 3 4 8.52 1.39 8 3 4 9.14 1.98 8 3 4 9.88 2.23 8 3 5 23.35 3.43 8 3 5 23.97 3.56 8 3 5 20.37 2.76 8 3 5 28.02 2.47 -8 -3 -5 27.49 2.94 8 3 5 24.66 3.16 8 3 5 22.49 3.02 8 3 6 11.69 2.46 8 3 6 8.34 2.15 8 3 6 13.03 2.14 -8 -3 -6 12.62 1.98 8 3 6 13.40 1.68 8 3 6 10.82 2.18 8 3 6 11.48 2.15 8 3 7 4.99 1.77 8 3 7 6.46 1.96 8 3 7 7.43 1.31 8 3 7 6.40 1.64 8 3 7 4.86 1.68 8 3 7 3.59 1.23 8 3 8 -0.46 1.07 8 3 8 0.51 1.11 8 3 8 0.37 0.57 8 3 8 -0.30 0.54 8 3 8 0.20 0.91 8 3 9 17.24 2.60 8 3 9 16.68 1.89 8 3 9 17.32 2.52 8 3 9 15.87 1.72 8 3 9 16.19 2.57 8 3 10 3.16 1.45 8 3 10 3.00 0.84 8 3 10 3.77 1.88 8 3 10 3.58 0.95 8 3 11 -0.15 0.79 8 3 11 1.11 0.67 8 3 11 0.21 1.70 8 3 11 1.18 0.65 8 3 12 0.65 0.77 8 3 12 1.05 0.56 8 3 12 0.56 0.62 8 3 12 1.14 1.06 -8 -3 -13 2.34 1.07 8 3 13 2.59 0.71 8 3 13 2.13 1.09 8 3 13 1.93 0.78 8 3 14 0.66 0.73 -8 -3 -14 1.48 0.97 8 3 14 1.73 0.57 8 3 15 2.55 0.77 -8 -4 10 168.51 8.22 -8 -4 9 219.25 10.61 8 4 -8 0.55 0.61 -8 -4 8 -0.13 0.83 8 4 -7 159.94 8.93 -8 -4 7 227.08 10.03 8 4 -6 70.52 4.72 -8 -4 6 86.20 5.54 8 4 -5 169.81 9.22 8 4 -5 179.63 9.23 8 4 -4 5.34 1.49 8 4 -4 4.35 1.26 8 4 -4 4.47 1.33 8 4 -3 98.19 7.21 8 4 -3 95.56 6.54 8 4 -3 116.95 6.66 8 4 -3 113.09 7.01 8 4 -2 1724.52 75.52 8 4 -2 1547.73 75.35 8 4 -2 1716.28 74.39 -8 -4 2 1828.39 74.77 8 4 -2 1824.87 74.07 8 4 -2 1840.09 74.80 8 4 -1 11.53 2.37 8 4 -1 11.70 2.05 -8 -4 1 17.30 2.45 8 4 -1 17.81 2.94 8 4 -1 12.97 2.07 8 4 -1 12.87 2.28 8 4 0 113.06 8.11 8 4 0 114.12 8.24 8 4 0 110.91 7.20 -8 -4 0 113.68 7.13 8 4 0 100.91 6.62 8 4 0 109.05 7.36 8 4 1 62.31 6.09 8 4 1 77.94 5.73 8 4 1 76.42 4.97 -8 -4 -1 83.31 5.69 8 4 1 77.66 5.38 8 4 1 75.21 6.42 8 4 2 18.05 2.99 8 4 2 14.58 2.77 8 4 2 17.82 2.18 -8 -4 -2 21.73 2.63 8 4 2 18.34 2.73 8 4 2 17.73 2.53 8 4 3 550.85 26.49 8 4 3 512.53 26.07 8 4 3 597.47 25.26 -8 -4 -3 565.62 25.88 8 4 3 553.91 25.79 8 4 3 597.56 26.13 8 4 4 49.13 4.36 8 4 4 52.27 5.28 8 4 4 50.57 5.27 8 4 4 59.34 4.82 8 4 4 59.13 4.05 -8 -4 -4 54.33 4.37 8 4 4 53.27 4.34 8 4 4 52.22 4.68 8 4 5 204.26 12.56 8 4 5 219.43 12.93 8 4 5 186.58 11.33 8 4 5 228.40 10.81 -8 -4 -5 213.42 11.16 8 4 5 210.81 11.42 8 4 5 203.88 11.66 8 4 6 33.03 4.06 8 4 6 38.75 4.42 8 4 6 27.02 3.17 8 4 6 31.84 2.89 8 4 6 31.08 3.46 8 4 6 35.81 3.54 8 4 7 488.67 22.67 8 4 7 521.53 23.98 8 4 7 468.82 23.92 8 4 7 525.68 21.84 8 4 7 460.93 22.57 8 4 7 485.16 21.00 8 4 8 42.74 4.05 8 4 8 47.79 3.57 8 4 8 49.32 4.65 8 4 8 44.94 3.16 8 4 8 42.00 3.92 8 4 9 55.74 4.75 8 4 9 69.19 5.36 8 4 9 65.37 4.32 8 4 9 64.96 4.01 8 4 9 55.96 4.53 8 4 10 4.94 1.13 8 4 10 2.59 1.21 8 4 10 2.43 0.80 8 4 10 1.65 0.99 -8 -4 -11 10.35 2.36 8 4 11 8.37 1.53 8 4 11 12.82 1.66 8 4 11 11.55 1.48 8 4 11 7.67 1.65 8 4 12 242.74 12.43 8 4 12 266.74 12.41 8 4 12 262.99 12.22 8 4 12 237.60 12.97 -8 -4 -13 16.75 2.12 8 4 13 12.06 1.46 8 4 13 14.21 1.57 8 4 13 15.03 1.55 8 4 13 12.35 1.82 8 4 14 26.88 2.07 8 4 14 27.02 2.39 8 4 14 27.07 2.07 -8 -4 -14 26.81 2.52 8 4 15 0.85 0.47 -8 -4 -15 0.91 0.73 -8 -5 10 149.23 7.31 -8 -5 9 17.42 1.86 8 5 -8 0.55 0.59 -8 -5 8 0.86 0.89 8 5 -7 68.72 4.51 -8 -5 7 88.30 5.17 8 5 -6 89.20 5.82 -8 -5 6 131.46 6.83 8 5 -5 86.22 5.63 8 5 -5 81.52 5.43 8 5 -4 56.19 4.75 8 5 -4 63.85 4.58 8 5 -4 60.59 4.38 8 5 -3 18.95 2.80 8 5 -3 21.64 2.64 8 5 -3 20.79 2.47 8 5 -2 4.00 1.56 8 5 -2 3.77 1.29 8 5 -2 4.53 1.47 8 5 -1 105.51 7.77 8 5 -1 95.65 7.62 8 5 -1 108.72 7.06 -8 -5 1 124.10 7.27 8 5 -1 106.57 6.72 8 5 -1 106.56 7.16 8 5 0 258.70 15.69 8 5 0 291.59 14.91 -8 -5 0 308.43 14.79 8 5 0 260.33 15.57 8 5 0 322.69 15.39 8 5 1 65.50 6.09 8 5 1 70.20 5.43 8 5 1 74.38 4.92 -8 -5 -1 71.93 5.24 8 5 1 77.60 5.30 8 5 1 64.55 6.02 8 5 2 2.27 1.41 8 5 2 2.14 1.21 -8 -5 -2 2.59 1.08 8 5 2 2.78 1.67 8 5 2 3.70 1.36 8 5 3 43.40 4.73 8 5 3 35.98 4.42 8 5 3 38.98 3.94 8 5 3 46.73 3.65 -8 -5 -3 47.58 3.89 8 5 3 41.69 3.80 8 5 3 42.33 3.62 8 5 4 6.89 1.96 8 5 4 4.76 1.39 8 5 4 5.20 1.39 -8 -5 -4 5.62 1.31 8 5 4 4.75 1.38 8 5 4 5.65 1.39 8 5 5 5.19 1.29 8 5 5 3.73 1.72 8 5 5 4.90 1.73 8 5 5 5.60 1.54 8 5 5 4.14 1.16 8 5 5 5.22 0.95 8 5 5 6.87 1.60 8 5 5 3.96 1.47 8 5 6 0.35 0.81 8 5 6 -0.92 1.37 8 5 6 0.32 0.88 8 5 6 1.54 1.05 8 5 6 0.15 0.86 8 5 6 0.30 0.51 8 5 6 0.68 1.05 8 5 7 30.68 3.12 -8 -5 -7 31.27 2.90 8 5 7 38.84 4.23 8 5 7 28.70 2.79 8 5 7 30.24 2.49 8 5 7 27.13 3.23 8 5 8 18.14 2.38 -8 -5 -8 20.09 2.39 8 5 8 21.63 3.06 8 5 8 21.43 2.34 8 5 8 20.09 2.02 8 5 8 18.23 2.61 8 5 9 6.05 1.44 -8 -5 -9 7.56 1.59 8 5 9 9.35 2.01 8 5 9 7.03 1.42 8 5 9 7.70 1.25 8 5 9 4.77 1.38 -8 -5 -10 50.25 4.07 8 5 10 54.67 4.49 8 5 10 57.91 3.96 8 5 10 53.29 3.62 8 5 10 49.44 4.04 -8 -5 -11 12.42 2.18 8 5 11 10.36 1.61 8 5 11 5.96 1.28 8 5 11 11.08 1.44 8 5 11 8.46 1.52 8 5 12 12.98 1.66 -8 -5 -12 12.57 1.96 8 5 12 12.86 1.57 8 5 12 12.19 1.60 8 5 13 37.61 2.68 8 5 13 37.77 2.82 -8 -5 -13 32.84 3.03 8 5 14 12.57 1.38 8 5 14 12.96 1.43 -8 -5 -14 13.45 1.75 8 5 15 21.72 1.65 8 5 15 19.51 1.64 -8 -5 -15 19.54 1.93 -8 -6 9 84.74 4.66 8 6 -8 21.97 1.87 8 6 -7 5.32 1.08 8 6 -6 11.53 1.61 8 6 -5 18.41 2.15 -8 -6 5 20.71 2.33 8 6 -4 150.53 8.52 8 6 -4 161.82 8.60 -8 -6 4 164.63 8.71 8 6 -3 55.45 4.90 8 6 -3 66.54 4.74 8 6 -3 62.39 4.50 8 6 -2 335.00 15.98 8 6 -2 298.85 16.39 8 6 -1 44.00 4.57 8 6 -1 48.77 4.02 8 6 0 22.96 2.76 8 6 1 319.81 14.11 8 6 1 231.44 13.66 8 6 2 0.32 1.13 8 6 2 0.55 1.03 8 6 3 121.91 7.25 8 6 3 124.59 7.00 8 6 4 10.07 1.76 8 6 4 5.75 1.52 8 6 4 8.30 1.19 8 6 4 7.65 1.70 8 6 5 42.62 3.71 8 6 5 35.19 2.72 8 6 5 45.87 3.55 8 6 5 28.96 3.36 8 6 6 585.51 27.35 8 6 6 647.25 28.33 8 6 7 13.47 2.58 8 6 7 11.50 1.77 8 6 7 9.41 1.38 8 6 7 13.29 2.57 -8 -6 -8 147.61 8.51 8 6 8 176.66 10.48 8 6 8 177.99 9.04 8 6 8 168.62 8.39 8 6 8 162.54 9.43 -8 -6 -9 525.90 25.11 8 6 9 598.73 25.39 8 6 9 579.73 24.81 8 6 9 497.02 25.44 8 6 10 23.22 2.41 8 6 10 22.49 2.83 -8 -6 -10 24.19 2.56 8 6 10 24.52 2.25 8 6 11 98.77 5.78 -8 -6 -11 96.10 5.92 8 6 11 96.52 5.46 8 6 12 6.46 1.25 -8 -6 -12 7.05 1.47 8 6 12 5.67 1.08 8 6 13 146.85 7.42 -8 -6 -13 134.49 7.57 8 6 13 147.84 7.24 8 6 14 191.82 8.95 -8 -6 -14 170.35 9.08 8 6 14 192.55 8.78 8 6 15 3.86 0.75 8 6 15 3.42 0.69 -8 -6 -15 3.92 0.89 8 7 -8 2.07 0.64 -8 -7 8 2.56 0.77 8 7 -7 8.83 1.22 -8 -7 7 12.11 1.47 8 7 -6 23.65 2.19 -8 -7 6 25.62 2.29 8 7 -5 21.16 2.21 -8 -7 5 22.53 2.26 -8 -7 4 1.70 1.01 -8 -7 3 112.46 6.25 8 7 -3 103.84 6.33 8 7 -3 95.35 6.64 8 7 -2 191.02 10.57 8 7 -2 161.81 10.84 8 7 -1 42.04 3.64 8 7 0 15.91 2.70 8 7 1 10.70 2.62 8 7 2 168.29 9.46 8 7 3 186.21 10.16 8 7 4 72.92 5.36 8 7 5 8.96 1.33 8 7 5 9.92 2.34 8 7 6 0.76 0.70 8 7 6 1.51 0.90 8 7 7 38.87 2.93 8 7 8 5.40 1.10 8 7 8 6.92 1.95 8 7 9 80.30 4.62 8 7 9 79.39 5.94 -8 -7 -10 45.49 3.53 8 7 10 57.06 3.61 8 7 10 46.63 3.75 8 7 10 57.31 4.54 -8 -7 -11 0.38 0.76 8 7 11 0.10 0.64 -8 -7 -12 35.93 2.94 8 7 12 41.07 2.84 -8 -7 -13 12.72 1.65 8 7 13 16.06 1.56 -8 -7 -14 20.54 1.86 8 7 14 16.91 1.56 8 7 15 30.64 1.96 8 8 -7 16.19 1.38 -8 -8 6 49.84 3.05 -8 -8 5 219.05 10.24 8 8 -4 70.85 4.46 -8 -8 4 74.93 4.37 -8 -8 3 12.74 1.57 8 8 -3 10.54 1.59 -8 -8 3 9.80 1.46 8 8 -2 74.73 5.62 -8 -8 2 93.14 5.11 8 8 -2 86.45 5.45 8 8 -2 82.28 5.22 -8 -8 1 3.93 1.02 8 8 -1 2.75 1.06 -8 -8 0 530.09 22.36 8 8 0 472.13 22.67 8 8 1 13.94 2.04 8 8 2 13.81 2.06 8 8 3 15.59 2.06 8 8 3 11.52 1.91 8 8 4 1.55 1.00 8 8 4 2.19 1.28 8 8 5 354.63 18.77 8 8 5 491.86 19.40 8 8 6 5.79 1.10 8 8 6 5.81 1.90 8 8 7 9.89 1.42 8 8 7 12.97 2.13 8 8 8 180.52 9.39 8 8 8 216.10 10.04 8 8 9 548.54 24.64 8 8 9 586.12 23.40 8 8 9 510.93 22.78 8 8 10 83.87 4.93 8 8 10 86.28 4.73 8 8 11 23.32 2.17 8 8 11 22.22 2.00 8 8 12 57.92 3.70 8 8 12 60.60 3.58 8 8 13 62.67 3.70 8 8 13 62.49 3.57 8 8 14 566.30 24.18 8 8 14 571.60 24.07 8 9 -5 6.60 0.92 8 9 -4 29.98 2.24 8 9 -3 59.39 3.68 8 9 -2 16.48 1.72 -8 -9 2 13.77 1.62 8 9 -2 12.57 1.75 8 9 -1 14.36 1.69 -8 -9 1 10.72 1.61 8 9 -1 14.27 2.06 8 9 0 46.13 3.40 8 9 1 29.15 2.61 8 9 2 20.44 2.14 8 9 3 5.88 1.26 8 9 4 45.16 3.33 8 9 5 42.67 3.21 8 9 5 50.20 3.47 8 9 6 20.10 1.89 8 9 6 23.85 2.24 8 9 7 13.69 1.52 8 9 7 12.06 1.59 8 9 8 2.97 0.87 8 9 8 1.44 0.74 8 9 9 34.13 2.69 8 9 9 38.63 3.51 8 9 9 39.52 2.69 -8 -9 -9 32.17 2.89 8 9 10 145.42 7.05 8 9 10 124.40 6.95 -8 -9 -10 122.27 6.85 8 9 10 158.78 6.99 8 9 11 98.21 5.40 8 9 11 107.47 5.35 8 9 12 5.01 0.89 8 9 12 5.19 0.84 8 9 13 62.00 3.41 8 9 13 64.67 3.38 8 10 -3 5.17 0.72 8 10 -2 10.65 1.12 8 10 -1 11.93 1.24 8 10 0 10.11 1.58 -8 -10 0 13.38 1.44 8 10 0 9.77 1.21 -8 -10 0 12.93 1.56 -8 -10 -1 219.34 10.11 8 10 1 192.78 9.56 -8 -10 -1 220.06 10.26 8 10 2 11.95 1.34 -8 -10 -2 15.64 1.78 -8 -10 -2 16.11 1.97 -8 -10 -3 116.24 6.64 -8 -10 -4 0.14 0.89 8 10 5 53.30 3.18 8 10 6 177.54 8.50 -8 -10 -6 190.17 9.48 -8 -10 -7 47.60 3.59 8 10 7 55.40 3.23 -8 -10 -7 56.98 3.93 -8 -10 -8 612.21 28.81 8 10 8 691.21 28.44 -8 -10 -8 707.65 29.14 8 10 9 41.93 3.14 8 10 9 37.24 2.41 8 10 9 28.15 2.43 -8 -10 -9 30.55 2.44 8 10 9 38.18 2.38 8 10 10 5.21 0.80 8 10 10 5.21 0.80 8 10 11 8.40 0.93 -8 -11 -2 29.83 2.03 8 11 2 25.65 1.58 8 11 3 0.17 0.30 -8 -11 -3 0.08 0.42 -8 -11 -3 0.26 0.56 8 11 4 13.59 1.15 -8 -11 -4 17.77 1.71 -8 -11 -5 18.51 1.73 8 11 5 19.28 1.40 -8 -11 -6 22.01 1.95 8 11 6 25.67 1.66 -8 -11 -6 24.54 2.12 -8 -11 -7 23.70 1.88 8 11 7 23.56 1.57 -8 -11 -7 21.87 1.90 8 11 7 22.80 2.17 -8 -11 -8 6.59 0.90 8 11 8 10.27 0.91 8 11 9 70.49 3.47 9 -4 -4 0.19 0.58 9 -4 -3 4.11 0.82 9 -4 -3 4.18 1.02 9 -4 -2 20.97 1.85 9 -4 0 9.85 1.31 9 -4 1 12.65 1.17 9 -4 1 14.42 1.54 9 -4 2 10.98 1.27 9 -4 2 10.25 1.06 9 -4 3 4.78 0.79 9 -4 3 5.30 0.76 9 -3 -6 50.94 3.61 9 -3 -5 66.27 4.50 9 -3 -4 218.53 11.43 9 -3 -4 235.09 10.76 9 -3 -3 115.72 7.13 9 -3 -3 130.42 6.74 9 -3 -2 14.13 2.13 9 -3 -2 20.77 2.14 9 -3 -1 0.96 0.98 9 -3 0 134.84 7.91 9 -3 0 156.18 8.00 9 -3 1 272.82 12.85 9 -3 1 259.63 12.00 9 -3 2 215.19 10.77 9 -3 2 219.76 10.23 9 -3 3 9.78 1.48 9 -3 3 10.51 1.34 9 -3 4 40.92 3.05 9 -3 4 49.15 3.06 9 -3 5 3.48 0.76 9 -3 5 4.04 0.86 9 -3 7 2.27 0.55 9 -2 -8 1.84 0.83 9 -2 -6 4.05 1.30 9 -2 -5 8.49 1.79 9 -2 -4 7.12 1.35 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512.35 24.40 9 1 6 528.57 25.76 9 1 7 23.82 2.96 9 1 7 25.02 3.04 9 1 7 23.93 3.05 9 1 8 32.61 3.11 9 1 8 42.60 3.77 9 1 9 31.02 2.80 9 1 9 30.82 3.13 9 1 10 3.17 1.04 9 1 10 3.31 1.19 9 1 11 794.06 34.52 9 1 11 832.25 35.12 9 1 12 2.57 0.76 9 1 12 2.16 0.80 -9 -1 -12 3.42 0.87 9 2 -10 3.78 1.00 9 2 -9 0.37 0.51 -9 -2 8 1.29 0.57 9 2 -8 1.00 0.70 9 2 -8 1.75 1.24 -9 -2 7 2.03 0.79 9 2 -7 1.21 0.93 9 2 -7 2.23 1.35 -9 -2 6 0.77 0.71 9 2 -6 0.90 1.26 9 2 -6 1.04 0.85 9 2 -5 0.19 0.91 9 2 -4 2.84 1.21 9 2 -4 1.98 1.07 9 2 -4 3.56 1.20 9 2 -3 4.36 1.82 9 2 -3 2.97 1.31 9 2 -3 2.90 1.31 9 2 -2 53.62 4.85 9 2 -2 41.62 4.47 9 2 -2 49.29 4.33 9 2 -2 55.24 5.54 9 2 -1 62.70 5.41 9 2 -1 51.65 4.85 9 2 -1 54.27 4.71 9 2 -1 55.13 5.27 9 2 0 56.13 5.16 9 2 0 42.87 4.29 9 2 0 42.39 4.22 9 2 0 40.67 4.64 9 2 1 7.75 1.86 9 2 1 12.57 2.49 9 2 1 15.03 2.87 9 2 2 1.18 1.28 9 2 2 0.21 1.15 9 2 2 1.89 2.18 9 2 2 0.62 1.15 9 2 3 7.72 1.88 9 2 3 4.92 2.38 9 2 4 -0.57 1.12 9 2 4 2.37 1.45 9 2 4 1.61 2.23 9 2 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9 3 1 35.31 4.17 9 3 2 29.58 3.94 9 3 2 31.02 3.40 9 3 3 106.12 7.28 9 3 3 94.69 6.63 9 3 4 168.96 10.63 9 3 4 181.18 10.44 9 3 4 154.01 9.47 9 3 5 135.31 9.36 9 3 5 147.40 9.17 9 3 5 152.80 8.89 9 3 6 2.27 1.50 9 3 6 0.81 1.10 9 3 6 0.64 1.33 9 3 6 4.34 1.56 9 3 7 183.67 10.59 9 3 7 176.36 10.34 9 3 7 188.14 10.09 9 3 8 61.00 4.99 9 3 8 55.97 4.73 9 3 8 46.30 4.03 9 3 8 51.32 4.10 9 3 8 69.25 5.05 9 3 9 139.24 8.03 9 3 9 157.09 8.67 9 3 10 44.54 3.44 9 3 10 41.73 3.67 9 3 11 30.72 2.93 9 3 11 30.59 2.65 -9 -3 -11 34.21 2.90 9 3 12 389.18 17.58 9 3 12 367.55 17.04 -9 -3 -12 401.41 17.48 9 3 13 8.51 1.23 -9 -3 -13 8.48 1.28 9 3 13 6.29 0.90 -9 -4 9 16.32 1.45 -9 -4 8 4.37 0.93 -9 -4 7 5.34 1.12 -9 -4 6 0.86 0.85 9 4 -6 0.82 0.58 9 4 -5 40.73 3.19 -9 -4 5 57.69 3.87 9 4 -4 77.74 5.41 9 4 -4 78.87 4.94 9 4 -4 84.63 5.29 9 4 -4 78.84 5.54 9 4 -3 17.40 2.57 9 4 -3 21.69 2.35 9 4 -3 19.78 2.44 9 4 -3 17.92 2.56 9 4 -2 24.75 3.12 9 4 -2 27.28 3.00 9 4 -2 22.38 2.53 9 4 -1 1.96 1.08 9 4 -1 1.04 1.10 9 4 -1 1.06 1.68 9 4 0 36.94 4.32 9 4 0 37.55 3.87 9 4 0 36.44 3.39 9 4 1 51.35 5.07 9 4 1 54.23 4.25 9 4 2 0.89 1.16 9 4 2 2.70 1.25 9 4 2 0.23 1.92 9 4 3 2.09 2.30 9 4 3 0.19 0.96 9 4 3 0.12 0.71 9 4 4 16.95 2.37 9 4 4 12.21 2.55 9 4 4 16.98 3.56 9 4 4 15.14 1.80 9 4 5 25.25 2.93 9 4 5 22.30 3.33 9 4 5 27.07 3.87 9 4 5 23.63 2.25 9 4 6 53.32 4.42 9 4 6 56.92 5.30 9 4 6 64.92 5.00 9 4 6 55.78 3.80 9 4 7 6.04 1.57 9 4 7 5.50 1.10 9 4 7 4.90 1.70 9 4 7 5.94 1.47 9 4 8 100.70 6.87 9 4 8 85.26 5.93 9 4 8 95.97 5.33 9 4 8 96.37 6.69 9 4 8 86.83 5.96 9 4 9 -0.21 0.80 9 4 9 0.17 0.84 9 4 9 0.51 0.55 9 4 9 -0.19 0.81 9 4 9 -0.30 0.74 9 4 10 6.23 1.02 9 4 10 5.07 1.29 9 4 10 5.11 1.24 -9 -4 -10 5.66 1.33 9 4 11 37.36 3.14 9 4 11 39.65 3.07 -9 -4 -11 38.93 3.13 9 4 12 40.88 3.13 9 4 12 44.84 3.03 -9 -4 -12 46.98 3.31 9 4 13 1.70 0.63 -9 -4 -13 2.17 0.86 9 4 13 1.64 0.55 -9 -4 -14 33.87 2.36 -9 -5 8 -0.40 0.76 -9 -5 7 9.46 1.34 9 5 -6 25.85 2.17 -9 -5 6 29.48 2.52 9 5 -5 18.96 1.94 -9 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9.24 1.20 9 8 -2 30.03 2.43 -9 -8 2 30.79 2.26 9 8 -1 10.52 1.74 -9 -8 1 13.77 1.51 9 8 -1 12.43 1.66 9 8 -1 11.23 1.62 -9 -8 0 35.51 2.59 9 8 0 30.35 2.71 9 8 0 34.38 3.06 9 8 0 31.35 3.29 -9 -8 -1 49.59 3.28 9 8 1 46.67 3.54 9 8 1 52.07 3.97 9 8 1 47.73 4.26 9 8 2 9.42 1.57 9 8 2 12.15 2.00 9 8 2 12.65 2.22 9 8 3 10.32 1.61 9 8 3 9.38 2.01 9 8 4 10.79 1.66 9 8 4 14.68 2.17 9 8 4 14.52 2.47 9 8 5 18.39 2.44 9 8 6 52.54 3.21 9 8 6 56.44 4.32 9 8 6 64.51 5.05 9 8 7 89.45 4.85 9 8 7 95.82 5.94 9 8 8 2.98 0.69 9 8 8 2.27 1.00 9 8 8 4.22 1.35 9 8 9 15.79 1.42 9 8 9 13.29 1.68 9 8 9 13.54 1.95 9 8 10 1.04 0.52 9 8 11 43.80 2.60 9 8 12 0.29 0.36 9 9 -3 0.54 0.43 9 9 -2 50.11 3.02 -9 -9 1 4.18 0.85 9 9 -1 2.07 0.70 9 9 -1 2.96 0.76 9 9 -1 2.71 0.77 -9 -9 0 112.75 5.95 9 9 0 103.60 6.25 9 9 0 113.00 5.99 9 9 0 106.69 5.71 9 9 1 5.37 1.05 9 9 1 7.04 1.31 9 9 1 8.06 1.50 9 9 2 52.45 4.14 9 9 2 50.70 3.70 9 9 2 47.33 3.26 9 9 3 70.60 5.10 9 9 3 67.24 4.09 9 9 4 1.02 0.85 9 9 4 1.94 1.15 9 9 5 62.61 4.38 9 9 6 20.97 2.58 9 9 6 19.45 1.53 9 9 6 19.03 2.22 9 9 7 0.52 0.81 9 9 7 0.09 0.58 9 9 7 0.43 0.44 9 9 7 1.41 0.92 -9 -9 -8 479.66 20.07 9 9 8 478.74 20.72 9 9 8 453.62 19.59 9 9 8 426.09 19.89 9 9 8 431.42 19.14 9 9 9 99.95 4.97 9 9 9 84.63 4.93 9 9 9 94.61 4.63 9 9 10 51.56 3.03 9 9 10 49.38 2.76 9 9 11 26.16 1.80 9 9 11 25.05 1.60 -9 -10 -1 35.65 2.29 9 10 1 34.07 2.38 9 10 2 8.37 1.34 -9 -10 -2 8.00 1.09 9 10 2 9.81 1.24 -9 -10 -2 9.34 1.23 9 10 3 1.04 0.76 -9 -10 -3 0.71 0.58 9 10 3 0.39 0.57 -9 -10 -3 0.58 0.67 9 10 4 22.72 2.36 9 10 4 23.94 2.16 -9 -10 -4 25.16 2.21 -9 -10 -5 9.15 1.28 9 10 5 9.47 1.35 9 10 6 7.72 1.38 -9 -10 -6 9.27 1.27 9 10 6 9.46 1.29 -9 -10 -6 10.27 1.38 9 10 7 61.42 3.88 -9 -10 -7 52.42 3.30 9 10 7 50.59 2.77 -9 -10 -7 59.14 3.48 9 10 7 53.93 3.38 9 10 8 5.70 0.85 -9 -10 -8 5.76 0.85 9 10 8 4.66 0.62 10 -2 -3 83.41 4.59 10 -2 -2 88.48 5.17 10 -2 -2 110.45 5.26 10 -2 -1 6.33 1.05 10 -2 1 0.67 0.66 10 -2 2 91.68 5.03 10 -2 3 2.19 0.67 10 -1 -6 2.84 0.77 10 -1 -5 6.80 1.20 10 -1 -4 4.66 1.12 10 -1 -3 7.41 1.14 10 -1 -3 6.10 1.26 10 -1 -2 0.97 0.76 10 -1 -2 -0.38 0.74 10 -1 -1 -0.24 0.69 10 -1 -1 0.73 0.79 10 -1 0 1.22 0.81 10 -1 1 0.91 0.85 10 -1 2 7.25 1.36 10 -1 3 1.32 0.86 10 -1 4 2.15 0.84 10 -1 4 2.19 0.64 10 -1 5 -0.27 0.54 10 -1 5 0.07 0.47 10 -1 5 0.06 0.39 10 -1 6 8.41 1.03 10 -1 6 7.43 0.94 10 -1 7 5.75 0.81 10 0 -7 13.91 1.48 10 0 -6 15.18 1.77 10 0 -5 29.70 2.69 10 0 -4 348.98 16.33 10 0 -3 9.51 1.40 10 0 -3 8.31 1.58 10 0 -2 38.27 3.36 10 0 -2 43.54 3.30 10 0 -1 1.27 0.91 10 0 -1 1.49 0.92 10 0 0 1.24 0.87 10 0 1 413.42 19.75 10 0 1 412.36 19.14 10 0 2 23.08 2.50 10 0 3 4.73 1.30 10 0 3 3.14 0.85 10 0 4 0.96 0.79 10 0 4 0.47 0.62 10 0 5 2.09 0.88 10 0 5 1.13 0.72 10 0 5 2.43 0.85 10 0 6 214.66 9.74 10 0 6 219.65 10.10 10 0 7 4.25 0.88 10 0 7 3.34 0.86 10 0 8 45.83 2.90 10 0 8 47.80 3.06 10 1 -7 6.57 1.15 10 1 -6 3.18 1.06 10 1 -5 1.90 1.04 10 1 -4 -0.80 0.95 10 1 -3 23.12 2.64 10 1 -3 21.41 2.39 10 1 -2 27.77 2.95 10 1 -2 32.33 3.11 10 1 -1 7.91 1.66 10 1 -1 10.63 1.87 10 1 -1 8.61 1.85 10 1 0 0.31 0.83 10 1 0 0.63 1.05 10 1 0 0.67 0.91 10 1 1 1.09 1.04 10 1 1 0.23 0.90 10 1 2 8.35 1.27 10 1 2 6.80 1.77 10 1 3 10.11 1.97 10 1 3 9.83 1.42 10 1 4 7.38 1.73 10 1 4 6.93 1.25 10 1 4 5.72 1.64 10 1 5 2.31 0.92 10 1 5 3.21 1.29 10 1 6 5.18 1.15 10 1 6 5.80 1.36 10 1 7 27.52 2.26 10 1 7 17.55 1.90 10 1 8 23.54 2.24 10 1 9 1.84 0.70 10 1 9 1.48 0.71 10 1 10 20.38 1.68 10 1 10 23.48 1.86 10 2 -7 1.30 0.81 10 2 -6 -0.27 0.86 -10 -2 5 114.69 5.85 10 2 -5 132.39 7.16 10 2 -4 14.41 2.12 10 2 -4 17.73 1.91 10 2 -3 4.86 1.42 10 2 -3 6.11 1.40 10 2 -3 6.14 1.45 10 2 -2 141.43 8.57 10 2 -2 165.67 9.00 10 2 -2 163.90 9.14 10 2 -1 121.00 7.57 10 2 -1 126.54 7.50 10 2 0 33.68 3.64 10 2 0 30.75 3.45 10 2 1 -0.49 0.99 10 2 1 0.11 0.65 10 2 1 0.23 0.99 10 2 2 94.88 6.64 10 2 2 83.49 6.21 10 2 2 79.61 4.95 10 2 3 37.00 2.99 10 2 4 54.90 4.06 10 2 4 42.89 4.31 10 2 4 44.64 4.24 10 2 4 48.63 3.56 10 2 5 299.55 14.35 10 2 5 297.40 15.19 10 2 5 285.50 14.87 10 2 5 290.13 13.84 10 2 6 35.99 3.28 10 2 6 44.24 3.93 10 2 6 42.50 3.75 10 2 6 39.67 3.15 10 2 7 112.62 6.68 10 2 7 121.82 7.18 10 2 7 121.12 7.04 10 2 8 19.37 1.88 10 2 8 27.15 2.47 10 2 9 386.09 17.30 10 2 9 390.31 17.56 -10 -2 -10 11.40 1.29 10 2 10 9.53 1.25 10 2 10 12.53 1.46 10 2 11 11.56 1.16 10 3 -7 0.10 0.62 10 3 -6 2.71 0.96 -10 -3 6 2.85 0.68 10 3 -5 7.40 1.51 -10 -3 5 6.97 1.09 10 3 -4 7.28 1.60 10 3 -3 18.48 2.44 10 3 -3 21.76 2.35 10 3 -3 18.42 2.30 10 3 -2 8.90 1.82 10 3 -2 9.28 1.71 10 3 -2 10.20 1.88 10 3 -1 0.82 0.92 10 3 -1 0.33 0.97 10 3 -1 2.16 1.21 10 3 -1 0.34 0.92 10 3 0 37.26 3.92 10 3 0 43.15 3.74 10 3 0 41.50 4.02 10 3 1 13.55 2.55 10 3 1 13.75 2.33 10 3 2 0.51 1.06 10 3 2 0.38 1.01 10 3 2 1.20 1.17 10 3 3 41.82 3.80 10 3 4 5.70 1.79 10 3 4 9.81 2.07 10 3 4 9.52 1.88 10 3 5 9.38 1.62 10 3 5 8.98 2.01 10 3 5 8.87 1.94 10 3 5 8.14 1.70 10 3 5 7.42 1.45 10 3 6 22.44 2.84 10 3 6 20.12 2.37 10 3 6 25.55 3.04 10 3 7 6.83 1.56 10 3 7 5.02 1.37 10 3 7 6.05 1.33 10 3 8 0.96 0.76 10 3 8 2.13 0.94 -10 -3 -9 9.27 1.29 10 3 9 11.60 1.50 10 3 9 12.74 1.65 -10 -3 -10 22.34 1.95 10 3 10 27.04 2.14 10 3 10 22.78 2.10 10 3 11 19.05 1.65 10 3 11 20.32 1.75 10 4 -7 16.10 1.64 10 4 -6 7.04 1.34 -10 -4 6 7.65 1.04 10 4 -5 0.13 0.79 -10 -4 5 0.18 0.59 10 4 -4 1.63 1.00 -10 -4 4 0.51 0.67 10 4 -3 43.34 3.66 10 4 -3 49.63 3.66 10 4 -3 46.80 3.64 10 4 -2 651.99 28.56 10 4 -2 653.70 28.70 10 4 -2 695.11 28.25 10 4 -1 420.11 20.19 10 4 -1 408.14 19.48 10 4 -1 434.38 20.14 10 4 0 11.83 2.21 10 4 0 11.61 1.94 10 4 0 13.94 2.24 10 4 1 8.44 1.98 10 4 1 8.87 1.79 10 4 1 8.33 1.97 10 4 2 148.06 9.28 10 4 2 147.35 9.13 10 4 3 448.31 20.33 10 4 3 368.05 18.88 10 4 4 1.50 1.10 10 4 4 3.56 1.46 10 4 5 62.36 5.21 10 4 5 59.70 5.04 10 4 5 64.75 4.78 10 4 6 867.87 37.60 10 4 6 890.02 37.51 10 4 6 875.43 36.35 10 4 7 103.75 6.61 10 4 7 105.17 6.51 10 4 7 81.85 5.68 10 4 7 97.08 5.74 10 4 7 101.76 5.80 10 4 8 96.71 6.18 10 4 8 100.97 6.14 10 4 8 95.55 5.66 10 4 8 99.98 5.71 10 4 9 16.63 1.81 -10 -4 -9 15.23 1.56 10 4 9 18.58 1.90 10 4 10 59.17 3.55 10 4 10 62.09 3.62 10 4 11 223.41 10.21 10 5 -6 13.72 1.58 -10 -5 6 21.13 1.60 10 5 -5 13.24 1.68 -10 -5 5 16.18 1.57 -10 -5 4 9.80 1.35 10 5 -4 8.73 1.14 10 5 -4 7.15 1.37 10 5 -3 -0.12 0.70 10 5 -3 0.09 0.57 10 5 -3 0.13 0.82 10 5 -3 -0.13 0.57 10 5 -2 11.56 1.76 10 5 -2 15.88 2.13 10 5 -2 18.48 1.88 10 5 -2 12.51 1.75 10 5 -2 17.33 2.15 10 5 -1 137.65 8.34 10 5 -1 149.51 7.60 10 5 -1 143.29 7.88 10 5 -1 133.71 8.19 10 5 0 73.44 4.76 10 5 0 77.28 5.18 10 5 0 73.04 5.46 10 5 1 5.24 1.45 10 5 1 3.77 1.46 10 5 2 73.19 5.69 10 5 3 0.37 0.92 10 5 3 0.23 1.09 10 5 4 -0.36 0.93 10 5 5 22.06 2.55 10 5 5 16.06 2.52 10 5 6 2.46 1.17 10 5 6 2.33 1.17 10 5 7 2.68 1.08 10 5 7 2.67 1.05 10 5 7 2.22 1.16 10 5 8 20.00 2.40 10 5 8 16.42 1.92 10 5 8 20.14 2.48 10 5 9 17.31 1.86 10 5 10 24.84 2.09 10 5 11 14.22 1.37 10 6 -5 54.08 3.16 -10 -6 5 78.56 3.69 10 6 -4 1.35 0.67 10 6 -4 2.19 0.64 10 6 -3 499.28 21.66 10 6 -2 58.48 4.08 10 6 -2 59.84 4.05 10 6 -2 55.46 3.75 10 6 -2 59.53 3.75 10 6 -1 119.40 7.26 10 6 -1 136.00 7.11 10 6 -1 125.83 6.77 10 6 0 3.69 1.15 10 6 0 3.34 1.26 10 6 1 20.12 2.41 10 6 1 23.15 2.78 10 6 2 154.91 9.20 10 6 3 19.54 2.40 10 6 3 21.44 2.83 10 6 4 6.32 1.53 10 6 5 228.26 11.94 10 6 5 246.64 12.74 10 6 6 233.94 12.12 10 6 6 257.68 12.95 10 6 7 38.83 2.68 10 6 7 45.32 3.76 10 6 8 0.24 0.50 10 6 8 1.10 0.92 10 6 8 0.24 0.62 10 6 8 0.83 0.79 10 6 9 22.48 1.98 10 6 9 23.48 1.78 10 6 10 131.48 6.50 10 6 11 287.33 12.53 10 7 -4 27.61 1.85 10 7 -3 119.25 6.35 -10 -7 3 146.75 6.52 10 7 -2 46.74 3.14 -10 -7 2 54.09 3.20 10 7 -1 -0.65 0.68 10 7 -1 -0.21 0.66 -10 -7 1 0.17 0.57 10 7 0 32.29 2.94 10 7 0 31.49 2.67 10 7 0 27.15 2.41 10 7 1 55.59 4.36 10 7 1 56.78 4.03 10 7 1 56.10 3.76 10 7 2 71.02 5.27 10 7 2 82.49 5.10 10 7 2 71.50 4.56 10 7 3 17.53 2.43 10 7 4 0.46 0.82 10 7 5 7.19 1.63 10 7 5 8.19 1.56 10 7 6 0.18 0.85 10 7 6 1.26 0.86 10 7 7 50.25 3.92 10 7 7 51.24 3.10 10 7 8 3.09 0.84 10 7 8 3.92 0.78 10 7 9 6.66 0.99 10 7 9 7.44 0.98 10 7 10 21.46 1.65 10 7 10 22.38 1.66 10 8 -1 1.98 0.67 10 8 0 81.46 4.84 10 8 0 81.62 4.61 10 8 0 82.43 4.51 10 8 1 2.45 0.87 10 8 1 2.48 0.82 10 8 1 1.72 0.77 10 8 2 25.37 2.55 10 8 2 23.22 2.22 10 8 3 15.97 2.09 10 8 4 5.28 1.31 10 8 4 6.45 1.27 10 8 5 281.58 13.32 10 8 6 148.09 7.63 10 8 6 118.12 6.79 10 8 7 7.75 1.39 10 8 7 7.94 1.24 10 8 8 122.64 6.08 10 8 8 94.87 5.39 10 8 9 0.32 0.38 10 9 1 34.06 2.26 10 9 2 11.60 1.30 -10 -9 -2 11.00 1.30 10 9 3 9.39 1.36 10 9 4 64.49 4.05 10 9 4 55.31 3.59 10 9 5 2.91 0.82 10 9 6 25.55 2.27 10 9 6 23.27 1.98 -10 -9 -6 25.92 2.08 10 9 7 1.09 0.52 11 0 0 0.46 0.43 11 0 2 13.20 1.31 11 1 -1 0.22 0.59 11 1 0 25.15 2.08 11 1 2 9.10 1.28 11 1 3 40.63 2.80 11 1 4 63.23 3.69 11 1 5 2.67 0.60 11 2 -2 8.27 1.01 11 2 -1 2.30 0.74 11 2 0 10.11 1.47 11 2 1 -0.13 0.64 11 2 2 1.53 0.75 11 2 4 4.58 0.79 11 2 4 4.25 1.11 11 2 5 1.05 0.63 11 2 5 0.46 0.45 11 2 6 4.92 0.82 11 2 6 5.18 0.80 11 2 7 5.41 0.79 -11 -3 2 75.17 3.93 11 3 -1 11.55 1.55 11 3 -1 16.89 1.77 11 3 0 85.84 5.38 11 3 0 90.30 5.36 11 3 1 126.23 7.28 11 3 1 129.81 7.21 11 3 2 2.21 0.99 11 3 2 1.63 0.90 11 3 3 51.53 3.10 11 3 4 4.28 1.13 11 3 4 2.88 0.74 11 3 4 2.00 0.86 11 3 5 10.68 1.61 11 3 5 9.69 1.52 11 3 5 11.75 1.29 11 3 6 87.44 5.13 11 3 6 89.85 4.71 11 3 7 15.18 1.41 -11 -4 2 3.61 0.76 11 4 -1 3.85 0.95 11 4 -1 4.95 0.96 11 4 0 10.53 1.62 11 4 0 10.73 1.54 11 4 1 3.14 1.11 11 4 1 2.83 0.97 11 4 2 6.17 1.36 11 4 2 8.43 1.08 11 4 2 5.82 1.30 11 4 3 0.48 0.83 11 4 3 0.88 0.64 11 4 3 1.51 0.88 11 4 4 10.38 1.29 11 4 4 11.08 1.67 11 4 5 9.17 1.56 11 4 5 7.57 1.11 11 4 5 7.60 1.38 11 4 6 8.25 1.41 11 4 6 8.03 1.32 11 4 6 7.49 1.08 11 4 8 0.79 0.51 11 4 9 8.34 0.90 -11 -5 2 1.28 0.58 11 5 0 212.54 10.45 11 5 0 213.10 10.37 11 5 1 72.83 4.75 11 5 1 71.41 4.38 11 5 1 72.39 4.65 11 5 2 -0.15 0.71 11 5 2 0.85 0.71 11 5 3 60.67 4.26 11 5 3 54.45 3.76 11 5 3 56.08 4.07 11 5 4 8.41 1.36 11 5 5 95.48 5.80 11 5 5 92.01 5.03 11 5 5 99.03 5.75 11 5 6 118.23 6.76 11 5 6 128.04 6.78 11 5 7 34.27 2.36 11 5 8 37.84 2.41 -11 -6 0 3.88 0.80 11 6 1 6.53 1.21 11 6 1 7.37 1.15 11 6 1 7.15 1.22 11 6 2 23.70 2.36 11 6 2 25.91 2.41 11 6 3 56.24 3.95 11 6 3 51.35 3.53 11 6 3 57.08 3.91 11 6 4 13.57 1.61 11 6 5 15.91 1.93 11 6 5 14.63 1.63 11 6 5 17.17 1.90 11 6 6 1.94 0.80 11 6 6 2.21 0.72 11 6 6 3.11 0.78 11 6 6 1.93 0.75 11 6 7 0.81 0.50 11 6 8 21.36 1.59 11 7 1 0.42 0.38 11 7 2 33.49 2.37 11 7 3 42.36 3.18 11 7 3 50.29 3.30 11 7 4 34.89 2.82 11 7 4 38.51 2.68 11 7 4 41.17 2.95 11 7 5 302.99 13.97 11 7 5 321.31 13.97 11 7 5 287.52 13.49 11 7 6 4.51 0.78 11 7 7 13.46 1.18 0 0 0 0.00 0.00 TITL gujy_a_241224_auto in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 9.297357 10.062488 15.864079 76.4892 82.2856 71.4025 ZERR 19.00 0.000204 0.000214 0.000352 0.0019 0.0018 0.0019 LATT 1 SFAC C H O S Cl UNIT 19.00 19.00 19.00 19.00 19.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0 TEMP -173 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 15189 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.831 _oxdiff_exptl_absorpt_empirical_full_min 0.523 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S2 S 0.45895(4) 0.92727(4) 0.38710(2) 0.01804(12) Uani 1 1 d . . . . . S1 S 0.95898(4) 0.39396(4) 0.40622(2) 0.02127(12) Uani 1 1 d . . . . . Cl2 Cl 0.39599(5) 0.86510(5) 0.01098(2) 0.03214(13) Uani 1 1 d . . . . . Cl1 Cl 0.90201(5) 0.36257(5) 0.02211(3) 0.03476(14) Uani 1 1 d . . . . . O2 O 0.30381(12) 1.00923(11) 0.41820(7) 0.0230(2) Uani 1 1 d . . . . . O1 O 0.81177(14) 0.49225(12) 0.43409(8) 0.0336(3) Uani 1 1 d . . . . . C25 C 0.43987(16) 0.89615(15) 0.28282(10) 0.0176(3) Uani 1 1 d . . . . . C16 C 0.62981(17) 0.47293(17) 0.75272(11) 0.0230(3) Uani 1 1 d . . . . . H16 H 0.666108 0.386776 0.731213 0.028 Uiso 1 1 calc R U . . . C20 C 0.51627(17) 0.72735(16) 0.73003(10) 0.0211(3) Uani 1 1 d . . . . . H20 H 0.473845 0.816789 0.692774 0.025 Uiso 1 1 calc R U . . . C30 C 0.56863(16) 0.83151(16) 0.23430(10) 0.0215(3) Uani 1 1 d . . . . . H30 H 0.665044 0.795280 0.258515 0.026 Uiso 1 1 calc R U . . . C22 C 0.55727(18) 0.60360(16) 0.60116(10) 0.0226(3) Uani 1 1 d . . . . . H22A H 0.481922 0.554781 0.597374 0.027 Uiso 1 1 calc R U . . . H22B H 0.657143 0.547507 0.578567 0.027 Uiso 1 1 calc R U . . . C10 C 0.94373(16) 0.38489(15) 0.29617(10) 0.0185(3) Uani 1 1 d . . . . . C5 C 1.02692(17) 0.25684(17) 0.72851(10) 0.0217(3) Uani 1 1 d . . . . . H5 H 0.985631 0.350062 0.694958 0.026 Uiso 1 1 calc R U . . . C23 C 0.51256(17) 0.75185(15) 0.54320(10) 0.0214(3) Uani 1 1 d . . . . . H23A H 0.589821 0.799844 0.544567 0.026 Uiso 1 1 calc R U . . . H23B H 0.414034 0.809573 0.566252 0.026 Uiso 1 1 calc R U . . . C15 C 1.07368(17) 0.32641(17) 0.24658(10) 0.0224(3) Uani 1 1 d . . . . . H15 H 1.170168 0.291359 0.270678 0.027 Uiso 1 1 calc R U . . . C21 C 0.56752(16) 0.60258(16) 0.69588(10) 0.0199(3) Uani 1 1 d . . . . . C19 C 0.52629(17) 0.72278(17) 0.81735(10) 0.0232(3) Uani 1 1 d . . . . . H19 H 0.491356 0.808736 0.839082 0.028 Uiso 1 1 calc R U . . . C26 C 0.29815(17) 0.95043(16) 0.24850(10) 0.0203(3) Uani 1 1 d . . . . . H26 H 0.211284 0.994888 0.282137 0.024 Uiso 1 1 calc R U . . . C24 C 0.49868(17) 0.74642(15) 0.44935(10) 0.0205(3) Uani 1 1 d . . . . . H24A H 0.415367 0.706683 0.446141 0.025 Uiso 1 1 calc R U . . . H24B H 0.594618 0.684805 0.426243 0.025 Uiso 1 1 calc R U . . . C17 C 0.63942(17) 0.46818(17) 0.83998(11) 0.0247(3) Uani 1 1 d . . . . . H17 H 0.681963 0.379078 0.877517 0.030 Uiso 1 1 calc R U . . . C4 C 1.02415(17) 0.23802(18) 0.81802(11) 0.0237(3) Uani 1 1 d . . . . . H4 H 0.983179 0.318262 0.845046 0.028 Uiso 1 1 calc R U . . . C6 C 1.08920(16) 0.14150(17) 0.68656(10) 0.0221(3) Uani 1 1 d . . . . . C28 C 0.41325(18) 0.87516(16) 0.11699(10) 0.0220(3) Uani 1 1 d . . . . . C27 C 0.28450(18) 0.93919(17) 0.16465(10) 0.0235(3) Uani 1 1 d . . . . . H27 H 0.188196 0.974934 0.140326 0.028 Uiso 1 1 calc R U . . . C8 C 0.94475(16) 0.18851(16) 0.55394(10) 0.0216(3) Uani 1 1 d . . . . . H8A H 0.910731 0.102868 0.578868 0.026 Uiso 1 1 calc R U . . . H8B H 0.868732 0.271466 0.573623 0.026 Uiso 1 1 calc R U . . . C29 C 0.55529(18) 0.82042(17) 0.15087(10) 0.0235(3) Uani 1 1 d . . . . . H29 H 0.641999 0.775997 0.117118 0.028 Uiso 1 1 calc R U . . . C14 C 1.06132(18) 0.31969(17) 0.16195(11) 0.0244(3) Uani 1 1 d . . . . . H14 H 1.148904 0.279550 0.127278 0.029 Uiso 1 1 calc R U . . . C1 C 1.14311(17) 0.00507(17) 0.73803(11) 0.0255(3) Uani 1 1 d . . . . . H1 H 1.182972 -0.075516 0.711246 0.031 Uiso 1 1 calc R U . . . C3 C 1.08110(17) 0.10222(19) 0.86827(10) 0.0253(3) Uani 1 1 d . . . . . H3 H 1.080337 0.089207 0.929582 0.030 Uiso 1 1 calc R U . . . C18 C 0.58713(17) 0.59314(17) 0.87284(10) 0.0228(3) Uani 1 1 d . . . . . H18 H 0.593051 0.589650 0.932677 0.027 Uiso 1 1 calc R U . . . C13 C 0.91904(19) 0.37247(17) 0.12839(10) 0.0227(3) Uani 1 1 d . . . . . C2 C 1.13925(18) -0.01454(18) 0.82812(11) 0.0268(3) Uani 1 1 d . . . . . H2 H 1.176502 -0.108065 0.862196 0.032 Uiso 1 1 calc R U . . . C9 C 0.95014(17) 0.21427(16) 0.45494(10) 0.0223(3) Uani 1 1 d . . . . . H9A H 0.858429 0.200956 0.437123 0.027 Uiso 1 1 calc R U . . . H9B H 1.040459 0.143426 0.433806 0.027 Uiso 1 1 calc R U . . . C11 C 0.80225(17) 0.44008(17) 0.26144(11) 0.0243(3) Uani 1 1 d . . . . . H11 H 0.714890 0.482379 0.295527 0.029 Uiso 1 1 calc R U . . . C7 C 1.09805(17) 0.16658(18) 0.58872(10) 0.0253(3) Uani 1 1 d . . . . . H7A H 1.174327 0.083386 0.569435 0.030 Uiso 1 1 calc R U . . . H7B H 1.132334 0.252162 0.564123 0.030 Uiso 1 1 calc R U . . . C12 C 0.78941(18) 0.43301(18) 0.17679(11) 0.0260(3) Uani 1 1 d . . . . . H12 H 0.693224 0.469111 0.152323 0.031 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S2 0.0177(2) 0.0189(2) 0.0186(2) -0.00732(14) -0.00365(14) -0.00333(14) S1 0.0250(2) 0.0208(2) 0.0186(2) -0.00727(15) -0.00241(15) -0.00493(15) Cl2 0.0470(3) 0.0385(2) 0.0157(2) -0.00387(16) -0.00695(17) -0.0185(2) Cl1 0.0503(3) 0.0428(3) 0.0175(2) -0.00406(17) -0.00822(17) -0.0217(2) O2 0.0203(5) 0.0225(5) 0.0245(6) -0.0103(4) -0.0014(4) -0.0003(4) O1 0.0407(7) 0.0242(6) 0.0251(6) -0.0090(5) 0.0005(5) 0.0071(5) C25 0.0169(7) 0.0176(7) 0.0190(7) -0.0036(5) -0.0040(5) -0.0049(5) C16 0.0203(7) 0.0197(7) 0.0273(8) -0.0048(6) -0.0032(6) -0.0031(6) C20 0.0200(7) 0.0201(7) 0.0194(7) -0.0027(6) -0.0021(6) -0.0013(6) C30 0.0165(7) 0.0253(8) 0.0230(8) -0.0072(6) -0.0035(6) -0.0045(6) C22 0.0274(8) 0.0184(7) 0.0213(8) -0.0051(6) -0.0003(6) -0.0057(6) C10 0.0192(7) 0.0175(7) 0.0185(7) -0.0034(6) -0.0023(6) -0.0047(6) C5 0.0188(7) 0.0229(7) 0.0225(8) -0.0057(6) -0.0038(6) -0.0034(6) C23 0.0236(7) 0.0198(7) 0.0204(7) -0.0049(6) -0.0038(6) -0.0043(6) C15 0.0170(7) 0.0258(8) 0.0231(8) -0.0058(6) -0.0038(6) -0.0030(6) C21 0.0168(7) 0.0213(7) 0.0201(7) -0.0037(6) -0.0008(5) -0.0039(6) C19 0.0211(7) 0.0255(8) 0.0215(8) -0.0070(6) -0.0018(6) -0.0033(6) C26 0.0173(7) 0.0214(7) 0.0206(7) -0.0037(6) -0.0024(6) -0.0036(6) C24 0.0220(7) 0.0183(7) 0.0208(7) -0.0061(6) -0.0041(6) -0.0028(6) C17 0.0208(7) 0.0245(8) 0.0257(8) 0.0015(6) -0.0059(6) -0.0053(6) C4 0.0195(7) 0.0291(8) 0.0229(8) -0.0096(6) -0.0024(6) -0.0045(6) C6 0.0154(7) 0.0276(8) 0.0233(8) -0.0083(6) -0.0042(6) -0.0031(6) C28 0.0308(8) 0.0219(7) 0.0159(7) -0.0017(6) -0.0049(6) -0.0115(6) C27 0.0212(7) 0.0261(8) 0.0239(8) -0.0004(6) -0.0093(6) -0.0083(6) C8 0.0204(7) 0.0231(7) 0.0216(8) -0.0042(6) -0.0022(6) -0.0065(6) C29 0.0222(8) 0.0248(8) 0.0230(8) -0.0069(6) 0.0013(6) -0.0058(6) C14 0.0225(8) 0.0270(8) 0.0230(8) -0.0088(6) 0.0020(6) -0.0054(6) C1 0.0205(7) 0.0237(8) 0.0318(9) -0.0094(7) -0.0073(6) -0.0009(6) C3 0.0189(7) 0.0372(9) 0.0199(8) -0.0050(7) -0.0020(6) -0.0088(6) C18 0.0194(7) 0.0304(8) 0.0175(7) -0.0030(6) -0.0022(6) -0.0071(6) C13 0.0300(8) 0.0239(8) 0.0171(7) -0.0016(6) -0.0057(6) -0.0121(6) C2 0.0223(8) 0.0253(8) 0.0311(9) 0.0005(7) -0.0087(6) -0.0063(6) C9 0.0243(7) 0.0207(7) 0.0217(8) -0.0048(6) -0.0045(6) -0.0051(6) C11 0.0174(7) 0.0270(8) 0.0261(8) -0.0062(6) -0.0008(6) -0.0031(6) C7 0.0198(7) 0.0322(8) 0.0233(8) -0.0088(7) -0.0031(6) -0.0037(6) C12 0.0209(7) 0.0311(8) 0.0258(8) -0.0013(7) -0.0084(6) -0.0078(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 S2 C25 106.58(6) . . ? O2 S2 C24 107.19(7) . . ? C25 S2 C24 99.56(7) . . ? O1 S1 C10 106.78(7) . . ? O1 S1 C9 105.54(7) . . ? C10 S1 C9 96.39(7) . . ? C30 C25 S2 119.79(11) . . ? C26 C25 S2 118.75(11) . . ? C26 C25 C30 121.13(14) . . ? C21 C16 H16 119.5 . . ? C17 C16 H16 119.5 . . ? C17 C16 C21 121.08(14) . . ? C21 C20 H20 119.4 . . ? C19 C20 H20 119.4 . . ? C19 C20 C21 121.28(14) . . ? C25 C30 H30 120.2 . . ? C29 C30 C25 119.56(14) . . ? C29 C30 H30 120.2 . . ? H22A C22 H22B 107.6 . . ? C23 C22 H22A 108.6 . . ? C23 C22 H22B 108.6 . . ? C21 C22 H22A 108.6 . . ? C21 C22 H22B 108.6 . . ? C21 C22 C23 114.61(12) . . ? C15 C10 S1 119.67(11) . . ? C11 C10 S1 119.16(11) . . ? C11 C10 C15 121.15(14) . . ? C4 C5 H5 119.3 . . ? C4 C5 C6 121.37(15) . . ? C6 C5 H5 119.3 . . ? C22 C23 H23A 109.2 . . ? C22 C23 H23B 109.2 . . ? C22 C23 C24 112.25(11) . . ? H23A C23 H23B 107.9 . . ? C24 C23 H23A 109.2 . . ? C24 C23 H23B 109.2 . . ? C10 C15 H15 120.3 . . ? C14 C15 C10 119.44(14) . . ? C14 C15 H15 120.3 . . ? C16 C21 C20 117.69(14) . . ? C16 C21 C22 119.66(13) . . ? C20 C21 C22 122.64(13) . . ? C20 C19 H19 119.9 . . ? C18 C19 C20 120.20(14) . . ? C18 C19 H19 119.9 . . ? C25 C26 H26 120.3 . . ? C27 C26 C25 119.38(14) . . ? C27 C26 H26 120.3 . . ? S2 C24 H24A 110.2 . . ? S2 C24 H24B 110.2 . . ? C23 C24 S2 107.34(9) . . ? C23 C24 H24A 110.2 . . ? C23 C24 H24B 110.2 . . ? H24A C24 H24B 108.5 . . ? C16 C17 H17 119.8 . . ? C16 C17 C18 120.42(15) . . ? C18 C17 H17 119.8 . . ? C5 C4 H4 119.9 . . ? C5 C4 C3 120.14(14) . . ? C3 C4 H4 119.9 . . ? C5 C6 C7 120.10(14) . . ? C1 C6 C5 117.85(14) . . ? C1 C6 C7 122.05(13) . . ? C27 C28 Cl2 118.73(12) . . ? C27 C28 C29 121.99(14) . . ? C29 C28 Cl2 119.28(12) . . ? C26 C27 H27 120.5 . . ? C28 C27 C26 118.98(14) . . ? C28 C27 H27 120.5 . . ? H8A C8 H8B 107.7 . . ? C9 C8 H8A 108.9 . . ? C9 C8 H8B 108.9 . . ? C9 C8 C7 113.21(12) . . ? C7 C8 H8A 108.9 . . ? C7 C8 H8B 108.9 . . ? C30 C29 C28 118.96(14) . . ? C30 C29 H29 120.5 . . ? C28 C29 H29 120.5 . . ? C15 C14 H14 120.5 . . ? C15 C14 C13 118.97(14) . . ? C13 C14 H14 120.5 . . ? C6 C1 H1 119.5 . . ? C2 C1 C6 120.94(14) . . ? C2 C1 H1 119.5 . . ? C4 C3 H3 120.3 . . ? C4 C3 C2 119.42(15) . . ? C2 C3 H3 120.3 . . ? C19 C18 C17 119.32(14) . . ? C19 C18 H18 120.3 . . ? C17 C18 H18 120.3 . . ? C14 C13 Cl1 119.30(12) . . ? C12 C13 Cl1 118.70(12) . . ? C12 C13 C14 122.00(14) . . ? C1 C2 H2 119.9 . . ? C3 C2 C1 120.22(15) . . ? C3 C2 H2 119.9 . . ? S1 C9 H9A 109.5 . . ? S1 C9 H9B 109.5 . . ? C8 C9 S1 110.90(10) . . ? C8 C9 H9A 109.5 . . ? C8 C9 H9B 109.5 . . ? H9A C9 H9B 108.0 . . ? C10 C11 H11 120.2 . . ? C12 C11 C10 119.52(14) . . ? C12 C11 H11 120.2 . . ? C6 C7 C8 112.00(12) . . ? C6 C7 H7A 109.2 . . ? C6 C7 H7B 109.2 . . ? C8 C7 H7A 109.2 . . ? C8 C7 H7B 109.2 . . ? H7A C7 H7B 107.9 . . ? C13 C12 C11 118.89(14) . . ? C13 C12 H12 120.6 . . ? C11 C12 H12 120.6 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S2 O2 1.4981(10) . ? S2 C25 1.7952(15) . ? S2 C24 1.8036(15) . ? S1 O1 1.4918(12) . ? S1 C10 1.7961(15) . ? S1 C9 1.8161(16) . ? Cl2 C28 1.7398(15) . ? Cl1 C13 1.7430(15) . ? C25 C30 1.392(2) . ? C25 C26 1.388(2) . ? C16 H16 0.9500 . ? C16 C21 1.400(2) . ? C16 C17 1.388(2) . ? C20 H20 0.9500 . ? C20 C21 1.401(2) . ? C20 C19 1.390(2) . ? C30 H30 0.9500 . ? C30 C29 1.379(2) . ? C22 H22A 0.9900 . ? C22 H22B 0.9900 . ? C22 C23 1.520(2) . ? C22 C21 1.516(2) . ? C10 C15 1.390(2) . ? C10 C11 1.389(2) . ? C5 H5 0.9500 . ? C5 C4 1.386(2) . ? C5 C6 1.398(2) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C23 C24 1.5266(19) . ? C15 H15 0.9500 . ? C15 C14 1.382(2) . ? C19 H19 0.9500 . ? C19 C18 1.387(2) . ? C26 H26 0.9500 . ? C26 C27 1.387(2) . ? C24 H24A 0.9900 . ? C24 H24B 0.9900 . ? C17 H17 0.9500 . ? C17 C18 1.392(2) . ? C4 H4 0.9500 . ? C4 C3 1.388(2) . ? C6 C1 1.396(2) . ? C6 C7 1.509(2) . ? C28 C27 1.383(2) . ? C28 C29 1.387(2) . ? C27 H27 0.9500 . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C8 C9 1.527(2) . ? C8 C7 1.529(2) . ? C29 H29 0.9500 . ? C14 H14 0.9500 . ? C14 C13 1.387(2) . ? C1 H1 0.9500 . ? C1 C2 1.393(2) . ? C3 H3 0.9500 . ? C3 C2 1.389(2) . ? C18 H18 0.9500 . ? C13 C12 1.384(2) . ? C2 H2 0.9500 . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C11 H11 0.9500 . ? C11 C12 1.384(2) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C12 H12 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag S2 C25 C30 C29 -173.73(12) . . . . ? S2 C25 C26 C27 173.88(12) . . . . ? S1 C10 C15 C14 180.00(12) . . . . ? S1 C10 C11 C12 -179.75(12) . . . . ? Cl2 C28 C27 C26 -178.55(12) . . . . ? Cl2 C28 C29 C30 178.63(12) . . . . ? Cl1 C13 C12 C11 179.50(13) . . . . ? O2 S2 C25 C30 174.93(12) . . . . ? O2 S2 C25 C26 1.39(14) . . . . ? O2 S2 C24 C23 -66.93(11) . . . . ? O1 S1 C10 C15 166.21(12) . . . . ? O1 S1 C10 C11 -12.13(15) . . . . ? O1 S1 C9 C8 -65.02(11) . . . . ? C25 S2 C24 C23 -177.73(10) . . . . ? C25 C30 C29 C28 0.4(2) . . . . ? C25 C26 C27 C28 -0.6(2) . . . . ? C16 C17 C18 C19 -0.5(2) . . . . ? C20 C19 C18 C17 0.7(2) . . . . ? C30 C25 C26 C27 0.4(2) . . . . ? C22 C23 C24 S2 -175.95(10) . . . . ? C10 S1 C9 C8 -174.45(10) . . . . ? C10 C15 C14 C13 0.4(2) . . . . ? C10 C11 C12 C13 -0.8(2) . . . . ? C5 C4 C3 C2 -0.7(2) . . . . ? C5 C6 C1 C2 -2.0(2) . . . . ? C5 C6 C7 C8 -78.30(18) . . . . ? C23 C22 C21 C16 -170.28(14) . . . . ? C23 C22 C21 C20 9.9(2) . . . . ? C15 C10 C11 C12 1.9(2) . . . . ? C15 C14 C13 Cl1 -179.26(12) . . . . ? C15 C14 C13 C12 0.7(3) . . . . ? C21 C16 C17 C18 -0.1(2) . . . . ? C21 C20 C19 C18 -0.3(2) . . . . ? C21 C22 C23 C24 -178.01(12) . . . . ? C19 C20 C21 C16 -0.2(2) . . . . ? C19 C20 C21 C22 179.55(14) . . . . ? C26 C25 C30 C29 -0.3(2) . . . . ? C24 S2 C25 C30 -73.80(13) . . . . ? C24 S2 C25 C26 112.66(13) . . . . ? C17 C16 C21 C20 0.4(2) . . . . ? C17 C16 C21 C22 -179.35(14) . . . . ? C4 C5 C6 C1 2.6(2) . . . . ? C4 C5 C6 C7 -176.76(14) . . . . ? C4 C3 C2 C1 1.3(2) . . . . ? C6 C5 C4 C3 -1.3(2) . . . . ? C6 C1 C2 C3 0.1(2) . . . . ? C27 C28 C29 C30 -0.6(2) . . . . ? C29 C28 C27 C26 0.7(2) . . . . ? C14 C13 C12 C11 -0.5(3) . . . . ? C1 C6 C7 C8 102.33(16) . . . . ? C9 S1 C10 C15 -85.41(13) . . . . ? C9 S1 C10 C11 96.25(13) . . . . ? C9 C8 C7 C6 179.96(12) . . . . ? C11 C10 C15 C14 -1.7(2) . . . . ? C7 C6 C1 C2 177.37(14) . . . . ? C7 C8 C9 S1 -74.69(14) . . . . ?