Crystallography Open Database

Information card for entry 7157338

Preview

Coordinates	7157338.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H74 B2 Co2 F8 N4 P2 S2
Calculated formula	C68 H74 B2 Co2 F8 N4 P2 S2
Title of publication	Cobalt-catalyzed regioselective hydrohydrazination of epoxides.
Authors of publication	Liu, Xiangyu; Song, Heng; Zhai, Xiaofang; Tung, Chen-Ho; Wang, Wenguang
Journal of publication	Organic & biomolecular chemistry
Year of publication	2020
Journal volume	18
Journal issue	8
Pages of publication	1572 - 1576
a	17.739 ± 0.0004 Å
b	10.70121 ± 0.00019 Å
c	33.541 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	6367 ± 0.2 Å³
Cell temperature	172.99 ± 0.1 K
Ambient diffraction temperature	172.99 ± 0.1 K
Number of distinct elements	8
Space group number	29
Hermann-Mauguin space group symbol	P c a 21
Hall space group symbol	P 2c -2ac
Residual factor for all reflections	0.0742
Residual factor for significantly intense reflections	0.0608
Weighted residual factors for significantly intense reflections	0.147
Weighted residual factors for all reflections included in the refinement	0.1681
Goodness-of-fit parameter for all reflections included in the refinement	1.145
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
249024 (current)	2020-03-05	cif/ Updating files of 7157336, 7157337, 7157338 Original log message: Adding full bibliography for 7157336--7157338.cif.	7157338.cif
247540	2020-02-04	cif/ Adding structures of 7157336, 7157337, 7157338 via cif-deposit CGI script.	7157338.cif