Crystallography Open Database

Information card for entry 7059162

Preview

Coordinates	7059162.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C107 H147 Cl4 Dy4 N30 O40
Calculated formula	C107 H125 Cl4 Dy4 N30 O40
Title of publication	Dysprosium-based linear helicate clusters: syntheses, structures, and magnetism
Authors of publication	Lu, Jingjing; Li, Xiao-Lei; Jin, Chaoyi; Yu, Yang; Tang, Jinkui
Journal of publication	New Journal of Chemistry
Year of publication	2020
Journal volume	44
Journal issue	3
Pages of publication	994 - 1000
a	20.0833 ± 0.0016 Å
b	30.421 ± 0.002 Å
c	21.9915 ± 0.0018 Å
α	90°
β	104.035 ± 0.0015°
γ	90°
Cell volume	13034.7 ± 1.7 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0916
Residual factor for significantly intense reflections	0.0617
Weighted residual factors for significantly intense reflections	0.1533
Weighted residual factors for all reflections included in the refinement	0.1762
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
257901 (current)	2020-10-06	cif/ Updating files of 7059162, 7059163, 7059164 Original log message: Adding full bibliography for 7059162--7059164.cif.	7059162.cif
247793	2020-02-04	cif/ Updating files of 7059162, 7059163, 7059164 Original log message: Adding full bibliography for 7059162--7059164.cif.	7059162.cif
245039	2019-12-13	cif/ Adding structures of 7059162, 7059163, 7059164 via cif-deposit CGI script.	7059162.cif