#------------------------------------------------------------------------------ #$Date: 2020-11-22 01:30:52 +0200 (Sun, 22 Nov 2020) $ #$Revision: 259219 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/00/38/4003826.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4003826 loop_ _publ_author_name 'Zuluaga, Andr\'es Reyes' 'Brock, Aidan J.' 'Pfrunder, Michael C.' 'Phonsri, Wasinee' 'Murray, Keith S.' 'Harding, Phimphaka' 'Micallef, Aaron S.' 'Mullen, Kathleen M.' 'Clegg, Jack K.' 'Harding, David J.' 'McMurtrie, John C.' _publ_section_title ; Three-Way Switchable Single-Crystal-to-Single-Crystal Solvatomorphic Spin Crossover in a Molecular Cocrystal ; _journal_name_full 'Chemistry of Materials' _journal_paper_doi 10.1021/acs.chemmater.0c03396 _journal_year 2020 _chemical_formula_moiety 'C6 F3 I3, C34 H26 Fe N4 O4, C N S' _chemical_formula_sum 'C41 H26 F3 Fe I3 N5 O4 S' _chemical_formula_weight 1178.28 _chemical_name_systematic 'bis(4-methoxy-2-(((quinolin-8-yl)imino)methyl)phenolato)-iron(iii) thiocyanate (2,4,5-tetrafluoro-1,3,5-triiodobenzene)' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2020-03-30 _audit_creation_method ; Olex2 1.3 (compiled 2020.02.04 svn.rd84adfe8 for OlexSys, GUI svn.r6032) ; _cell_angle_alpha 82.753(2) _cell_angle_beta 77.209(2) _cell_angle_gamma 89.246(2) _cell_formula_units_Z 2 _cell_length_a 11.8332(2) _cell_length_b 12.3448(3) _cell_length_c 13.9874(3) _cell_measurement_reflns_used 24115 _cell_measurement_temperature 179.98(16) _cell_measurement_theta_max 31.0110 _cell_measurement_theta_min 2.4260 _cell_volume 1976.41(7) _computing_cell_refinement 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 179.98(16) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 5.8140 _diffrn_detector_type 'Pilatus 300K' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -17.00 34.00 0.50 1.00 -- 7.84 93.00-131.00 102 2 \w -13.00 38.00 0.50 1.00 -- 7.84 -93.00 117.00 102 3 \w -43.00 -16.00 0.50 1.00 -- -9.41 93.00-131.00 54 4 \w -42.00 -16.00 0.50 1.00 -- 7.84 -57.00 -30.00 52 5 \w 0.00 37.00 0.50 1.00 -- 7.84 -99.00 -90.00 74 6 \w -59.00 22.00 0.50 1.00 -- 7.84 -57.00 60.00 162 7 \w -18.00 75.00 0.50 1.00 -- 7.84 77.00 0.00 186 8 \w 5.00 36.00 0.50 1.00 -- 7.84 -99.00 0.00 62 9 \w -7.00 79.00 0.50 1.00 -- 7.84 57.00 60.00 172 10 \w 3.00 40.00 0.50 1.00 -- 7.84 -99.00-180.00 74 11 \w -61.00 -36.00 0.50 1.00 -- 7.84 153.00-168.43 50 12 \w -26.00 68.00 0.50 1.00 -- -9.41 37.00 150.00 188 13 \w -30.00 49.00 0.50 1.00 -- -9.41 77.00 150.00 158 14 \w 6.00 31.00 0.50 1.00 -- -9.41 93.00-131.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 300K' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0271289000 _diffrn_orient_matrix_UB_12 -0.0258665000 _diffrn_orient_matrix_UB_13 -0.0414726000 _diffrn_orient_matrix_UB_21 -0.0202434000 _diffrn_orient_matrix_UB_22 -0.0515284000 _diffrn_orient_matrix_UB_23 0.0262720000 _diffrn_orient_matrix_UB_31 -0.0513152000 _diffrn_orient_matrix_UB_32 0.0055928000 _diffrn_orient_matrix_UB_33 -0.0183781000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0785 _diffrn_reflns_av_unetI/netI 0.0515 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 48855 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.282 _diffrn_reflns_theta_min 2.050 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 2.842 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.10068 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.61a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'dark brown' _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 1.980 _exptl_crystal_description block _exptl_crystal_F_000 1134 _exptl_crystal_preparation 'Combined equal ratios of starting materials' _exptl_crystal_recrystallization_method 'Slow evaporation of the solvent' _exptl_crystal_size_max 2 _exptl_crystal_size_mid 1 _exptl_crystal_size_min 1 _refine_diff_density_max 1.140 _refine_diff_density_min -1.205 _refine_diff_density_rms 0.131 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.109 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 525 _refine_ls_number_reflns 9814 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.109 _refine_ls_R_factor_all 0.0556 _refine_ls_R_factor_gt 0.0414 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0495P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1033 _refine_ls_wR_factor_ref 0.1102 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7591 _reflns_number_total 9814 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cm0c03396_si_006.cif _cod_data_source_block sjcm19ar19a_13_180_00 _cod_database_code 4003826 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C40 H40 N5 O2 Fe S I3 F3' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.163 _shelx_estimated_absorpt_t_min 0.070 _reflns_odcompleteness_completeness 84.19 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 33.33 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C25(H25), C23(H23), C6(H6), C19(H19), C28(H28), C8(H8), C2(H2), C16(H16), C27(H27), C3(H3), C33(H33), C10(H10), C20(H20), C12(H12), C29(H29), C31(H31), C11(H11), C32(H32), C15(H15), C14(H14) 2.b Idealised Me refined as rotating group: C5(H5A,H5B,H5C), C22(H22A,H22B,H22C) ; _shelx_res_file ; TITL sjcm19ar19a_13_180_00_a.res in P-1 sjcm19ar19a_13_180_00.res created by SHELXL-2018/3 at 15:53:01 on 30-Mar-2020 REM Old TITL Sjcm19ar19a_13_180_00 in P-1 REM SHELXT solution in P-1: R1 0.182, Rweak 0.011, Alpha 0.052 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C41 N7 O4 F S Fe2 I2 CELL 0.71073 11.8332 12.3448 13.9874 82.753 77.209 89.246 ZERR 2 0.0002 0.0003 0.0003 0.002 0.002 0.002 LATT 1 SFAC C H F Fe I N O S UNIT 82 52 6 2 6 10 8 2 L.S. 15 PLAN 5 SIZE 2 1 1 TEMP -93 CONF HTAB BOND list 4 MORE -1 BOND $H fmap 2 acta SHEL 50 0.75 REM REM REM WGHT 0.049500 FVAR 0.18022 I1 5 -0.082928 0.237099 0.385830 11.00000 0.02688 0.03955 = 0.03717 -0.00859 -0.00826 0.00459 I3 5 0.283898 0.055123 0.605192 11.00000 0.03552 0.03348 = 0.05847 -0.00294 -0.01769 0.00580 I2 5 -0.008596 0.428472 0.744319 11.00000 0.05546 0.04289 = 0.04963 -0.01942 -0.00772 0.00249 FE1 4 0.514800 0.364315 0.789528 11.00000 0.01983 0.02136 = 0.01849 -0.00449 -0.00377 0.00245 S1 8 -0.201334 0.290672 0.196570 11.00000 0.05484 0.05623 = 0.03586 -0.01403 -0.01444 0.02152 F3 3 0.118553 0.088201 0.450544 11.00000 0.04385 0.03680 = 0.03965 -0.01167 -0.01284 0.01064 O3 7 0.592008 0.309934 0.888764 11.00000 0.02602 0.02742 = 0.01932 -0.00584 -0.00625 0.00613 F1 3 -0.105762 0.383971 0.558867 11.00000 0.04055 0.04462 = 0.04998 -0.01219 -0.01697 0.01678 O1 7 0.628972 0.471992 0.735476 11.00000 0.02371 0.02795 = 0.02158 -0.00483 -0.00166 0.00135 F2 3 0.187270 0.252002 0.717355 11.00000 0.05728 0.04216 = 0.04768 -0.00707 -0.02965 0.00278 O4 7 0.969009 0.039387 0.875790 11.00000 0.03004 0.03840 = 0.04073 -0.00881 -0.01789 0.01132 N3 6 0.596805 0.271824 0.695059 11.00000 0.02234 0.02095 = 0.01883 -0.00289 -0.00534 0.00371 O2 7 0.693694 0.875207 0.846735 11.00000 0.03415 0.02921 = 0.04483 -0.01050 -0.00191 -0.00822 N1 6 0.423104 0.454603 0.880154 11.00000 0.01995 0.02147 = 0.01997 0.00038 -0.00133 0.00261 N4 6 0.432328 0.410396 0.682220 11.00000 0.02351 0.02660 = 0.02113 -0.00441 -0.00398 -0.00135 N2 6 0.385760 0.257475 0.847723 11.00000 0.02347 0.02277 = 0.02022 -0.00357 -0.00897 0.00093 C25 1 0.687013 0.214532 0.704996 11.00000 0.02149 0.02485 = 0.02164 -0.00839 -0.00371 0.00473 AFIX 43 H25 2 0.724608 0.178703 0.650591 11.00000 -1.20000 AFIX 0 C34 1 0.465994 0.353618 0.602529 11.00000 0.02058 0.02454 = 0.01866 -0.00127 -0.00369 -0.00146 C7 1 0.560920 0.604144 0.849541 11.00000 0.01887 0.02847 = 0.02239 -0.00258 -0.00459 0.00004 C18 1 0.684413 0.248192 0.877268 11.00000 0.02269 0.02198 = 0.02334 -0.00312 -0.00619 -0.00287 C24 1 0.734122 0.200991 0.790408 11.00000 0.01902 0.02612 = 0.02266 -0.00620 -0.00487 0.00019 C26 1 0.554095 0.275890 0.607883 11.00000 0.02385 0.02774 = 0.01690 -0.00287 -0.00426 0.00042 C17 1 0.296874 0.300633 0.912194 11.00000 0.02192 0.02472 = 0.02069 -0.00330 -0.00570 0.00214 C9 1 0.312596 0.408991 0.929726 11.00000 0.01826 0.02333 = 0.02409 -0.00219 -0.00582 -0.00005 C23 1 0.830009 0.130372 0.788709 11.00000 0.02322 0.02394 = 0.02622 -0.00442 -0.00226 0.00417 AFIX 43 H23 2 0.861718 0.098159 0.730583 11.00000 -1.20000 AFIX 0 C6 1 0.578012 0.707541 0.877371 11.00000 0.02264 0.02721 = 0.02566 -0.00162 -0.00451 0.00070 AFIX 43 H6 2 0.523960 0.733242 0.930322 11.00000 -1.20000 AFIX 0 C19 1 0.737309 0.223927 0.958756 11.00000 0.02745 0.02978 = 0.02068 -0.00576 -0.01026 0.00218 AFIX 43 H19 2 0.706962 0.254784 1.017886 11.00000 -1.20000 AFIX 0 C1 1 0.641928 0.563208 0.771563 11.00000 0.02017 0.02991 = 0.02187 -0.00352 -0.00711 0.00030 C28 1 0.538973 0.230145 0.448838 11.00000 0.04265 0.03521 = 0.01936 -0.00703 -0.00872 0.00572 AFIX 43 H28 2 0.563264 0.186745 0.396734 11.00000 -1.20000 AFIX 0 C21 1 0.877552 0.108019 0.870124 11.00000 0.02277 0.02454 = 0.03129 -0.00427 -0.01006 0.00192 C38 1 0.038615 0.319701 0.641333 11.00000 0.03758 0.02535 = 0.03695 -0.00926 -0.00409 0.00055 C8 1 0.456524 0.547564 0.900132 11.00000 0.02242 0.02110 = 0.02142 -0.00416 -0.00199 0.00141 AFIX 43 H8 2 0.407824 0.579936 0.952132 11.00000 -1.20000 AFIX 0 C2 1 0.741178 0.629275 0.726818 11.00000 0.02050 0.03682 = 0.02252 -0.00505 -0.00163 0.00107 AFIX 43 H2 2 0.799089 0.603126 0.676779 11.00000 -1.20000 AFIX 0 C16 1 0.376320 0.154709 0.831998 11.00000 0.03300 0.02239 = 0.02846 -0.00429 -0.00924 0.00447 AFIX 43 H16 2 0.437882 0.124463 0.787902 11.00000 -1.20000 AFIX 0 C40 1 0.157001 0.168678 0.583963 11.00000 0.02913 0.03035 = 0.03507 0.00016 -0.00733 -0.00191 C27 1 0.588451 0.213692 0.531667 11.00000 0.03070 0.03111 = 0.02665 -0.00896 -0.00916 0.00627 AFIX 43 H27 2 0.645730 0.159602 0.535256 11.00000 -1.20000 AFIX 0 C4 1 0.673067 0.771658 0.827942 11.00000 0.02581 0.02732 = 0.03028 -0.00322 -0.00982 -0.00382 C3 1 0.755392 0.729773 0.754083 11.00000 0.02023 0.03381 = 0.03337 0.00002 -0.00530 -0.00825 AFIX 43 H3 2 0.822696 0.772213 0.722185 11.00000 -1.20000 AFIX 0 C36 1 0.005769 0.237026 0.500791 11.00000 0.02942 0.03267 = 0.03437 -0.00047 -0.00699 -0.00300 C33 1 0.352893 0.486347 0.679071 11.00000 0.02873 0.02780 = 0.02807 -0.00215 -0.00866 0.00524 AFIX 43 H33 2 0.329428 0.526169 0.733823 11.00000 -1.20000 AFIX 0 C30 1 0.416821 0.370916 0.518500 11.00000 0.02912 0.03424 = 0.02228 -0.00246 -0.00623 -0.00421 C35 1 -0.303020 0.194868 0.216328 11.00000 0.05925 0.05016 = 0.02392 -0.01563 -0.01705 0.03246 C37 1 -0.019691 0.312949 0.567287 11.00000 0.02712 0.03014 = 0.03925 -0.00416 -0.00412 0.00171 C13 1 0.194858 0.240907 0.958487 11.00000 0.02471 0.03210 = 0.02357 -0.00113 -0.00579 -0.00412 C10 1 0.224191 0.458473 0.989285 11.00000 0.02395 0.03076 = 0.03143 -0.01249 0.00157 -0.00184 AFIX 43 H10 2 0.232976 0.531773 1.000834 11.00000 -1.20000 AFIX 0 C20 1 0.831020 0.157157 0.954448 11.00000 0.02973 0.03151 = 0.02753 -0.00235 -0.01493 -0.00220 AFIX 43 H20 2 0.865185 0.143951 1.010139 11.00000 -1.20000 AFIX 0 C12 1 0.105577 0.293767 1.020225 11.00000 0.02088 0.03457 = 0.03392 -0.00636 0.00110 -0.00689 AFIX 43 H12 2 0.035700 0.255420 1.052465 11.00000 -1.20000 AFIX 0 C29 1 0.456492 0.307368 0.441538 11.00000 0.03591 0.03822 = 0.02231 -0.00259 -0.01092 -0.00035 AFIX 43 H29 2 0.425683 0.318194 0.383897 11.00000 -1.20000 AFIX 0 N5 6 -0.375113 0.127962 0.230415 11.00000 0.06953 0.05414 = 0.04594 -0.02149 -0.01773 0.01884 C41 1 0.092695 0.164506 0.512862 11.00000 0.03113 0.02683 = 0.03165 -0.00269 -0.00625 0.00343 C31 1 0.332439 0.454011 0.518047 11.00000 0.03307 0.03265 = 0.02932 0.00105 -0.01301 0.00385 AFIX 43 H31 2 0.297760 0.470073 0.462885 11.00000 -1.20000 AFIX 0 C11 1 0.120323 0.399839 1.033183 11.00000 0.02467 0.03746 = 0.03554 -0.01116 0.00034 0.00200 AFIX 43 H11 2 0.058897 0.435270 1.072909 11.00000 -1.20000 AFIX 0 C32 1 0.301977 0.509960 0.596759 11.00000 0.02793 0.03087 = 0.03580 0.00071 -0.00753 0.00241 AFIX 43 H32 2 0.245809 0.565647 0.596642 11.00000 -1.20000 AFIX 0 C39 1 0.127081 0.247059 0.647010 11.00000 0.03699 0.02929 = 0.03518 0.00334 -0.01526 0.00145 C15 1 0.279118 0.088992 0.877866 11.00000 0.03883 0.02611 = 0.03412 -0.00425 -0.01046 -0.00871 AFIX 43 H15 2 0.275822 0.015318 0.865467 11.00000 -1.20000 AFIX 0 C14 1 0.189445 0.131152 0.940257 11.00000 0.02951 0.03254 = 0.02830 0.00036 -0.00478 -0.00856 AFIX 43 H14 2 0.123224 0.086961 0.971577 11.00000 -1.20000 AFIX 0 C5 1 0.600403 0.927248 0.904455 11.00000 0.04115 0.02523 = 0.04070 -0.00723 -0.00786 -0.00319 AFIX 137 H5A 2 0.534396 0.931007 0.872500 11.00000 -1.50000 H5B 2 0.624360 1.001297 0.910545 11.00000 -1.50000 H5C 2 0.577818 0.885496 0.970309 11.00000 -1.50000 AFIX 0 C22 1 0.997672 -0.031215 0.801599 11.00000 0.03544 0.03700 = 0.03536 -0.00496 -0.00732 0.01189 AFIX 137 H22A 2 1.024002 0.012322 0.736963 11.00000 -1.50000 H22B 2 0.929159 -0.074697 0.801096 11.00000 -1.50000 H22C 2 1.059640 -0.080000 0.815532 11.00000 -1.50000 AFIX 0 HKLF 4 REM sjcm19ar19a_13_180_00_a.res in P-1 REM wR2 = 0.1102, GooF = S = 1.109, Restrained GooF = 1.109 for all data REM R1 = 0.0414 for 7591 Fo > 4sig(Fo) and 0.0556 for all 9814 data REM 525 parameters refined using 0 restraints END WGHT 0.0495 0.0000 REM Instructions for potential hydrogen bonds EQIV $1 -x+1, -y+1, -z+2 HTAB C6 O3_$1 EQIV $2 x+1, y, z+1 HTAB C19 S1_$2 EQIV $3 x+1, y, z HTAB C2 I2_$3 HTAB C16 N3 EQIV $4 -x+1, -y+1, -z+1 HTAB C3 I1_$4 EQIV $5 -x, -y+1, -z+1 HTAB C33 S1_$5 HTAB C33 N1 HTAB C32 I1_$5 EQIV $6 -x, -y, -z+1 HTAB C15 N5_$6 HTAB C22 I3_$3 REM Highest difference peak 1.140, deepest hole -1.205, 1-sigma level 0.131 Q1 1 0.3098 0.0599 0.5437 11.00000 0.05 1.14 Q2 1 -0.0597 0.3401 0.3405 11.00000 0.05 1.05 Q3 1 0.0305 0.4455 0.6811 11.00000 0.05 0.77 Q4 1 -0.1232 0.2169 0.4540 11.00000 0.05 0.73 Q5 1 -0.1054 0.1329 0.4374 11.00000 0.05 0.70 ; _shelx_res_checksum 49401 _shelx_hkl_file ; 0 0 2 278.91 14.72 0 0 -2 258.52 14.65 0 0 -3 39.64 3.23 0 0 3 40.60 3.28 0 0 -4 61.03 4.33 0 0 4 64.97 4.87 0 0 -4 62.31 4.82 0 0 4 60.61 4.71 0 0 -5 629.52 33.88 0 0 5 588.52 34.43 0 0 -5 661.37 34.81 0 0 5 655.13 34.79 0 0 6 684.58 31.11 0 0 -6 661.36 30.98 0 0 6 700.86 31.22 0 0 -6 678.11 29.89 0 0 6 705.29 31.08 0 0 7 0.25 0.74 0 0 7 0.52 0.98 0 0 -7 2.32 1.39 0 0 -7 -0.17 0.65 0 0 7 0.50 1.22 0 0 -8 459.05 22.04 0 0 -8 425.37 21.87 0 0 -8 364.15 22.38 0 0 -8 340.39 23.68 0 0 8 314.10 22.99 0 0 -8 379.59 23.59 0 0 8 392.79 23.75 0 0 8 382.62 23.80 0 0 -9 130.04 8.29 0 0 -9 128.00 10.87 0 0 9 125.56 10.38 0 0 9 149.92 10.96 0 0 -9 136.58 10.57 0 0 9 139.96 10.90 0 0 10 109.02 8.63 0 0 10 110.90 9.60 0 0 -10 104.12 9.59 0 0 10 100.22 9.12 0 0 -10 90.61 8.77 0 0 -11 14.92 2.01 0 0 11 10.92 2.75 0 0 11 16.89 3.18 0 0 -11 13.48 1.83 0 0 11 22.16 4.04 0 0 -11 10.27 2.59 0 0 -11 15.94 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2.70 3.44 0 -4 16 2.96 2.82 0 4 -15 -1.18 2.52 0 -4 15 1.13 1.80 0 4 -15 -0.37 2.15 0 -4 15 3.31 2.56 0 4 -15 1.16 0.98 0 4 -15 5.87 3.37 0 4 -15 0.82 2.51 0 -4 15 2.04 2.60 0 4 -14 78.04 8.30 0 -4 14 102.96 8.54 0 4 -14 79.87 8.18 0 -4 14 108.25 10.19 0 4 -14 103.47 10.63 0 -4 14 106.55 10.97 0 4 -14 99.07 11.50 0 4 -14 88.34 6.48 0 4 -13 16.07 2.47 0 -4 13 16.50 3.27 0 4 -13 20.68 3.84 0 4 -13 19.64 4.54 0 4 -13 17.56 4.81 0 4 -13 16.29 3.67 0 4 -12 24.52 2.99 0 -4 12 28.68 3.88 0 4 -12 21.67 3.94 0 4 -12 26.29 4.83 0 4 -12 25.68 5.59 0 4 -12 20.49 4.10 0 4 -11 53.85 6.19 0 -4 11 54.75 5.22 0 4 -11 47.22 4.47 0 4 -11 50.85 7.19 0 -4 11 63.48 7.22 0 4 -10 36.97 3.58 0 4 -10 45.38 5.59 0 -4 10 30.58 3.69 0 -4 10 37.39 5.21 0 -4 10 31.06 4.36 0 -4 9 10.52 2.49 0 4 -9 9.92 3.44 0 -4 9 15.37 2.22 0 4 -9 13.83 2.10 0 -4 9 13.07 3.00 0 4 -9 7.35 3.66 0 -4 8 18.65 2.89 0 4 -8 21.91 3.51 0 4 -8 19.35 5.19 0 -4 8 20.11 3.42 0 4 -8 22.19 4.04 0 4 -8 28.22 6.35 0 -4 7 199.70 12.71 0 4 -7 206.58 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118.45 0 -4 -3 2253.93 118.75 0 4 4 708.24 38.27 0 -4 -4 674.11 38.51 0 -4 -4 750.15 39.08 0 4 4 689.88 37.02 0 -4 -5 328.37 19.49 0 -4 -5 319.53 19.16 0 4 5 331.67 19.08 0 4 5 311.96 19.03 0 4 5 305.62 17.07 0 -4 -6 186.28 12.58 0 4 6 180.88 12.32 0 4 6 174.01 12.20 0 4 6 166.13 11.88 0 -4 -7 85.92 7.62 0 4 7 81.29 7.37 0 4 7 88.99 7.63 0 4 7 75.48 7.05 0 4 8 246.96 16.46 0 -4 -8 228.56 16.13 0 4 8 228.80 16.19 0 4 8 232.93 15.89 0 -4 -9 511.44 30.87 0 4 9 506.44 30.64 0 4 9 508.81 30.88 0 4 9 485.80 30.27 0 4 10 84.24 8.29 0 -4 -10 74.28 8.10 0 4 10 78.87 8.12 0 4 11 209.96 16.07 0 4 11 226.99 16.44 0 -4 -11 198.26 16.09 0 4 12 181.16 14.69 0 -4 -12 158.78 14.31 0 4 12 185.13 14.68 0 4 13 1.15 2.23 0 4 13 0.55 2.15 0 -4 -13 1.81 2.30 0 4 14 8.20 3.55 0 4 14 7.21 3.53 0 4 15 -0.65 2.52 0 4 15 2.09 2.56 0 4 15 1.38 3.04 0 4 15 -0.70 3.05 0 4 16 8.89 3.97 0 4 16 11.82 4.14 0 4 16 12.97 4.62 0 4 16 7.70 3.72 0 4 16 14.87 4.52 0 4 17 34.06 6.99 0 4 17 35.98 7.51 0 4 18 10.47 4.22 0 4 18 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9.08 0 -5 9 127.05 10.73 0 5 -9 122.88 11.69 0 5 -8 75.95 9.64 0 5 -8 77.55 7.34 0 -5 8 70.97 6.29 0 5 -8 56.83 8.42 0 -5 8 68.75 5.07 0 -5 8 76.04 6.37 0 5 -8 74.20 8.23 0 -5 8 68.51 6.84 0 5 -7 8.04 2.22 0 -5 7 11.62 2.17 0 5 -7 16.52 6.83 0 5 -7 2.37 2.05 0 -5 6 105.57 8.06 0 5 -6 107.72 7.48 0 -5 6 107.87 7.65 0 5 -6 110.53 8.63 0 5 -6 129.07 10.79 0 5 -5 -0.17 0.79 0 -5 5 1.76 1.10 0 -5 5 0.57 0.48 0 5 -5 -0.25 1.02 0 -5 5 0.82 0.88 0 -5 4 0.84 0.90 0 5 -4 0.86 0.76 0 5 -4 1.09 0.93 0 -5 4 1.25 0.82 0 5 -4 0.93 0.55 0 -5 3 92.72 7.14 0 5 -3 89.23 6.56 0 -5 3 78.45 6.56 0 5 -3 97.01 6.83 0 -5 3 95.47 6.09 0 5 -3 81.93 5.36 0 -5 2 11.78 2.12 0 -5 2 12.94 2.09 0 -5 2 12.48 1.70 0 5 -2 13.89 1.96 0 5 -2 10.91 1.26 0 -5 1 173.63 11.09 0 -5 1 165.29 10.11 0 -5 1 161.02 10.76 0 5 -1 162.58 10.13 0 5 0 30.80 3.51 0 -5 0 40.11 4.16 0 -5 0 35.59 3.60 0 5 0 35.06 3.12 0 5 1 3.70 0.95 0 -5 -1 3.98 0.88 0 -5 -1 1.25 1.02 0 5 1 2.02 0.90 0 -5 -1 1.67 1.02 0 5 2 130.24 7.30 0 -5 -2 145.77 9.58 0 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201.57 15.11 0 -6 9 228.14 16.47 0 6 -9 243.64 18.83 0 -6 8 95.57 7.60 0 6 -8 110.26 11.58 0 -6 8 90.04 5.98 0 -6 8 83.54 7.56 0 6 -8 100.42 7.40 0 6 -8 91.24 10.00 0 -6 8 84.16 8.09 0 -6 7 29.15 2.33 0 6 -7 23.25 6.40 0 6 -7 29.26 4.30 0 -6 7 26.13 3.28 0 6 -7 29.77 7.45 0 6 -7 16.51 4.51 0 -6 6 5.00 1.43 0 6 -6 1.29 1.47 0 6 -6 0.55 2.25 0 6 -6 3.20 1.35 0 -6 5 19.68 3.08 0 6 -5 21.73 2.90 0 6 -5 16.30 7.53 0 -6 5 21.68 2.62 0 6 -5 17.43 3.10 0 -6 4 345.99 19.69 0 6 -4 315.26 18.57 0 -6 4 318.96 19.06 0 6 -4 287.68 16.74 0 -6 4 318.51 17.85 0 6 -4 314.09 19.08 0 -6 3 206.51 12.01 0 6 -3 201.96 12.84 0 -6 3 191.81 12.88 0 -6 3 212.32 13.37 0 6 -3 191.77 11.12 0 -6 2 54.97 5.24 0 -6 2 57.00 5.07 0 6 -2 46.83 3.56 0 6 -2 52.85 4.65 0 -6 2 50.42 4.30 0 -6 1 26.95 3.53 0 -6 1 26.52 3.30 0 6 -1 30.48 3.08 0 -6 0 1117.43 58.80 0 6 0 1103.14 60.63 0 -6 0 1136.41 60.61 0 -6 0 1225.36 61.35 0 6 0 1093.09 59.43 0 6 1 132.83 9.55 0 -6 -1 190.70 8.95 0 6 1 127.50 8.76 0 -6 -1 121.60 9.65 0 -6 -1 124.81 9.70 0 6 1 66.97 11.66 0 6 2 7.66 3.24 0 6 2 10.94 3.44 0 6 2 14.08 2.37 0 -6 -2 16.24 2.70 0 -6 -2 12.67 2.47 0 6 3 14.56 2.90 0 6 3 10.26 2.82 0 6 3 15.63 1.44 0 -6 -3 6.71 2.03 0 6 3 11.35 2.02 0 -6 -3 7.72 2.15 0 6 4 112.49 7.72 0 6 4 112.66 7.73 0 6 4 84.62 6.31 0 -6 -4 121.07 7.59 0 6 4 103.92 7.76 0 -6 -4 91.38 8.10 0 -6 -4 105.18 8.71 0 6 5 12.62 1.87 0 6 5 16.31 2.54 0 -6 -5 11.86 2.67 0 -6 -5 15.99 2.66 0 -6 -5 8.35 2.46 0 6 5 11.59 1.85 0 6 6 436.19 26.00 0 6 6 475.01 25.99 0 -6 -6 434.24 26.41 0 -6 -6 460.10 27.15 0 6 6 430.31 26.28 0 6 6 411.27 23.80 0 6 7 0.69 1.28 0 -6 -7 0.40 1.33 0 6 7 -0.33 1.03 0 -6 -7 0.71 1.38 0 6 7 -0.30 0.93 0 6 8 379.72 23.37 0 -6 -8 361.44 23.77 0 6 8 342.36 22.85 0 6 8 356.15 22.51 0 6 9 26.21 4.30 0 -6 -9 22.43 4.37 0 6 9 27.21 4.06 0 6 9 14.96 3.52 0 6 10 90.88 8.89 0 -6 -10 83.53 9.06 0 6 10 84.70 8.31 0 6 10 90.60 8.91 0 6 10 71.76 5.81 0 6 11 28.26 3.07 0 6 11 39.53 5.59 0 -6 -11 30.54 5.57 0 6 11 31.05 5.45 0 6 12 8.77 3.12 0 6 12 9.31 3.31 0 -6 -12 11.78 4.12 0 6 13 72.20 8.78 0 6 13 80.83 9.42 0 6 14 62.43 8.59 0 6 14 60.93 8.54 0 6 15 2.07 2.53 0 6 16 17.90 5.25 0 6 17 -0.78 3.25 0 6 17 -1.59 3.99 0 6 17 0.85 2.93 0 -6 -18 -1.55 2.61 0 6 18 0.82 2.83 0 6 18 -0.92 3.17 0 6 18 -1.74 3.15 0 -6 -19 -0.52 2.35 0 -7 18 4.54 3.35 0 -7 17 9.82 3.70 0 -7 17 4.25 3.33 0 -7 16 1.62 2.46 0 -7 16 3.97 3.60 0 -7 15 0.20 1.30 0 -7 15 0.50 2.13 0 -7 15 0.74 2.53 0 7 -15 -3.93 3.01 0 -7 14 2.73 2.29 0 -7 14 4.08 3.13 0 -7 14 2.95 1.43 0 7 -14 0.54 3.63 0 -7 13 63.31 6.96 0 7 -13 40.55 6.60 0 -7 13 52.64 4.53 0 7 -13 45.99 8.26 0 -7 13 45.90 7.31 0 -7 12 102.53 8.77 0 7 -12 93.56 9.65 0 -7 12 88.48 6.18 0 7 -12 61.98 9.46 0 -7 12 103.40 10.35 0 7 -12 68.86 9.04 0 -7 11 -1.02 2.65 0 7 -11 -0.54 3.42 0 -7 11 1.04 0.95 0 -7 11 1.70 1.64 0 7 -11 0.71 2.49 0 7 -10 18.85 4.14 0 -7 10 16.99 3.21 0 7 -10 24.81 5.20 0 -7 10 17.43 2.04 0 7 -10 10.59 4.22 0 -7 9 0.66 1.29 0 7 -9 0.26 1.30 0 7 -9 0.95 1.81 0 -7 9 1.99 0.87 0 7 -9 -1.20 3.46 0 7 -9 0.58 2.55 0 7 -8 51.87 8.47 0 7 -8 52.39 8.03 0 7 -8 52.85 5.12 0 -7 8 36.98 4.94 0 7 -7 187.38 16.84 0 7 -7 211.04 18.04 0 7 -7 160.78 15.69 0 7 -6 40.68 5.20 0 -7 6 47.69 4.36 0 7 -6 30.46 6.91 0 7 -6 30.95 7.78 0 7 -5 101.82 8.55 0 -7 5 95.82 7.01 0 -7 5 80.40 7.63 0 -7 5 108.28 8.76 0 7 -5 68.55 11.13 0 7 -5 91.59 13.23 0 -7 4 379.70 22.62 0 -7 4 328.29 21.85 0 7 -4 386.33 22.59 0 -7 4 419.90 21.22 0 -7 3 315.55 18.57 0 -7 3 280.96 17.94 0 7 -3 276.48 17.72 0 -7 3 308.00 16.99 0 7 -2 16.25 2.56 0 -7 2 20.62 3.14 0 -7 2 20.79 3.30 0 -7 2 14.71 2.24 0 7 -2 15.82 1.80 0 -7 1 75.54 6.80 0 -7 1 68.55 6.31 0 7 -1 66.03 5.51 0 -7 0 13.32 2.42 0 7 0 11.07 1.85 0 7 0 11.11 2.36 0 -7 0 8.03 1.36 0 -7 0 15.09 2.77 0 7 0 5.13 0.93 0 7 1 455.79 37.68 0 7 1 429.15 36.99 0 7 1 629.81 33.15 0 -7 -1 655.46 34.77 0 -7 -1 594.55 32.49 0 7 1 666.56 34.51 0 -7 -1 639.20 34.88 0 -7 -1 592.88 34.64 0 7 2 605.22 39.48 0 7 2 582.34 39.17 0 7 2 723.18 37.23 0 7 2 672.98 36.06 0 -7 -2 626.17 37.49 0 -7 -2 670.28 37.83 0 7 3 168.27 13.09 0 7 3 187.06 13.47 0 7 3 199.54 12.94 0 -7 -3 177.38 13.22 0 -7 -3 182.20 13.34 0 7 4 156.89 10.01 0 -7 -4 137.48 10.78 0 7 4 142.00 9.86 0 -7 -4 131.07 10.79 0 7 4 158.04 10.08 0 7 5 390.58 22.54 0 7 5 403.75 23.57 0 -7 -5 401.49 24.81 0 -7 -5 419.09 23.06 0 -7 -5 388.51 25.06 0 7 5 356.05 23.73 0 7 5 386.72 22.59 0 -7 -6 24.44 3.67 0 -7 -6 38.98 5.03 0 7 6 31.52 4.05 0 -7 -6 36.52 5.20 0 7 6 35.16 4.58 0 7 7 70.23 6.95 0 -7 -7 71.46 7.66 0 7 7 70.07 6.46 0 -7 -7 72.88 7.27 0 -7 -7 51.37 6.02 0 7 7 54.95 6.23 0 7 7 57.92 4.84 0 -7 -8 131.61 11.65 0 7 8 128.08 10.89 0 7 8 126.31 10.22 0 7 8 124.84 10.54 0 7 8 121.43 8.03 0 7 9 56.03 6.70 0 -7 -9 40.90 6.52 0 7 9 53.54 6.49 0 7 9 54.72 6.16 0 -7 -10 403.62 27.20 0 7 10 414.33 26.30 0 7 10 393.75 25.54 0 7 10 383.30 26.08 0 -7 -11 81.01 9.58 0 7 11 95.50 9.61 0 7 11 93.41 8.96 0 7 11 70.24 8.58 0 7 11 74.45 5.95 0 7 12 44.74 6.81 0 7 12 50.60 6.70 0 7 12 36.52 6.37 0 7 12 40.62 3.72 0 7 13 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6 60.48 6.72 0 8 -6 43.55 8.43 0 8 -6 50.67 8.43 0 -8 5 8.89 2.67 0 -8 5 4.13 1.61 0 8 -5 9.18 5.22 0 8 -5 6.21 1.00 0 8 -5 10.64 6.68 0 8 -4 1.08 1.51 0 -8 4 2.02 1.58 0 -8 4 0.21 0.94 0 -8 4 0.37 1.59 0 8 -4 1.07 0.67 0 8 -4 4.80 5.12 0 8 -3 118.91 9.26 0 -8 3 96.93 8.88 0 -8 3 125.28 9.87 0 -8 3 121.69 8.43 0 8 -3 102.56 13.48 0 8 -3 91.15 13.30 0 8 -2 147.90 10.28 0 -8 2 139.75 10.78 0 -8 2 164.26 11.54 0 8 -2 111.58 14.44 0 8 -2 101.77 14.36 0 8 -1 20.51 6.02 0 8 -1 12.07 2.21 0 8 -1 11.86 4.94 0 -8 1 21.68 3.80 0 -8 1 13.90 2.84 0 8 0 6.27 4.11 0 8 0 10.44 4.33 0 -8 0 7.31 2.15 0 8 0 7.78 2.19 0 8 0 6.89 1.63 0 -8 0 4.99 1.32 0 -8 0 7.63 2.49 0 -8 0 7.91 2.12 0 8 1 35.60 6.38 0 8 1 25.75 5.52 0 8 1 50.26 4.35 0 -8 -1 47.24 5.17 0 8 1 42.51 4.84 0 -8 -1 33.41 3.47 0 -8 -1 45.99 5.37 0 -8 -1 47.06 5.35 0 8 2 155.28 13.04 0 -8 -2 168.82 11.83 0 8 2 153.97 13.00 0 8 2 152.01 10.33 0 8 2 160.68 11.42 0 -8 -2 135.15 11.56 0 -8 -2 137.59 11.54 0 8 3 83.97 7.70 0 -8 -3 85.85 7.59 0 8 3 76.88 7.49 0 8 3 73.42 6.83 0 -8 -3 56.07 6.91 0 -8 -3 64.04 7.13 0 8 4 17.85 3.02 0 -8 -4 15.95 3.22 0 8 4 19.90 3.19 0 8 4 21.73 3.41 0 -8 -4 17.69 3.66 0 -8 -4 21.67 4.13 0 8 5 12.47 2.45 0 8 5 25.60 2.26 0 -8 -5 13.03 3.47 0 8 5 16.12 2.97 0 -8 -5 19.58 3.93 0 -8 -5 19.14 3.46 0 -8 -6 152.06 11.44 0 8 6 146.68 9.96 0 -8 -6 152.74 11.94 0 8 6 133.06 10.26 0 8 7 205.01 13.47 0 -8 -7 220.11 16.34 0 8 7 250.85 15.59 0 8 7 201.45 15.26 0 -8 -7 234.43 17.38 0 8 7 220.65 15.83 0 8 8 0.18 1.00 0 -8 -8 0.47 1.82 0 8 8 0.71 1.39 0 8 8 1.24 1.73 0 -8 -8 -1.11 1.71 0 8 8 -0.86 1.69 0 8 9 0.61 0.94 0 -8 -9 0.59 2.17 0 8 9 1.88 1.83 0 8 9 -0.46 1.85 0 8 9 3.11 1.58 0 -8 -10 25.98 5.49 0 8 10 20.08 4.42 0 8 10 16.89 4.07 0 8 10 15.77 3.62 0 8 11 35.85 5.83 0 8 11 32.79 5.17 0 8 11 33.38 5.74 0 8 12 173.01 13.38 0 8 12 178.06 14.36 0 8 13 106.54 10.74 0 8 13 90.93 9.54 0 -8 -14 18.42 5.92 0 8 14 88.28 9.80 0 8 15 33.82 6.94 0 -8 -15 5.94 4.65 0 -8 -16 0.59 1.77 0 -8 -16 -0.93 3.87 0 8 16 -0.80 3.70 0 8 16 -0.72 3.88 0 -8 -17 7.21 3.63 0 -8 -17 -2.06 4.99 0 8 17 9.41 4.50 0 8 17 10.88 4.45 0 8 18 8.35 4.46 0 -8 -18 8.68 3.59 0 -8 -19 3.17 2.65 0 -9 17 2.79 2.70 0 -9 17 -0.89 3.27 0 -9 16 2.08 2.48 0 -9 16 1.68 2.97 0 9 -16 -2.90 4.00 0 -9 15 28.47 4.97 0 9 -15 14.75 5.94 0 -9 15 28.36 6.32 0 9 -15 11.15 4.79 0 -9 14 7.60 2.90 0 9 -14 1.94 3.34 0 -9 14 7.32 3.64 0 9 -14 2.66 3.15 0 -9 13 8.62 3.04 0 9 -13 14.75 5.30 0 -9 13 7.40 3.47 0 9 -13 2.57 3.49 0 9 -12 -1.25 3.53 0 -9 12 -0.62 3.28 0 -9 12 3.04 2.10 0 -9 11 -0.57 2.30 0 9 -11 1.00 2.82 0 9 -11 -1.32 2.47 0 -9 11 1.05 1.76 0 9 -10 71.15 9.30 0 -9 10 100.97 8.08 0 9 -10 101.77 10.58 0 -9 10 65.67 7.97 0 9 -10 65.57 11.39 0 -9 10 74.37 8.72 0 -9 9 15.80 3.82 0 -9 9 14.14 2.98 0 9 -9 15.57 4.49 0 9 -9 11.79 4.29 0 9 -9 12.85 5.57 0 -9 8 63.46 5.83 0 9 -8 56.67 7.64 0 -9 8 35.98 5.87 0 9 -8 60.39 8.64 0 9 -8 58.94 8.23 0 9 -7 126.83 12.70 0 9 -7 107.12 10.77 0 -9 7 113.86 8.70 0 -9 7 94.87 9.52 0 -9 7 122.64 10.90 0 9 -7 128.19 13.20 0 9 -7 90.96 12.57 0 9 -6 0.50 1.75 0 -9 6 1.22 1.59 0 9 -6 -0.73 3.75 0 9 -6 0.76 3.30 0 -9 6 0.46 1.98 0 9 -5 28.36 6.76 0 9 -5 30.36 7.17 0 -9 5 24.76 4.56 0 -9 4 75.97 7.49 0 -9 4 97.10 8.55 0 9 -4 66.74 4.92 0 9 -4 85.68 10.94 0 9 -4 73.17 10.70 0 9 -3 3.24 3.69 0 9 -3 -0.56 0.85 0 9 -3 0.35 1.41 0 -9 3 0.37 1.32 0 -9 3 -0.41 1.56 0 9 -2 139.65 10.45 0 -9 2 144.82 11.31 0 -9 2 165.53 12.21 0 9 -2 129.92 14.29 0 9 -2 137.04 8.79 0 9 -2 126.05 14.50 0 9 -1 17.88 5.50 0 9 -1 23.62 3.30 0 9 -1 21.80 6.21 0 -9 1 32.06 4.76 0 -9 1 29.06 4.28 0 9 0 0.70 2.71 0 -9 0 -0.37 1.44 0 9 0 2.69 2.50 0 9 0 0.67 0.93 0 -9 0 0.78 1.64 0 -9 0 -0.37 1.54 0 9 1 4.16 2.77 0 9 1 0.58 1.92 0 -9 -1 -0.37 1.51 0 9 1 0.68 1.20 0 9 1 2.45 1.19 0 -9 -1 2.43 1.77 0 -9 -1 3.15 1.72 0 9 2 20.35 4.19 0 9 2 18.01 3.88 0 9 2 18.91 2.80 0 -9 -2 14.73 3.19 0 -9 -2 14.85 3.44 0 9 2 14.52 3.00 0 -9 -2 13.13 3.34 0 9 3 3.89 1.95 0 -9 -3 1.16 1.52 0 9 3 3.18 1.97 0 9 3 2.55 1.33 0 -9 -3 1.43 1.85 0 9 3 2.32 1.47 0 -9 -3 4.08 2.05 0 9 4 6.17 2.28 0 -9 -4 5.98 2.32 0 -9 -4 3.91 2.49 0 9 4 5.56 2.10 0 -9 -4 5.65 2.62 0 -9 -5 34.49 5.11 0 9 5 47.82 5.45 0 -9 -5 34.77 5.81 0 -9 -5 38.59 6.10 0 -9 -6 1.70 1.66 0 9 6 3.35 1.56 0 9 6 0.76 0.92 0 9 6 1.39 1.58 0 -9 -6 3.78 2.51 0 -9 -6 1.77 1.38 0 -9 -6 3.93 2.69 0 9 7 153.50 12.24 0 9 7 127.11 10.17 0 -9 -7 169.30 13.05 0 -9 -7 169.93 14.39 0 9 7 152.92 10.01 0 9 7 164.79 12.18 0 -9 -7 203.09 12.15 0 -9 -7 182.70 14.18 0 9 7 136.97 10.47 0 9 8 4.78 1.61 0 9 8 2.31 1.89 0 -9 -8 3.77 2.62 0 -9 -8 -0.36 1.59 0 -9 -8 4.32 2.42 0 9 8 0.88 1.54 0 -9 -8 2.77 1.88 0 9 9 21.89 3.03 0 -9 -9 22.07 5.19 0 9 9 22.97 4.50 0 -9 -9 18.55 4.39 0 9 9 26.16 4.89 0 9 9 32.63 4.74 0 9 10 2.17 2.20 0 9 10 -0.53 2.38 0 9 10 -0.77 1.16 0 9 10 1.76 1.70 0 9 11 75.50 8.45 0 9 11 76.25 7.55 0 9 12 0.52 2.48 0 -9 -12 1.26 3.11 0 9 12 3.19 2.88 0 -9 -13 28.05 6.67 0 9 13 33.52 6.62 0 9 13 27.89 3.15 0 -9 -14 13.17 5.19 0 9 14 13.27 4.74 0 -9 -14 16.63 4.56 0 9 15 28.99 6.74 0 -9 -15 17.93 6.00 0 -9 -15 22.15 4.93 0 -9 -16 -0.64 2.41 0 9 16 0.84 2.88 0 -9 -16 -0.93 3.55 0 9 16 -1.43 2.96 0 -9 -17 5.87 3.23 0 -9 -17 1.03 4.82 0 9 17 3.08 3.29 0 -9 -18 -0.67 2.27 0 -9 -19 -0.69 2.66 0 -10 16 4.34 3.61 0 -10 16 5.83 3.13 0 10 -15 -3.05 4.21 0 -10 15 -0.82 2.90 0 -10 15 -0.49 2.43 0 10 -14 6.58 4.50 0 10 -14 1.13 3.65 0 10 -14 13.33 5.47 0 -10 14 12.95 4.50 0 -10 14 11.50 3.45 0 10 -13 1.40 3.32 0 -10 13 5.99 2.81 0 10 -13 1.15 3.94 0 -10 13 3.54 2.91 0 -10 12 0.66 2.40 0 -10 12 6.37 2.55 0 10 -12 4.07 3.83 0 10 -12 1.17 3.54 0 -10 11 43.15 7.10 0 -10 11 39.20 6.31 0 10 -11 47.94 10.11 0 -10 11 61.66 6.44 0 10 -10 28.12 6.07 0 -10 10 25.69 5.11 0 -10 10 20.27 4.83 0 -10 10 30.39 4.54 0 10 -10 37.46 6.59 0 10 -10 17.50 6.61 0 10 -9 10.80 4.03 0 -10 9 11.99 3.49 0 -10 9 14.17 3.09 0 10 -9 18.02 5.13 0 10 -9 12.67 5.72 0 -10 8 24.95 5.07 0 10 -8 45.40 7.32 0 10 -8 37.32 6.61 0 -10 8 41.90 4.93 0 -10 7 3.30 1.89 0 10 -7 -1.36 3.08 0 10 -7 3.67 2.80 0 -10 7 3.32 2.14 0 -10 6 136.91 9.89 0 10 -6 114.95 11.78 0 -10 6 96.18 10.26 0 10 -6 155.19 14.12 0 10 -6 152.10 14.30 0 -10 5 232.70 17.88 0 10 -5 291.82 21.40 0 10 -5 251.75 20.79 0 10 -5 230.40 18.12 0 10 -4 1.51 0.83 0 10 -4 2.22 3.47 0 -10 4 2.86 2.33 0 10 -4 -2.30 3.75 0 10 -3 18.60 5.97 0 10 -3 11.33 2.01 0 -10 3 10.59 3.13 0 -10 3 17.78 3.92 0 10 -3 23.27 6.86 0 -10 2 37.00 5.24 0 -10 2 47.77 6.28 0 10 -2 28.23 6.56 0 10 -2 39.62 3.56 0 10 -2 33.15 7.19 0 10 -1 91.39 10.64 0 10 -1 81.03 7.15 0 -10 1 92.55 8.71 0 -10 1 86.23 6.50 0 -10 1 102.65 9.26 0 10 -1 82.40 5.17 0 10 -1 101.31 11.20 0 10 0 253.33 19.56 0 10 0 260.69 19.52 0 10 0 238.90 15.27 0 -10 0 234.91 17.11 0 -10 0 233.80 14.54 0 -10 0 236.33 17.27 0 -10 0 246.74 17.16 0 10 1 65.80 8.09 0 10 1 60.81 7.63 0 10 1 50.09 5.07 0 -10 -1 47.16 6.14 0 10 1 50.17 6.15 0 -10 -1 47.29 6.43 0 -10 -1 54.16 6.53 0 10 2 84.65 8.67 0 10 2 73.38 6.50 0 -10 -2 76.92 7.92 0 10 2 64.66 7.08 0 -10 -2 68.82 8.18 0 -10 -2 68.08 8.01 0 10 3 230.55 15.68 0 -10 -3 208.61 15.55 0 10 3 233.18 15.74 0 10 3 197.34 13.75 0 10 3 190.62 14.64 0 -10 -3 184.48 16.03 0 -10 -3 210.62 16.19 0 10 4 240.40 16.40 0 -10 -4 262.41 17.59 0 10 4 245.50 15.78 0 10 4 226.50 16.40 0 -10 -4 201.27 17.87 0 -10 -4 230.13 17.98 0 10 5 -0.33 1.67 0 -10 -5 3.19 1.93 0 10 5 3.64 2.02 0 -10 -5 2.55 2.66 0 -10 -5 4.13 2.56 0 10 6 3.25 1.71 0 -10 -6 6.12 2.48 0 10 6 3.07 1.86 0 -10 -6 7.12 3.27 0 10 6 5.76 2.33 0 -10 -6 4.43 2.84 0 10 7 0.27 1.14 0 -10 -7 -0.97 1.89 0 10 7 0.57 1.24 0 10 7 0.55 0.89 0 -10 -7 0.64 2.33 0 10 7 0.81 1.77 0 -10 -7 -0.26 1.46 0 -10 -7 0.67 2.68 0 -10 -8 134.77 11.37 0 10 8 131.32 9.08 0 10 8 88.04 7.44 0 10 8 135.78 10.67 0 -10 -8 96.33 8.82 0 -10 -8 140.17 13.31 0 -10 -9 232.06 17.26 0 10 9 216.21 14.18 0 -10 -9 265.56 16.62 0 10 9 267.58 17.10 0 10 9 232.72 17.31 0 10 10 17.71 2.95 0 10 10 24.02 4.39 0 -10 -10 36.48 5.73 0 -10 -10 37.19 5.77 0 10 10 27.53 5.46 0 -10 -11 43.89 6.71 0 -10 -11 37.64 6.25 0 10 11 44.02 6.30 0 10 11 31.89 3.36 0 10 11 52.47 7.40 0 10 12 60.60 8.29 0 -10 -12 72.00 8.44 0 10 13 -0.57 1.15 0 -10 -13 -1.36 3.24 0 10 13 -0.72 2.64 0 -10 -14 0.64 2.56 0 -10 -14 1.52 3.61 0 10 14 -0.77 2.81 0 -10 -15 9.19 4.53 0 10 15 13.17 4.67 0 -10 -15 10.64 4.00 0 10 15 12.76 4.53 0 -10 -16 -1.83 4.42 0 10 16 -0.88 4.14 0 -10 -16 1.38 2.48 0 10 16 0.72 2.60 0 -10 -17 14.78 6.31 0 10 17 24.76 6.11 0 -10 -17 24.84 5.94 0 -10 -18 5.12 3.18 0 -10 -19 11.36 4.14 0 -11 15 -0.85 2.67 0 -11 15 -0.52 2.25 0 11 -14 2.64 3.92 0 -11 14 2.39 2.83 0 -11 14 4.39 2.86 0 11 -13 -2.29 4.16 0 -11 13 2.75 2.49 0 11 -13 2.69 3.73 0 -11 13 -0.75 3.05 0 -11 12 0.71 2.27 0 11 -12 -2.93 4.20 0 11 -12 2.72 4.10 0 -11 12 -0.43 2.18 0 11 -11 1.36 4.41 0 -11 11 2.00 2.75 0 -11 11 -0.56 2.72 0 -11 11 1.61 2.07 0 -11 10 -1.72 3.08 0 -11 10 -0.63 2.72 0 -11 10 -0.76 2.01 0 11 -10 -3.43 4.12 0 11 -10 2.70 4.11 0 11 -9 66.82 9.49 0 -11 9 84.96 7.62 0 -11 9 49.52 7.70 0 11 -9 81.75 10.12 0 11 -9 48.75 11.10 0 11 -8 8.64 3.73 0 -11 8 -0.55 2.28 0 -11 8 2.76 2.00 0 11 -8 0.68 3.27 0 11 -8 8.86 5.29 0 -11 7 1.66 1.73 0 -11 7 3.16 2.12 0 11 -7 0.69 3.20 0 11 -7 2.74 2.58 0 -11 6 9.26 2.61 0 -11 6 12.25 3.56 0 11 -6 8.97 3.69 0 11 -6 16.65 5.09 0 -11 5 3.49 2.54 0 11 -5 0.70 3.49 0 11 -5 2.32 2.30 0 11 -4 47.42 3.74 0 11 -4 55.58 7.09 0 11 -3 104.43 9.87 0 -11 3 109.37 10.36 0 -11 3 123.82 11.43 0 11 -3 100.18 7.34 0 11 -3 127.69 12.72 0 11 -3 135.25 13.37 0 11 -2 23.68 5.54 0 11 -2 11.39 2.04 0 -11 2 13.36 3.42 0 -11 2 14.07 2.62 0 -11 2 12.72 3.67 0 11 -2 14.01 4.75 0 11 -1 223.04 16.95 0 11 -1 233.79 17.08 0 11 -1 176.42 10.96 0 -11 1 158.45 13.70 0 -11 1 144.48 10.95 0 -11 1 196.47 14.63 0 -11 1 182.74 13.99 0 11 0 90.86 9.39 0 -11 0 67.56 7.55 0 11 0 92.96 9.70 0 -11 0 45.44 4.88 0 -11 0 63.51 7.69 0 -11 0 59.94 7.25 0 -11 -1 0.48 1.58 0 11 1 -1.67 3.07 0 11 1 1.33 1.88 0 11 1 -0.27 1.30 0 -11 -1 -0.52 1.79 0 11 1 -1.08 2.62 0 11 2 22.80 3.53 0 11 2 19.68 3.88 0 11 2 27.90 5.05 0 -11 -2 20.74 4.58 0 -11 -2 23.24 4.55 0 11 3 3.73 2.14 0 11 3 6.16 2.06 0 -11 -3 6.39 2.72 0 -11 -3 6.84 3.14 0 11 3 5.28 2.54 0 -11 -4 148.66 12.66 0 11 4 145.09 11.82 0 11 4 148.80 11.04 0 -11 -4 118.56 13.07 0 -11 -4 137.42 13.09 0 -11 -5 90.98 9.84 0 11 5 118.13 9.55 0 11 5 108.55 9.86 0 11 5 105.62 9.10 0 -11 -5 112.81 12.37 0 -11 -5 93.03 10.89 0 11 6 9.11 2.60 0 11 6 16.18 3.35 0 -11 -6 18.82 4.13 0 -11 -6 13.86 4.90 0 11 6 18.48 4.08 0 -11 -6 15.44 4.76 0 -11 -7 5.38 2.82 0 11 7 3.36 1.74 0 11 7 0.48 2.40 0 11 7 4.09 1.95 0 -11 -8 113.77 10.63 0 11 8 103.97 8.53 0 11 8 83.47 6.40 0 11 8 131.72 10.71 0 -11 -8 102.94 8.30 0 11 8 91.89 9.76 0 -11 -9 24.10 5.00 0 11 9 27.93 4.10 0 11 9 21.12 3.05 0 11 9 33.05 5.25 0 -11 -9 25.31 4.42 0 11 9 34.05 5.69 0 -11 -10 2.98 2.60 0 11 10 1.33 1.34 0 11 10 1.49 2.25 0 -11 -10 4.29 2.54 0 11 10 1.20 2.04 0 11 10 1.90 1.46 0 -11 -11 24.79 5.38 0 11 11 12.28 2.95 0 -11 -11 27.84 5.20 0 11 11 33.72 5.46 0 11 11 19.57 2.87 0 -11 -12 5.80 3.18 0 -11 -12 5.79 1.83 0 -11 -12 10.45 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0 12 -4 -1.39 3.03 0 12 -4 4.94 2.58 0 -12 3 74.27 6.48 0 12 -3 62.75 7.60 0 12 -3 64.79 5.26 0 -12 2 3.79 1.79 0 -12 2 1.08 2.10 0 12 -2 0.40 1.58 0 12 -2 -0.52 1.07 0 12 -2 2.64 3.09 0 -12 1 27.12 3.83 0 -12 1 51.15 6.88 0 12 -1 46.25 5.30 0 12 -1 39.21 3.83 0 12 -1 45.82 7.16 0 12 0 2.95 2.59 0 -12 0 5.40 2.82 0 12 0 1.83 3.50 0 -12 0 -1.06 1.48 0 -12 0 2.74 2.09 0 -12 0 4.29 2.82 0 12 1 2.76 2.60 0 -12 -1 4.91 2.57 0 12 1 4.55 3.21 0 -12 -1 4.60 2.81 0 -12 -1 6.70 2.95 0 12 2 -1.53 2.46 0 12 2 -0.95 2.08 0 -12 -2 -1.09 1.80 0 -12 -2 0.63 2.16 0 -12 -2 -0.59 2.80 0 12 3 -0.47 1.64 0 -12 -3 -1.10 2.13 0 12 3 1.84 2.29 0 -12 -3 -2.08 3.47 0 -12 -3 0.62 2.38 0 -12 -4 6.66 2.98 0 12 4 5.85 2.74 0 12 4 4.35 2.16 0 12 4 3.25 2.38 0 -12 -4 2.32 3.44 0 -12 -4 0.67 2.45 0 -12 -5 9.58 3.45 0 12 5 8.02 2.91 0 12 5 11.73 3.13 0 12 5 10.45 3.36 0 12 5 7.74 2.69 0 12 6 -0.40 1.73 0 -12 -6 2.31 2.02 0 12 6 0.98 2.22 0 12 6 0.77 1.74 0 12 7 3.13 2.10 0 -12 -7 2.96 2.58 0 12 7 -0.52 2.09 0 12 7 0.36 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10 -2 46.58 5.68 4 10 -2 46.59 6.81 4 10 -2 63.36 7.16 -4 -10 2 54.75 7.74 -4 -10 2 57.13 6.15 -4 -10 2 49.81 6.86 -4 -10 2 44.58 5.28 4 10 -1 26.03 3.93 4 10 -1 28.04 4.86 -4 -10 1 15.12 4.49 4 10 -1 35.69 5.40 -4 -10 1 37.39 4.74 -4 -10 1 25.34 4.99 -4 -10 1 31.26 4.30 4 10 0 1.18 1.19 4 10 0 2.39 1.84 -4 -10 0 1.17 1.94 4 10 0 0.95 1.74 4 10 0 1.42 1.76 -4 -10 0 3.61 2.30 -4 -10 0 1.71 1.48 4 10 1 0.36 1.31 4 10 1 0.97 1.94 -4 -10 -1 -0.57 1.88 4 10 1 0.88 1.55 -4 -10 -1 1.61 1.96 -4 -10 -1 0.37 1.47 4 10 2 21.99 4.14 -4 -10 -2 18.21 4.24 4 10 2 21.38 3.63 4 10 2 25.15 3.68 -4 -10 -2 19.97 4.56 -4 -10 -3 10.33 3.41 -4 -10 -3 7.41 3.15 4 10 3 10.70 2.81 4 10 3 10.97 3.09 4 10 3 8.69 2.42 -4 -10 -4 25.46 4.83 4 10 4 19.97 3.59 -4 -10 -4 17.81 4.81 4 10 4 15.35 3.82 4 10 4 24.79 4.18 4 10 5 94.78 8.25 -4 -10 -5 99.95 9.94 -4 -10 -5 94.58 10.82 -4 -10 -5 93.58 9.33 4 10 6 175.76 12.70 -4 -10 -6 161.19 13.96 -4 -10 -6 163.09 15.49 4 10 6 180.87 13.79 -4 -10 -6 151.17 13.52 4 10 6 146.33 12.47 -4 -10 -7 36.38 6.03 4 10 7 38.78 5.29 -4 -10 -7 35.64 6.87 4 10 7 40.90 5.90 4 10 7 43.60 5.76 -4 -10 -7 42.89 6.55 -4 -10 -8 11.88 3.77 4 10 8 9.19 3.14 -4 -10 -8 8.98 3.96 4 10 8 9.64 3.28 -4 -10 -8 11.27 4.10 -4 -10 -8 5.32 3.69 -4 -10 -9 10.40 3.46 -4 -10 -9 15.36 4.87 4 10 9 19.12 4.35 -4 -10 -9 16.24 4.84 4 10 9 16.79 4.18 -4 -10 -10 1.19 2.50 -4 -10 -10 2.42 2.98 4 10 10 -1.63 3.24 4 10 10 0.56 0.62 4 10 10 -0.53 2.47 4 10 10 -0.57 2.09 -4 -10 -11 143.75 12.94 4 10 11 159.78 10.73 4 10 11 150.82 12.79 4 10 11 162.12 13.64 4 10 11 138.26 10.28 4 10 12 2.88 1.20 -4 -10 -12 2.32 1.76 4 10 12 4.30 1.35 -4 -10 -12 5.10 2.94 4 10 12 2.99 2.78 4 10 12 4.02 2.81 4 10 13 37.36 7.13 -4 -10 -13 45.22 6.93 4 10 13 44.45 7.02 -4 -10 -13 31.29 5.86 4 10 14 6.98 3.82 -4 -10 -14 14.85 4.68 4 10 14 4.18 3.43 -4 -10 -14 4.47 3.05 4 10 15 7.77 2.94 4 10 15 9.02 4.14 -4 -10 -15 10.38 4.28 4 10 15 9.76 4.59 -4 -10 -15 9.08 3.59 4 10 16 0.98 2.28 4 10 16 -0.88 2.65 -4 -10 -16 -0.65 2.87 4 10 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1.63 5 -6 -8 0.50 2.03 5 -6 -8 4.04 1.63 -5 6 8 1.90 2.10 5 -6 -8 2.54 1.40 5 -6 -7 13.57 3.89 -5 6 7 19.24 2.68 5 -6 -7 20.15 4.24 -5 6 7 23.05 4.19 5 -6 -7 16.00 2.74 -5 6 6 0.79 1.23 5 -6 -6 -0.45 1.75 5 -6 -6 1.29 1.13 5 -6 -5 1.86 1.21 5 -6 -5 -0.52 1.93 -5 6 5 1.07 1.39 -5 6 5 0.36 1.28 5 -6 -5 -0.43 1.96 -5 6 5 -0.32 0.98 -5 6 4 539.26 31.80 5 -6 -4 577.69 31.23 -5 6 4 517.96 31.38 5 -6 -4 548.83 30.84 -5 6 4 532.25 31.71 -5 6 4 551.76 29.91 5 -6 -4 511.48 29.80 5 -6 -4 503.52 32.41 5 -6 -3 218.12 14.19 5 -6 -3 225.58 14.12 -5 6 3 199.30 13.98 -5 6 3 218.11 12.66 -5 6 3 210.96 14.36 -5 6 3 195.29 14.62 5 -6 -3 170.78 14.57 5 -6 -2 156.16 10.92 5 -6 -2 145.26 10.59 -5 6 2 139.03 10.31 -5 6 2 171.02 11.01 -5 6 2 139.84 11.36 -5 6 1 397.23 22.68 -5 6 1 375.87 22.70 -5 6 1 379.74 22.34 5 -6 -1 350.95 22.72 5 -6 -1 385.10 23.28 -5 6 1 371.14 23.84 -5 6 0 4.12 1.97 5 -6 0 4.59 1.74 -5 6 0 3.07 1.51 5 -6 0 7.07 2.39 -5 6 0 1.18 1.16 5 -6 0 7.27 2.04 -5 6 0 4.70 1.46 -5 6 -1 27.87 4.36 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0.73 1.06 5 5 7 -0.41 1.84 5 5 7 -0.68 1.34 -5 -5 -7 -0.37 1.63 5 5 7 1.14 1.15 -5 -5 -7 0.32 1.19 -5 -5 -8 90.83 8.81 5 5 8 92.14 8.63 -5 -5 -8 108.49 9.20 5 5 8 90.05 8.76 -5 -5 -8 78.23 7.93 -5 -5 -8 94.23 8.11 5 5 9 -0.42 1.58 -5 -5 -9 -1.38 1.93 -5 -5 -9 1.70 1.94 5 5 9 0.46 1.21 5 5 9 0.23 0.91 -5 -5 -9 -0.32 1.07 -5 -5 -10 155.59 13.50 5 5 10 167.43 13.46 -5 -5 -10 181.63 13.94 5 5 10 176.01 14.12 5 5 10 166.40 10.98 5 5 10 128.02 12.31 5 5 11 16.76 3.97 -5 -5 -11 13.97 3.88 5 5 11 12.00 2.04 -5 -5 -11 19.99 4.42 5 5 11 20.14 4.44 5 5 11 10.21 3.30 -5 -5 -12 26.29 5.54 5 5 12 28.16 5.28 -5 -5 -12 24.12 3.84 -5 -5 -12 33.36 5.94 5 5 12 39.02 6.38 5 5 12 23.41 4.71 5 5 13 4.67 3.03 5 5 13 2.99 2.89 5 5 13 6.36 3.97 -5 -5 -13 4.50 3.76 -5 -5 -13 0.33 1.54 5 5 14 1.51 1.94 5 5 14 1.30 2.39 5 5 14 1.55 3.14 -5 -5 -14 0.71 3.31 -5 -5 -14 1.31 1.61 5 5 15 30.10 5.38 -5 -5 -15 27.35 4.07 5 5 15 26.69 6.06 -5 -5 -15 21.15 6.21 5 5 15 40.83 7.73 -5 -5 -16 11.97 2.97 5 5 16 9.12 4.26 -5 -5 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21.33 4.60 5 6 -6 21.51 4.36 -5 -6 6 25.65 4.33 5 6 -6 23.39 5.06 -5 -6 6 29.21 4.16 -5 -6 5 117.58 9.45 5 6 -5 96.19 9.23 -5 -6 5 80.84 9.49 -5 -6 5 97.62 6.49 5 6 -5 112.91 10.71 -5 -6 5 103.13 8.42 -5 -6 4 417.34 24.09 5 6 -4 437.24 26.78 5 6 -4 411.40 25.50 -5 -6 4 392.70 26.67 -5 -6 4 443.06 25.26 5 6 -4 414.88 25.29 -5 -6 4 446.33 23.66 -5 -6 4 360.92 21.38 -5 -6 4 396.05 21.67 -5 -6 3 48.29 4.94 -5 -6 3 46.91 4.63 5 6 -3 51.81 6.40 5 6 -3 54.94 6.11 -5 -6 3 58.17 7.20 -5 -6 3 52.19 5.87 5 6 -3 49.69 5.78 -5 -6 3 43.27 3.39 5 6 -2 4.00 2.04 -5 -6 2 3.39 1.52 5 6 -2 1.47 1.67 -5 -6 2 5.44 2.61 -5 -6 2 3.76 1.96 5 6 -2 4.70 1.88 5 6 -1 167.61 12.99 -5 -6 1 188.10 12.17 5 6 -1 180.55 13.29 -5 -6 1 188.50 14.66 5 6 -1 180.43 13.27 -5 -6 1 187.63 13.12 5 6 -1 167.20 12.54 5 6 0 19.75 3.03 -5 -6 0 18.53 2.80 5 6 0 19.73 3.17 -5 -6 0 12.58 3.20 5 6 0 15.39 3.08 5 6 0 20.08 3.30 -5 -6 0 15.76 3.13 -5 -6 0 13.08 1.94 5 6 1 280.93 17.08 -5 -6 -1 291.40 17.10 5 6 1 256.12 17.03 5 6 1 271.56 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6.19 6 -6 2 44.45 5.69 -6 6 -2 48.76 4.79 6 -6 2 71.97 7.40 -6 6 -2 52.12 6.26 6 -6 2 99.01 6.07 -6 6 -2 97.69 9.78 -6 6 -2 44.64 6.25 6 -6 3 21.64 3.54 -6 6 -3 25.35 4.38 -6 6 -3 24.17 4.07 6 -6 3 7.64 2.76 6 -6 3 19.71 3.48 -6 6 -3 5.82 3.17 6 -6 4 1.57 1.70 -6 6 -4 2.28 1.98 6 -6 4 0.39 1.22 -6 6 -4 4.06 2.98 6 -6 4 4.56 2.21 -6 6 -4 -0.46 1.59 6 -6 5 237.79 15.80 6 -6 5 190.70 11.47 -6 6 -5 206.50 15.59 6 -6 5 212.27 15.40 -6 6 -5 197.66 17.43 6 -6 5 196.13 14.32 -6 6 -5 180.79 15.12 6 -6 6 12.24 1.50 6 -6 6 21.48 4.46 -6 6 -6 15.03 3.80 6 -6 6 16.90 3.77 -6 6 -6 16.20 5.03 6 -6 6 15.58 3.23 -6 6 -6 16.34 4.07 6 -6 7 49.52 7.47 6 -6 7 43.90 3.01 6 -6 7 41.65 5.57 -6 6 -7 43.07 6.57 6 -6 7 63.44 8.15 -6 6 -7 51.26 6.68 -6 6 -7 43.81 7.59 6 -6 8 46.33 8.91 6 -6 8 69.83 5.03 -6 6 -8 68.36 9.82 6 -6 8 52.09 9.19 -6 6 -8 80.38 8.65 -6 6 -8 81.73 9.40 -6 6 -9 30.50 6.47 -6 6 -9 55.36 7.04 -6 6 -9 43.96 6.94 6 -6 10 2.43 2.85 -6 6 -10 2.57 3.32 6 -6 11 5.27 3.29 -6 6 -11 15.94 5.39 6 -6 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66.98 6.65 6 -4 -4 91.87 7.50 -6 4 3 -0.31 1.14 -6 4 3 0.30 1.05 6 -4 -3 -1.11 1.84 -6 4 3 0.36 1.51 -6 4 3 1.02 1.38 6 -4 -3 0.32 1.12 -6 4 2 17.57 2.87 -6 4 2 21.41 3.26 6 -4 -2 18.84 3.10 -6 4 2 27.48 3.85 6 -4 -2 23.01 4.83 6 -4 -2 18.83 3.26 -6 4 2 21.06 3.57 -6 4 2 24.34 3.88 -6 4 1 9.83 1.98 -6 4 1 9.33 2.21 6 -4 -1 10.12 2.23 -6 4 1 12.76 2.51 6 -4 -1 13.06 2.74 6 -4 -1 9.08 3.17 -6 4 1 9.86 2.56 -6 4 1 14.06 3.07 -6 4 0 764.11 42.71 -6 4 0 812.41 43.74 6 -4 0 781.87 43.35 -6 4 0 823.52 44.24 6 -4 0 770.14 44.65 -6 4 0 888.65 46.66 6 -4 0 832.54 47.35 -6 4 0 731.30 45.10 -6 4 -1 194.38 11.43 6 -4 1 200.00 12.36 -6 4 -1 196.95 12.47 -6 4 -1 175.22 12.72 6 -4 1 163.58 13.67 -6 4 -1 196.72 14.93 -6 4 -1 196.72 14.34 6 -4 1 206.24 13.84 6 -4 2 96.58 8.43 -6 4 -2 100.07 5.98 6 -4 2 88.32 8.54 -6 4 -2 99.08 8.69 -6 4 -2 97.94 7.24 6 -4 2 102.13 7.29 6 -4 2 107.52 7.49 -6 4 -2 95.80 9.62 -6 4 -2 101.43 9.09 6 -4 3 67.68 6.67 6 -4 3 71.35 6.91 -6 4 -3 68.04 6.99 -6 4 -3 72.73 5.45 6 -4 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6 8 94.67 7.77 -7 -6 -8 95.04 9.16 7 6 8 94.08 8.98 -7 -6 -8 95.07 9.10 7 6 8 85.12 8.35 7 6 8 87.16 7.10 -7 -6 -9 7.72 2.97 7 6 9 22.53 3.57 7 6 9 15.66 2.90 7 6 9 20.73 4.37 -7 -6 -9 17.49 4.12 7 6 9 13.47 3.62 7 6 10 18.73 4.15 -7 -6 -10 14.28 3.98 -7 -6 -10 7.77 3.09 7 6 10 7.79 2.25 7 6 10 13.62 3.75 7 6 10 6.52 2.18 7 6 11 12.40 3.67 7 6 11 10.12 2.43 7 6 11 6.63 3.21 7 6 11 16.07 3.14 -7 -6 -11 15.04 4.12 -7 -6 -11 10.80 3.41 7 6 12 240.45 18.06 -7 -6 -12 205.45 15.95 -7 -6 -12 205.83 17.43 7 6 12 250.34 19.21 7 6 12 210.00 14.65 -7 -6 -13 90.31 9.01 7 6 13 81.26 10.09 7 6 13 100.21 11.26 -7 -6 -13 92.87 10.56 7 6 13 102.50 11.74 7 6 13 90.51 7.29 7 6 14 29.13 6.22 7 6 14 28.23 6.11 -7 -6 -14 31.08 6.68 7 6 14 38.11 7.32 -7 -6 -14 23.11 4.48 7 6 15 20.14 2.13 7 6 15 21.40 2.19 -7 -6 -15 35.31 5.27 -7 -6 -15 32.13 6.70 7 6 15 63.07 9.56 7 6 15 42.34 7.60 7 6 15 49.25 7.74 -7 -6 -16 1.23 1.69 -7 -6 -16 -0.81 3.38 7 6 16 -0.97 2.96 7 6 16 -0.80 2.45 7 6 16 0.69 2.39 -7 -6 -17 -0.39 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3.15 -7 -8 3 1.22 3.79 -7 -8 2 54.00 8.28 7 8 -2 54.76 7.04 -7 -8 2 64.12 11.13 -7 -8 2 46.12 6.32 -7 -8 2 50.20 5.72 7 8 -2 35.47 6.69 -7 -8 1 13.32 6.44 7 8 -1 17.02 3.90 -7 -8 1 25.89 3.88 7 8 -1 16.74 4.29 7 8 -1 18.38 4.13 -7 -8 1 14.26 4.51 -7 -8 1 13.34 3.78 -7 -8 1 15.89 2.00 -7 -8 0 137.91 16.56 7 8 0 141.98 12.07 -7 -8 0 146.90 11.45 7 8 0 151.85 12.82 -7 -8 0 163.58 14.83 7 8 0 154.76 12.84 -7 -8 0 137.00 10.89 7 8 0 172.05 12.92 -7 -8 0 161.63 13.12 -7 -8 0 142.20 9.61 -7 -8 -1 33.89 7.91 7 8 1 34.29 5.10 7 8 1 32.53 5.22 -7 -8 -1 41.33 6.86 7 8 1 44.21 6.06 -7 -8 -1 42.45 5.13 -7 -8 -1 34.45 4.14 7 8 1 32.79 4.97 -7 -8 -1 47.94 6.54 -7 -8 -1 39.54 4.13 -7 -8 -2 1.04 1.21 7 8 2 3.09 1.89 7 8 2 2.46 1.95 -7 -8 -2 1.26 1.96 7 8 2 0.92 1.77 -7 -8 -2 0.36 1.58 -7 -8 -2 -0.18 1.12 -7 -8 -2 2.71 2.66 7 8 2 0.40 1.71 -7 -8 -2 8.52 4.45 7 8 3 123.50 10.10 7 8 3 123.09 10.15 -7 -8 -3 110.89 11.72 7 8 3 125.53 10.88 7 8 3 139.85 10.97 7 8 3 107.24 9.96 -7 -8 -3 138.30 12.21 -7 -8 -3 121.19 9.48 -7 -8 -4 80.46 10.87 7 8 4 64.23 6.82 7 8 4 68.93 6.89 7 8 4 68.74 7.51 -7 -8 -4 62.44 8.19 7 8 4 77.04 8.01 7 8 4 81.64 7.96 -7 -8 -4 73.24 8.62 7 8 4 62.34 6.18 -7 -8 -4 58.86 6.46 7 8 5 36.69 4.68 -7 -8 -5 32.78 4.81 7 8 5 33.32 4.69 7 8 5 42.30 5.05 7 8 5 24.49 4.91 7 8 5 47.14 5.84 -7 -8 -5 24.27 6.46 -7 -8 -5 33.35 5.78 7 8 5 44.83 5.83 7 8 6 79.24 7.36 -7 -8 -6 50.11 8.99 -7 -8 -6 77.97 9.23 7 8 6 82.27 8.15 7 8 6 65.35 7.93 7 8 6 78.22 8.12 -7 -8 -6 66.00 8.55 7 8 7 0.71 1.58 7 8 7 -0.56 2.48 7 8 7 -0.90 2.05 -7 -8 -7 -0.62 2.78 -7 -8 -7 -0.58 1.80 7 8 7 0.45 1.73 7 8 8 0.74 1.74 7 8 8 -0.59 2.88 -7 -8 -8 -0.64 2.21 7 8 8 1.43 1.93 -7 -8 -8 1.76 2.28 -7 -8 -9 3.55 2.40 7 8 9 1.91 2.16 7 8 9 1.02 2.07 -7 -8 -9 -0.66 2.18 7 8 9 0.20 1.53 7 8 9 0.76 1.80 7 8 10 9.40 3.48 7 8 10 12.19 3.81 -7 -8 -10 6.58 3.23 7 8 10 10.41 2.45 7 8 11 69.12 8.38 7 8 11 55.66 5.41 7 8 11 74.20 8.83 -7 -8 -12 31.14 5.71 7 8 12 22.46 5.30 7 8 12 19.02 3.17 7 8 12 24.91 5.67 -7 -8 -12 25.38 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14.21 4.29 10 -5 -7 19.19 4.07 10 -5 -7 18.72 4.77 -10 5 6 9.31 3.26 -10 5 6 6.24 3.71 10 -5 -6 2.87 2.42 10 -5 -6 10.00 5.79 10 -5 -6 5.12 2.29 10 -5 -6 2.45 2.57 -10 5 5 1.63 2.30 -10 5 5 1.28 2.25 10 -5 -5 -1.11 4.20 10 -5 -5 4.13 2.08 10 -5 -5 0.98 2.38 -10 5 4 2.04 2.23 10 -5 -4 5.78 2.78 -10 5 4 4.17 2.87 -10 5 4 1.29 1.66 10 -5 -4 2.07 1.46 10 -5 -4 -0.50 1.73 -10 5 3 2.89 2.19 -10 5 3 9.19 2.84 10 -5 -3 3.46 2.78 10 -5 -3 -1.08 3.73 -10 5 3 5.54 3.11 -10 5 3 6.68 2.67 10 -5 -3 3.72 1.76 10 -5 -3 1.52 1.75 -10 5 2 1.82 2.00 -10 5 2 2.09 1.68 10 -5 -2 -1.15 1.90 10 -5 -2 2.11 3.83 -10 5 2 1.54 2.40 -10 5 2 1.56 2.10 10 -5 -2 2.00 1.34 10 -5 -2 2.50 2.37 -10 5 1 7.71 2.30 10 -5 -1 6.25 2.93 10 -5 -1 17.40 5.89 -10 5 1 13.83 3.68 -10 5 1 6.39 2.53 -10 5 1 5.02 2.71 -10 5 0 0.24 1.06 10 -5 0 4.91 3.91 10 -5 0 -1.69 2.38 -10 5 0 -1.36 2.32 -10 5 0 0.40 1.62 10 -5 0 0.10 0.78 -10 5 -1 31.80 5.33 10 -5 1 25.31 7.02 -10 5 -1 49.77 4.35 10 -5 1 42.27 5.56 10 -5 2 50.16 5.70 -10 5 -2 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55.58 8.58 10 -5 11 49.43 8.77 10 -5 11 54.75 5.67 10 -5 12 -0.86 3.30 10 -5 12 0.28 1.53 10 -5 12 0.76 2.47 -10 5 -13 -0.76 2.90 10 -5 13 1.02 2.88 10 -5 13 3.67 3.96 10 -5 14 1.96 3.19 -10 5 -14 9.30 4.17 -10 5 -15 -0.79 3.38 -10 5 -16 9.64 4.20 -10 5 -17 -0.81 2.88 10 -4 -13 7.69 4.21 10 -4 -13 5.05 2.67 10 -4 -12 7.04 3.81 10 -4 -12 18.34 4.43 10 -4 -11 60.85 8.39 -10 4 11 81.33 10.71 -10 4 11 78.82 10.53 -10 4 10 5.18 3.53 10 -4 -10 2.32 2.49 -10 4 10 3.80 3.29 10 -4 -10 4.55 3.17 10 -4 -10 3.57 2.74 -10 4 9 34.44 6.81 10 -4 -9 30.17 5.75 -10 4 9 29.19 6.09 10 -4 -9 23.47 4.61 -10 4 8 2.60 3.20 -10 4 8 -0.65 2.60 10 -4 -8 1.20 2.50 -10 4 8 -1.51 3.40 10 -4 -8 2.65 2.21 10 -4 -8 -0.90 2.05 -10 4 7 10.35 3.77 -10 4 7 8.92 3.61 -10 4 7 2.89 3.27 10 -4 -7 8.48 3.46 10 -4 -7 1.11 4.56 10 -4 -7 8.12 3.05 10 -4 -7 5.52 2.58 -10 4 6 94.58 9.80 -10 4 6 62.09 9.14 10 -4 -6 57.00 10.86 10 -4 -6 83.06 8.19 10 -4 -6 77.06 8.02 -10 4 5 52.69 7.09 -10 4 5 37.49 6.91 10 -4 -5 55.94 6.24 10 -4 -5 52.34 6.44 -10 4 4 0.61 2.67 10 -4 -4 1.82 2.35 -10 4 4 1.00 1.85 10 -4 -4 -2.07 2.47 -10 4 3 56.80 7.97 10 -4 -3 104.40 10.27 10 -4 -3 87.22 8.77 -10 4 3 77.15 8.07 10 -4 -3 73.04 7.69 10 -4 -2 152.55 12.16 -10 4 2 152.34 12.02 10 -4 -2 176.73 14.11 -10 4 2 119.26 11.71 10 -4 -2 125.47 11.15 -10 4 1 37.71 5.67 10 -4 -1 36.82 5.37 -10 4 1 27.43 4.69 -10 4 1 33.15 4.20 10 -4 -1 36.58 6.27 10 -4 -1 35.74 8.49 -10 4 0 28.50 4.79 -10 4 0 28.27 4.34 -10 4 0 27.53 3.54 10 -4 0 35.51 5.87 -10 4 -1 23.95 4.46 -10 4 -1 23.99 3.89 10 -4 1 19.05 6.03 10 -4 1 17.22 4.41 -10 4 -1 24.53 3.01 -10 4 -2 38.83 3.45 -10 4 -2 40.25 5.02 -10 4 -2 35.08 5.14 10 -4 2 34.59 2.60 10 -4 2 36.89 2.71 10 -4 2 25.59 6.59 10 -4 2 43.60 6.50 10 -4 3 119.42 11.05 -10 4 -3 109.65 6.56 -10 4 -3 109.94 8.84 10 -4 3 111.65 9.25 10 -4 3 48.82 8.69 10 -4 3 114.25 7.44 10 -4 3 78.77 8.19 10 -4 3 79.96 11.46 10 -4 4 109.64 8.83 10 -4 4 108.62 10.47 10 -4 4 62.23 9.17 10 -4 4 75.22 8.30 10 -4 4 95.52 7.33 -10 4 -4 100.79 10.58 10 -4 4 59.80 10.04 10 -4 4 97.18 6.16 10 -4 5 6.27 2.14 10 -4 5 8.45 3.00 10 -4 5 1.68 2.18 10 -4 5 6.54 2.72 10 -4 5 1.90 2.64 10 -4 5 1.46 2.18 10 -4 5 6.45 1.39 -10 4 -5 4.86 2.58 10 -4 6 30.16 6.63 10 -4 6 50.57 6.67 10 -4 6 41.45 5.99 10 -4 6 48.19 5.39 10 -4 6 22.40 5.45 -10 4 -6 47.35 6.96 10 -4 6 18.49 4.81 10 -4 7 15.24 5.14 10 -4 7 55.42 6.89 10 -4 7 43.20 5.77 10 -4 7 52.73 5.38 -10 4 -7 46.86 6.92 10 -4 8 18.19 4.75 10 -4 8 16.97 3.57 -10 4 -8 21.54 5.04 10 -4 8 7.80 4.62 10 -4 8 15.99 4.02 10 -4 9 19.27 3.45 10 -4 9 26.71 5.87 10 -4 9 29.78 4.11 -10 4 -9 20.67 5.09 10 -4 9 23.98 4.88 -10 4 -10 -0.66 2.03 10 -4 10 -1.52 3.42 10 -4 10 -0.20 0.90 10 -4 10 0.63 1.52 10 -4 11 61.07 5.62 10 -4 11 77.60 10.06 10 -4 12 77.91 7.24 10 -4 12 75.10 11.06 10 -4 12 78.55 9.45 10 -4 13 0.31 1.65 -10 4 -13 -0.70 2.57 10 -4 13 0.93 3.05 10 -4 13 0.71 2.47 10 -4 14 -0.31 1.38 10 -4 14 -0.98 3.36 10 -4 14 0.99 2.55 -10 4 -14 0.72 2.33 10 -4 15 -1.05 4.01 -10 4 -15 0.73 2.35 10 -3 -13 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1.75 2.13 -10 -3 -3 2.49 2.12 -10 -3 -3 -0.32 1.58 10 3 3 1.36 1.27 10 3 3 1.40 1.28 10 3 4 231.72 17.87 -10 -3 -4 212.82 19.48 10 3 4 155.80 18.94 10 3 4 262.06 17.13 10 3 4 256.31 16.01 10 3 4 257.50 18.27 -10 -3 -4 237.54 15.85 10 3 4 136.20 14.76 10 3 4 286.38 15.74 10 3 4 263.59 15.59 10 3 5 205.52 16.00 -10 -3 -5 215.82 18.41 10 3 5 226.05 15.07 10 3 5 207.43 13.68 10 3 5 217.69 14.31 10 3 5 155.89 14.30 10 3 5 214.27 13.83 10 3 6 -0.96 4.43 -10 -3 -6 2.25 2.78 10 3 6 1.52 1.61 10 3 6 1.93 1.60 10 3 6 2.49 1.50 10 3 6 0.89 1.92 10 3 6 1.66 2.39 10 3 6 4.28 2.47 10 3 6 1.49 2.97 10 3 7 87.54 6.85 10 3 7 92.48 11.09 10 3 7 83.11 8.01 10 3 7 61.21 7.72 10 3 7 90.99 7.96 10 3 8 18.12 5.94 10 3 8 38.91 5.07 10 3 8 40.63 4.21 10 3 8 31.51 4.61 10 3 8 35.32 5.64 10 3 8 21.34 5.44 10 3 8 32.93 7.03 10 3 9 23.05 3.34 10 3 9 28.19 4.47 10 3 9 24.77 4.01 10 3 9 19.89 4.60 10 3 9 14.27 5.82 10 3 9 42.77 8.15 10 3 9 32.53 5.60 10 3 10 9.25 2.25 10 3 10 10.64 3.57 10 3 10 9.78 4.14 10 3 10 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5.96 -10 -4 -2 46.13 5.21 10 4 2 41.79 6.64 -10 -4 -2 40.35 5.61 10 4 2 35.90 4.68 -10 -4 -2 39.49 5.15 10 4 2 37.73 3.55 10 4 3 106.01 9.96 -10 -4 -3 111.20 9.20 -10 -4 -3 95.69 9.23 10 4 3 113.23 9.03 10 4 3 112.75 7.87 -10 -4 -3 114.21 9.55 10 4 3 103.06 10.78 -10 -4 -4 125.66 14.68 10 4 4 171.32 12.86 10 4 4 133.99 12.74 -10 -4 -4 139.78 13.45 -10 -4 -4 181.28 12.33 10 4 4 169.39 11.55 -10 -4 -4 170.91 12.37 10 4 4 96.33 11.00 10 4 4 161.48 10.88 10 4 5 31.09 5.35 10 4 5 28.12 4.64 10 4 5 27.46 4.09 10 4 5 30.98 4.22 -10 -4 -5 30.84 5.70 10 4 5 23.93 4.97 -10 -4 -5 36.34 6.99 -10 -4 -6 45.23 7.51 10 4 6 30.60 4.44 10 4 6 28.18 4.55 10 4 6 24.45 3.76 -10 -4 -6 28.98 5.36 10 4 6 29.53 5.85 10 4 6 27.45 5.14 10 4 7 29.89 4.73 10 4 7 27.85 4.41 10 4 7 29.61 4.00 10 4 7 28.77 4.77 -10 -4 -7 37.12 5.83 10 4 7 31.22 5.11 10 4 7 33.41 6.33 -10 -4 -7 33.43 6.60 10 4 8 39.00 5.31 10 4 8 40.47 4.58 10 4 8 42.09 5.36 10 4 8 33.15 5.57 10 4 8 50.96 6.28 -10 -4 -8 30.53 6.59 10 4 8 38.97 6.00 10 4 9 114.94 11.40 -10 -4 -9 132.41 12.20 10 4 9 133.81 10.81 10 4 9 144.74 10.31 10 4 9 165.42 13.09 10 4 10 154.52 13.76 10 4 10 193.56 13.51 -10 -4 -10 169.25 14.60 10 4 10 203.16 13.05 10 4 10 187.94 15.18 10 4 11 46.33 5.26 10 4 11 37.25 5.79 10 4 11 36.83 7.38 10 4 11 39.43 6.27 10 4 11 56.36 7.92 -10 -4 -11 35.62 5.88 10 4 11 34.74 4.85 10 4 12 11.15 2.97 10 4 12 3.63 2.52 10 4 12 14.88 4.93 -10 -4 -12 11.06 3.24 10 4 12 19.85 5.43 10 4 12 12.88 3.85 10 4 13 17.69 5.08 10 4 13 18.55 5.39 10 4 13 22.65 4.57 10 4 13 8.78 4.31 10 4 14 25.69 6.18 10 4 14 32.76 7.14 10 4 14 24.93 4.48 10 4 14 29.75 5.82 10 4 15 16.53 5.44 10 4 15 12.76 5.29 10 4 15 11.47 3.20 10 4 16 10.37 4.84 10 4 16 11.31 4.83 10 4 16 3.59 1.78 10 4 16 1.98 3.77 10 4 17 3.77 3.04 -10 -5 12 1.47 4.67 -10 -5 11 -1.43 4.28 -10 -5 11 -0.61 2.62 -10 -5 10 1.39 4.20 -10 -5 10 13.30 4.10 -10 -5 9 6.83 3.07 -10 -5 9 9.42 5.98 -10 -5 9 1.09 2.35 -10 -5 9 0.61 2.22 -10 -5 8 0.44 1.92 -10 -5 8 -1.30 4.25 -10 -5 7 0.41 1.78 -10 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6.22 -10 -6 0 54.03 8.57 -10 -6 0 33.01 5.77 -10 -6 0 58.28 7.02 -10 -6 0 28.34 8.10 10 6 1 119.96 11.16 -10 -6 -1 108.14 9.09 -10 -6 -1 80.68 10.78 -10 -6 -1 89.45 9.04 10 6 1 101.22 9.12 -10 -6 -1 112.43 10.31 -10 -6 -1 66.29 11.65 10 6 2 1.04 2.06 -10 -6 -2 7.37 3.56 10 6 2 3.59 2.48 -10 -6 -2 3.09 1.98 -10 -6 -2 3.51 2.14 10 6 2 3.38 2.02 -10 -6 -2 3.50 2.37 -10 -6 -2 2.03 3.57 10 6 3 6.66 1.71 10 6 3 3.32 2.38 -10 -6 -3 7.18 2.63 -10 -6 -3 2.79 2.05 10 6 3 3.79 2.14 -10 -6 -3 7.13 2.83 10 6 3 6.87 2.95 -10 -6 -3 5.00 3.46 -10 -6 -3 6.86 4.15 10 6 4 75.46 8.81 -10 -6 -4 79.49 9.92 10 6 4 94.98 7.13 10 6 4 58.59 7.85 -10 -6 -4 92.18 9.36 -10 -6 -4 74.01 11.24 10 6 5 3.63 2.68 -10 -6 -5 8.08 3.62 10 6 5 7.24 2.16 10 6 5 5.41 2.92 -10 -6 -5 5.50 3.57 -10 -6 -6 87.51 10.38 10 6 6 104.63 8.64 -10 -6 -6 71.98 11.10 -10 -6 -7 3.22 2.82 10 6 7 1.85 2.06 10 6 7 4.28 2.20 -10 -6 -7 2.56 3.46 10 6 7 4.25 1.97 10 6 8 12.83 2.93 10 6 8 11.90 3.14 10 6 8 14.82 3.62 10 6 8 14.06 3.69 10 6 9 22.44 4.60 10 6 9 25.71 3.99 10 6 9 23.25 4.31 10 6 9 15.10 3.93 10 6 9 24.77 5.09 10 6 9 16.46 4.04 10 6 10 -0.54 1.99 10 6 10 0.37 1.92 10 6 10 2.19 2.55 -10 -6 -10 0.76 2.50 10 6 10 0.48 1.55 10 6 10 -0.59 2.68 10 6 10 1.28 1.68 -10 -6 -10 -0.61 2.66 10 6 11 33.71 5.23 -10 -6 -11 31.24 6.01 10 6 11 28.50 5.84 10 6 11 32.52 5.43 10 6 11 53.21 7.64 10 6 11 39.81 5.86 10 6 12 5.21 2.81 -10 -6 -12 8.21 3.20 10 6 12 8.50 3.96 10 6 12 8.84 3.01 10 6 13 5.42 3.60 -10 -6 -13 5.70 2.88 10 6 13 6.92 2.73 -10 -6 -14 -0.55 1.99 10 6 14 0.84 3.06 10 6 14 -0.43 1.93 10 6 14 -1.32 2.21 -10 -6 -15 3.11 2.21 10 6 15 1.82 3.77 10 6 15 2.18 1.81 10 6 15 1.82 3.30 -10 -6 -16 8.13 3.09 10 6 16 6.26 2.28 10 6 17 -0.95 3.59 10 6 18 0.95 2.84 -10 -7 10 6.11 3.10 -10 -7 9 3.16 5.70 -10 -7 9 5.31 2.78 -10 -7 8 4.52 2.76 -10 -7 8 3.55 2.40 -10 -7 7 16.46 4.27 -10 -7 7 14.09 3.83 -10 -7 6 11.73 3.44 -10 -7 6 14.56 3.95 -10 -7 5 31.37 5.13 -10 -7 5 14.06 6.84 -10 -7 5 25.96 4.98 -10 -7 4 -1.36 1.97 -10 -7 4 0.48 1.89 -10 -7 4 2.72 4.74 -10 -7 3 68.85 7.10 -10 -7 3 63.20 7.34 -10 -7 3 27.65 8.68 -10 -7 3 24.65 5.65 -10 -7 2 63.84 6.86 -10 -7 2 56.00 7.22 -10 -7 2 40.71 9.83 -10 -7 2 38.34 6.73 -10 -7 1 0.87 2.69 -10 -7 1 1.05 2.44 -10 -7 1 0.83 1.87 -10 -7 1 3.10 2.77 -10 -7 1 3.69 4.53 -10 -7 0 31.87 4.86 -10 -7 0 29.16 5.12 -10 -7 0 27.17 8.16 -10 -7 0 29.05 5.55 -10 -7 0 17.83 5.61 -10 -7 -1 6.96 2.77 -10 -7 -1 7.80 2.88 10 7 1 5.25 2.77 -10 -7 -1 10.23 5.48 -10 -7 -1 5.04 3.03 -10 -7 -1 6.58 3.74 -10 -7 -2 121.66 10.98 -10 -7 -2 178.98 12.69 10 7 2 164.87 12.42 -10 -7 -2 91.02 14.47 -10 -7 -2 174.41 14.13 -10 -7 -2 146.04 14.98 -10 -7 -3 231.13 19.67 10 7 3 221.03 13.68 -10 -7 -3 208.77 15.04 10 7 3 231.21 16.33 -10 -7 -3 252.69 16.76 -10 -7 -3 255.50 18.41 10 7 4 3.46 1.59 -10 -7 -4 6.59 3.44 -10 -7 -4 3.07 3.59 -10 -7 -4 5.96 3.27 10 7 5 10.59 2.52 -10 -7 -5 11.65 4.26 10 7 6 4.43 2.15 -10 -7 -6 6.68 4.46 -10 -7 -6 3.57 3.13 -10 -7 -7 52.73 6.53 10 7 7 49.55 6.02 -10 -7 -7 36.94 8.23 -10 -7 -7 51.96 8.08 10 7 7 51.85 6.80 10 7 8 56.92 6.79 10 7 8 54.39 7.07 -10 -7 -9 26.92 6.66 10 7 9 34.07 5.48 -10 -7 -9 37.34 6.02 10 7 9 39.33 5.91 10 7 9 46.49 6.72 10 7 9 32.27 5.49 -10 -7 -10 12.04 4.95 -10 -7 -10 35.69 6.38 -10 -7 -10 31.04 6.13 10 7 10 39.83 5.75 10 7 10 34.13 5.80 10 7 10 16.93 4.05 10 7 10 51.95 7.30 10 7 10 31.88 5.10 -10 -7 -11 43.91 7.41 10 7 11 56.85 7.76 10 7 11 58.88 8.17 10 7 11 46.90 6.37 -10 -7 -12 7.84 3.56 10 7 12 10.44 3.86 10 7 12 5.63 2.79 10 7 12 9.24 3.79 10 7 12 6.53 2.65 -10 -7 -13 24.99 5.43 10 7 13 28.42 6.18 10 7 13 16.37 3.94 10 7 13 25.48 6.46 10 7 13 21.91 4.45 -10 -7 -14 1.25 2.02 10 7 14 -0.84 3.35 10 7 14 -0.44 2.05 10 7 14 1.29 2.31 10 7 14 -0.81 3.08 -10 -7 -15 19.94 4.72 10 7 15 23.67 6.43 10 7 15 18.52 3.75 10 7 15 20.05 5.99 -10 -7 -16 16.09 4.64 10 7 16 23.94 6.36 10 7 17 31.33 7.46 -10 -8 10 5.54 2.94 -10 -8 7 -0.55 2.28 -10 -8 6 3.16 4.81 -10 -8 6 0.52 2.42 -10 -8 5 1.54 5.34 -10 -8 5 4.01 2.73 -10 -8 4 1.49 4.57 -10 -8 4 2.90 2.38 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12 3.98 2.27 -10 -9 -12 4.14 3.56 10 9 13 5.07 3.23 10 9 13 5.54 3.87 10 9 13 5.24 2.57 -10 -9 -13 4.90 3.38 10 9 14 2.36 2.99 10 9 14 0.85 3.07 -10 -9 -14 0.80 2.57 -10 -9 -15 12.47 4.54 10 9 15 15.35 5.35 10 9 15 10.35 4.19 -10 -9 -16 -0.76 2.83 -10 -10 5 1.87 6.82 -10 -10 5 20.16 4.69 -10 -10 4 19.53 6.69 -10 -10 4 12.74 8.18 -10 -10 4 28.12 5.39 -10 -10 3 17.07 6.34 -10 -10 3 21.12 9.10 -10 -10 3 22.05 4.80 -10 -10 3 12.20 4.10 -10 -10 2 14.50 5.91 -10 -10 2 15.24 7.83 -10 -10 2 8.61 3.51 -10 -10 2 7.04 3.23 -10 -10 1 7.59 4.72 -10 -10 1 6.49 6.24 -10 -10 1 10.02 3.28 -10 -10 1 11.70 3.73 -10 -10 0 7.38 4.89 -10 -10 0 1.55 4.76 -10 -10 0 7.89 3.36 -10 -10 0 5.39 2.46 -10 -10 -1 40.93 8.97 -10 -10 -1 35.43 10.20 -10 -10 -1 37.20 4.92 -10 -10 -1 55.79 7.11 -10 -10 -2 21.88 6.87 -10 -10 -2 35.23 9.76 10 10 2 28.10 5.50 -10 -10 -3 0.83 1.37 -10 -10 -3 0.97 3.73 -10 -10 -3 -1.35 4.71 -10 -10 -4 60.14 10.02 -10 -10 -4 32.74 9.97 -10 -10 -4 56.90 6.44 -10 -10 -5 8.01 3.32 -10 -10 -5 19.80 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49.77 4.79 11 1 10 44.94 5.39 11 1 10 57.83 9.16 11 1 10 68.49 8.18 11 1 10 64.24 8.06 11 1 11 39.04 6.40 11 1 11 34.13 3.77 11 1 11 27.71 3.95 11 1 11 46.85 8.26 11 1 11 41.68 6.59 11 1 11 35.43 6.38 11 1 11 24.69 7.75 11 1 12 8.55 4.24 11 1 12 12.54 2.25 11 1 12 9.60 2.16 11 1 12 13.41 5.11 11 1 12 10.60 3.95 11 1 12 9.13 3.59 11 1 12 2.39 3.61 11 1 13 2.94 1.64 11 1 13 3.16 2.28 11 1 13 -1.21 4.52 11 1 13 1.84 3.02 11 1 13 2.88 3.22 11 1 13 8.28 4.52 11 1 14 0.30 1.74 11 1 14 -0.48 1.83 11 1 14 -2.43 5.10 11 1 14 -0.78 2.71 11 1 14 0.99 3.60 11 1 14 0.94 2.88 11 1 15 3.61 2.43 11 1 15 11.01 6.09 11 1 15 3.18 3.86 11 1 16 0.45 1.84 11 1 16 -1.13 4.09 11 1 17 0.48 2.04 11 1 17 -0.57 2.03 -11 -2 13 -1.24 4.56 -11 -2 12 13.57 6.53 -11 -2 11 2.44 3.66 -11 -2 10 1.43 3.06 -11 -2 10 -2.40 4.11 -11 -2 9 31.80 6.29 -11 -2 9 25.48 3.56 -11 -2 9 19.95 5.20 -11 -2 8 -0.61 2.82 -11 -2 8 -0.96 1.50 -11 -2 8 -1.16 3.27 -11 -2 8 1.21 2.53 -11 -2 7 15.20 4.25 -11 -2 7 14.69 2.62 -11 -2 7 13.66 5.79 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11 3 2 195.27 17.82 11 3 2 205.96 14.02 -11 -3 -2 216.54 16.28 -11 -3 -2 185.49 19.20 11 3 2 219.40 13.12 11 3 3 70.47 12.70 11 3 3 109.79 10.64 -11 -3 -3 111.44 9.14 11 3 3 111.61 9.92 11 3 3 107.47 11.40 11 3 3 117.98 12.15 -11 -3 -3 98.90 9.81 11 3 3 102.01 8.44 11 3 3 106.37 8.12 11 3 3 113.25 11.76 -11 -3 -3 82.42 11.92 11 3 4 1.28 2.20 11 3 4 0.69 2.24 11 3 4 3.13 2.01 11 3 4 0.99 2.13 11 3 4 9.03 5.19 -11 -3 -4 0.89 2.76 11 3 4 0.87 1.63 11 3 4 1.33 2.09 11 3 4 -0.30 1.36 11 3 5 2.48 2.66 11 3 5 5.18 2.47 11 3 5 2.49 1.88 11 3 5 2.85 1.91 11 3 5 6.25 2.00 11 3 5 -2.25 4.47 -11 -3 -5 -1.73 3.66 11 3 6 2.24 3.41 11 3 6 5.73 2.30 11 3 6 3.24 1.87 11 3 6 4.25 2.74 11 3 6 6.40 2.25 -11 -3 -6 5.09 3.59 11 3 6 4.89 2.63 11 3 7 124.98 9.71 11 3 7 119.37 11.13 11 3 7 89.96 10.73 11 3 7 160.65 11.63 11 3 7 153.43 11.98 11 3 8 171.30 13.27 11 3 8 144.79 10.34 11 3 8 172.17 14.11 11 3 8 181.16 13.12 11 3 8 147.12 11.83 11 3 9 -1.12 3.83 11 3 9 0.57 1.99 11 3 9 -0.39 1.72 11 3 9 1.51 2.49 11 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9.40 2.82 -11 -4 3 8.77 4.15 -11 -4 3 23.85 4.54 -11 -4 3 23.03 4.23 -11 -4 3 20.53 3.64 -11 -4 3 12.65 5.73 11 4 -2 4.63 2.35 -11 -4 2 4.57 3.14 -11 -4 2 1.78 2.14 -11 -4 2 5.02 2.35 -11 -4 2 2.66 1.83 -11 -4 2 -3.36 4.52 11 4 -1 1.29 1.78 -11 -4 1 6.12 3.57 -11 -4 1 3.89 2.32 -11 -4 1 2.56 1.92 -11 -4 1 2.73 1.84 -11 -4 1 3.27 4.22 11 4 0 1.42 1.80 -11 -4 0 -0.35 1.51 -11 -4 0 1.06 3.03 -11 -4 0 1.77 1.55 11 4 1 2.08 2.39 -11 -4 -1 0.71 1.85 11 4 1 1.28 1.49 -11 -4 -1 -0.36 1.54 -11 -4 -1 -1.03 3.18 -11 -4 -2 1.99 3.49 11 4 2 0.14 0.88 11 4 2 1.52 2.25 11 4 2 2.82 1.79 -11 -4 -2 2.52 1.79 11 4 2 0.57 2.19 -11 -4 -2 -0.75 1.66 11 4 2 2.11 2.80 11 4 3 37.98 3.90 11 4 3 26.73 5.85 -11 -4 -3 39.54 5.14 11 4 3 33.28 4.58 -11 -4 -3 36.04 5.00 -11 -4 -3 22.12 6.79 11 4 4 50.92 6.54 11 4 4 59.04 8.14 11 4 4 67.84 6.60 -11 -4 -4 55.36 6.50 11 4 4 53.68 5.46 -11 -4 -4 47.42 8.83 -11 -4 -5 13.52 5.10 11 4 5 15.75 3.36 11 4 5 12.66 2.91 11 4 5 10.94 2.93 11 4 5 17.71 4.33 11 4 6 36.42 4.81 11 4 6 30.79 4.69 11 4 6 27.72 5.43 11 4 6 34.53 5.89 -11 -4 -6 27.23 6.53 11 4 7 45.60 5.86 11 4 7 37.25 4.89 11 4 7 38.87 5.92 11 4 7 46.04 5.85 -11 -4 -7 38.60 7.91 11 4 8 0.49 1.80 11 4 8 0.31 1.82 11 4 8 2.22 1.90 11 4 8 -3.64 3.42 11 4 8 0.48 2.08 11 4 8 1.17 2.00 11 4 9 34.24 5.67 11 4 9 26.54 3.95 11 4 9 26.45 4.52 11 4 9 31.38 6.04 11 4 9 33.57 5.70 11 4 9 24.54 5.18 11 4 10 27.73 3.94 11 4 10 25.05 4.30 11 4 10 25.87 5.24 11 4 10 31.21 5.87 11 4 10 24.32 5.30 11 4 11 19.66 3.42 11 4 11 14.77 3.48 11 4 11 17.08 5.32 11 4 11 6.96 3.30 11 4 11 18.44 4.95 11 4 11 17.85 4.48 11 4 12 114.74 13.48 11 4 12 91.56 9.10 11 4 12 134.24 12.20 11 4 12 122.99 9.89 11 4 13 -0.90 1.82 11 4 13 -0.92 2.82 11 4 13 -0.55 2.19 11 4 14 6.76 4.59 11 4 14 2.48 2.42 11 4 15 5.71 2.76 11 4 16 -1.01 3.06 11 4 16 2.65 1.87 11 4 17 45.19 9.32 -11 -5 9 -1.44 4.64 -11 -5 8 0.43 1.79 -11 -5 8 2.40 2.68 -11 -5 7 0.81 2.08 -11 -5 7 3.35 2.66 -11 -5 6 7.83 2.66 -11 -5 6 3.96 4.83 -11 -5 6 7.77 3.13 -11 -5 6 4.17 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8.51 2.57 11 5 6 11.37 2.96 11 5 6 10.32 3.54 -11 -5 -6 11.47 4.04 11 5 6 6.84 2.81 -11 -5 -6 3.68 3.74 11 5 7 19.23 3.64 11 5 7 16.05 3.58 11 5 7 21.53 4.42 11 5 7 19.89 4.03 -11 -5 -7 16.10 5.69 11 5 8 21.51 4.28 11 5 8 17.90 3.45 11 5 8 13.63 3.60 11 5 8 22.43 4.46 11 5 8 20.55 4.64 11 5 9 12.36 2.90 11 5 9 9.19 2.98 -11 -5 -9 8.84 3.55 11 5 9 1.54 3.12 11 5 9 13.50 3.96 11 5 9 7.85 3.19 11 5 10 12.79 4.22 -11 -5 -10 28.93 5.85 11 5 10 32.30 4.95 11 5 10 29.23 4.34 11 5 10 27.83 5.53 11 5 11 5.28 2.31 11 5 11 4.75 3.12 11 5 11 5.42 2.23 -11 -5 -11 4.78 2.77 11 5 11 6.78 3.00 11 5 11 4.46 3.06 11 5 12 28.77 5.47 11 5 12 36.12 7.33 -11 -5 -12 31.48 5.76 11 5 12 37.93 6.16 11 5 12 45.37 7.39 11 5 13 6.16 3.67 11 5 13 7.02 3.06 11 5 13 3.81 3.53 11 5 14 14.10 3.97 11 5 15 0.88 1.95 11 5 16 6.74 2.49 11 5 16 9.06 5.01 -11 -6 9 11.25 3.78 -11 -6 9 3.09 4.97 -11 -6 8 30.01 9.31 -11 -6 8 48.01 6.93 -11 -6 7 1.08 2.24 -11 -6 7 1.13 2.25 -11 -6 7 5.15 2.60 -11 -6 6 22.81 4.76 -11 -6 6 19.46 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15 4 13 1.49 2.22 15 4 14 23.12 5.54 15 4 15 32.56 6.37 -15 -5 2 0.84 3.16 -15 -5 1 0.58 2.20 -15 -5 1 1.59 3.37 -15 -5 0 1.14 2.25 -15 -5 0 -0.75 3.08 -15 -5 -1 2.82 2.67 -15 -5 -1 5.68 3.62 -15 -5 -2 -2.99 5.68 -15 -5 -2 1.36 3.09 -15 -5 -2 2.25 2.58 -15 -5 -3 1.46 4.11 -15 -5 -3 1.68 2.56 -15 -5 -4 4.31 4.66 15 5 5 -0.45 2.21 -15 -5 -5 -1.41 3.62 15 5 5 0.80 1.35 15 5 6 0.37 1.50 15 5 6 -0.96 2.32 15 5 7 0.54 2.36 15 5 8 25.62 5.07 15 5 8 18.46 4.72 15 5 9 5.54 3.20 15 5 9 5.28 3.27 15 5 10 22.22 5.52 15 5 10 15.46 4.58 15 5 11 8.51 4.12 15 5 11 9.86 3.96 15 5 12 2.56 3.60 15 5 12 1.49 2.79 15 5 12 1.40 2.84 15 5 13 -0.94 3.64 15 5 13 1.47 2.61 15 5 13 -1.44 2.69 15 5 14 1.40 2.82 -15 -6 2 12.29 5.01 -15 -6 1 22.28 6.12 -15 -6 0 2.43 2.30 -15 -6 0 0.72 2.70 -15 -6 -1 2.03 2.98 -15 -6 -1 0.60 2.57 -15 -6 -2 -0.65 2.75 -15 -6 -2 2.38 2.72 15 6 4 1.43 2.03 -15 -6 -5 5.83 5.30 15 6 5 13.79 3.79 -15 -6 -6 -1.43 4.34 15 6 6 4.21 2.87 15 6 7 1.71 2.50 15 6 8 8.95 3.14 15 6 8 4.47 3.00 15 6 9 8.10 3.42 15 6 9 9.08 4.04 15 6 10 9.91 4.02 15 6 10 3.30 2.80 15 6 11 22.99 5.76 15 6 11 20.11 5.36 15 6 12 -0.82 3.57 15 6 12 1.47 2.61 15 6 13 -0.90 3.18 15 6 13 3.52 3.14 15 6 14 -0.68 3.12 -15 -7 2 0.79 3.17 -15 -7 1 0.73 3.30 -15 -7 -1 2.57 3.32 -15 -7 -1 3.19 3.00 -15 -7 -2 -0.61 2.49 -15 -7 -2 0.63 2.67 15 7 4 3.22 2.51 15 7 5 8.70 3.61 15 7 6 1.14 2.33 15 7 7 30.53 6.02 15 7 8 46.03 7.68 15 7 9 7.24 3.93 15 7 9 3.81 2.53 15 7 10 -1.44 3.54 15 7 10 -0.63 2.55 15 7 11 -0.74 3.32 15 7 11 0.71 2.75 15 7 12 13.48 4.65 15 7 13 35.87 7.38 -15 -8 2 3.00 3.01 -15 -8 1 0.70 3.20 -15 -8 0 1.29 2.79 -15 -8 -1 10.21 3.73 15 8 4 3.59 2.78 15 8 5 11.91 4.07 15 8 6 -0.62 2.41 15 8 7 -1.97 3.06 15 8 8 2.79 2.83 15 8 9 12.26 4.99 15 8 10 12.24 4.80 15 8 12 9.24 4.13 -15 -9 1 -0.65 2.59 -15 -9 0 6.57 3.53 -15 -9 -1 0.56 2.32 15 9 5 0.65 2.64 15 9 6 -0.67 2.48 15 9 7 0.70 2.85 15 9 8 -0.75 3.13 15 10 5 17.99 5.22 -16 8 -2 -0.67 2.59 -16 7 -2 -1.36 2.86 -16 6 -2 -1.37 3.09 16 -6 5 10.97 4.75 16 -6 6 -0.94 2.98 -16 5 5 10.65 3.61 -16 5 4 7.59 3.21 -16 5 3 5.88 2.64 -16 5 2 10.18 3.16 -16 5 -1 7.60 3.86 16 -5 3 8.58 3.95 16 -5 4 -0.81 2.90 16 -5 5 39.12 7.75 16 -5 6 35.60 7.53 16 -5 7 -0.93 3.15 -16 4 4 1.54 2.07 -16 4 3 15.90 3.86 -16 4 2 9.37 3.10 -16 4 1 6.24 2.61 -16 4 0 -0.36 1.61 -16 4 -1 25.48 5.69 16 -4 1 22.56 5.15 -16 4 -1 16.77 3.47 16 -4 2 50.50 7.76 16 -4 3 12.62 4.38 16 -4 4 7.49 3.71 16 -4 5 3.19 3.37 16 -4 6 -0.85 3.95 16 -4 7 38.64 7.98 16 -4 8 26.63 6.66 -16 3 4 2.63 2.43 -16 3 3 0.97 1.80 -16 3 2 0.44 1.87 -16 3 1 14.03 3.30 -16 3 0 0.78 1.45 -16 3 -1 2.18 1.79 16 -3 1 1.59 2.24 -16 3 -2 1.62 1.46 16 -3 2 -3.56 3.19 16 -3 2 2.92 2.63 16 -3 3 2.79 3.36 16 -3 3 10.18 3.88 16 -3 4 17.29 4.84 16 -3 5 2.24 2.40 16 -3 6 18.50 5.55 16 -3 7 31.08 6.95 16 -3 8 -1.85 3.91 16 -3 9 -0.99 4.17 -16 2 4 4.32 2.72 -16 2 3 7.43 3.04 16 -2 -3 12.91 4.32 -16 2 2 3.71 2.62 16 -2 -2 0.74 2.75 -16 2 1 5.66 2.66 16 -2 -1 3.96 3.23 -16 2 0 1.25 2.10 16 -2 0 -0.84 3.16 16 -2 1 0.46 2.02 -16 2 -1 2.38 2.11 16 -2 1 1.78 3.49 16 -2 2 1.56 1.95 -16 2 -2 1.11 1.88 16 -2 2 -0.93 3.35 16 -2 3 0.58 2.53 -16 2 -3 1.62 1.68 16 -2 3 0.97 2.92 16 -2 4 1.91 2.70 16 -2 4 1.00 3.61 16 -2 5 -0.70 2.62 16 -2 5 1.03 3.32 16 -2 6 1.52 2.58 16 -2 7 6.60 4.19 16 -2 8 -1.79 4.17 16 -2 9 -0.96 4.22 16 -2 10 1.04 3.51 -16 1 4 13.22 3.93 -16 1 3 10.27 3.42 16 -1 -3 11.09 4.17 -16 1 2 0.48 2.04 16 -1 -2 1.59 2.53 -16 1 1 15.58 3.88 16 -1 -1 20.28 5.87 -16 1 0 36.70 5.60 16 -1 0 40.16 7.94 -16 1 -1 9.03 3.15 16 -1 1 7.49 4.28 -16 1 -2 0.82 1.98 16 -1 2 1.95 3.33 16 -1 3 17.21 4.28 -16 1 -3 12.14 3.13 16 -1 3 21.20 6.65 16 -1 4 36.26 6.44 16 -1 4 48.76 9.32 16 -1 5 8.44 3.72 16 -1 5 18.04 6.31 16 -1 6 2.86 2.81 16 -1 7 -0.79 3.21 16 -1 7 -1.10 3.54 16 -1 8 24.03 6.56 16 -1 9 47.56 8.84 16 -1 10 7.05 4.11 16 -1 11 -1.09 3.46 16 0 -4 25.99 5.94 -16 0 3 8.49 3.31 16 0 -3 7.16 3.70 -16 0 2 10.07 3.39 16 0 -2 3.38 3.82 -16 0 1 1.93 2.32 16 0 -1 1.78 3.19 -16 0 0 5.17 2.78 16 0 0 2.81 3.53 -16 0 -1 43.52 6.18 -16 0 -1 39.62 8.02 16 0 1 37.20 7.99 -16 0 -2 8.29 4.76 -16 0 -2 9.44 3.06 16 0 2 10.17 4.80 -16 0 -3 0.43 1.81 16 0 3 -1.05 3.38 16 0 4 4.23 2.95 16 0 4 11.82 5.21 16 0 5 25.13 5.44 16 0 6 40.71 7.20 16 0 7 0.74 2.64 16 0 7 -1.12 3.62 16 0 8 21.88 5.69 16 0 9 3.77 2.31 16 0 9 2.65 3.47 16 0 10 35.58 7.81 16 0 11 22.89 4.99 16 0 11 24.99 6.64 16 0 12 -0.60 2.02 16 0 13 23.76 5.42 16 1 -4 13.41 4.78 -16 -1 3 0.55 2.41 -16 -1 2 3.16 2.47 16 1 -2 7.07 3.99 -16 -1 1 0.51 2.45 16 1 -1 2.79 3.49 -16 -1 0 0.99 2.26 16 1 0 -0.98 3.13 -16 -1 -1 -0.49 2.29 16 1 1 -1.02 3.27 -16 -1 -2 -1.44 2.79 16 1 2 3.16 3.98 -16 -1 -3 2.81 2.20 16 1 3 1.08 3.90 16 1 4 1.81 2.11 16 1 4 7.73 4.88 16 1 5 -1.60 2.69 16 1 6 -1.14 3.43 16 1 7 1.36 2.44 16 1 8 6.99 2.55 16 1 8 11.33 4.46 16 1 9 3.11 2.25 16 1 9 6.63 3.75 16 1 10 2.49 2.32 16 1 10 6.36 3.97 16 1 11 0.56 2.07 16 1 11 0.99 2.94 16 1 12 1.07 3.80 16 1 13 1.32 2.55 16 2 -4 -0.83 2.91 16 2 -3 0.88 2.40 -16 -2 2 28.23 5.58 -16 -2 1 -0.54 2.36 16 2 -1 2.93 3.30 -16 -2 0 -1.58 2.23 -16 -2 0 -0.86 3.39 16 2 0 -1.02 3.06 -16 -2 -1 14.13 5.07 -16 -2 -1 31.28 5.38 16 2 1 37.14 8.27 -16 -2 -2 7.31 4.15 -16 -2 -2 6.69 3.17 16 2 2 6.57 4.51 -16 -2 -3 6.06 2.95 16 2 3 7.85 5.12 16 2 6 18.97 4.49 16 2 6 23.27 7.22 16 2 7 10.83 3.06 16 2 7 13.66 4.37 16 2 8 12.68 3.56 16 2 8 16.76 4.85 16 2 9 -0.78 2.62 16 2 10 1.57 2.04 16 2 10 2.56 3.47 16 2 11 4.59 2.81 16 2 11 2.80 2.98 16 2 12 1.25 2.70 16 2 12 2.04 3.43 16 2 13 -0.67 2.36 -16 -3 1 2.84 2.73 -16 -3 0 9.48 3.74 -16 -3 0 16.10 5.30 -16 -3 -1 -0.82 3.59 -16 -3 -1 2.76 2.59 -16 -3 -2 22.28 5.85 -16 -3 -2 25.72 5.28 -16 -3 -3 46.87 7.02 16 3 6 0.94 1.84 16 3 7 19.69 4.07 16 3 7 14.55 4.28 16 3 8 38.02 6.78 16 3 9 0.51 1.99 16 3 9 2.90 2.83 16 3 10 -2.22 2.79 16 3 10 -0.81 2.72 16 3 11 8.41 3.31 16 3 11 1.77 3.31 16 3 12 46.86 7.40 16 3 12 38.83 8.42 16 3 13 6.85 3.34 -16 -4 0 8.25 3.43 -16 -4 -1 3.97 3.73 -16 -4 -1 9.92 3.82 -16 -4 -2 -1.55 3.61 -16 -4 -2 1.75 2.29 -16 -4 -3 0.57 2.34 16 4 6 -0.85 2.40 16 4 8 0.55 2.24 16 4 9 6.20 3.13 16 4 9 10.71 3.93 16 4 10 3.54 2.57 16 4 10 4.52 3.17 16 4 11 0.63 2.55 16 4 11 1.67 3.37 16 4 12 6.71 3.36 16 4 12 2.76 3.99 -16 -5 0 32.75 7.16 -16 -5 -1 3.83 3.56 -16 -5 -1 2.48 2.54 -16 -5 -2 10.41 4.56 -16 -5 -2 11.63 4.03 16 5 5 14.16 3.69 16 5 7 4.69 2.76 16 5 8 0.58 2.53 16 5 9 0.64 2.70 16 5 10 2.56 3.13 16 5 10 4.91 3.43 16 5 11 -0.67 3.25 16 5 11 1.57 2.78 16 5 12 6.34 3.60 16 5 12 4.36 3.64 -16 -6 0 5.39 3.86 -16 -6 -1 19.07 5.42 16 6 5 15.54 4.24 16 6 6 4.20 2.77 16 6 7 7.39 3.27 16 6 8 -0.62 2.40 16 6 9 22.17 5.70 16 6 10 20.02 5.45 16 6 11 4.28 3.47 -16 -7 0 8.04 4.01 -16 -7 -1 4.86 3.56 16 7 6 18.50 4.71 16 7 8 1.98 2.86 16 7 9 0.71 3.08 16 7 10 0.80 3.69 -16 -8 0 4.83 3.41 -16 -8 -1 7.87 3.86 16 8 6 2.53 2.73 16 8 7 0.66 2.55 16 8 8 -0.71 2.72 16 8 9 1.50 2.77 17 -6 3 1.87 3.44 17 -5 3 4.88 3.39 17 -5 4 30.92 6.74 17 -5 5 3.61 3.19 17 -4 4 16.96 5.23 17 -4 5 29.76 6.70 17 -4 6 9.70 4.64 17 -4 7 -0.94 2.56 -17 3 3 2.01 2.54 17 -3 4 -0.70 2.69 17 -3 6 0.82 2.90 17 -3 7 -0.88 3.12 17 -3 8 -0.95 2.60 -17 2 2 30.59 5.27 -17 2 1 0.47 1.90 17 -2 -1 2.48 2.76 -17 2 0 14.52 3.74 17 -2 0 18.53 5.55 -17 2 -1 4.76 2.53 17 -2 1 8.41 4.45 17 -2 2 1.97 3.67 17 -2 3 1.03 3.27 17 -2 5 34.16 6.57 17 -2 7 0.83 2.80 17 -2 8 3.63 3.37 17 -2 9 2.95 3.10 -17 1 2 7.77 3.39 17 -1 -2 7.40 3.66 -17 1 1 2.00 2.37 17 -1 -1 -0.88 3.09 -17 1 0 6.80 2.99 17 -1 0 4.66 3.91 -17 1 -1 0.47 2.04 17 -1 1 0.98 2.92 -17 1 -2 30.81 5.06 17 -1 2 38.04 8.27 17 -1 3 42.75 9.04 17 -1 6 1.43 2.53 17 -1 8 28.35 6.68 17 -1 9 0.94 2.95 -17 0 2 2.18 2.58 17 0 -2 -0.88 2.58 -17 0 1 9.51 3.32 17 0 -1 7.47 4.19 -17 0 0 -0.52 2.24 17 0 0 1.97 3.67 -17 0 -1 2.52 2.40 17 0 1 4.15 3.86 -17 0 -2 -0.49 2.26 17 0 2 1.08 3.22 17 0 7 3.64 2.94 17 0 9 4.40 3.94 17 0 10 -0.96 3.03 17 1 -2 3.73 3.28 -17 -1 1 27.39 5.28 17 1 -1 20.74 6.55 -17 -1 0 0.55 2.61 17 1 0 2.08 3.87 -17 -1 -1 1.61 2.26 17 1 1 -1.09 3.68 -17 -1 -2 1.05 2.37 17 1 8 2.98 2.89 17 1 9 4.12 3.19 17 1 10 4.52 3.63 17 1 11 2.96 3.10 -17 -2 0 10.42 3.66 -17 -2 -1 30.26 5.73 -17 -2 -2 10.70 3.84 17 2 10 31.58 6.90 17 2 11 9.38 4.44 -17 -3 -1 9.06 3.81 -17 -3 -2 1.79 2.60 -17 -4 -2 2.51 3.08 -18 -1 -1 -0.58 2.24 -18 -2 -2 1.20 2.58 0 0 0 0.00 0.00 TITL Sjcm19ar19a_13_180_00 in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 11.833248 12.344786 13.987357 82.7527 77.2090 89.2463 ZERR 2.00 0.000230 0.000285 0.000320 0.0019 0.0018 0.0018 LATT 1 SFAC C H N O F S Fe I UNIT 80.00 80.00 10.00 4.00 6.00 2.00 2.00 6.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 50027 _olex2_exptl_crystal_mounting_method 'Paratone oil' _olex2_submission_original_sample_id Sjcm19ar19a_13_180_00 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 5.546 _oxdiff_exptl_absorpt_empirical_full_min 0.532 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I -0.08293(2) 0.23710(2) 0.38583(2) 0.03406(8) Uani 1 1 d . . . . . I3 I 0.28390(2) 0.05512(2) 0.60519(2) 0.04165(9) Uani 1 1 d . . . . . I2 I -0.00860(3) 0.42847(3) 0.74432(2) 0.04877(10) Uani 1 1 d . . . . . Fe1 Fe 0.51480(4) 0.36431(4) 0.78953(3) 0.01982(11) Uani 1 1 d . . . . . S1 S -0.20133(11) 0.29067(11) 0.19657(9) 0.0478(3) Uani 1 1 d . . . . . F3 F 0.1186(2) 0.0882(2) 0.45054(18) 0.0390(6) Uani 1 1 d . . . . . O3 O 0.5920(2) 0.3099(2) 0.88876(17) 0.0239(5) Uani 1 1 d . . . . . F1 F -0.1058(2) 0.3840(2) 0.55887(19) 0.0436(6) Uani 1 1 d . . . . . O1 O 0.6290(2) 0.4720(2) 0.73548(17) 0.0248(5) Uani 1 1 d . . . . . F2 F 0.1873(2) 0.2520(2) 0.71736(19) 0.0461(6) Uani 1 1 d . . . . . O4 O 0.9690(2) 0.0394(2) 0.8758(2) 0.0346(6) Uani 1 1 d . . . . . N3 N 0.5968(2) 0.2718(2) 0.6951(2) 0.0206(6) Uani 1 1 d . . . . . O2 O 0.6937(2) 0.8752(2) 0.8467(2) 0.0365(7) Uani 1 1 d . . . . . N1 N 0.4231(2) 0.4546(2) 0.8802(2) 0.0212(6) Uani 1 1 d . . . . . N4 N 0.4323(2) 0.4104(2) 0.6822(2) 0.0238(6) Uani 1 1 d . . . . . N2 N 0.3858(2) 0.2575(2) 0.8477(2) 0.0214(6) Uani 1 1 d . . . . . C25 C 0.6870(3) 0.2145(3) 0.7050(3) 0.0224(7) Uani 1 1 d . . . . . H25 H 0.724608 0.178703 0.650591 0.027 Uiso 1 1 calc R U . . . C34 C 0.4660(3) 0.3536(3) 0.6025(2) 0.0215(7) Uani 1 1 d . . . . . C7 C 0.5609(3) 0.6041(3) 0.8495(3) 0.0233(7) Uani 1 1 d . . . . . C18 C 0.6844(3) 0.2482(3) 0.8773(3) 0.0224(7) Uani 1 1 d . . . . . C24 C 0.7341(3) 0.2010(3) 0.7904(3) 0.0223(7) Uani 1 1 d . . . . . C26 C 0.5541(3) 0.2759(3) 0.6079(2) 0.0229(7) Uani 1 1 d . . . . . C17 C 0.2969(3) 0.3006(3) 0.9122(2) 0.0223(7) Uani 1 1 d . . . . . C9 C 0.3126(3) 0.4090(3) 0.9297(3) 0.0218(7) Uani 1 1 d . . . . . C23 C 0.8300(3) 0.1304(3) 0.7887(3) 0.0249(7) Uani 1 1 d . . . . . H23 H 0.861718 0.098159 0.730583 0.030 Uiso 1 1 calc R U . . . C6 C 0.5780(3) 0.7075(3) 0.8774(3) 0.0255(7) Uani 1 1 d . . . . . H6 H 0.523960 0.733242 0.930322 0.031 Uiso 1 1 calc R U . . . C19 C 0.7373(3) 0.2239(3) 0.9588(3) 0.0250(7) Uani 1 1 d . . . . . H19 H 0.706962 0.254784 1.017886 0.030 Uiso 1 1 calc R U . . . C1 C 0.6419(3) 0.5632(3) 0.7716(3) 0.0236(7) Uani 1 1 d . . . . . C28 C 0.5390(3) 0.2301(3) 0.4488(3) 0.0319(9) Uani 1 1 d . . . . . H28 H 0.563264 0.186745 0.396734 0.038 Uiso 1 1 calc R U . . . C21 C 0.8776(3) 0.1080(3) 0.8701(3) 0.0255(7) Uani 1 1 d . . . . . C38 C 0.0386(4) 0.3197(3) 0.6413(3) 0.0335(9) Uani 1 1 d . . . . . C8 C 0.4565(3) 0.5476(3) 0.9001(2) 0.0220(7) Uani 1 1 d . . . . . H8 H 0.407824 0.579936 0.952132 0.026 Uiso 1 1 calc R U . . . C2 C 0.7412(3) 0.6293(3) 0.7268(3) 0.0270(8) Uani 1 1 d . . . . . H2 H 0.799089 0.603126 0.676779 0.032 Uiso 1 1 calc R U . . . C16 C 0.3763(3) 0.1547(3) 0.8320(3) 0.0275(8) Uani 1 1 d . . . . . H16 H 0.437882 0.124463 0.787902 0.033 Uiso 1 1 calc R U . . . C40 C 0.1570(3) 0.1687(3) 0.5840(3) 0.0318(8) Uani 1 1 d . . . . . C27 C 0.5885(3) 0.2137(3) 0.5317(3) 0.0286(8) Uani 1 1 d . . . . . H27 H 0.645730 0.159602 0.535256 0.034 Uiso 1 1 calc R U . . . C4 C 0.6731(3) 0.7717(3) 0.8279(3) 0.0272(8) Uani 1 1 d . . . . . C3 C 0.7554(3) 0.7298(3) 0.7541(3) 0.0295(8) Uani 1 1 d . . . . . H3 H 0.822696 0.772213 0.722185 0.035 Uiso 1 1 calc R U . . . C36 C 0.0058(3) 0.2370(3) 0.5008(3) 0.0325(9) Uani 1 1 d . . . . . C33 C 0.3529(3) 0.4863(3) 0.6791(3) 0.0280(8) Uani 1 1 d . . . . . H33 H 0.329428 0.526169 0.733823 0.034 Uiso 1 1 calc R U . . . C30 C 0.4168(3) 0.3709(3) 0.5185(3) 0.0285(8) Uani 1 1 d . . . . . C35 C -0.3030(4) 0.1949(4) 0.2163(3) 0.0425(11) Uani 1 1 d . . . . . C37 C -0.0197(3) 0.3129(3) 0.5673(3) 0.0327(9) Uani 1 1 d . . . . . C13 C 0.1949(3) 0.2409(3) 0.9585(3) 0.0269(8) Uani 1 1 d . . . . . C10 C 0.2242(3) 0.4585(3) 0.9893(3) 0.0291(8) Uani 1 1 d . . . . . H10 H 0.232976 0.531773 1.000834 0.035 Uiso 1 1 calc R U . . . C20 C 0.8310(3) 0.1572(3) 0.9544(3) 0.0283(8) Uani 1 1 d . . . . . H20 H 0.865185 0.143951 1.010139 0.034 Uiso 1 1 calc R U . . . C12 C 0.1056(3) 0.2938(3) 1.0202(3) 0.0307(8) Uani 1 1 d . . . . . H12 H 0.035700 0.255420 1.052465 0.037 Uiso 1 1 calc R U . . . C29 C 0.4565(3) 0.3074(3) 0.4415(3) 0.0315(8) Uani 1 1 d . . . . . H29 H 0.425683 0.318194 0.383897 0.038 Uiso 1 1 calc R U . . . N5 N -0.3751(4) 0.1280(4) 0.2304(3) 0.0546(11) Uani 1 1 d . . . . . C41 C 0.0927(3) 0.1645(3) 0.5129(3) 0.0301(8) Uani 1 1 d . . . . . C31 C 0.3324(3) 0.4540(3) 0.5180(3) 0.0312(8) Uani 1 1 d . . . . . H31 H 0.297760 0.470073 0.462885 0.037 Uiso 1 1 calc R U . . . C11 C 0.1203(3) 0.3998(3) 1.0332(3) 0.0331(9) Uani 1 1 d . . . . . H11 H 0.058897 0.435270 1.072909 0.040 Uiso 1 1 calc R U . . . C32 C 0.3020(3) 0.5100(3) 0.5968(3) 0.0319(9) Uani 1 1 d . . . . . H32 H 0.245809 0.565647 0.596642 0.038 Uiso 1 1 calc R U . . . C39 C 0.1271(3) 0.2471(3) 0.6470(3) 0.0333(9) Uani 1 1 d . . . . . C15 C 0.2791(3) 0.0890(3) 0.8779(3) 0.0325(9) Uani 1 1 d . . . . . H15 H 0.275822 0.015318 0.865467 0.039 Uiso 1 1 calc R U . . . C14 C 0.1894(3) 0.1312(3) 0.9403(3) 0.0307(8) Uani 1 1 d . . . . . H14 H 0.123224 0.086961 0.971577 0.037 Uiso 1 1 calc R U . . . C5 C 0.6004(4) 0.9272(3) 0.9045(3) 0.0356(9) Uani 1 1 d . . . . . H5A H 0.534396 0.931007 0.872500 0.053 Uiso 1 1 calc R U . . . H5B H 0.624360 1.001297 0.910545 0.053 Uiso 1 1 calc R U . . . H5C H 0.577818 0.885496 0.970309 0.053 Uiso 1 1 calc R U . . . C22 C 0.9977(4) -0.0312(3) 0.8016(3) 0.0361(9) Uani 1 1 d . . . . . H22A H 1.024002 0.012322 0.736963 0.054 Uiso 1 1 calc R U . . . H22B H 0.929159 -0.074697 0.801096 0.054 Uiso 1 1 calc R U . . . H22C H 1.059640 -0.080000 0.815532 0.054 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.02688(13) 0.03955(16) 0.03717(15) -0.00859(12) -0.00826(10) 0.00459(11) I3 0.03552(15) 0.03348(16) 0.0585(2) -0.00294(13) -0.01769(13) 0.00580(12) I2 0.0555(2) 0.04289(19) 0.04963(19) -0.01942(14) -0.00772(15) 0.00249(14) Fe1 0.0198(2) 0.0214(3) 0.0185(2) -0.00449(19) -0.00377(18) 0.00245(19) S1 0.0548(7) 0.0562(8) 0.0359(6) -0.0140(5) -0.0144(5) 0.0215(6) F3 0.0439(14) 0.0368(14) 0.0397(13) -0.0117(11) -0.0128(11) 0.0106(11) O3 0.0260(12) 0.0274(13) 0.0193(12) -0.0058(10) -0.0062(10) 0.0061(10) F1 0.0406(13) 0.0446(15) 0.0500(15) -0.0122(12) -0.0170(11) 0.0168(11) O1 0.0237(12) 0.0280(14) 0.0216(12) -0.0048(10) -0.0017(10) 0.0014(10) F2 0.0573(16) 0.0422(15) 0.0477(15) -0.0071(12) -0.0296(13) 0.0028(12) O4 0.0300(14) 0.0384(16) 0.0407(16) -0.0088(13) -0.0179(12) 0.0113(12) N3 0.0223(14) 0.0209(15) 0.0188(13) -0.0029(11) -0.0053(11) 0.0037(11) O2 0.0341(15) 0.0292(15) 0.0448(17) -0.0105(13) -0.0019(12) -0.0082(12) N1 0.0200(13) 0.0215(15) 0.0200(14) 0.0004(11) -0.0013(11) 0.0026(11) N4 0.0235(14) 0.0266(16) 0.0211(14) -0.0044(12) -0.0040(11) -0.0013(12) N2 0.0235(14) 0.0228(15) 0.0202(14) -0.0036(11) -0.0090(11) 0.0009(11) C25 0.0215(16) 0.0248(18) 0.0216(16) -0.0084(14) -0.0037(13) 0.0047(13) C34 0.0206(16) 0.0245(18) 0.0187(16) -0.0013(13) -0.0037(13) -0.0015(13) C7 0.0189(15) 0.0285(19) 0.0224(17) -0.0026(14) -0.0046(13) 0.0000(14) C18 0.0227(16) 0.0220(18) 0.0233(17) -0.0031(14) -0.0062(13) -0.0029(14) C24 0.0190(16) 0.0261(19) 0.0227(17) -0.0062(14) -0.0049(13) 0.0002(13) C26 0.0239(16) 0.0277(19) 0.0169(15) -0.0029(14) -0.0043(13) 0.0004(14) C17 0.0219(16) 0.0247(18) 0.0207(16) -0.0033(14) -0.0057(13) 0.0021(13) C9 0.0183(15) 0.0233(18) 0.0241(17) -0.0022(14) -0.0058(13) 0.0000(13) C23 0.0232(17) 0.0239(18) 0.0262(18) -0.0044(14) -0.0023(14) 0.0042(14) C6 0.0226(17) 0.0272(19) 0.0257(18) -0.0016(15) -0.0045(14) 0.0007(14) C19 0.0274(17) 0.030(2) 0.0207(17) -0.0058(14) -0.0103(14) 0.0022(15) C1 0.0202(16) 0.030(2) 0.0219(17) -0.0035(14) -0.0071(13) 0.0003(14) C28 0.043(2) 0.035(2) 0.0194(17) -0.0070(15) -0.0087(15) 0.0057(18) C21 0.0228(17) 0.0245(19) 0.0313(19) -0.0043(15) -0.0101(14) 0.0019(14) C38 0.038(2) 0.025(2) 0.037(2) -0.0093(17) -0.0041(17) 0.0006(16) C8 0.0224(16) 0.0211(17) 0.0214(16) -0.0042(13) -0.0020(13) 0.0014(13) C2 0.0205(16) 0.037(2) 0.0225(17) -0.0051(15) -0.0016(13) 0.0011(15) C16 0.0330(19) 0.0224(18) 0.0285(19) -0.0043(15) -0.0092(15) 0.0045(15) C40 0.0291(19) 0.030(2) 0.035(2) 0.0002(17) -0.0073(16) -0.0019(16) C27 0.0307(19) 0.031(2) 0.0266(18) -0.0090(15) -0.0092(15) 0.0063(16) C4 0.0258(18) 0.027(2) 0.0303(19) -0.0032(15) -0.0098(15) -0.0038(15) C3 0.0202(17) 0.034(2) 0.033(2) 0.0000(16) -0.0053(14) -0.0083(15) C36 0.0294(19) 0.033(2) 0.034(2) -0.0005(17) -0.0070(16) -0.0030(16) C33 0.0287(18) 0.028(2) 0.0281(19) -0.0021(15) -0.0087(15) 0.0052(15) C30 0.0291(18) 0.034(2) 0.0223(17) -0.0025(15) -0.0062(14) -0.0042(16) C35 0.059(3) 0.050(3) 0.024(2) -0.0156(19) -0.0171(19) 0.032(2) C37 0.0271(18) 0.030(2) 0.039(2) -0.0042(17) -0.0041(16) 0.0017(16) C13 0.0247(17) 0.032(2) 0.0236(17) -0.0011(15) -0.0058(14) -0.0041(15) C10 0.0240(17) 0.031(2) 0.0314(19) -0.0125(16) 0.0016(15) -0.0018(15) C20 0.0297(19) 0.032(2) 0.0275(18) -0.0024(15) -0.0149(15) -0.0022(15) C12 0.0209(17) 0.035(2) 0.034(2) -0.0064(17) 0.0011(15) -0.0069(15) C29 0.036(2) 0.038(2) 0.0223(18) -0.0026(16) -0.0109(15) -0.0003(17) N5 0.070(3) 0.054(3) 0.046(2) -0.021(2) -0.018(2) 0.019(2) C41 0.0311(19) 0.027(2) 0.032(2) -0.0027(16) -0.0063(16) 0.0034(16) C31 0.033(2) 0.033(2) 0.0293(19) 0.0011(16) -0.0130(16) 0.0039(16) C11 0.0247(18) 0.037(2) 0.036(2) -0.0112(18) 0.0003(15) 0.0020(16) C32 0.0279(19) 0.031(2) 0.036(2) 0.0007(17) -0.0075(16) 0.0024(16) C39 0.037(2) 0.029(2) 0.035(2) 0.0033(17) -0.0153(17) 0.0015(17) C15 0.039(2) 0.026(2) 0.034(2) -0.0043(16) -0.0105(17) -0.0087(16) C14 0.0295(19) 0.033(2) 0.0283(19) 0.0004(16) -0.0048(15) -0.0086(16) C5 0.041(2) 0.025(2) 0.041(2) -0.0072(17) -0.0079(18) -0.0032(17) C22 0.035(2) 0.037(2) 0.035(2) -0.0050(18) -0.0073(17) 0.0119(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 Fe1 N3 94.10(11) . . ? O3 Fe1 N1 89.15(11) . . ? O3 Fe1 N4 175.68(12) . . ? O3 Fe1 N2 89.79(11) . . ? O1 Fe1 O3 92.36(11) . . ? O1 Fe1 N3 88.13(11) . . ? O1 Fe1 N1 94.35(11) . . ? O1 Fe1 N4 90.40(11) . . ? O1 Fe1 N2 176.27(11) . . ? N3 Fe1 N4 82.66(12) . . ? N3 Fe1 N2 94.76(12) . . ? N1 Fe1 N3 175.83(12) . . ? N1 Fe1 N4 93.96(12) . . ? N1 Fe1 N2 82.62(12) . . ? N4 Fe1 N2 87.63(12) . . ? C18 O3 Fe1 126.0(2) . . ? C1 O1 Fe1 126.0(2) . . ? C21 O4 C22 116.3(3) . . ? C25 N3 Fe1 125.2(2) . . ? C25 N3 C26 120.6(3) . . ? C26 N3 Fe1 114.2(2) . . ? C4 O2 C5 116.9(3) . . ? C9 N1 Fe1 114.3(2) . . ? C8 N1 Fe1 125.5(2) . . ? C8 N1 C9 120.2(3) . . ? C34 N4 Fe1 112.8(2) . . ? C33 N4 Fe1 128.6(3) . . ? C33 N4 C34 118.6(3) . . ? C17 N2 Fe1 112.7(2) . . ? C16 N2 Fe1 128.8(2) . . ? C16 N2 C17 118.5(3) . . ? N3 C25 H25 117.3 . . ? N3 C25 C24 125.3(3) . . ? C24 C25 H25 117.3 . . ? N4 C34 C26 116.5(3) . . ? N4 C34 C30 122.7(3) . . ? C30 C34 C26 120.8(3) . . ? C6 C7 C1 120.8(3) . . ? C6 C7 C8 116.1(3) . . ? C8 C7 C1 123.0(3) . . ? O3 C18 C24 125.4(3) . . ? O3 C18 C19 117.8(3) . . ? C19 C18 C24 116.8(3) . . ? C25 C24 C18 122.8(3) . . ? C25 C24 C23 116.8(3) . . ? C18 C24 C23 120.3(3) . . ? N3 C26 C34 113.6(3) . . ? C27 C26 N3 127.3(3) . . ? C27 C26 C34 119.1(3) . . ? N2 C17 C9 116.6(3) . . ? N2 C17 C13 122.2(3) . . ? C13 C17 C9 121.2(3) . . ? C17 C9 N1 113.3(3) . . ? C10 C9 N1 127.5(3) . . ? C10 C9 C17 119.2(3) . . ? C24 C23 H23 119.6 . . ? C21 C23 C24 120.8(3) . . ? C21 C23 H23 119.6 . . ? C7 C6 H6 119.9 . . ? C4 C6 C7 120.3(3) . . ? C4 C6 H6 119.9 . . ? C18 C19 H19 119.2 . . ? C20 C19 C18 121.6(3) . . ? C20 C19 H19 119.2 . . ? O1 C1 C7 125.1(3) . . ? O1 C1 C2 118.0(3) . . ? C2 C1 C7 116.8(3) . . ? C27 C28 H28 119.3 . . ? C29 C28 H28 119.3 . . ? C29 C28 C27 121.3(4) . . ? O4 C21 C20 116.2(3) . . ? C23 C21 O4 124.9(3) . . ? C23 C21 C20 118.9(3) . . ? C37 C38 I2 122.0(3) . . ? C37 C38 C39 116.9(4) . . ? C39 C38 I2 121.1(3) . . ? N1 C8 C7 124.6(3) . . ? N1 C8 H8 117.7 . . ? C7 C8 H8 117.7 . . ? C1 C2 H2 119.3 . . ? C3 C2 C1 121.4(3) . . ? C3 C2 H2 119.3 . . ? N2 C16 H16 118.7 . . ? N2 C16 C15 122.5(4) . . ? C15 C16 H16 118.7 . . ? C41 C40 I3 122.7(3) . . ? C39 C40 I3 120.3(3) . . ? C39 C40 C41 116.9(4) . . ? C26 C27 C28 120.1(3) . . ? C26 C27 H27 120.0 . . ? C28 C27 H27 120.0 . . ? O2 C4 C6 124.3(3) . . ? O2 C4 C3 116.7(3) . . ? C6 C4 C3 119.0(4) . . ? C2 C3 C4 121.5(3) . . ? C2 C3 H3 119.2 . . ? C4 C3 H3 119.2 . . ? C37 C36 I1 120.7(3) . . ? C41 C36 I1 122.6(3) . . ? C41 C36 C37 116.7(4) . . ? N4 C33 H33 119.0 . . ? N4 C33 C32 121.9(4) . . ? C32 C33 H33 119.0 . . ? C34 C30 C31 116.7(3) . . ? C29 C30 C34 118.1(3) . . ? C29 C30 C31 125.2(4) . . ? N5 C35 S1 179.6(5) . . ? F1 C37 C38 118.4(4) . . ? F1 C37 C36 118.4(4) . . ? C38 C37 C36 123.3(4) . . ? C17 C13 C12 118.3(3) . . ? C17 C13 C14 117.1(3) . . ? C14 C13 C12 124.6(3) . . ? C9 C10 H10 120.2 . . ? C9 C10 C11 119.6(4) . . ? C11 C10 H10 120.2 . . ? C19 C20 C21 121.5(3) . . ? C19 C20 H20 119.3 . . ? C21 C20 H20 119.3 . . ? C13 C12 H12 120.1 . . ? C11 C12 C13 119.8(3) . . ? C11 C12 H12 120.1 . . ? C28 C29 C30 120.6(4) . . ? C28 C29 H29 119.7 . . ? C30 C29 H29 119.7 . . ? F3 C41 C40 118.6(3) . . ? F3 C41 C36 118.4(4) . . ? C36 C41 C40 123.0(4) . . ? C30 C31 H31 120.3 . . ? C32 C31 C30 119.5(4) . . ? C32 C31 H31 120.3 . . ? C10 C11 H11 119.1 . . ? C12 C11 C10 121.9(4) . . ? C12 C11 H11 119.1 . . ? C33 C32 H32 119.7 . . ? C31 C32 C33 120.6(4) . . ? C31 C32 H32 119.7 . . ? F2 C39 C38 118.8(4) . . ? F2 C39 C40 118.0(4) . . ? C38 C39 C40 123.2(4) . . ? C16 C15 H15 120.2 . . ? C14 C15 C16 119.7(4) . . ? C14 C15 H15 120.2 . . ? C13 C14 H14 120.0 . . ? C15 C14 C13 119.9(3) . . ? C15 C14 H14 120.0 . . ? O2 C5 H5A 109.5 . . ? O2 C5 H5B 109.5 . . ? O2 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? O4 C22 H22A 109.5 . . ? O4 C22 H22B 109.5 . . ? O4 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 C36 2.106(4) . ? I3 C40 2.084(4) . ? I2 C38 2.074(4) . ? Fe1 O3 1.877(2) . ? Fe1 O1 1.872(2) . ? Fe1 N3 1.943(3) . ? Fe1 N1 1.934(3) . ? Fe1 N4 1.987(3) . ? Fe1 N2 1.991(3) . ? S1 C35 1.652(6) . ? F3 C41 1.350(5) . ? O3 C18 1.317(4) . ? F1 C37 1.350(4) . ? O1 C1 1.315(4) . ? F2 C39 1.344(5) . ? O4 C21 1.376(4) . ? O4 C22 1.420(5) . ? N3 C25 1.296(4) . ? N3 C26 1.415(4) . ? O2 C4 1.373(5) . ? O2 C5 1.414(5) . ? N1 C9 1.424(4) . ? N1 C8 1.301(5) . ? N4 C34 1.373(4) . ? N4 C33 1.323(5) . ? N2 C17 1.375(4) . ? N2 C16 1.325(5) . ? C25 H25 0.9500 . ? C25 C24 1.417(5) . ? C34 C26 1.415(5) . ? C34 C30 1.415(5) . ? C7 C6 1.410(5) . ? C7 C1 1.424(5) . ? C7 C8 1.423(5) . ? C18 C24 1.419(5) . ? C18 C19 1.416(5) . ? C24 C23 1.420(5) . ? C26 C27 1.378(5) . ? C17 C9 1.412(5) . ? C17 C13 1.406(5) . ? C9 C10 1.374(5) . ? C23 H23 0.9500 . ? C23 C21 1.375(5) . ? C6 H6 0.9500 . ? C6 C4 1.382(5) . ? C19 H19 0.9500 . ? C19 C20 1.368(5) . ? C1 C2 1.417(5) . ? C28 H28 0.9500 . ? C28 C27 1.401(5) . ? C28 C29 1.366(5) . ? C21 C20 1.395(5) . ? C38 C37 1.377(6) . ? C38 C39 1.379(6) . ? C8 H8 0.9500 . ? C2 H2 0.9500 . ? C2 C3 1.366(6) . ? C16 H16 0.9500 . ? C16 C15 1.400(5) . ? C40 C41 1.386(5) . ? C40 C39 1.381(6) . ? C27 H27 0.9500 . ? C4 C3 1.400(5) . ? C3 H3 0.9500 . ? C36 C37 1.387(6) . ? C36 C41 1.379(5) . ? C33 H33 0.9500 . ? C33 C32 1.411(5) . ? C30 C29 1.405(5) . ? C30 C31 1.423(5) . ? C35 N5 1.163(7) . ? C13 C12 1.417(5) . ? C13 C14 1.415(6) . ? C10 H10 0.9500 . ? C10 C11 1.410(5) . ? C20 H20 0.9500 . ? C12 H12 0.9500 . ? C12 C11 1.363(6) . ? C29 H29 0.9500 . ? C31 H31 0.9500 . ? C31 C32 1.352(6) . ? C11 H11 0.9500 . ? C32 H32 0.9500 . ? C15 H15 0.9500 . ? C15 C14 1.360(6) . ? C14 H14 0.9500 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag I1 C36 C37 F1 2.6(5) . . . . ? I1 C36 C37 C38 -177.2(3) . . . . ? I1 C36 C41 F3 -2.5(5) . . . . ? I1 C36 C41 C40 175.4(3) . . . . ? I3 C40 C41 F3 -4.5(5) . . . . ? I3 C40 C41 C36 177.6(3) . . . . ? I3 C40 C39 F2 4.3(5) . . . . ? I3 C40 C39 C38 -175.4(3) . . . . ? I2 C38 C37 F1 3.8(5) . . . . ? I2 C38 C37 C36 -176.3(3) . . . . ? I2 C38 C39 F2 -3.9(5) . . . . ? I2 C38 C39 C40 175.9(3) . . . . ? Fe1 O3 C18 C24 -7.9(5) . . . . ? Fe1 O3 C18 C19 173.9(2) . . . . ? Fe1 O1 C1 C7 -10.2(5) . . . . ? Fe1 O1 C1 C2 173.0(2) . . . . ? Fe1 N3 C25 C24 6.7(5) . . . . ? Fe1 N3 C26 C34 5.0(4) . . . . ? Fe1 N3 C26 C27 -174.6(3) . . . . ? Fe1 N1 C9 C17 7.3(4) . . . . ? Fe1 N1 C9 C10 -172.2(3) . . . . ? Fe1 N1 C8 C7 7.9(5) . . . . ? Fe1 N4 C34 C26 -1.8(4) . . . . ? Fe1 N4 C34 C30 178.5(3) . . . . ? Fe1 N4 C33 C32 179.9(3) . . . . ? Fe1 N2 C17 C9 -2.5(4) . . . . ? Fe1 N2 C17 C13 177.2(3) . . . . ? Fe1 N2 C16 C15 -179.4(3) . . . . ? O3 Fe1 O1 C1 -76.7(3) . . . . ? O3 C18 C24 C25 -1.0(6) . . . . ? O3 C18 C24 C23 -176.2(3) . . . . ? O3 C18 C19 C20 177.6(3) . . . . ? O1 Fe1 O3 C18 -76.5(3) . . . . ? O1 C1 C2 C3 173.9(3) . . . . ? O4 C21 C20 C19 -177.7(3) . . . . ? N3 Fe1 O3 C18 11.8(3) . . . . ? N3 Fe1 O1 C1 -170.7(3) . . . . ? N3 C25 C24 C18 1.5(6) . . . . ? N3 C25 C24 C23 176.9(3) . . . . ? N3 C26 C27 C28 -178.3(4) . . . . ? O2 C4 C3 C2 -177.5(3) . . . . ? N1 Fe1 O3 C18 -170.8(3) . . . . ? N1 Fe1 O1 C1 12.7(3) . . . . ? N1 C9 C10 C11 -179.5(4) . . . . ? N4 Fe1 O1 C1 106.7(3) . . . . ? N4 C34 C26 N3 -2.0(5) . . . . ? N4 C34 C26 C27 177.7(3) . . . . ? N4 C34 C30 C29 -179.2(3) . . . . ? N4 C34 C30 C31 2.3(5) . . . . ? N4 C33 C32 C31 0.7(6) . . . . ? N2 Fe1 O3 C18 106.6(3) . . . . ? N2 C17 C9 N1 -3.0(4) . . . . ? N2 C17 C9 C10 176.5(3) . . . . ? N2 C17 C13 C12 -177.1(3) . . . . ? N2 C17 C13 C14 3.4(5) . . . . ? N2 C16 C15 C14 0.8(6) . . . . ? C25 N3 C26 C34 -171.5(3) . . . . ? C25 N3 C26 C27 8.8(6) . . . . ? C25 C24 C23 C21 -176.7(3) . . . . ? C34 N4 C33 C32 0.3(5) . . . . ? C34 C26 C27 C28 2.0(6) . . . . ? C34 C30 C29 C28 0.9(6) . . . . ? C34 C30 C31 C32 -1.3(6) . . . . ? C7 C6 C4 O2 176.7(3) . . . . ? C7 C6 C4 C3 -3.8(5) . . . . ? C7 C1 C2 C3 -3.1(5) . . . . ? C18 C24 C23 C21 -1.1(5) . . . . ? C18 C19 C20 C21 -1.3(6) . . . . ? C24 C18 C19 C20 -0.7(5) . . . . ? C24 C23 C21 O4 178.9(3) . . . . ? C24 C23 C21 C20 -0.9(6) . . . . ? C26 N3 C25 C24 -177.2(3) . . . . ? C26 C34 C30 C29 1.1(5) . . . . ? C26 C34 C30 C31 -177.4(3) . . . . ? C17 N2 C16 C15 0.5(5) . . . . ? C17 C9 C10 C11 1.1(6) . . . . ? C17 C13 C12 C11 0.0(6) . . . . ? C17 C13 C14 C15 -2.0(5) . . . . ? C9 N1 C8 C7 -174.9(3) . . . . ? C9 C17 C13 C12 2.7(5) . . . . ? C9 C17 C13 C14 -176.9(3) . . . . ? C9 C10 C11 C12 1.6(6) . . . . ? C23 C21 C20 C19 2.1(6) . . . . ? C6 C7 C1 O1 -174.5(3) . . . . ? C6 C7 C1 C2 2.3(5) . . . . ? C6 C7 C8 N1 175.7(3) . . . . ? C6 C4 C3 C2 3.0(6) . . . . ? C19 C18 C24 C25 177.2(3) . . . . ? C19 C18 C24 C23 1.9(5) . . . . ? C1 C7 C6 C4 1.1(5) . . . . ? C1 C7 C8 N1 -1.1(6) . . . . ? C1 C2 C3 C4 0.5(6) . . . . ? C8 N1 C9 C17 -170.2(3) . . . . ? C8 N1 C9 C10 10.3(5) . . . . ? C8 C7 C6 C4 -175.8(3) . . . . ? C8 C7 C1 O1 2.2(6) . . . . ? C8 C7 C1 C2 178.9(3) . . . . ? C16 N2 C17 C9 177.6(3) . . . . ? C16 N2 C17 C13 -2.7(5) . . . . ? C16 C15 C14 C13 0.0(6) . . . . ? C27 C28 C29 C30 -1.6(6) . . . . ? C33 N4 C34 C26 177.9(3) . . . . ? C33 N4 C34 C30 -1.8(5) . . . . ? C30 C34 C26 N3 177.7(3) . . . . ? C30 C34 C26 C27 -2.6(5) . . . . ? C30 C31 C32 C33 -0.2(6) . . . . ? C37 C38 C39 F2 179.0(4) . . . . ? C37 C38 C39 C40 -1.2(6) . . . . ? C37 C36 C41 F3 178.9(3) . . . . ? C37 C36 C41 C40 -3.2(6) . . . . ? C13 C17 C9 N1 177.3(3) . . . . ? C13 C17 C9 C10 -3.2(5) . . . . ? C13 C12 C11 C10 -2.1(6) . . . . ? C12 C13 C14 C15 178.5(4) . . . . ? C29 C28 C27 C26 0.1(6) . . . . ? C29 C30 C31 C32 -179.6(4) . . . . ? C41 C40 C39 F2 179.3(3) . . . . ? C41 C40 C39 C38 -0.5(6) . . . . ? C41 C36 C37 F1 -178.8(3) . . . . ? C41 C36 C37 C38 1.4(6) . . . . ? C31 C30 C29 C28 179.3(4) . . . . ? C39 C38 C37 F1 -179.1(4) . . . . ? C39 C38 C37 C36 0.7(6) . . . . ? C39 C40 C41 F3 -179.3(3) . . . . ? C39 C40 C41 C36 2.8(6) . . . . ? C14 C13 C12 C11 179.5(4) . . . . ? C5 O2 C4 C6 -14.1(5) . . . . ? C5 O2 C4 C3 166.4(4) . . . . ? C22 O4 C21 C23 -15.1(5) . . . . ? C22 O4 C21 C20 164.7(3) . . . . ?