#------------------------------------------------------------------------------ #$Date: 2020-11-22 01:30:52 +0200 (Sun, 22 Nov 2020) $ #$Revision: 259219 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/00/38/4003825.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4003825 loop_ _publ_author_name 'Zuluaga, Andr\'es Reyes' 'Brock, Aidan J.' 'Pfrunder, Michael C.' 'Phonsri, Wasinee' 'Murray, Keith S.' 'Harding, Phimphaka' 'Micallef, Aaron S.' 'Mullen, Kathleen M.' 'Clegg, Jack K.' 'Harding, David J.' 'McMurtrie, John C.' _publ_section_title ; Three-Way Switchable Single-Crystal-to-Single-Crystal Solvatomorphic Spin Crossover in a Molecular Cocrystal ; _journal_name_full 'Chemistry of Materials' _journal_paper_doi 10.1021/acs.chemmater.0c03396 _journal_year 2020 _chemical_formula_moiety 'C6 F3 I3, C34 H26 Fe N4 O4, C N S' _chemical_formula_sum 'C41 H26 F3 Fe I3 N5 O4 S' _chemical_formula_weight 1178.28 _chemical_name_systematic 'bis(4-methoxy-2-(((quinolin-8-yl)imino)methyl)phenolato)-iron(iii) thiocyanate (2,4,5-tetrafluoro-1,3,5-triiodobenzene)' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2020-04-03 _audit_creation_method ; Olex2 1.3 (compiled 2020.02.04 svn.rd84adfe8 for OlexSys, GUI svn.r6032) ; _cell_angle_alpha 82.790(2) _cell_angle_beta 77.247(2) _cell_angle_gamma 89.251(2) _cell_formula_units_Z 2 _cell_length_a 11.8326(2) _cell_length_b 12.3511(3) _cell_length_c 13.9910(3) _cell_measurement_reflns_used 23506 _cell_measurement_temperature 189.99(14) _cell_measurement_theta_max 31.9060 _cell_measurement_theta_min 2.5260 _cell_volume 1978.29(7) _computing_cell_refinement 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.61a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 189.99(14) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 5.8140 _diffrn_detector_type 'Pilatus 300K' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -17.00 34.00 0.50 1.00 -- 7.84 93.00-131.00 102 2 \w -13.00 38.00 0.50 1.00 -- 7.84 -93.00 117.00 102 3 \w -43.00 -16.00 0.50 1.00 -- -9.41 93.00-131.00 54 4 \w -42.00 -16.00 0.50 1.00 -- 7.84 -57.00 -30.00 52 5 \w 0.00 37.00 0.50 1.00 -- 7.84 -99.00 -90.00 74 6 \w -59.00 22.00 0.50 1.00 -- 7.84 -57.00 60.00 162 7 \w -18.00 75.00 0.50 1.00 -- 7.84 77.00 0.00 186 8 \w 5.00 36.00 0.50 1.00 -- 7.84 -99.00 0.00 62 9 \w -7.00 79.00 0.50 1.00 -- 7.84 57.00 60.00 172 10 \w 3.00 40.00 0.50 1.00 -- 7.84 -99.00-180.00 74 11 \w -61.00 -36.00 0.50 1.00 -- 7.84 153.00-168.43 50 12 \w -26.00 68.00 0.50 1.00 -- -9.41 37.00 150.00 188 13 \w -30.00 49.00 0.50 1.00 -- -9.41 77.00 150.00 158 14 \w 6.00 31.00 0.50 1.00 -- -9.41 93.00-131.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, Pilatus 300K' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0270620000 _diffrn_orient_matrix_UB_12 -0.0258777000 _diffrn_orient_matrix_UB_13 -0.0414654000 _diffrn_orient_matrix_UB_21 -0.0202501000 _diffrn_orient_matrix_UB_22 -0.0514813000 _diffrn_orient_matrix_UB_23 0.0262483000 _diffrn_orient_matrix_UB_31 -0.0513407000 _diffrn_orient_matrix_UB_32 0.0056172000 _diffrn_orient_matrix_UB_33 -0.0183540000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0733 _diffrn_reflns_av_unetI/netI 0.0489 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 48961 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.281 _diffrn_reflns_theta_min 2.051 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 2.839 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.11783 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.61a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'dark brown' _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 1.978 _exptl_crystal_description block _exptl_crystal_F_000 1134 _exptl_crystal_preparation 'Combined equal ratios of starting materials' _exptl_crystal_recrystallization_method 'Slow evaporation of the solvent' _exptl_crystal_size_max 2 _exptl_crystal_size_mid 1 _exptl_crystal_size_min 1 _refine_diff_density_max 1.078 _refine_diff_density_min -1.482 _refine_diff_density_rms 0.122 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.086 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 525 _refine_ls_number_reflns 9821 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.086 _refine_ls_R_factor_all 0.0542 _refine_ls_R_factor_gt 0.0395 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0415P)^2^+0.6981P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0940 _refine_ls_wR_factor_ref 0.1007 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7585 _reflns_number_total 9821 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cm0c03396_si_006.cif _cod_data_source_block sjcm19ar19a_12_190_00 _cod_database_code 4003825 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C40 H40 N5 O2 Fe S I3 F3' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.164 _shelx_estimated_absorpt_t_min 0.070 _reflns_odcompleteness_completeness 84.29 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 33.32 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C25(H25), C23(H23), C8(H8), C19(H19), C6(H6), C16(H16), C20(H20), C27(H27), C2(H2), C33(H33), C12(H12), C28(H28), C32(H32), C10(H10), C3(H3), C11(H11), C29(H29), C15(H15), C14(H14), C31(H31) 2.b Idealised Me refined as rotating group: C5(H5a,H5b,H5c), C22(H22a,H22b,H22c) ; _shelx_res_file ; TITL sjcm19ar19a_12_190_00_a.res in P-1 sjcm19ar19a_12_190_00.res created by SHELXL-2018/3 at 15:52:39 on 30-Mar-2020 REM Old TITL Sjcm19ar19a_12_190_00 in P-1 REM SHELXT solution in P-1: R1 0.185, Rweak 0.012, Alpha 0.043 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C41 N7 O4 F S Fe2 I2 CELL 0.71073 11.8326 12.3511 13.991 82.79 77.247 89.251 ZERR 2 0.0002 0.0003 0.0003 0.002 0.002 0.002 LATT 1 SFAC C H F Fe I N O S UNIT 82 52 6 2 6 10 8 2 L.S. 15 PLAN 5 SIZE 2 1 1 TEMP -83 CONF HTAB BOND list 4 MORE -1 BOND $H fmap 2 acta SHEL 50 0.75 REM REM REM WGHT 0.041500 0.698100 FVAR 0.18380 I1 5 -0.082841 0.237507 0.385670 11.00000 0.02814 0.04144 = 0.03880 -0.00868 -0.00876 0.00477 I3 5 0.283724 0.055148 0.604936 11.00000 0.03718 0.03482 = 0.06127 -0.00267 -0.01884 0.00619 I2 5 -0.008575 0.428192 0.744405 11.00000 0.05814 0.04466 = 0.05202 -0.02012 -0.00819 0.00272 FE04 4 0.514881 0.364305 0.789437 11.00000 0.02083 0.02179 = 0.01932 -0.00448 -0.00416 0.00297 S1 8 -0.201185 0.291098 0.196435 11.00000 0.05678 0.05788 = 0.03706 -0.01407 -0.01504 0.02224 F3 3 0.118663 0.088313 0.450435 11.00000 0.04502 0.03958 = 0.04002 -0.01270 -0.01076 0.01034 O1 7 0.628705 0.471930 0.735445 11.00000 0.02182 0.02997 = 0.02158 -0.00549 -0.00275 0.00178 F1 3 -0.105835 0.383970 0.558828 11.00000 0.04240 0.04623 = 0.05360 -0.01380 -0.01762 0.01793 O3 7 0.591950 0.309984 0.888458 11.00000 0.02618 0.03244 = 0.02000 -0.00701 -0.00640 0.00596 F2 3 0.186972 0.251664 0.717764 11.00000 0.05970 0.04327 = 0.05171 -0.00716 -0.03105 0.00236 O4 7 0.968648 0.039182 0.875780 11.00000 0.03217 0.03845 = 0.04416 -0.00809 -0.01894 0.01077 N3 6 0.597026 0.271916 0.695022 11.00000 0.02313 0.02329 = 0.01817 -0.00279 -0.00396 0.00190 O2 7 0.693470 0.874818 0.846896 11.00000 0.03456 0.02964 = 0.04675 -0.00853 -0.00140 -0.00966 N4 6 0.432628 0.410242 0.682159 11.00000 0.02195 0.02603 = 0.02499 -0.00294 -0.00634 -0.00001 N2 6 0.386283 0.257688 0.847624 11.00000 0.02472 0.02334 = 0.02152 -0.00545 -0.00689 0.00075 N1 6 0.422820 0.454185 0.880311 11.00000 0.02192 0.02391 = 0.02194 -0.00268 -0.00230 0.00155 C25 1 0.686694 0.213843 0.705197 11.00000 0.02249 0.02428 = 0.02096 -0.00821 -0.00393 0.00596 AFIX 43 H25 2 0.723711 0.177119 0.651227 11.00000 -1.20000 AFIX 0 C23 1 0.829637 0.130332 0.789022 11.00000 0.02214 0.02726 = 0.02728 -0.00627 -0.00371 0.00447 AFIX 43 H23 2 0.861257 0.098134 0.730894 11.00000 -1.20000 AFIX 0 C18 1 0.684687 0.248033 0.877385 11.00000 0.02252 0.02524 = 0.02026 -0.00306 -0.00721 -0.00240 C34 1 0.466313 0.353622 0.602843 11.00000 0.02018 0.02172 = 0.02223 -0.00105 -0.00418 -0.00132 C7 1 0.561109 0.603958 0.849573 11.00000 0.02098 0.02516 = 0.02350 -0.00170 -0.00577 0.00121 C24 1 0.733640 0.200990 0.790608 11.00000 0.02024 0.02567 = 0.02407 -0.00390 -0.00563 0.00165 C8 1 0.456217 0.547471 0.899943 11.00000 0.02459 0.02246 = 0.02010 -0.00380 -0.00102 0.00117 AFIX 43 H8 2 0.407218 0.580229 0.951491 11.00000 -1.20000 AFIX 0 C19 1 0.737499 0.223610 0.959125 11.00000 0.03175 0.02981 = 0.02228 -0.00554 -0.01133 0.00197 AFIX 43 H19 2 0.707167 0.254434 1.018253 11.00000 -1.20000 AFIX 0 C9 1 0.312788 0.409111 0.929881 11.00000 0.02107 0.02555 = 0.02331 -0.00423 -0.00331 -0.00017 C17 1 0.297353 0.300488 0.911806 11.00000 0.02607 0.02465 = 0.02104 -0.00327 -0.00848 0.00408 C26 1 0.554180 0.275964 0.607722 11.00000 0.02454 0.03017 = 0.01954 -0.00422 -0.00506 0.00042 C21 1 0.877240 0.107944 0.869886 11.00000 0.02161 0.02741 = 0.03168 -0.00353 -0.00931 0.00164 C6 1 0.577946 0.707661 0.877305 11.00000 0.02593 0.02818 = 0.02735 -0.00308 -0.00521 0.00067 AFIX 43 H6 2 0.523758 0.733428 0.930094 11.00000 -1.20000 AFIX 0 C16 1 0.376523 0.155023 0.831617 11.00000 0.03291 0.02582 = 0.02578 -0.00597 -0.00625 0.00100 AFIX 43 H16 2 0.437779 0.124922 0.787154 11.00000 -1.20000 AFIX 0 C1 1 0.641671 0.563345 0.771670 11.00000 0.02103 0.02784 = 0.02379 -0.00203 -0.00811 0.00165 C20 1 0.830689 0.156988 0.954787 11.00000 0.03034 0.03590 = 0.02391 -0.00095 -0.01451 -0.00194 AFIX 43 H20 2 0.864831 0.143493 1.010469 11.00000 -1.20000 AFIX 0 C13 1 0.195075 0.240551 0.958429 11.00000 0.02662 0.03013 = 0.02555 -0.00212 -0.00823 -0.00350 C27 1 0.588916 0.213406 0.531733 11.00000 0.03500 0.03433 = 0.02622 -0.00785 -0.01036 0.00576 AFIX 43 H27 2 0.646321 0.159464 0.535285 11.00000 -1.20000 AFIX 0 C4 1 0.672527 0.771501 0.828158 11.00000 0.02639 0.02829 = 0.03363 -0.00362 -0.00948 -0.00388 C2 1 0.741012 0.629296 0.726616 11.00000 0.02074 0.03959 = 0.02391 -0.00428 -0.00129 -0.00061 AFIX 43 H2 2 0.798676 0.603412 0.676273 11.00000 -1.20000 AFIX 0 C33 1 0.352632 0.485849 0.678902 11.00000 0.02864 0.02694 = 0.02927 -0.00188 -0.00585 0.00321 AFIX 43 H33 2 0.328642 0.525441 0.733729 11.00000 -1.20000 AFIX 0 C12 1 0.106137 0.294023 1.020185 11.00000 0.02242 0.03626 = 0.03362 -0.00842 -0.00032 -0.00397 AFIX 43 H12 2 0.036096 0.256039 1.052439 11.00000 -1.20000 AFIX 0 C30 1 0.417023 0.371412 0.518358 11.00000 0.02805 0.03290 = 0.02313 -0.00035 -0.00656 -0.00194 C28 1 0.538829 0.230019 0.449097 11.00000 0.04368 0.03867 = 0.02222 -0.01086 -0.00825 0.00386 AFIX 43 H28 2 0.562719 0.186409 0.397117 11.00000 -1.20000 AFIX 0 C36 1 0.005081 0.237478 0.501007 11.00000 0.02812 0.03489 = 0.03338 -0.00311 -0.00664 -0.00127 C32 1 0.301959 0.509339 0.596356 11.00000 0.02818 0.03242 = 0.03549 0.00114 -0.00946 0.00644 AFIX 43 H32 2 0.245897 0.565062 0.595943 11.00000 -1.20000 AFIX 0 C41 1 0.093079 0.164952 0.512311 11.00000 0.03367 0.02894 = 0.03364 -0.00345 -0.00475 0.00002 C38 1 0.038765 0.319441 0.641411 11.00000 0.03861 0.02762 = 0.03694 -0.00879 -0.00651 -0.00163 C10 1 0.224222 0.458474 0.989264 11.00000 0.02674 0.02911 = 0.03257 -0.00870 -0.00090 -0.00004 AFIX 43 H10 2 0.232556 0.531902 1.000574 11.00000 -1.20000 AFIX 0 N5 6 -0.374060 0.127820 0.230489 11.00000 0.07192 0.05915 = 0.04616 -0.02300 -0.01771 0.02300 C3 1 0.755037 0.729556 0.754542 11.00000 0.02273 0.03644 = 0.03311 -0.00284 -0.00479 -0.00811 AFIX 43 H3 2 0.822552 0.771863 0.723162 11.00000 -1.20000 AFIX 0 C37 1 -0.019492 0.313149 0.567141 11.00000 0.02845 0.02897 = 0.04119 -0.00193 -0.00579 0.00209 C11 1 0.121311 0.399578 1.033102 11.00000 0.02617 0.03727 = 0.03379 -0.00907 0.00115 0.00016 AFIX 43 H11 2 0.060102 0.434795 1.073230 11.00000 -1.20000 AFIX 0 C29 1 0.456844 0.307092 0.441579 11.00000 0.03776 0.03807 = 0.02352 -0.00233 -0.01152 -0.00046 AFIX 43 H29 2 0.426101 0.317657 0.383901 11.00000 -1.20000 AFIX 0 C35 1 -0.301859 0.195326 0.215841 11.00000 0.06393 0.05127 = 0.02636 -0.01847 -0.01861 0.03498 C15 1 0.279645 0.089339 0.877594 11.00000 0.03996 0.02370 = 0.03527 -0.00351 -0.01151 -0.00748 AFIX 43 H15 2 0.276775 0.015601 0.865349 11.00000 -1.20000 AFIX 0 C14 1 0.189444 0.131030 0.939895 11.00000 0.03221 0.03013 = 0.03425 -0.00118 -0.01007 -0.00942 AFIX 43 H14 2 0.123120 0.086845 0.970737 11.00000 -1.20000 AFIX 0 C40 1 0.156878 0.167746 0.584160 11.00000 0.02985 0.02961 = 0.03951 0.00040 -0.00926 0.00165 C31 1 0.332612 0.453194 0.518065 11.00000 0.03434 0.03785 = 0.02843 -0.00016 -0.01544 0.00280 AFIX 43 H31 2 0.297573 0.468624 0.463058 11.00000 -1.20000 AFIX 0 C39 1 0.127290 0.247391 0.646717 11.00000 0.03662 0.03382 = 0.03572 0.00114 -0.01349 0.00118 C5 1 0.600175 0.926355 0.904760 11.00000 0.04360 0.02546 = 0.04300 -0.00733 -0.00763 -0.00472 AFIX 137 H5A 2 0.532837 0.926714 0.874624 11.00000 -1.50000 H5B 2 0.622581 1.001610 0.908289 11.00000 -1.50000 H5C 2 0.580385 0.886495 0.971509 11.00000 -1.50000 AFIX 0 C22 1 0.997458 -0.031401 0.801974 11.00000 0.03380 0.03972 = 0.03854 -0.00715 -0.00876 0.01385 AFIX 137 H22A 2 1.022414 0.012007 0.737180 11.00000 -1.50000 H22B 2 0.929436 -0.075972 0.802274 11.00000 -1.50000 H22C 2 1.060461 -0.079084 0.815391 11.00000 -1.50000 AFIX 0 HKLF 4 REM sjcm19ar19a_12_190_00_a.res in P-1 REM wR2 = 0.1007, GooF = S = 1.086, Restrained GooF = 1.086 for all data REM R1 = 0.0395 for 7585 Fo > 4sig(Fo) and 0.0542 for all 9821 data REM 525 parameters refined using 0 restraints END WGHT 0.0415 0.6981 REM Instructions for potential hydrogen bonds EQIV $1 x+1, y, z+1 HTAB C19 S1_$1 EQIV $2 -x+1, -y+1, -z+2 HTAB C6 O3_$2 HTAB C16 N3 EQIV $3 -x, -y+1, -z+1 HTAB C33 S1_$3 HTAB C33 N1 HTAB C32 I1_$3 EQIV $4 -x+1, -y+1, -z+1 HTAB C3 I1_$4 EQIV $5 -x, -y, -z+1 HTAB C15 N5_$5 EQIV $6 x+1, y, z HTAB C22 I3_$6 REM Highest difference peak 1.078, deepest hole -1.482, 1-sigma level 0.122 Q1 1 0.3167 0.0660 0.5442 11.00000 0.05 1.08 Q2 1 -0.0589 0.3412 0.3406 11.00000 0.05 0.90 Q3 1 -0.0164 0.2570 0.3237 11.00000 0.05 0.68 Q4 1 0.2593 0.0413 0.5573 11.00000 0.05 0.67 Q5 1 0.0381 0.4507 0.6876 11.00000 0.05 0.67 ; _shelx_res_checksum 80017 _shelx_hkl_file ; 0 0 2 271.56 14.67 0 0 -2 276.84 14.65 0 0 -3 47.37 3.51 0 0 3 43.98 3.45 0 0 -4 60.84 4.27 0 0 -4 66.37 4.81 0 0 4 66.45 4.80 0 0 4 61.61 4.62 0 0 -5 661.46 35.54 0 0 5 691.87 36.21 0 0 5 687.37 36.37 0 0 -5 690.63 36.39 0 0 -6 677.44 37.03 0 0 6 753.12 38.03 0 0 6 722.19 38.08 0 0 -6 665.41 37.86 0 0 6 721.51 38.04 0 0 7 0.79 0.98 0 0 7 -0.27 1.00 0 0 -7 1.86 1.15 0 0 -7 1.29 0.82 0 0 7 1.03 1.07 0 0 -8 449.85 21.69 0 0 -8 426.99 21.49 0 0 -8 379.05 22.11 0 0 -8 363.10 23.54 0 0 8 324.26 22.58 0 0 -8 388.93 23.16 0 0 8 389.71 23.23 0 0 8 364.62 23.16 0 0 -9 139.75 8.19 0 0 9 108.49 9.68 0 0 -9 122.15 10.52 0 0 -9 140.78 10.27 0 0 9 142.52 10.47 0 0 9 139.65 10.50 0 0 10 102.38 7.92 0 0 10 79.04 8.09 0 0 -10 97.82 8.94 0 0 -10 91.41 8.18 0 0 10 100.81 8.59 0 0 -11 11.21 1.84 0 0 11 11.67 3.22 0 0 11 22.48 3.49 0 0 -11 15.01 1.90 0 0 11 25.08 4.31 0 0 -11 19.00 2.98 0 0 -11 13.89 3.56 0 0 11 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117.15 0 4 4 759.82 40.26 0 -4 -4 731.53 40.48 0 -4 -4 756.97 40.74 0 4 4 767.39 39.09 0 -4 -5 339.30 19.88 0 4 5 342.76 19.49 0 -4 -5 338.48 19.72 0 4 5 345.20 19.64 0 4 5 325.39 17.68 0 4 6 162.76 11.35 0 -4 -6 164.34 11.55 0 4 6 169.45 11.49 0 4 6 169.98 11.20 0 4 7 88.79 7.28 0 -4 -7 73.81 6.95 0 4 7 83.59 7.23 0 4 7 73.77 6.59 0 4 8 231.54 15.76 0 -4 -8 239.07 15.93 0 4 8 246.95 16.16 0 4 8 227.23 15.31 0 -4 -9 525.57 30.73 0 4 9 524.31 30.43 0 4 9 532.52 30.89 0 4 9 479.99 29.74 0 4 10 73.71 7.67 0 4 10 87.29 8.30 0 -4 -10 94.48 8.73 0 4 11 218.07 15.72 0 4 11 224.04 15.95 0 -4 -11 198.38 15.81 0 4 12 159.08 13.44 0 4 12 169.99 13.82 0 -4 -12 188.41 14.71 0 4 13 0.59 1.84 0 4 13 1.15 1.91 0 -4 -13 5.82 2.81 0 4 14 7.70 3.34 0 4 14 7.48 3.39 0 4 15 1.35 2.58 0 4 15 3.54 2.81 0 4 15 -0.76 3.56 0 4 15 1.44 2.76 0 4 16 14.62 4.80 0 4 16 14.31 4.47 0 4 16 6.18 3.64 0 4 16 15.88 4.82 0 4 16 13.92 4.44 0 4 17 28.44 6.73 0 4 17 38.19 7.35 0 4 18 7.93 3.96 0 4 18 3.60 3.54 0 4 18 10.42 4.50 0 4 19 2.56 2.91 0 -4 -19 0.42 1.68 0 4 19 -1.01 3.24 0 4 19 0.92 3.14 0 -5 18 2.73 3.07 0 -5 18 1.90 2.63 0 -5 17 8.13 2.65 0 5 -17 6.50 4.40 0 -5 17 8.44 4.18 0 -5 17 11.34 3.94 0 5 -16 0.52 1.99 0 -5 16 -1.10 1.85 0 5 -16 -0.99 3.74 0 -5 16 3.11 3.48 0 -5 16 0.56 2.28 0 5 -15 -0.50 3.28 0 -5 15 1.57 2.29 0 -5 15 1.36 1.48 0 5 -15 -0.47 2.29 0 5 -15 1.82 2.81 0 -5 15 2.16 2.72 0 5 -14 4.33 2.59 0 5 -14 5.05 2.58 0 -5 14 6.85 2.19 0 -5 14 5.32 2.72 0 5 -14 4.83 1.48 0 5 -14 5.81 3.98 0 -5 14 6.67 3.44 0 5 -13 7.86 3.02 0 -5 13 9.56 2.38 0 5 -13 8.47 2.89 0 -5 13 8.03 2.89 0 5 -13 6.85 1.71 0 5 -13 5.10 2.94 0 5 -13 12.85 4.26 0 -5 13 7.36 3.46 0 -5 12 -0.81 1.79 0 5 -12 0.78 1.04 0 -5 12 1.00 1.49 0 5 -12 1.33 2.25 0 5 -12 0.69 2.52 0 5 -12 -0.93 3.01 0 5 -11 18.14 2.54 0 -5 11 15.43 2.43 0 5 -11 16.51 4.26 0 5 -11 16.71 4.09 0 5 -10 4.71 1.50 0 -5 10 4.58 1.59 0 5 -10 8.31 3.08 0 -5 10 6.76 2.46 0 -5 9 127.20 9.58 0 -5 9 132.06 8.40 0 5 -9 133.89 11.67 0 5 -9 134.79 8.76 0 -5 9 139.55 10.74 0 5 -9 122.09 11.44 0 5 -8 53.34 8.10 0 5 -8 72.97 6.93 0 -5 8 79.70 6.31 0 -5 8 70.24 4.99 0 5 -8 50.93 7.66 0 -5 8 75.23 6.19 0 5 -8 78.80 8.12 0 -5 8 73.28 6.81 0 5 -7 10.60 2.45 0 -5 7 11.91 2.11 0 5 -7 17.56 5.86 0 5 -7 3.90 2.42 0 5 -6 122.40 7.76 0 -5 6 122.60 8.42 0 -5 6 120.79 7.90 0 5 -6 112.74 8.65 0 5 -6 141.40 10.94 0 -5 5 2.38 1.33 0 5 -5 0.18 0.72 0 -5 5 0.79 0.45 0 -5 5 0.17 0.74 0 5 -5 1.81 1.22 0 5 -4 0.36 0.66 0 -5 4 0.68 0.92 0 -5 4 1.15 0.85 0 5 -4 2.25 1.09 0 5 -4 0.98 0.55 0 -5 3 85.87 6.64 0 -5 3 86.76 6.57 0 5 -3 94.24 6.44 0 -5 3 87.72 5.79 0 5 -3 90.97 6.47 0 5 -3 83.88 5.26 0 -5 2 15.69 2.28 0 -5 2 17.14 2.32 0 5 -2 12.35 1.82 0 -5 2 13.59 1.70 0 5 -2 13.72 1.39 0 -5 1 145.66 10.14 0 -5 1 169.11 9.60 0 -5 1 159.40 10.17 0 5 -1 156.73 9.54 0 -5 0 33.02 3.57 0 5 0 29.02 3.30 0 -5 0 36.51 3.50 0 5 0 33.35 2.96 0 5 1 2.66 0.83 0 -5 -1 2.71 0.72 0 5 1 2.04 1.03 0 -5 -1 1.83 1.09 0 -5 -1 1.37 0.99 0 5 2 139.76 7.24 0 -5 -2 136.10 9.23 0 -5 -2 138.04 9.08 0 5 2 141.54 8.59 0 5 3 38.80 4.28 0 5 3 31.16 3.83 0 -5 -3 34.15 3.83 0 5 3 36.34 3.60 0 -5 -3 39.96 4.25 0 5 4 830.03 43.17 0 5 4 775.35 43.63 0 -5 -4 720.72 43.96 0 -5 -4 798.73 44.39 0 5 4 840.69 43.27 0 5 5 54.50 4.10 0 -5 -5 60.03 5.48 0 5 5 62.46 5.28 0 -5 -5 52.53 5.42 0 5 5 57.40 4.15 0 -5 -6 438.08 25.00 0 5 6 427.77 24.17 0 -5 -6 386.89 24.28 0 5 6 399.04 24.30 0 5 6 429.11 22.22 0 -5 -7 208.13 13.93 0 5 7 196.15 13.53 0 5 7 195.10 13.51 0 5 7 189.50 13.01 0 -5 -8 324.60 20.27 0 5 8 326.02 20.07 0 5 8 274.49 18.99 0 5 8 331.29 20.23 0 -5 -9 9.10 3.01 0 5 9 7.86 2.53 0 5 9 11.10 2.69 0 5 9 7.13 2.65 0 5 9 11.89 1.82 0 -5 -10 14.12 3.55 0 5 10 11.42 3.15 0 5 10 10.89 2.78 0 5 10 9.54 2.92 0 5 10 11.70 1.77 0 5 11 100.27 9.21 0 5 11 91.47 9.16 0 -5 -11 92.13 9.57 0 5 12 4.23 2.35 0 -5 -12 1.87 2.55 0 5 12 5.49 2.52 0 5 13 79.76 8.95 0 -5 -13 77.67 9.45 0 5 13 83.00 9.08 0 5 14 29.97 5.73 0 5 14 25.18 5.55 0 5 15 -1.43 2.61 0 5 15 0.70 2.55 0 5 16 3.20 3.40 0 5 16 7.15 3.93 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11.70 1.97 0 -6 -2 14.67 2.52 0 -6 -2 11.94 2.36 0 6 3 17.94 3.19 0 6 3 12.08 2.89 0 6 3 13.89 1.34 0 -6 -3 13.44 2.49 0 6 3 12.36 2.05 0 -6 -3 8.65 2.16 0 6 4 114.84 7.86 0 6 4 121.00 7.91 0 6 4 101.01 6.63 0 6 4 98.84 7.64 0 -6 -4 100.50 8.27 0 -6 -4 111.36 7.35 0 -6 -4 114.89 8.80 0 6 5 8.10 1.59 0 6 5 10.87 2.16 0 -6 -5 8.68 2.40 0 -6 -5 8.46 2.28 0 6 5 12.80 1.87 0 6 6 446.11 26.43 0 6 6 464.23 26.19 0 -6 -6 454.77 26.74 0 -6 -6 461.02 27.19 0 6 6 483.01 27.01 0 6 6 444.63 24.44 0 6 7 0.36 1.14 0 -6 -7 -0.41 1.20 0 -6 -7 -0.36 1.14 0 6 7 -0.30 1.07 0 -6 -8 388.48 24.17 0 6 8 383.69 23.58 0 6 8 357.68 23.39 0 6 8 388.27 22.80 0 6 9 18.25 3.66 0 -6 -9 20.18 4.06 0 6 9 24.02 3.71 0 6 9 26.86 4.40 0 -6 -10 90.96 9.02 0 6 10 93.19 8.71 0 6 10 80.06 7.88 0 6 10 94.77 8.99 0 6 10 76.36 5.92 0 6 11 25.92 2.87 0 6 11 30.81 4.90 0 6 11 36.11 5.48 0 -6 -11 28.40 5.28 0 6 12 12.56 3.46 0 6 12 9.14 3.14 0 -6 -12 6.55 3.37 0 6 13 83.07 9.08 0 6 13 77.55 9.05 0 6 14 56.67 7.83 0 6 14 51.63 7.66 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52.29 4.98 0 7 -7 161.44 14.89 0 7 -7 189.72 16.44 0 7 -7 157.79 14.66 0 -7 6 36.16 3.67 0 7 -6 39.39 4.83 0 7 -6 29.13 6.37 0 7 -6 26.92 6.78 0 -7 5 94.90 7.92 0 -7 5 83.23 7.53 0 7 -5 98.45 8.11 0 -7 5 94.05 6.61 0 -7 4 391.02 21.70 0 -7 4 354.61 21.33 0 7 -4 390.33 21.66 0 -7 4 388.36 20.06 0 -7 3 285.29 17.28 0 -7 3 302.58 17.44 0 -7 3 297.62 16.05 0 7 -3 285.11 16.91 0 7 -2 16.17 2.50 0 -7 2 22.90 3.16 0 -7 2 20.52 3.12 0 -7 2 19.38 2.44 0 7 -2 16.96 1.84 0 -7 1 70.93 6.26 0 -7 1 64.36 6.01 0 7 -1 68.31 5.38 0 7 0 13.09 1.96 0 -7 0 7.73 1.98 0 -7 0 9.87 1.45 0 7 0 8.41 2.09 0 7 0 5.18 0.82 0 -7 0 12.71 2.48 0 7 1 402.97 35.06 0 7 1 372.67 34.12 0 7 1 652.39 32.23 0 -7 -1 677.77 33.74 0 -7 -1 593.52 31.45 0 7 1 660.95 33.31 0 -7 -1 647.21 34.00 0 -7 -1 639.92 33.89 0 7 2 597.76 38.62 0 7 2 546.93 37.73 0 7 2 716.67 36.44 0 7 2 685.41 35.65 0 -7 -2 650.54 37.27 0 -7 -2 724.33 37.43 0 7 3 181.73 12.76 0 7 3 168.29 11.55 0 -7 -3 171.56 12.66 0 -7 -3 162.22 12.40 0 7 4 168.44 9.85 0 -7 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1.53 0 -8 4 3.23 1.32 0 -8 4 0.74 1.41 0 8 -4 0.97 0.66 0 8 -4 4.74 3.84 0 8 -4 5.51 5.06 0 8 -3 107.62 8.53 0 -8 3 107.59 8.89 0 -8 3 120.75 7.99 0 -8 3 120.17 9.18 0 8 -3 73.96 10.51 0 8 -3 81.38 11.72 0 8 -2 135.65 9.14 0 -8 2 139.28 9.98 0 -8 2 149.72 10.14 0 8 -2 74.40 10.76 0 8 -2 81.02 11.89 0 8 -1 11.62 4.18 0 8 -1 11.49 2.07 0 8 -1 10.10 4.41 0 -8 1 16.29 2.99 0 -8 1 10.72 2.58 0 8 0 9.00 3.99 0 8 0 8.57 3.47 0 -8 0 7.03 2.03 0 8 0 8.24 2.23 0 8 0 5.42 1.46 0 -8 0 3.20 1.01 0 -8 0 4.59 2.01 0 -8 0 8.07 2.07 0 8 1 33.37 6.19 0 8 1 32.13 5.73 0 8 1 46.16 4.18 0 -8 -1 46.91 5.04 0 8 1 44.39 4.73 0 -8 -1 39.97 3.66 0 -8 -1 44.92 5.28 0 -8 -1 45.57 5.19 0 8 2 154.00 12.35 0 -8 -2 172.42 11.53 0 8 2 171.53 13.18 0 8 2 150.56 10.06 0 8 2 145.09 10.68 0 -8 -2 128.19 11.26 0 -8 -2 150.83 11.54 0 8 3 84.75 7.56 0 -8 -3 71.08 6.87 0 8 3 95.22 8.00 0 8 3 64.08 6.23 0 -8 -3 77.13 7.68 0 -8 -3 63.48 6.97 0 8 4 17.38 2.94 0 -8 -4 21.53 3.41 0 8 4 24.59 3.54 0 8 4 18.05 2.89 0 -8 -4 13.59 3.26 0 -8 -4 18.78 3.68 0 8 5 13.81 2.56 0 -8 -5 12.76 3.35 0 -8 -5 17.25 3.63 0 8 5 14.54 2.76 0 -8 -5 16.23 3.00 0 -8 -6 151.58 11.03 0 8 6 144.69 9.62 0 -8 -6 141.56 11.17 0 8 6 130.24 10.11 0 8 7 223.76 13.75 0 8 7 215.48 14.86 0 -8 -7 225.48 16.11 0 8 7 237.37 15.89 0 -8 -7 234.81 16.82 0 8 7 227.87 15.94 0 8 8 -0.40 1.02 0 -8 -8 0.47 1.64 0 8 8 1.43 1.38 0 8 8 3.64 2.06 0 8 8 -0.92 1.62 0 -8 -8 -2.21 2.01 0 8 9 1.66 1.16 0 -8 -9 1.79 2.35 0 8 9 1.49 2.14 0 8 9 1.02 1.77 0 8 9 1.91 1.28 0 -8 -10 12.11 3.94 0 8 10 26.36 4.80 0 8 10 21.54 4.52 0 8 10 10.36 2.90 0 8 11 37.28 5.82 0 8 11 35.97 5.15 0 8 11 38.65 6.15 0 8 12 166.90 12.80 0 8 12 176.33 14.00 0 8 12 133.01 9.26 0 8 13 85.53 9.47 0 8 13 89.48 8.96 0 -8 -14 30.49 7.10 0 8 14 92.21 9.94 0 -8 -15 5.90 4.66 0 8 15 27.51 6.12 0 -8 -16 2.99 2.15 0 -8 -16 -0.93 3.50 0 8 16 -0.84 3.30 0 8 16 -1.50 3.74 0 -8 -17 9.91 3.79 0 -8 -17 -2.05 5.09 0 8 17 10.77 4.68 0 8 17 13.04 4.59 0 8 18 7.03 4.34 0 -8 -18 7.75 3.40 0 -8 -19 0.66 1.72 0 -9 17 4.20 2.66 0 -9 17 1.92 3.02 0 -9 16 1.50 2.13 0 -9 16 0.91 3.05 0 9 -16 -2.35 4.42 0 -9 15 19.92 4.16 0 9 -15 25.73 7.09 0 -9 15 24.05 5.92 0 9 -15 24.08 5.88 0 -9 14 4.03 2.47 0 9 -14 2.07 3.54 0 -9 14 0.80 2.59 0 9 -14 0.73 3.51 0 -9 13 7.08 2.80 0 9 -13 4.18 4.09 0 -9 13 6.67 3.51 0 9 -13 4.21 3.52 0 -9 12 2.34 2.09 0 -9 12 2.73 3.49 0 9 -12 0.68 2.96 0 9 -11 -1.03 2.99 0 -9 11 -0.36 1.57 0 9 -11 1.36 2.72 0 -9 10 98.65 7.71 0 9 -10 84.71 9.58 0 9 -10 103.83 10.49 0 -9 10 58.91 7.64 0 9 -10 75.80 11.48 0 -9 10 74.37 8.68 0 -9 9 12.32 3.42 0 9 -9 13.69 4.04 0 -9 9 14.47 2.86 0 9 -9 23.67 5.44 0 9 -9 17.24 6.07 0 -9 8 59.27 5.45 0 9 -8 45.68 6.79 0 -9 8 36.46 5.61 0 9 -8 72.92 9.33 0 9 -8 53.94 7.70 0 9 -7 113.92 11.67 0 9 -7 103.39 10.21 0 -9 7 107.04 8.06 0 -9 7 94.95 9.27 0 -9 7 104.89 9.75 0 9 -7 120.24 12.74 0 9 -7 92.48 12.53 0 9 -6 0.52 1.90 0 -9 6 -0.46 1.43 0 9 -6 0.75 2.76 0 9 -6 -0.83 4.26 0 -9 6 -0.46 2.20 0 9 -5 32.45 6.42 0 9 -5 42.78 8.30 0 -9 5 34.27 4.96 0 -9 4 74.25 7.31 0 -9 4 80.75 7.62 0 9 -4 70.70 9.62 0 9 -4 70.61 4.94 0 9 -4 83.23 10.79 0 9 -3 6.83 3.39 0 9 -3 0.44 0.71 0 9 -3 1.07 1.36 0 -9 3 0.40 1.18 0 -9 3 0.40 1.45 0 9 -3 -0.86 3.99 0 9 -2 129.30 9.78 0 -9 2 157.49 11.20 0 -9 2 151.38 10.91 0 9 -2 137.82 8.33 0 9 -2 95.89 11.88 0 9 -2 112.92 13.01 0 9 -1 32.24 3.63 0 -9 1 28.76 4.24 0 9 -1 25.22 6.13 0 -9 1 30.79 4.30 0 9 -1 21.73 5.39 0 -9 0 -0.39 1.43 0 9 0 -1.46 3.12 0 9 0 1.40 1.00 0 -9 0 -0.40 1.53 0 9 0 -0.65 2.41 0 9 1 3.46 2.50 0 -9 -1 0.39 1.62 0 9 1 3.19 2.81 0 9 1 1.41 1.00 0 9 1 1.73 1.40 0 -9 -1 2.17 1.73 0 -9 -1 0.42 1.45 0 9 2 26.01 4.40 0 -9 -2 22.73 3.66 0 9 2 27.92 4.74 0 9 2 16.41 2.62 0 -9 -2 13.96 3.47 0 9 2 20.46 3.26 0 -9 -2 10.66 2.95 0 9 3 0.83 1.60 0 -9 -3 1.20 1.48 0 9 3 2.18 1.80 0 9 3 2.67 1.32 0 -9 -3 -1.58 2.24 0 9 3 2.00 1.39 0 -9 -3 1.42 1.65 0 9 4 7.03 2.33 0 -9 -4 5.29 2.10 0 -9 -4 7.16 2.79 0 9 4 5.01 2.06 0 -9 -4 3.55 2.18 0 -9 -5 34.93 4.87 0 9 5 41.19 4.86 0 -9 -5 46.93 6.36 0 -9 -5 38.30 5.85 0 -9 -6 0.43 1.84 0 9 6 1.71 1.44 0 9 6 1.21 0.95 0 -9 -6 4.91 2.40 0 9 6 3.52 1.96 0 -9 -6 1.27 1.20 0 -9 -6 2.27 2.07 0 9 7 167.39 12.86 0 9 7 156.67 11.00 0 -9 -7 155.58 12.69 0 -9 -7 168.45 14.12 0 9 7 173.81 10.62 0 9 7 168.85 12.25 0 -9 -7 152.28 13.21 0 9 7 152.80 11.08 0 9 8 4.78 1.68 0 9 8 1.51 1.68 0 -9 -8 0.62 2.05 0 -9 -8 -0.71 1.67 0 9 8 1.90 1.63 0 -9 -8 4.27 2.19 0 9 8 2.45 2.01 0 -9 -8 4.11 2.16 0 9 9 20.41 2.96 0 9 9 30.41 4.99 0 -9 -9 22.94 4.30 0 -9 -9 21.23 4.94 0 9 9 22.14 4.57 0 9 9 33.14 4.52 0 9 10 -2.29 2.54 0 9 10 -1.20 2.60 0 9 10 -0.17 1.12 0 9 10 -1.28 2.06 0 9 11 74.02 8.16 0 -9 -11 37.50 3.83 0 9 11 62.44 6.66 0 -9 -11 45.71 6.70 0 9 12 3.01 2.60 0 9 12 2.00 2.44 0 -9 -12 3.12 3.15 0 -9 -13 36.15 6.69 0 9 13 43.12 6.97 0 9 13 27.55 3.19 0 -9 -14 3.84 3.68 0 9 14 10.82 4.34 0 -9 -14 11.94 3.83 0 -9 -15 11.84 5.04 0 9 15 23.99 5.78 0 -9 -15 20.00 4.60 0 -9 -16 0.65 1.98 0 -9 -16 -0.92 3.47 0 9 16 1.77 3.04 0 9 16 -0.74 2.53 0 -9 -17 2.71 2.62 0 -9 -17 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0 10 -4 3.73 3.11 0 10 -4 2.54 0.97 0 -10 4 -0.47 1.77 0 10 -4 -2.46 3.90 0 10 -3 11.94 1.94 0 10 -3 12.70 5.03 0 -10 3 11.49 3.13 0 -10 3 15.61 3.47 0 10 -3 15.78 5.49 0 -10 2 30.18 4.71 0 -10 2 35.83 5.03 0 10 -2 41.99 3.49 0 10 -2 31.12 6.30 0 10 -2 33.76 7.28 0 10 -1 100.98 10.43 0 10 -1 88.79 7.12 0 -10 1 98.15 8.62 0 -10 1 92.13 6.27 0 -10 1 91.68 8.36 0 10 -1 76.03 4.88 0 10 -1 94.74 10.60 0 10 0 279.62 19.66 0 10 0 246.14 18.60 0 10 0 249.27 14.88 0 -10 0 255.59 16.86 0 -10 0 220.28 13.79 0 -10 0 234.59 16.60 0 -10 0 213.30 16.09 0 10 1 67.12 8.26 0 10 1 56.58 7.36 0 10 1 61.70 5.46 0 -10 -1 53.28 6.34 0 10 1 58.02 6.30 0 -10 -1 52.04 6.73 0 -10 -1 55.80 6.60 0 10 2 93.11 9.06 0 10 2 92.94 8.80 0 10 2 70.72 6.23 0 -10 -2 75.96 7.60 0 10 2 67.36 6.90 0 -10 -2 60.09 7.71 0 -10 -2 71.46 7.83 0 10 3 227.99 14.88 0 -10 -3 195.41 14.29 0 10 3 229.72 15.05 0 10 3 168.57 13.22 0 10 3 182.67 12.61 0 -10 -3 181.18 15.27 0 -10 -3 178.05 14.54 0 10 4 267.46 16.70 0 -10 -4 245.38 16.93 0 10 4 239.22 15.47 0 10 4 247.46 16.33 0 -10 -4 206.21 17.84 0 -10 -4 229.22 17.57 0 -10 -5 4.65 2.20 0 10 5 5.07 1.96 0 -10 -5 1.33 2.20 0 10 5 5.40 2.15 0 -10 -5 3.64 2.40 0 10 6 1.29 1.40 0 -10 -6 2.39 1.77 0 10 6 4.02 1.88 0 10 6 3.17 0.94 0 10 6 1.96 1.63 0 -10 -6 2.63 2.17 0 -10 -6 3.20 2.62 0 10 7 0.60 1.19 0 -10 -7 1.96 1.89 0 10 7 0.32 1.34 0 10 7 0.86 0.95 0 10 7 -0.40 1.54 0 -10 -7 0.24 1.40 0 -10 -7 0.64 1.97 0 -10 -7 -0.67 1.94 0 -10 -8 130.04 10.67 0 10 8 114.08 8.61 0 10 8 95.21 7.30 0 10 8 126.44 9.87 0 -10 -8 98.79 8.36 0 -10 -8 123.98 11.92 0 -10 -9 249.41 16.69 0 10 9 217.50 13.76 0 10 9 249.18 15.75 0 -10 -9 250.21 15.36 0 10 9 255.87 17.37 0 10 10 20.43 3.13 0 10 10 24.57 4.29 0 -10 -10 25.60 4.80 0 10 10 14.81 4.36 0 -10 -11 43.15 6.24 0 10 11 36.05 5.44 0 -10 -11 30.19 5.55 0 10 11 34.47 3.48 0 10 11 50.61 7.08 0 10 12 64.14 8.48 0 -10 -12 73.11 8.11 0 10 13 -0.86 1.22 0 10 13 -1.51 2.75 0 -10 -13 -1.34 3.03 0 -10 -14 1.94 2.55 0 10 14 3.25 3.20 0 -10 -14 3.76 3.38 0 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4.82 2.77 0 11 -4 56.58 8.17 0 11 -4 44.94 3.51 0 11 -4 46.73 6.40 0 11 -3 105.38 9.18 0 -11 3 87.46 9.19 0 -11 3 101.31 9.62 0 11 -3 115.71 11.98 0 11 -3 97.43 6.82 0 11 -3 120.86 12.57 0 11 -2 19.01 4.73 0 11 -2 9.11 1.83 0 -11 2 11.74 3.44 0 -11 2 8.85 2.18 0 -11 2 13.98 3.53 0 11 -2 16.03 5.09 0 11 -1 193.22 15.41 0 11 -1 179.98 10.45 0 -11 1 165.58 13.28 0 -11 1 174.24 13.26 0 -11 1 181.59 13.47 0 11 0 83.13 8.76 0 -11 0 72.93 7.57 0 11 0 78.35 8.88 0 -11 0 46.25 4.66 0 -11 0 76.31 7.79 0 -11 0 50.76 6.58 0 11 1 -1.72 2.63 0 -11 -1 -1.00 1.83 0 11 1 -0.87 1.45 0 11 1 0.86 1.28 0 -11 -1 -0.54 1.67 0 -11 -1 0.52 1.81 0 11 2 26.25 4.19 0 11 2 19.57 3.26 0 11 2 29.77 5.16 0 -11 -2 15.05 4.04 0 -11 -2 24.16 4.43 0 11 3 10.85 2.46 0 11 3 4.65 2.22 0 -11 -3 4.07 2.48 0 -11 -3 5.43 3.07 0 11 3 6.19 2.55 0 -11 -4 146.35 12.05 0 11 4 147.32 10.46 0 11 4 124.53 10.79 0 -11 -4 119.82 12.81 0 -11 -4 134.38 12.40 0 -11 -5 96.47 9.56 0 11 5 96.98 8.64 0 11 5 104.92 8.53 0 11 5 98.92 8.94 0 -11 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3 5.61 3.17 -4 7 -3 15.21 3.21 4 -7 3 20.40 3.04 4 -7 3 16.94 2.70 -4 7 -4 8.13 2.49 4 -7 4 2.02 3.21 -4 7 -4 13.81 4.24 4 -7 4 9.24 2.13 4 -7 4 11.50 2.34 -4 7 -5 2.43 0.99 -4 7 -5 2.23 2.02 -4 7 -5 0.75 2.22 -4 7 -6 188.75 10.73 4 -7 6 181.99 11.37 -4 7 -6 167.28 13.35 4 -7 7 75.90 6.06 4 -7 7 86.03 5.24 -4 7 -7 85.77 8.45 4 -7 8 23.12 2.20 4 -7 8 17.73 2.52 -4 7 -8 13.92 3.92 -4 7 -8 15.53 3.72 -4 7 -8 14.94 4.80 4 -7 9 65.02 4.39 4 -7 9 43.88 4.39 -4 7 -9 61.78 7.88 -4 7 -9 73.40 6.75 -4 7 -9 37.29 7.36 -4 7 -9 63.25 7.35 4 -7 10 12.67 3.93 -4 7 -10 9.05 4.15 -4 7 -10 7.66 2.72 4 -7 10 8.68 1.70 4 -7 11 6.87 1.70 -4 7 -11 7.48 3.19 4 -7 11 6.07 3.18 -4 7 -11 16.34 4.81 -4 7 -11 5.58 2.71 -4 7 -11 9.43 4.55 -4 7 -12 30.35 5.61 4 -7 12 30.40 6.12 -4 7 -12 10.48 4.75 -4 7 -12 29.44 5.41 4 -7 13 1.56 2.83 -4 7 -13 2.31 3.37 -4 7 -13 -0.63 2.06 4 -7 13 1.01 1.23 4 -7 14 33.22 6.83 -4 7 -14 30.52 6.18 4 -7 14 51.24 4.77 -4 7 -15 0.92 3.59 -4 7 -15 -1.54 2.77 4 -7 15 1.27 1.64 -4 7 -16 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6.50 -4 5 12 32.70 6.05 -4 5 12 24.43 5.16 4 -5 -12 14.90 2.56 -4 5 12 29.37 4.78 4 -5 -12 28.55 5.62 4 -5 -11 6.01 2.84 -4 5 11 7.27 3.45 -4 5 11 3.93 2.50 4 -5 -11 3.00 1.24 4 -5 -11 2.46 1.28 -4 5 11 7.47 2.43 4 -5 -11 6.97 3.03 -4 5 11 8.78 3.10 4 -5 -10 25.49 4.51 -4 5 10 28.06 4.96 -4 5 10 27.37 4.84 4 -5 -10 23.38 2.75 4 -5 -10 26.44 2.81 -4 5 10 26.69 4.11 -4 5 10 33.40 4.85 -4 5 9 109.12 10.14 4 -5 -9 97.20 7.01 -4 5 9 106.04 9.66 4 -5 -9 95.69 8.97 -4 5 9 116.38 9.51 4 -5 -9 127.75 10.37 4 -5 -9 103.66 7.20 -4 5 8 51.52 6.32 4 -5 -8 64.64 6.46 -4 5 8 54.31 6.09 4 -5 -8 62.35 6.65 4 -5 -8 77.97 7.76 -4 5 7 187.79 13.45 4 -5 -7 178.22 13.24 4 -5 -7 188.22 12.97 4 -5 -6 115.24 9.65 4 -5 -6 105.46 8.23 -4 5 6 101.26 8.72 -4 5 6 101.62 7.25 4 -5 -6 109.12 8.99 4 -5 -6 105.98 7.59 -4 5 5 4.58 1.61 -4 5 5 3.55 1.68 -4 5 5 7.04 1.32 4 -5 -5 4.75 1.87 4 -5 -5 7.44 1.65 4 -5 -5 3.59 2.01 -4 5 4 253.62 15.74 4 -5 -4 243.53 15.13 -4 5 4 235.17 15.63 -4 5 4 252.15 14.09 4 -5 -4 265.26 16.61 -4 5 3 27.08 3.63 4 -5 -3 36.68 3.83 -4 5 3 36.66 3.95 -4 5 3 35.95 2.99 -4 5 3 28.95 3.08 4 -5 -3 29.30 3.02 4 -5 -3 35.17 4.44 -4 5 2 411.11 23.59 4 -5 -2 395.87 22.74 -4 5 2 401.45 22.68 -4 5 2 379.32 22.23 -4 5 2 412.03 21.69 -4 5 2 461.77 23.29 4 -5 -2 392.51 22.91 4 -5 -2 386.31 21.71 4 -5 -2 362.56 23.75 4 -5 -1 104.67 7.51 -4 5 1 91.15 6.95 4 -5 -1 98.06 6.64 -4 5 1 88.10 7.59 4 -5 -1 94.93 7.41 -4 5 1 94.03 7.09 -4 5 1 102.30 7.17 -4 5 0 7.59 1.58 4 -5 0 6.63 1.72 4 -5 0 4.63 1.33 -4 5 0 6.04 1.86 4 -5 0 4.42 1.54 4 -5 0 5.62 1.93 -4 5 0 6.02 1.52 -4 5 0 4.41 1.54 4 -5 1 158.69 10.79 -4 5 -1 157.31 9.62 -4 5 -1 147.10 10.62 4 -5 1 171.32 11.28 4 -5 1 153.35 9.74 4 -5 1 156.57 9.06 4 -5 1 157.38 10.84 -4 5 -1 157.87 11.11 -4 5 -2 103.61 5.96 -4 5 -2 95.94 6.53 -4 5 -2 96.19 8.05 -4 5 -2 93.30 8.12 -4 5 -3 284.66 15.32 -4 5 -3 308.08 15.83 -4 5 -3 287.53 18.32 4 -5 3 327.33 17.99 -4 5 -3 287.41 15.54 -4 5 -3 294.21 18.33 -4 5 -4 34.47 2.48 -4 5 -4 36.59 4.61 4 -5 4 44.60 5.00 -4 5 -4 39.17 4.57 4 -5 4 43.00 5.00 -4 5 -5 54.70 5.55 4 -5 5 52.02 6.21 -4 5 -5 56.57 5.91 -4 5 -5 43.10 4.32 -4 5 -5 34.27 5.77 -4 5 -5 45.91 3.98 4 -5 5 52.11 6.09 4 -5 6 -0.66 2.34 -4 5 -6 0.36 1.43 4 -5 6 -0.59 2.46 -4 5 -6 0.65 0.90 -4 5 -6 0.60 2.01 -4 5 -7 309.08 21.53 -4 5 -7 286.65 17.47 4 -5 7 286.10 15.41 4 -5 7 268.17 15.84 -4 5 -7 295.40 19.71 -4 5 -7 275.03 18.47 -4 5 -8 202.84 13.94 4 -5 8 182.80 10.08 4 -5 8 182.57 10.10 4 -5 8 233.21 11.23 4 -5 8 187.96 10.73 -4 5 -8 239.84 15.84 -4 5 -8 254.44 15.26 -4 5 -8 230.39 17.15 -4 5 -8 203.84 13.23 -4 5 -9 1.65 1.58 4 -5 9 2.18 0.65 4 -5 9 2.78 0.72 4 -5 9 2.24 0.99 4 -5 9 2.54 2.04 -4 5 -9 5.06 2.69 -4 5 -9 1.81 1.56 -4 5 -9 3.53 2.49 -4 5 -9 1.00 2.00 4 -5 10 4.32 0.91 4 -5 10 3.77 1.38 4 -5 10 3.29 2.20 -4 5 -10 3.08 2.43 -4 5 -10 2.92 1.91 -4 5 -10 3.72 2.75 -4 5 -10 3.99 3.17 4 -5 11 0.48 0.86 4 -5 11 0.92 1.19 4 -5 11 -0.60 1.87 -4 5 -11 -0.67 2.06 -4 5 -11 3.94 2.89 4 -5 12 35.38 3.36 4 -5 12 48.58 4.66 4 -5 12 39.90 6.43 -4 5 -12 42.87 6.96 -4 5 -12 38.30 7.32 -4 5 -12 36.00 5.44 -4 5 -13 76.27 8.30 4 -5 13 72.73 5.41 4 -5 13 96.14 7.15 4 -5 13 87.37 9.76 -4 5 -14 1.11 2.45 4 -5 14 0.97 1.12 4 -5 14 2.99 2.60 4 -5 14 -1.02 2.03 4 -5 15 62.10 6.18 4 -5 15 47.19 4.57 -4 5 -15 40.24 6.54 -4 5 -15 51.41 7.75 4 -5 15 45.17 7.78 -4 5 -16 -0.61 2.32 -4 5 -16 -0.82 2.81 4 -5 16 0.23 1.23 4 -5 16 0.80 1.99 4 -5 17 2.22 1.61 -4 5 -17 3.22 4.50 4 -5 17 1.29 2.01 -4 5 -18 9.40 3.45 4 -5 18 11.34 3.25 -4 4 18 -0.79 2.80 -4 4 17 3.10 2.89 -4 4 17 0.74 2.38 -4 4 16 0.81 2.81 -4 4 16 2.83 3.25 -4 4 16 -1.37 2.45 -4 4 16 0.99 2.85 4 -4 -15 26.42 6.15 -4 4 15 13.22 3.05 -4 4 15 34.50 6.51 -4 4 15 36.33 6.18 -4 4 15 25.93 5.23 -4 4 15 34.08 7.01 -4 4 14 12.55 2.83 4 -4 -14 20.88 5.17 -4 4 14 18.63 4.87 -4 4 14 17.74 4.37 -4 4 14 20.40 4.67 -4 4 14 15.34 5.28 4 -4 -13 32.46 6.03 -4 4 13 27.31 4.05 -4 4 13 36.14 6.23 -4 4 13 36.17 5.62 -4 4 13 34.94 5.62 4 -4 -13 29.46 5.89 -4 4 13 36.72 6.71 4 -4 -12 6.71 2.97 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-4 -10 -7 41.64 6.20 4 10 7 48.79 5.59 4 10 7 44.10 5.90 -4 -10 -7 38.81 6.90 4 10 7 37.83 5.31 -4 -10 -7 37.41 6.15 -4 -10 -8 8.70 3.32 4 10 8 10.51 3.18 -4 -10 -8 16.43 4.62 4 10 8 12.83 3.67 -4 -10 -8 12.81 3.92 -4 -10 -8 3.85 4.42 -4 -10 -9 17.66 4.23 -4 -10 -9 14.14 4.99 4 10 9 9.26 3.24 -4 -10 -9 13.15 4.30 4 10 9 18.01 3.95 -4 -10 -10 -0.60 2.00 4 10 10 -1.43 3.20 -4 -10 -10 3.43 3.11 4 10 10 0.43 0.57 4 10 10 0.53 1.96 4 10 10 -1.14 2.09 -4 -10 -11 131.76 12.01 4 10 11 149.78 10.33 4 10 11 121.95 11.42 4 10 11 135.26 12.36 4 10 11 143.67 10.40 4 10 12 4.24 1.40 -4 -10 -12 2.52 1.85 4 10 12 3.54 1.29 -4 -10 -12 2.67 2.35 4 10 12 1.79 2.79 4 10 12 2.71 2.58 4 10 13 45.69 7.25 -4 -10 -13 42.95 6.32 4 10 13 35.25 6.00 -4 -10 -13 32.93 5.80 4 10 13 19.45 2.00 4 10 14 12.04 4.50 -4 -10 -14 10.97 4.26 4 10 14 8.32 3.67 -4 -10 -14 10.39 3.71 4 10 15 7.31 3.38 4 10 15 7.79 4.02 -4 -10 -15 9.31 3.91 4 10 15 4.53 3.31 -4 -10 -15 9.30 3.40 4 10 16 -0.56 2.17 4 10 16 1.86 3.64 -4 -10 -16 3.35 3.07 4 10 16 -0.82 3.21 -4 -10 -16 1.55 3.45 4 10 17 1.00 2.00 -4 -10 -17 2.07 2.57 -4 -10 -17 -0.84 3.28 -4 -10 -18 2.80 2.58 -4 -11 12 6.19 3.04 -4 -11 11 0.54 2.09 -4 -11 11 2.06 2.39 4 11 -11 -2.21 3.55 -4 -11 10 1.53 2.08 4 11 -10 4.79 4.28 -4 -11 10 3.02 2.30 -4 -11 9 9.30 3.14 4 11 -9 12.68 6.00 -4 -11 9 6.28 2.59 -4 -11 9 14.88 5.13 4 11 -8 1.30 4.25 -4 -11 8 2.73 2.21 -4 -11 8 -0.86 2.49 4 11 -8 1.44 1.62 -4 -11 7 127.01 13.91 -4 -11 7 128.27 10.78 -4 -11 7 137.44 10.66 4 11 -7 139.37 10.78 -4 -11 6 24.61 5.88 4 11 -6 19.05 3.75 -4 -11 6 14.13 3.22 4 11 -5 5.23 2.50 -4 -11 5 5.40 2.15 -4 -11 5 6.05 2.58 -4 -11 4 -0.81 2.68 4 11 -4 0.90 1.75 -4 -11 4 0.36 1.47 -4 -11 4 2.54 2.09 -4 -11 3 8.62 3.72 4 11 -3 18.54 3.73 -4 -11 3 8.85 2.51 -4 -11 3 14.23 3.36 -4 -11 2 133.66 13.09 -4 -11 2 135.87 10.74 4 11 -2 120.24 10.20 -4 -11 2 135.37 10.38 -4 -11 1 110.04 12.12 4 11 -1 139.20 11.63 4 11 -1 126.49 11.20 4 11 -1 127.78 10.01 -4 -11 1 126.38 10.18 4 11 0 8.98 2.96 4 11 0 6.14 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12 -4 5.75 2.51 -4 -12 4 11.17 2.92 -4 -12 4 15.12 3.74 -4 -12 3 18.82 5.50 4 12 -3 22.22 4.05 -4 -12 3 16.86 3.69 -4 -12 3 23.02 4.33 -4 -12 2 18.93 5.30 -4 -12 2 19.95 3.87 4 12 -2 18.65 3.63 -4 -12 1 -0.79 2.31 4 12 -1 0.38 1.58 -4 -12 1 0.91 1.70 4 12 0 18.83 3.53 -4 -12 0 9.89 4.18 4 12 0 12.93 2.70 -4 -12 0 15.14 3.77 4 12 1 12.78 2.90 -4 -12 -1 10.40 4.04 4 12 1 9.32 3.29 4 12 1 5.69 2.18 -4 -12 -1 5.97 2.78 4 12 2 18.26 3.34 -4 -12 -2 8.68 3.52 4 12 2 4.81 2.30 -4 -12 -2 11.00 3.40 4 12 2 23.42 4.66 -4 -12 -3 42.71 6.73 -4 -12 -3 41.98 5.99 4 12 3 54.29 6.48 -4 -12 -4 25.74 5.01 -4 -12 -4 26.72 5.44 4 12 4 30.79 5.32 -4 -12 -5 8.73 3.41 4 12 5 11.07 3.68 -4 -12 -5 12.55 3.89 4 12 6 22.45 4.86 -4 -12 -6 11.22 4.03 4 12 7 21.40 4.76 -4 -12 -7 21.71 5.00 4 12 8 -1.19 2.17 -4 -12 -8 -0.71 2.34 -4 -12 -9 -1.18 4.49 4 12 9 4.17 3.82 4 12 9 2.94 3.24 4 12 9 4.78 2.87 -4 -12 -10 45.90 7.31 4 12 10 35.87 5.88 4 12 10 54.35 7.04 -4 -12 -10 28.70 7.45 4 12 10 42.21 6.51 4 12 10 40.84 6.57 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36.75 4.87 5 5 -8 38.10 4.13 -5 -5 8 29.82 3.22 -5 -5 7 30.66 2.75 5 5 -7 25.21 4.95 -5 -5 7 27.35 4.08 5 5 -7 24.89 4.50 -5 -5 7 28.45 4.06 5 5 -7 11.50 2.80 -5 -5 7 19.02 6.68 -5 -5 6 4.96 1.84 -5 -5 6 4.11 1.82 5 5 -6 7.70 3.08 5 5 -6 6.48 2.56 -5 -5 6 7.68 2.41 -5 -5 6 8.69 4.99 -5 -5 6 6.92 1.18 5 5 -5 80.65 7.60 -5 -5 5 83.64 6.65 5 5 -5 81.39 8.29 -5 -5 5 92.97 7.30 -5 -5 5 61.30 7.61 5 5 -5 66.15 7.31 -5 -5 5 84.22 7.13 -5 -5 5 75.77 4.70 -5 -5 4 3.03 3.75 5 5 -4 6.89 2.25 -5 -5 4 7.01 1.80 5 5 -4 5.43 2.41 -5 -5 4 11.10 2.27 -5 -5 4 5.03 2.47 5 5 -4 3.74 1.97 -5 -5 4 6.53 2.03 -5 -5 4 6.22 0.76 -5 -5 3 81.19 6.67 -5 -5 3 69.12 7.54 5 5 -3 77.70 7.27 -5 -5 3 71.12 5.80 5 5 -3 76.67 6.99 -5 -5 3 63.89 5.94 5 5 -3 65.52 6.95 5 5 -2 43.03 5.04 -5 -5 2 32.20 3.78 5 5 -2 37.56 4.71 -5 -5 2 34.27 5.15 -5 -5 2 43.31 4.61 -5 -5 2 39.55 3.93 5 5 -2 46.69 4.95 -5 -5 1 139.85 14.98 5 5 -1 154.42 10.95 5 5 -1 163.67 11.37 -5 -5 1 160.73 10.31 5 5 -1 157.45 11.39 -5 -5 1 168.14 12.75 5 5 -1 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35.87 6.31 8 -6 -9 29.56 4.56 8 -6 -9 9.39 5.74 -8 6 9 24.65 2.63 8 -6 -9 31.10 4.96 -8 6 9 13.11 3.04 8 -6 -9 23.18 4.83 -8 6 8 6.31 3.29 -8 6 8 9.67 3.57 8 -6 -8 11.77 3.12 8 -6 -8 6.96 4.70 -8 6 8 4.03 3.07 8 -6 -8 4.90 2.52 -8 6 8 5.64 2.32 8 -6 -8 6.77 2.94 -8 6 7 5.28 2.75 -8 6 7 0.59 1.83 8 -6 -7 -0.85 1.56 8 -6 -7 -0.95 3.42 -8 6 7 -0.63 2.60 8 -6 -7 0.39 1.60 -8 6 7 1.68 1.85 8 -6 -7 -0.55 1.80 -8 6 6 -2.18 2.42 -8 6 6 -0.53 1.95 8 -6 -6 0.92 2.99 -8 6 6 -1.18 2.53 8 -6 -6 -0.67 1.61 -8 6 6 -0.91 1.81 8 -6 -6 -0.56 2.09 -8 6 5 103.40 9.48 -8 6 5 100.77 9.12 -8 6 5 68.44 8.39 8 -6 -5 86.37 9.34 -8 6 5 82.66 8.56 8 -6 -5 92.59 7.28 8 -6 -5 90.70 8.43 8 -6 -4 142.17 10.83 -8 6 4 127.47 10.73 -8 6 4 102.04 10.08 -8 6 4 118.72 10.86 8 -6 -4 118.62 13.48 8 -6 -4 120.13 8.40 8 -6 -4 113.43 11.02 -8 6 3 71.85 7.46 8 -6 -3 77.85 7.61 -8 6 3 66.31 7.21 8 -6 -3 72.70 10.20 -8 6 2 34.21 4.74 8 -6 -2 24.75 6.25 8 -6 -2 41.06 5.20 -8 6 2 29.82 4.51 -8 6 2 26.90 4.82 -8 6 1 207.82 13.44 8 -6 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13.17 -8 5 -2 161.89 9.63 -8 5 -2 163.61 11.50 8 -5 2 162.23 14.06 8 -5 2 165.23 10.17 -8 5 -2 164.11 14.38 8 -5 2 184.67 16.26 -8 5 -2 163.57 13.84 8 -5 3 0.44 1.20 -8 5 -3 -0.27 1.11 8 -5 3 0.27 1.05 8 -5 3 -1.15 2.53 8 -5 3 -0.35 1.78 -8 5 -3 -0.67 2.24 -8 5 -3 2.24 2.07 8 -5 4 308.26 18.52 8 -5 4 292.03 21.11 8 -5 4 309.73 20.74 8 -5 4 334.70 20.16 -8 5 -4 334.09 23.51 -8 5 -4 318.17 21.90 8 -5 5 137.68 11.41 8 -5 5 144.63 11.89 -8 5 -5 159.64 14.23 -8 5 -5 131.77 12.19 8 -5 5 146.63 11.51 8 -5 5 137.16 9.54 -8 5 -6 156.37 15.24 8 -5 6 167.38 13.08 -8 5 -6 174.71 14.33 8 -5 6 176.35 11.05 8 -5 6 170.44 13.03 8 -5 6 159.65 12.93 8 -5 7 64.18 6.92 8 -5 7 51.26 6.43 -8 5 -7 43.23 7.68 -8 5 -7 60.68 7.61 8 -5 7 61.37 5.09 8 -5 7 54.31 6.50 8 -5 8 -1.27 1.63 8 -5 8 -0.49 1.97 8 -5 8 1.43 1.94 -8 5 -8 1.72 2.86 -8 5 -8 -0.60 1.90 8 -5 8 0.50 1.94 8 -5 8 0.21 1.02 8 -5 9 323.44 20.15 -8 5 -9 351.09 24.38 8 -5 9 410.79 24.52 8 -5 9 374.61 20.30 8 -5 10 285.71 16.87 -8 5 -10 260.44 20.67 8 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11.15 8 6 0 115.29 10.15 8 6 1 109.04 9.53 8 6 1 106.87 9.44 -8 -6 -1 101.77 8.35 8 6 1 97.25 9.36 -8 -6 -1 92.44 10.34 8 6 1 104.85 8.76 -8 -6 -1 108.81 9.47 -8 -6 -1 104.67 13.05 -8 -6 -2 7.95 4.14 8 6 2 4.31 2.21 8 6 2 2.87 1.85 8 6 2 2.77 2.09 -8 -6 -2 1.66 1.09 -8 -6 -2 3.13 2.21 -8 -6 -2 1.68 1.40 8 6 2 2.71 1.60 -8 -6 -2 1.80 2.10 8 6 2 3.11 1.14 8 6 3 1.77 1.21 8 6 3 4.15 1.94 8 6 3 3.76 1.94 8 6 3 4.01 2.30 -8 -6 -3 5.46 1.68 -8 -6 -3 6.03 2.77 -8 -6 -3 3.53 1.93 8 6 3 2.63 1.56 -8 -6 -3 9.27 3.02 -8 -6 -3 -2.85 3.00 8 6 4 67.93 6.91 8 6 4 74.49 6.82 -8 -6 -4 67.13 9.78 8 6 4 72.15 7.42 -8 -6 -4 82.23 8.78 -8 -6 -4 76.08 7.76 8 6 4 69.74 6.66 8 6 4 79.39 8.29 8 6 4 70.06 6.03 -8 -6 -4 72.34 6.35 8 6 5 21.18 3.71 8 6 5 22.07 3.46 -8 -6 -5 17.05 5.05 8 6 5 27.46 4.24 -8 -6 -5 19.26 4.28 8 6 5 26.74 3.89 8 6 5 29.08 5.17 -8 -6 -5 17.57 3.91 8 6 5 21.54 3.22 8 6 6 374.79 22.24 8 6 6 355.43 21.48 -8 -6 -6 354.30 24.01 8 6 6 380.32 22.69 -8 -6 -6 345.10 23.33 8 6 6 362.46 22.51 8 6 6 341.87 23.92 -8 -6 -6 340.94 25.83 8 6 7 9.69 2.61 8 6 7 6.28 2.05 8 6 7 7.64 2.24 -8 -6 -7 9.07 3.96 -8 -6 -7 12.68 3.54 8 6 7 9.97 4.06 8 6 7 11.36 2.95 -8 -6 -7 10.34 3.29 8 6 8 130.44 10.18 8 6 8 134.06 9.48 -8 -6 -8 120.85 10.39 8 6 9 3.18 1.94 8 6 9 2.80 2.86 8 6 9 0.47 1.65 8 6 9 2.67 1.75 8 6 9 4.26 2.29 8 6 9 4.43 2.47 -8 -6 -10 0.68 2.25 8 6 10 -1.05 1.92 -8 -6 -10 -0.60 1.95 8 6 10 -0.30 1.39 8 6 10 -1.76 2.76 8 6 10 -0.47 1.69 8 6 11 32.37 5.63 8 6 11 36.40 4.87 8 6 11 29.26 4.13 8 6 11 39.09 5.59 8 6 11 40.22 6.39 -8 -6 -11 28.73 5.16 -8 -6 -11 30.20 5.52 8 6 12 21.38 3.76 8 6 12 30.52 4.71 -8 -6 -12 26.34 5.00 8 6 12 29.97 6.09 8 6 12 32.92 5.79 8 6 13 15.84 4.42 8 6 13 12.50 3.00 -8 -6 -13 11.23 3.39 8 6 13 26.02 5.87 8 6 13 16.91 3.44 8 6 14 37.25 6.73 8 6 14 29.65 4.51 -8 -6 -14 32.66 5.29 8 6 14 40.69 7.76 8 6 14 24.90 3.77 8 6 15 1.61 2.92 8 6 15 0.98 3.02 -8 -6 -15 -0.49 1.69 8 6 15 -0.95 3.88 -8 -6 -15 1.48 2.68 8 6 15 0.97 1.13 -8 -6 -16 3.77 1.97 -8 -6 -16 3.16 3.55 8 6 16 1.03 3.72 8 6 16 0.86 2.49 8 6 16 2.88 3.13 -8 -6 -17 0.44 1.81 -8 -6 -17 -0.84 3.77 8 6 17 1.12 3.84 8 6 17 -1.86 2.85 8 6 18 7.00 4.10 -8 -7 14 4.58 2.70 -8 -7 13 1.80 5.41 -8 -7 13 -1.09 2.25 -8 -7 12 -1.76 5.34 -8 -7 12 -0.52 2.01 -8 -7 11 1.71 5.23 -8 -7 11 6.24 3.04 -8 -7 11 6.42 2.73 -8 -7 10 -1.67 4.44 -8 -7 10 3.51 2.78 -8 -7 10 0.47 1.89 -8 -7 9 3.25 5.88 -8 -7 9 6.51 2.92 -8 -7 9 6.21 2.58 -8 -7 8 30.59 4.48 -8 -7 8 29.81 4.97 8 7 -7 -0.66 1.86 -8 -7 7 -1.54 4.13 -8 -7 7 0.80 1.71 -8 -7 7 -0.95 2.15 -8 -7 6 -0.48 2.44 -8 -7 6 1.49 5.20 -8 -7 6 1.55 1.65 -8 -7 6 3.54 2.24 8 7 -5 0.73 2.47 -8 -7 5 2.92 2.12 -8 -7 5 1.39 2.24 -8 -7 5 1.45 5.30 -8 -7 4 14.25 3.18 -8 -7 4 15.74 3.61 -8 -7 4 18.19 6.97 -8 -7 4 22.70 5.56 -8 -7 3 3.79 2.07 -8 -7 3 4.95 3.66 -8 -7 3 4.02 2.24 8 7 -2 2.63 2.85 -8 -7 2 0.80 2.50 8 7 -2 4.62 2.67 -8 -7 2 1.46 1.52 8 7 -2 3.01 2.45 -8 -7 2 3.89 4.55 8 7 -1 4.21 2.94 8 7 -1 7.73 3.02 -8 -7 1 4.61 3.09 -8 -7 1 5.36 2.04 -8 -7 1 5.46 2.39 8 7 -1 6.72 3.00 -8 -7 1 11.19 5.86 -8 -7 0 30.76 4.07 8 7 0 24.68 4.67 8 7 0 24.68 4.64 -8 -7 0 20.61 5.15 -8 -7 0 13.25 3.32 8 7 0 28.17 4.84 -8 -7 0 10.76 5.42 -8 -7 -1 133.11 15.36 8 7 1 125.74 10.75 -8 -7 -1 128.47 9.76 8 7 1 106.55 10.29 8 7 1 127.93 10.91 -8 -7 -1 135.33 12.63 -8 -7 -1 120.52 9.41 8 7 1 123.08 10.05 -8 -7 -1 124.03 10.78 -8 -7 -1 112.35 7.56 8 7 2 -0.46 2.13 8 7 2 0.91 1.79 -8 -7 -2 2.54 1.21 8 7 2 2.93 2.00 -8 -7 -2 0.68 1.85 -8 -7 -2 1.85 1.54 -8 -7 -2 -0.27 1.46 -8 -7 -2 1.04 2.05 8 7 2 1.53 1.75 -8 -7 -2 1.10 3.23 -8 -7 -3 3.19 1.44 8 7 3 2.17 1.32 8 7 3 2.09 1.71 8 7 3 2.23 1.69 8 7 3 1.41 1.99 -8 -7 -3 5.26 3.01 -8 -7 -3 0.93 1.27 8 7 3 2.23 1.66 -8 -7 -3 2.68 2.20 -8 -7 -3 6.35 3.72 -8 -7 -4 96.44 12.35 8 7 4 88.96 8.17 8 7 4 91.75 8.00 -8 -7 -4 75.42 9.14 8 7 4 78.65 8.23 8 7 4 90.86 8.06 -8 -7 -4 91.57 9.21 8 7 4 96.98 9.18 8 7 4 88.26 7.18 -8 -7 -4 81.98 7.24 8 7 5 17.23 3.42 8 7 5 11.66 2.67 -8 -7 -5 11.36 2.82 8 7 5 14.54 2.89 -8 -7 -5 18.83 4.52 8 7 5 16.42 3.66 8 7 5 16.21 3.33 8 7 5 15.17 4.16 -8 -7 -5 10.55 3.45 -8 -7 -5 13.47 5.17 -8 -7 -6 53.30 8.73 8 7 6 60.37 6.01 8 7 6 61.70 6.37 8 7 6 58.39 6.50 -8 -7 -6 54.91 7.41 -8 -7 -6 68.03 7.73 8 7 6 61.70 6.62 8 7 6 32.59 6.25 -8 -7 -6 61.20 6.52 8 7 6 56.70 5.85 -8 -7 -7 59.28 6.65 8 7 7 64.59 6.53 8 7 7 59.06 5.88 -8 -7 -7 62.39 7.59 8 7 7 32.59 6.48 8 7 7 59.21 6.63 -8 -7 -7 53.66 7.09 -8 -7 -7 30.36 6.99 8 7 8 59.39 5.93 -8 -7 -8 85.66 9.12 8 7 8 91.37 8.58 -8 -7 -8 71.63 8.50 8 7 8 59.23 8.44 8 7 8 85.39 7.32 8 7 9 10.25 2.82 8 7 9 8.81 2.39 8 7 9 3.57 3.32 8 7 9 15.05 3.79 -8 -7 -9 8.15 3.69 8 7 10 17.60 3.64 8 7 10 9.81 2.48 8 7 10 14.08 3.88 -8 -7 -10 7.07 3.35 -8 -7 -11 3.37 2.77 -8 -7 -11 0.60 2.08 8 7 11 3.52 2.89 8 7 11 -1.29 2.84 8 7 11 -0.47 1.99 8 7 11 -0.30 1.66 8 7 12 18.71 4.96 8 7 12 17.55 3.27 8 7 12 15.52 4.57 8 7 12 28.70 4.85 -8 -7 -13 12.30 3.60 8 7 13 7.75 3.31 8 7 13 10.79 2.67 8 7 13 3.10 3.22 8 7 13 9.54 2.91 8 7 14 3.06 3.14 8 7 14 7.45 2.53 8 7 14 9.50 4.29 -8 -7 -14 4.64 2.69 8 7 14 3.40 3.50 8 7 14 5.01 2.08 8 7 15 3.30 2.99 8 7 15 5.54 2.38 8 7 15 4.98 3.76 -8 -7 -15 3.99 2.23 8 7 15 4.65 4.19 8 7 15 1.19 1.23 -8 -7 -16 6.71 2.84 8 7 16 1.01 3.12 8 7 16 7.98 3.98 8 7 16 2.99 3.42 8 7 17 -0.96 3.86 -8 -7 -17 0.54 2.09 -8 -7 -17 2.55 3.68 8 7 18 7.28 3.78 -8 -8 13 -0.52 2.18 -8 -8 12 15.40 3.78 -8 -8 11 7.14 2.81 -8 -8 11 -1.89 5.39 -8 -8 10 -1.36 2.30 -8 -8 10 -1.17 2.37 -8 -8 10 -3.71 6.34 -8 -8 9 1.74 2.06 -8 -8 9 2.73 2.31 -8 -8 9 3.62 5.90 -8 -8 8 15.92 3.71 -8 -8 8 13.44 3.36 -8 -8 7 22.41 8.75 8 8 -7 17.81 4.53 -8 -8 6 36.98 10.94 -8 -8 6 95.82 8.52 -8 -8 5 18.58 5.76 -8 -8 5 15.87 3.74 -8 -8 5 19.62 8.29 8 8 -4 0.73 2.34 -8 -8 4 4.59 3.92 -8 -8 4 -0.42 1.69 -8 -8 4 -1.01 2.44 8 8 -3 62.96 8.39 -8 -8 3 57.92 6.28 -8 -8 3 59.21 7.17 -8 -8 3 53.71 8.73 -8 -8 3 33.52 10.21 -8 -8 2 113.86 13.12 -8 -8 2 125.77 16.82 -8 -8 2 130.97 10.27 -8 -8 1 26.13 4.55 -8 -8 1 25.68 5.91 -8 -8 1 18.20 7.08 -8 -8 1 38.09 4.85 -8 -8 0 -0.11 0.69 8 8 0 0.55 1.80 -8 -8 0 0.80 2.34 -8 -8 0 0.37 1.81 8 8 0 -0.47 1.82 -8 -8 0 1.57 1.75 8 8 0 -0.55 1.80 -8 -8 0 1.34 4.19 -8 -8 -1 -1.28 4.01 8 8 1 3.62 2.46 8 8 1 1.10 2.54 8 8 1 2.66 2.39 -8 -8 -1 2.30 2.82 -8 -8 -1 7.91 2.57 8 8 1 4.42 2.41 -8 -8 -1 4.49 1.94 -8 -8 -1 2.30 3.01 -8 -8 -1 4.15 1.41 -8 -8 -2 92.83 14.12 8 8 2 120.94 10.89 8 8 2 150.36 11.78 -8 -8 -2 126.67 12.85 8 8 2 126.35 11.21 -8 -8 -2 121.75 8.89 8 8 2 120.09 10.44 -8 -8 -2 136.44 10.63 -8 -8 -2 147.83 12.60 -8 -8 -2 139.03 9.22 -8 -8 -3 228.71 21.39 8 8 3 222.01 15.69 8 8 3 206.19 15.25 -8 -8 -3 228.96 18.16 8 8 3 206.34 15.58 8 8 3 196.84 14.77 -8 -8 -3 222.36 17.04 -8 -8 -3 210.41 13.90 8 8 4 0.45 2.12 8 8 4 -0.43 1.62 -8 -8 -4 2.25 3.94 -8 -8 -4 0.70 2.21 8 8 4 0.49 1.85 8 8 4 3.08 2.38 8 8 4 0.42 1.69 -8 -8 -4 0.63 2.27 -8 -8 -4 0.71 1.50 8 8 4 1.54 1.40 8 8 5 5.62 2.55 8 8 5 8.94 2.59 -8 -8 -5 -1.08 3.79 -8 -8 -5 3.46 2.89 8 8 5 5.81 2.55 8 8 5 12.27 3.28 -8 -8 -5 10.21 3.76 8 8 5 0.54 2.32 -8 -8 -5 9.25 2.70 8 8 5 12.24 2.68 8 8 6 97.83 8.80 8 8 6 103.71 8.56 -8 -8 -6 98.08 8.92 8 8 6 107.55 8.61 8 8 6 97.14 9.08 -8 -8 -6 92.19 10.21 8 8 6 102.34 9.24 -8 -8 -6 97.38 10.28 8 8 6 60.60 8.54 -8 -8 -6 68.48 11.08 -8 -8 -7 10.30 3.89 8 8 7 5.87 2.30 8 8 7 3.83 3.04 8 8 7 12.26 3.49 -8 -8 -7 5.19 2.83 8 8 7 6.76 2.35 -8 -8 -7 4.02 2.34 -8 -8 -8 62.41 8.51 8 8 8 87.64 7.72 8 8 8 85.88 8.60 -8 -8 -8 80.55 9.23 -8 -8 -8 79.83 8.47 8 8 8 73.02 7.51 -8 -8 -9 75.33 8.76 -8 -8 -9 67.00 7.92 8 8 9 83.40 8.34 -8 -8 -9 59.92 8.64 8 8 10 21.86 3.50 8 8 10 28.07 5.42 -8 -8 -10 31.77 6.24 -8 -8 -11 74.23 8.84 8 8 11 71.84 7.45 8 8 11 46.52 5.30 8 8 11 83.06 9.12 -8 -8 -11 49.82 7.93 8 8 12 5.24 2.27 -8 -8 -12 5.31 2.92 8 8 12 7.65 3.06 8 8 12 9.80 3.71 -8 -8 -12 9.48 3.73 -8 -8 -13 -0.67 2.84 8 8 13 1.44 2.23 8 8 13 2.13 1.73 8 8 13 0.77 3.36 8 8 13 1.38 2.15 8 8 14 0.33 1.77 -8 -8 -14 0.67 2.29 8 8 14 -1.67 3.99 8 8 14 -1.56 3.31 8 8 15 0.85 2.44 8 8 15 1.77 1.59 8 8 15 1.00 3.25 8 8 15 2.74 3.44 8 8 15 1.06 1.26 -8 -8 -15 0.66 1.75 -8 -8 -16 18.16 4.59 8 8 16 18.87 6.37 8 8 16 30.92 6.84 8 8 17 5.00 4.30 -8 -8 -17 3.18 2.81 8 8 18 0.95 2.68 8 8 19 4.48 3.28 -8 -9 10 4.09 6.61 -8 -9 9 8.05 6.89 -8 -9 9 6.77 3.09 -8 -9 8 4.28 2.68 8 9 -8 -0.53 2.29 -8 -9 7 13.71 3.64 -8 -9 7 1.94 6.00 -8 -9 6 -3.79 5.87 -8 -9 6 4.88 2.68 -8 -9 5 -1.85 5.74 -8 -9 5 1.01 3.14 -8 -9 5 0.47 1.87 -8 -9 4 1.79 6.83 -8 -9 4 -1.00 3.46 -8 -9 4 5.52 2.63 -8 -9 3 10.61 4.91 -8 -9 3 10.37 7.40 8 9 -3 10.75 4.11 -8 -9 3 13.91 3.48 -8 -9 2 8.38 4.29 -8 -9 2 22.91 4.05 -8 -9 2 1.66 5.22 8 9 -2 18.78 4.78 -8 -9 1 17.64 3.78 -8 -9 1 24.39 1.95 -8 -9 1 34.17 6.86 -8 -9 1 33.21 9.97 -8 -9 0 30.04 4.73 -8 -9 0 31.90 4.37 -8 -9 0 28.12 3.06 -8 -9 0 30.08 9.37 -8 -9 0 24.19 6.06 -8 -9 -1 1.67 2.45 -8 -9 -1 2.12 1.59 8 9 1 3.39 2.51 -8 -9 -1 4.35 2.31 -8 -9 -1 1.28 1.41 -8 -9 -1 3.88 3.14 -8 -9 -1 -2.86 5.24 -8 -9 -2 28.56 8.89 8 9 2 56.08 6.90 -8 -9 -2 62.11 8.76 -8 -9 -2 49.00 4.38 8 9 2 49.86 6.35 -8 -9 -2 53.06 7.88 -8 -9 -2 55.01 5.33 -8 -9 -3 12.12 2.72 -8 -9 -3 7.88 3.51 8 9 3 4.66 2.71 8 9 3 5.17 2.67 -8 -9 -3 6.37 3.54 -8 -9 -3 1.30 4.33 -8 -9 -4 27.71 4.46 8 9 4 34.06 5.22 -8 -9 -4 17.40 6.59 8 9 4 27.48 4.68 -8 -9 -4 27.60 5.90 -8 -9 -4 24.11 5.61 -8 -9 -5 142.14 13.52 8 9 5 124.54 10.09 -8 -9 -5 131.14 10.78 8 9 5 119.93 10.87 -8 -9 -5 120.54 12.54 -8 -9 -5 138.07 16.14 8 9 6 8.03 3.02 -8 -9 -6 1.53 2.93 8 9 6 6.07 2.80 -8 -9 -6 1.14 3.78 8 9 6 0.40 1.54 -8 -9 -6 4.44 2.28 8 9 7 148.12 12.50 -8 -9 -7 134.53 13.72 -8 -9 -7 158.01 12.74 8 9 7 140.55 11.47 -8 -9 -8 60.57 8.55 8 9 8 69.30 7.89 -8 -9 -8 44.22 8.73 -8 -9 -8 60.14 7.84 8 9 8 58.55 6.77 -8 -9 -9 1.54 3.17 -8 -9 -9 3.26 2.43 8 9 9 1.99 1.90 8 9 9 -1.17 2.73 -8 -9 -9 1.83 2.25 8 9 10 -1.85 2.80 -8 -9 -10 -1.66 3.28 8 9 11 4.90 1.88 -8 -9 -11 1.54 2.79 8 9 11 1.97 2.61 -8 -9 -11 3.07 2.53 -8 -9 -12 39.81 7.06 8 9 12 28.22 4.73 8 9 12 25.66 3.74 8 9 12 35.26 6.50 -8 -9 -12 29.74 6.01 8 9 13 41.39 4.90 8 9 13 53.51 6.60 8 9 13 62.29 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6 40.52 6.57 10 0 6 61.83 7.51 10 0 6 34.98 6.66 10 0 6 71.69 6.52 10 0 6 62.42 9.15 10 0 6 66.48 7.68 10 0 7 146.75 16.05 10 0 7 146.08 12.87 10 0 7 163.25 13.39 10 0 7 151.91 9.75 10 0 7 154.80 11.85 10 0 7 136.24 12.28 10 0 7 156.99 13.43 10 0 7 167.78 12.12 10 0 7 113.86 12.49 10 0 7 153.99 15.38 10 0 8 77.05 8.69 10 0 8 80.18 8.83 10 0 8 64.09 5.20 10 0 8 76.68 6.95 10 0 8 67.30 7.75 10 0 8 46.12 7.28 10 0 8 86.70 8.09 10 0 8 66.34 9.05 10 0 8 86.80 11.14 10 0 9 59.35 10.02 10 0 9 86.31 7.24 10 0 9 70.54 5.08 10 0 9 48.95 5.49 10 0 9 47.62 6.74 10 0 9 71.61 8.71 10 0 9 54.91 9.61 10 0 9 74.73 8.01 10 0 9 88.95 9.53 10 0 9 46.19 8.00 10 0 10 166.54 11.60 10 0 10 149.49 8.97 10 0 10 124.12 9.42 10 0 10 116.35 11.34 10 0 10 154.50 14.07 10 0 10 103.85 14.15 10 0 10 168.11 13.17 10 0 10 143.43 13.72 10 0 11 19.61 5.11 10 0 11 21.98 3.93 10 0 11 14.34 2.30 10 0 11 13.05 2.37 10 0 11 20.22 5.35 10 0 11 21.09 4.95 10 0 11 17.91 4.53 10 0 11 9.86 5.23 10 0 12 12.12 3.20 10 0 12 11.02 2.07 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11.08 10 1 7 128.55 9.46 10 1 7 136.07 11.18 10 1 7 172.73 13.04 10 1 7 140.64 12.85 10 1 7 194.62 15.17 10 1 7 148.46 11.57 10 1 7 190.21 16.49 10 1 7 136.65 12.61 10 1 8 27.58 3.14 10 1 8 25.49 3.88 10 1 8 20.57 4.85 10 1 8 42.28 7.78 10 1 8 30.56 6.43 10 1 8 29.17 5.09 10 1 9 2.31 3.44 10 1 9 0.62 2.29 10 1 9 2.40 1.15 10 1 9 2.44 1.38 10 1 9 -0.71 1.94 10 1 9 -0.98 4.14 10 1 9 -1.10 3.58 10 1 10 6.07 3.26 10 1 10 5.33 2.27 10 1 10 3.23 1.48 10 1 10 9.18 3.60 10 1 10 5.57 3.08 10 1 10 -3.31 5.22 10 1 11 155.49 12.63 10 1 11 145.77 11.05 10 1 11 129.24 8.68 10 1 11 105.80 8.49 10 1 11 125.11 13.21 10 1 11 119.92 12.03 10 1 11 115.24 12.27 10 1 12 114.32 9.81 10 1 12 104.96 7.63 10 1 12 107.51 12.15 10 1 12 105.01 11.56 10 1 12 78.14 10.08 10 1 12 62.71 11.23 10 1 12 83.27 9.18 10 1 13 0.50 1.97 10 1 13 1.13 3.84 10 1 13 1.03 1.48 10 1 13 2.75 3.02 10 1 13 -0.84 3.20 10 1 14 0.48 2.16 10 1 14 0.96 2.78 10 1 14 2.26 1.73 10 1 14 0.91 1.40 10 1 14 -1.14 4.04 10 1 14 2.70 2.96 10 1 15 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11 9.33 3.70 10 2 11 1.12 4.20 10 2 11 7.64 3.84 10 2 11 3.95 1.78 10 2 12 4.53 1.86 10 2 12 -0.91 2.47 10 2 12 5.18 2.69 10 2 12 2.23 3.81 10 2 12 8.08 4.05 10 2 13 0.41 1.87 10 2 13 0.96 2.80 10 2 13 2.56 2.17 10 2 13 2.24 3.99 10 2 13 -0.79 2.61 10 2 14 6.12 3.15 10 2 14 11.06 4.80 10 2 14 4.51 2.37 10 2 14 1.11 4.46 10 2 14 2.55 3.23 10 2 14 2.56 2.65 10 2 15 -0.41 1.57 10 2 15 4.05 3.53 10 2 15 0.82 1.40 10 2 15 -1.10 3.52 10 2 15 -0.93 3.37 10 2 15 -0.92 3.18 10 2 16 10.33 6.36 10 2 16 1.01 2.91 10 2 16 0.99 3.24 10 2 16 2.94 2.13 10 2 17 -1.27 2.54 10 2 17 1.10 3.78 -10 -3 13 1.39 4.41 -10 -3 12 1.36 4.13 -10 -3 11 0.69 2.57 -10 -3 11 1.34 3.52 -10 -3 10 23.25 4.06 -10 -3 10 36.38 8.91 -10 -3 10 37.43 6.52 -10 -3 9 5.01 2.21 -10 -3 9 5.07 4.38 -10 -3 9 10.21 3.71 -10 -3 8 18.95 4.59 -10 -3 8 14.69 3.06 -10 -3 8 20.98 7.07 -10 -3 8 25.88 5.17 -10 -3 7 0.60 1.49 -10 -3 7 4.88 2.80 -10 -3 7 2.17 2.39 -10 -3 6 132.24 11.24 -10 -3 6 121.43 9.09 -10 -3 6 100.49 14.27 -10 -3 6 133.54 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9.30 -10 -4 0 61.85 7.54 -10 -4 0 70.11 6.78 -10 -4 0 64.88 10.19 -10 -4 -1 197.46 18.51 10 4 1 207.72 15.16 -10 -4 -1 202.57 13.05 10 4 1 214.72 16.16 -10 -4 -1 181.35 14.05 10 4 1 176.93 12.70 -10 -4 -1 187.05 13.24 10 4 1 178.58 10.18 -10 -4 -2 38.24 7.94 10 4 2 32.92 5.46 -10 -4 -2 39.14 4.63 10 4 2 43.28 6.39 -10 -4 -2 46.62 5.70 10 4 2 38.47 4.61 -10 -4 -2 37.76 4.86 10 4 2 36.60 3.41 -10 -4 -3 79.05 11.15 10 4 3 112.29 9.74 -10 -4 -3 102.95 8.46 -10 -4 -3 98.69 8.89 10 4 3 96.62 7.81 10 4 3 100.81 7.17 -10 -4 -3 92.47 8.44 10 4 3 88.05 9.60 -10 -4 -4 145.73 15.30 10 4 4 178.12 12.91 10 4 4 160.77 13.16 -10 -4 -4 135.45 13.24 -10 -4 -4 175.19 12.08 10 4 4 136.23 13.23 10 4 4 154.72 10.99 -10 -4 -4 147.47 11.69 10 4 4 163.29 10.78 10 4 5 27.36 5.14 10 4 5 30.31 4.78 10 4 5 23.07 3.92 10 4 5 31.85 4.04 -10 -4 -5 22.45 4.99 10 4 5 26.81 5.68 -10 -4 -5 41.79 7.60 -10 -4 -6 48.13 7.95 10 4 6 29.57 4.26 10 4 6 28.51 4.58 10 4 6 32.70 4.17 -10 -4 -6 35.91 5.75 10 4 6 42.48 7.05 10 4 6 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10 4 16 5.84 2.30 10 4 16 3.13 3.94 10 4 17 4.54 4.42 -10 -5 12 3.15 5.30 -10 -5 11 -1.53 4.01 -10 -5 11 -0.67 2.49 -10 -5 10 1.49 4.57 -10 -5 10 8.71 3.45 -10 -5 9 2.33 2.08 -10 -5 9 1.45 4.46 -10 -5 9 3.54 2.57 -10 -5 9 3.13 2.65 -10 -5 8 0.44 1.79 -10 -5 8 -2.83 4.36 -10 -5 8 -0.58 2.11 -10 -5 7 2.47 2.20 -10 -5 7 3.77 2.37 -10 -5 6 -1.18 2.24 -10 -5 6 -1.33 3.87 -10 -5 6 -0.50 1.89 -10 -5 6 0.98 2.02 -10 -5 5 0.38 1.49 -10 -5 5 -2.61 4.07 -10 -5 5 -0.46 2.05 -10 -5 5 1.86 2.05 10 5 -4 13.50 2.77 -10 -5 4 18.20 3.86 -10 -5 4 21.13 3.88 -10 -5 4 15.22 6.16 -10 -5 4 19.76 3.64 -10 -5 3 -0.40 1.61 -10 -5 3 1.28 1.89 -10 -5 3 1.23 4.31 -10 -5 3 0.77 1.66 -10 -5 2 76.23 7.34 -10 -5 2 70.06 6.90 -10 -5 2 70.62 7.15 -10 -5 2 56.48 10.88 10 5 -1 8.86 3.51 -10 -5 1 7.94 2.53 -10 -5 1 9.36 2.77 -10 -5 1 5.79 4.46 10 5 0 8.01 3.49 10 5 0 9.35 3.32 10 5 0 6.68 3.35 -10 -5 0 11.27 2.60 -10 -5 0 13.49 3.34 -10 -5 0 1.12 3.07 10 5 1 0.58 2.19 10 5 1 -0.54 2.26 -10 -5 -1 0.75 2.88 10 5 1 -0.63 2.29 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4.20 2.69 -10 -6 -5 7.09 3.52 10 6 5 7.88 2.10 10 6 5 2.10 3.15 -10 -6 -5 3.06 3.40 -10 -6 -6 84.37 9.90 10 6 6 91.63 7.74 -10 -6 -6 68.45 10.68 -10 -6 -7 0.68 2.37 10 6 7 0.95 1.72 10 6 7 5.25 2.26 -10 -6 -7 0.96 3.20 10 6 7 2.75 1.79 10 6 8 16.10 3.13 10 6 8 10.53 3.04 10 6 8 11.61 3.18 10 6 8 13.45 3.79 10 6 9 21.12 4.40 10 6 9 24.60 3.76 10 6 9 16.18 3.60 10 6 9 14.78 3.53 10 6 9 21.94 4.71 10 6 9 19.17 4.49 10 6 10 2.24 2.22 10 6 10 0.78 1.78 10 6 10 0.87 2.10 -10 -6 -10 1.80 3.13 10 6 10 1.19 2.13 10 6 10 0.60 2.66 10 6 10 1.34 1.80 -10 -6 -10 -0.64 2.63 10 6 11 33.39 5.07 -10 -6 -11 38.62 6.30 10 6 11 29.74 5.64 10 6 11 24.35 4.70 10 6 11 35.97 6.50 10 6 11 39.00 6.36 10 6 12 1.74 2.19 -10 -6 -12 3.10 2.88 10 6 12 4.40 3.32 10 6 12 7.60 3.59 10 6 13 2.41 3.05 -10 -6 -13 -1.22 2.48 10 6 13 5.26 2.52 -10 -6 -14 2.36 2.31 10 6 14 -0.88 3.59 10 6 14 1.58 2.35 10 6 14 -0.45 1.79 -10 -6 -15 -0.57 2.03 10 6 15 3.83 3.90 10 6 15 1.70 1.72 10 6 15 3.45 4.14 -10 -6 -16 4.75 2.72 10 6 16 5.56 2.12 10 6 17 -1.19 4.25 10 6 18 2.35 4.15 -10 -7 10 1.71 2.52 -10 -7 9 3.50 5.66 -10 -7 9 1.63 2.43 -10 -7 8 7.28 3.00 -10 -7 8 3.49 2.54 -10 -7 7 14.80 3.87 -10 -7 7 16.47 3.81 -10 -7 6 3.22 5.00 -10 -7 6 9.17 3.15 -10 -7 6 10.38 3.29 -10 -7 5 34.32 5.12 -10 -7 5 23.60 8.71 -10 -7 5 19.04 4.19 -10 -7 4 -0.47 1.86 -10 -7 4 2.99 2.39 -10 -7 4 3.05 5.29 -10 -7 3 53.88 6.23 -10 -7 3 51.97 6.62 -10 -7 3 38.35 10.35 -10 -7 3 26.03 5.55 -10 -7 2 56.65 6.35 -10 -7 2 45.28 6.90 -10 -7 2 47.53 6.49 -10 -7 2 41.45 10.50 -10 -7 1 -0.53 2.34 -10 -7 1 3.40 2.05 -10 -7 1 6.93 5.73 -10 -7 1 0.54 2.17 -10 -7 1 2.80 3.25 -10 -7 0 30.21 4.58 -10 -7 0 29.31 4.93 -10 -7 0 22.71 7.66 -10 -7 0 27.83 5.10 -10 -7 0 30.72 6.85 -10 -7 -1 5.48 2.44 -10 -7 -1 7.87 2.64 10 7 1 4.10 2.43 -10 -7 -1 12.89 5.88 -10 -7 -1 4.04 2.81 -10 -7 -1 6.11 3.62 -10 -7 -2 118.22 10.06 -10 -7 -2 157.21 11.48 10 7 2 136.95 11.04 -10 -7 -2 101.00 14.58 -10 -7 -2 142.70 12.42 -10 -7 -2 127.62 13.62 -10 -7 -3 246.17 19.73 10 7 3 244.23 13.98 -10 -7 -3 221.78 14.98 10 7 3 210.78 15.58 -10 -7 -3 203.40 15.62 -10 -7 -3 268.02 18.36 -10 -7 -3 199.59 21.12 10 7 4 4.13 1.78 -10 -7 -4 4.24 2.88 -10 -7 -4 4.64 4.45 -10 -7 -4 10.98 3.98 10 7 5 9.20 2.44 -10 -7 -5 1.12 3.50 -10 -7 -5 5.36 3.07 10 7 6 3.21 1.89 -10 -7 -6 -1.06 3.33 -10 -7 -6 1.50 2.20 -10 -7 -7 45.92 5.96 10 7 7 52.45 5.85 -10 -7 -7 40.19 8.29 -10 -7 -7 36.20 6.78 10 7 7 54.89 6.72 10 7 8 48.40 5.97 10 7 8 43.39 5.92 -10 -7 -9 46.19 8.46 10 7 9 37.38 5.53 -10 -7 -9 29.83 5.49 10 7 9 40.22 5.63 10 7 9 36.75 5.96 10 7 9 34.31 5.76 -10 -7 -10 22.38 6.30 -10 -7 -10 36.10 6.10 10 7 10 27.66 4.81 -10 -7 -10 29.11 5.90 10 7 10 45.34 6.16 10 7 10 15.96 3.88 10 7 10 42.31 6.56 10 7 10 32.33 5.57 -10 -7 -11 48.40 7.50 10 7 11 56.51 7.52 10 7 11 33.03 5.36 10 7 11 66.85 8.35 -10 -7 -11 48.81 8.77 10 7 11 51.12 7.20 -10 -7 -12 8.29 3.56 10 7 12 10.91 3.90 10 7 12 4.70 2.49 10 7 12 9.49 3.85 10 7 12 6.80 2.97 -10 -7 -13 18.41 4.89 10 7 13 23.85 5.52 10 7 13 24.52 4.36 10 7 13 26.41 6.11 10 7 13 25.87 5.24 -10 -7 -14 0.67 2.40 10 7 14 -2.62 3.80 10 7 14 -0.55 2.43 10 7 14 2.18 2.35 10 7 14 -3.15 3.78 -10 -7 -15 16.98 4.54 10 7 15 19.00 5.81 10 7 15 18.95 3.89 10 7 15 15.89 5.96 -10 -7 -16 15.11 4.45 10 7 16 22.66 6.86 10 7 17 26.68 7.47 -10 -8 10 5.09 2.84 -10 -8 7 -1.70 2.47 -10 -8 6 -1.78 4.76 -10 -8 6 -1.08 2.36 -10 -8 5 6.72 2.90 -10 -8 5 1.74 5.04 -10 -8 4 1.00 1.98 -10 -8 4 1.69 4.89 -10 -8 3 0.49 1.85 -10 -8 3 -1.20 2.63 -10 -8 3 -1.63 4.74 -10 -8 2 8.98 3.00 -10 -8 2 1.69 2.40 -10 -8 2 -1.58 4.90 -10 -8 2 6.43 3.20 -10 -8 2 -1.04 4.11 -10 -8 1 18.19 4.30 -10 -8 1 32.96 5.07 -10 -8 1 29.68 5.53 -10 -8 1 25.11 6.64 -10 -8 0 24.94 4.44 -10 -8 0 19.37 4.11 -10 -8 0 16.09 7.28 -10 -8 0 19.55 4.86 -10 -8 0 16.47 5.43 -10 -8 -1 0.93 1.84 10 8 1 -0.50 2.13 -10 -8 -1 1.51 1.61 -10 -8 -1 1.42 4.43 -10 -8 -1 0.65 2.54 -10 -8 -1 -0.93 2.52 10 8 2 5.71 2.69 -10 -8 -2 8.59 2.37 -10 -8 -2 3.73 2.32 -10 -8 -2 4.72 2.93 -10 -8 -2 1.36 3.97 -10 -8 -2 9.00 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11 4 11 11.27 3.51 11 4 11 20.23 4.76 11 4 11 25.28 5.42 11 4 12 111.20 13.60 11 4 12 98.02 9.19 11 4 12 131.69 12.46 11 4 12 124.56 9.89 11 4 13 1.98 2.28 11 4 13 -1.06 3.29 11 4 13 -1.33 2.71 11 4 14 5.69 4.31 11 4 14 4.17 2.51 11 4 15 0.51 2.15 11 4 16 1.23 3.53 11 4 16 3.94 2.30 11 4 17 40.19 8.97 -11 -5 9 -4.63 5.26 -11 -5 9 0.64 2.57 -11 -5 8 1.75 1.95 -11 -5 8 3.08 2.60 -11 -5 7 0.42 1.66 -11 -5 7 1.15 2.35 -11 -5 6 6.88 2.61 -11 -5 6 2.86 4.70 -11 -5 6 11.85 3.56 -11 -5 6 7.51 2.97 -11 -5 5 52.68 11.32 -11 -5 5 55.26 6.84 -11 -5 5 56.35 6.33 -11 -5 5 64.11 7.32 -11 -5 4 6.05 2.63 -11 -5 4 5.94 2.68 -11 -5 4 3.61 2.25 -11 -5 4 8.09 5.34 11 5 -4 5.50 1.85 -11 -5 3 10.51 3.21 -11 -5 3 3.50 2.22 -11 -5 3 4.10 2.31 -11 -5 3 1.31 2.90 11 5 -3 5.81 2.34 -11 -5 2 20.11 4.03 -11 -5 2 19.91 3.79 -11 -5 2 21.03 3.93 -11 -5 2 6.41 5.36 11 5 -2 13.93 3.58 -11 -5 1 33.72 4.60 -11 -5 1 21.13 7.39 -11 -5 1 24.83 4.42 -11 -5 0 8.93 2.67 -11 -5 0 6.09 4.68 -11 -5 0 6.69 2.59 -11 -5 -1 5.03 2.19 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5 11 8.41 3.35 11 5 11 3.08 2.12 -11 -5 -11 3.20 2.73 11 5 11 6.29 3.26 11 5 11 6.59 3.08 11 5 12 30.20 5.34 11 5 12 45.41 8.26 -11 -5 -12 31.60 5.73 11 5 12 38.68 6.74 11 5 12 40.31 6.96 11 5 13 5.27 4.00 11 5 13 7.37 3.18 11 5 13 2.35 2.71 11 5 14 14.74 4.22 11 5 15 -1.06 2.72 11 5 16 4.80 2.40 11 5 16 11.27 5.41 -11 -6 9 11.59 3.82 -11 -6 9 11.68 6.24 -11 -6 8 17.89 7.66 -11 -6 8 47.59 6.64 -11 -6 7 0.55 2.17 -11 -6 7 -0.58 2.10 -11 -6 7 -0.48 1.52 -11 -6 6 16.39 3.95 -11 -6 6 26.70 4.50 -11 -6 5 14.86 3.64 -11 -6 5 14.34 3.49 11 6 -4 3.72 1.94 -11 -6 4 12.08 3.29 -11 -6 4 9.51 3.12 -11 -6 4 8.80 2.82 -11 -6 4 2.92 4.81 -11 -6 4 0.72 2.61 -11 -6 3 56.57 6.52 -11 -6 3 54.52 6.51 -11 -6 3 35.52 9.63 -11 -6 3 29.60 6.31 -11 -6 2 3.40 2.46 -11 -6 2 -1.38 3.73 -11 -6 2 3.23 3.17 -11 -6 2 2.65 2.18 -11 -6 1 64.74 6.85 -11 -6 1 59.73 7.27 -11 -6 1 44.12 10.29 -11 -6 1 51.81 7.55 -11 -6 0 65.17 6.78 -11 -6 0 69.92 7.85 -11 -6 0 36.63 9.43 -11 -6 0 45.19 6.53 -11 -6 -1 42.93 5.42 -11 -6 -1 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4.83 2.43 11 6 11 5.83 3.18 11 6 11 3.40 3.08 11 6 12 1.54 2.32 -11 -6 -12 -1.38 2.59 11 6 12 2.13 2.57 11 6 12 2.79 2.46 -11 -6 -13 -0.67 2.41 11 6 13 -0.77 2.92 11 6 13 -1.03 2.96 11 6 13 2.57 2.43 -11 -6 -14 67.72 8.86 11 6 14 81.31 9.55 11 6 14 87.92 10.95 -11 -6 -15 14.58 4.16 11 6 15 34.39 7.08 11 6 15 34.71 8.26 11 6 16 11.67 3.30 11 6 16 13.85 5.94 -11 -7 9 4.80 2.89 -11 -7 8 -0.57 2.23 -11 -7 8 1.77 5.38 -11 -7 7 2.22 2.56 -11 -7 7 0.59 2.74 -11 -7 6 14.52 3.85 -11 -7 6 6.70 6.34 -11 -7 5 -0.53 2.54 11 7 -5 0.73 1.50 -11 -7 5 6.57 5.67 -11 -7 4 43.75 5.94 -11 -7 4 39.11 5.76 -11 -7 4 30.28 9.18 -11 -7 3 8.11 3.28 -11 -7 3 1.55 5.10 -11 -7 3 14.22 3.63 -11 -7 3 4.07 3.25 -11 -7 2 1.66 2.38 -11 -7 2 -1.50 4.67 -11 -7 2 3.80 3.18 -11 -7 2 1.43 2.03 -11 -7 1 -1.14 2.21 -11 -7 1 5.85 5.80 -11 -7 1 4.01 3.01 -11 -7 1 -0.93 1.91 -11 -7 0 -0.98 2.86 -11 -7 0 -1.38 1.89 -11 -7 0 0.51 2.02 -11 -7 0 -1.18 3.12 -11 -7 0 -1.41 5.37 -11 -7 -1 39.57 5.47 11 7 1 41.89 5.89 -11 -7 -1 31.82 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3 10 37.70 7.69 15 3 10 35.18 5.93 15 3 11 4.35 3.24 15 3 11 0.93 3.17 15 3 11 5.56 3.04 15 3 12 -0.95 2.87 15 3 12 -1.88 2.67 15 3 12 -0.67 2.26 15 3 13 -1.03 2.69 15 3 13 -0.72 2.03 15 3 13 0.95 2.68 15 3 14 12.48 4.36 15 3 14 17.85 5.77 15 3 15 -1.83 3.33 -15 -4 3 10.64 3.73 -15 -4 3 3.57 3.97 -15 -4 2 5.11 2.75 -15 -4 2 1.69 3.41 -15 -4 1 1.65 2.14 -15 -4 1 1.60 3.00 -15 -4 0 -0.54 2.40 -15 -4 0 1.53 2.99 -15 -4 -1 25.65 9.16 -15 -4 -1 23.53 4.60 -15 -4 -1 21.40 5.54 -15 -4 -2 -1.69 4.86 -15 -4 -2 1.44 2.71 -15 -4 -2 11.41 3.55 15 4 2 17.48 5.38 -15 -4 -3 -1.10 2.81 -15 -4 -3 1.67 4.05 15 4 4 7.34 2.66 15 4 4 8.01 2.06 15 4 5 12.04 3.20 15 4 5 11.57 2.77 15 4 6 79.60 8.25 15 4 6 79.95 8.00 15 4 7 11.21 3.34 15 4 7 15.99 3.98 15 4 8 12.32 3.65 15 4 8 14.88 5.57 15 4 8 4.79 2.77 15 4 9 10.86 3.67 15 4 9 6.58 3.15 15 4 10 5.28 3.15 15 4 10 7.08 3.18 15 4 11 19.92 5.49 15 4 11 17.44 5.74 15 4 11 18.41 4.55 15 4 12 11.79 5.07 15 4 12 13.85 5.16 15 4 12 9.58 3.70 15 4 13 -3.95 3.64 15 4 13 2.93 3.02 15 4 13 2.78 3.42 15 4 14 25.88 6.61 15 4 15 32.38 6.93 -15 -5 2 1.80 2.59 -15 -5 2 4.15 3.78 -15 -5 1 -0.58 2.27 -15 -5 1 1.57 3.04 -15 -5 0 -1.15 2.32 -15 -5 0 0.75 2.66 -15 -5 -1 2.28 2.32 -15 -5 -1 5.00 3.53 -15 -5 -2 1.74 4.61 -15 -5 -2 0.69 2.99 -15 -5 -2 0.58 2.65 -15 -5 -3 10.27 6.16 -15 -5 -3 5.23 3.17 -15 -5 -4 -1.69 4.85 15 5 5 -0.50 2.39 -15 -5 -5 1.67 5.13 15 5 5 -0.28 1.29 15 5 6 1.54 1.75 15 5 6 2.07 2.23 15 5 7 -0.53 2.36 15 5 8 23.19 4.68 15 5 8 8.85 3.69 15 5 9 6.33 3.05 15 5 9 4.07 2.94 15 5 10 14.26 4.24 15 5 10 13.61 4.15 15 5 11 4.76 3.60 15 5 11 5.93 3.24 15 5 12 -2.61 3.59 15 5 12 -1.82 3.36 15 5 12 2.82 2.91 15 5 13 -0.95 3.35 15 5 13 -0.75 2.53 15 5 13 0.91 2.90 15 5 14 -0.91 3.02 -15 -6 2 7.26 4.05 -15 -6 1 15.16 4.99 -15 -6 0 0.61 2.19 -15 -6 0 -0.72 2.55 -15 -6 -1 1.36 3.02 -15 -6 -1 1.22 2.28 -15 -6 -2 -1.97 2.91 -15 -6 -2 2.44 2.80 15 6 4 4.73 2.34 -15 -6 -5 13.80 7.47 15 6 5 5.47 3.23 -15 -6 -6 -1.70 4.51 15 6 6 2.27 2.44 15 6 7 2.90 2.57 15 6 8 4.67 2.67 15 6 8 7.78 3.53 15 6 9 9.03 3.30 15 6 9 6.83 3.73 15 6 10 1.37 2.07 15 6 10 5.87 3.35 15 6 11 18.38 5.03 15 6 11 30.34 5.77 15 6 12 -0.85 2.98 15 6 12 2.18 2.68 15 6 13 0.93 3.10 15 6 13 2.69 3.55 15 6 14 -0.89 2.82 -15 -7 2 4.67 3.51 -15 -7 1 3.63 3.54 -15 -7 -1 1.93 2.93 -15 -7 -1 3.25 3.21 -15 -7 -2 1.24 2.48 -15 -7 -2 -0.64 2.60 15 7 4 4.08 2.93 15 7 5 11.92 3.71 15 7 6 1.23 2.18 15 7 7 26.47 5.56 15 7 8 34.95 6.13 15 7 9 3.34 3.20 15 7 9 5.73 3.05 15 7 10 -2.78 3.85 15 7 10 0.66 2.52 15 7 11 2.18 2.99 15 7 11 1.48 2.84 15 7 12 9.93 3.94 15 7 13 19.14 5.84 -15 -8 2 2.22 2.82 -15 -8 1 0.69 2.91 -15 -8 0 0.64 2.35 -15 -8 -1 12.64 3.84 15 8 4 6.37 3.41 15 8 5 18.08 4.45 15 8 6 0.66 2.74 15 8 7 2.05 2.72 15 8 8 -1.40 2.69 15 8 9 17.26 4.80 15 8 10 21.51 5.10 15 8 12 9.67 4.09 -15 -9 1 0.64 2.53 -15 -9 0 5.96 2.95 -15 -9 -1 3.91 2.89 15 9 5 1.39 2.96 15 9 6 0.71 2.73 15 9 7 -1.47 3.02 15 9 8 -1.51 2.77 15 10 5 15.75 4.68 -16 7 -2 3.43 2.83 -16 6 -2 -0.69 2.09 16 -6 5 14.24 5.24 16 -6 6 2.13 3.00 -16 5 5 14.85 4.01 -16 5 4 3.75 2.82 -16 5 3 6.65 2.81 -16 5 2 2.96 2.24 -16 5 -1 4.89 2.92 16 -5 3 7.57 3.93 16 -5 4 0.89 2.70 16 -5 5 35.05 7.22 16 -5 6 29.18 7.03 16 -5 7 2.14 3.43 -16 4 4 -0.54 1.90 -16 4 3 13.24 3.51 -16 4 2 10.61 3.05 -16 4 1 2.79 2.04 -16 4 0 2.90 1.73 -16 4 -1 8.37 3.73 16 -4 1 18.36 4.56 -16 4 -1 11.40 2.70 16 -4 2 49.53 7.65 16 -4 3 12.97 4.36 16 -4 4 9.87 4.16 16 -4 5 7.09 4.15 16 -4 6 -0.95 3.81 16 -4 7 42.96 8.46 16 -4 8 36.12 7.96 -16 3 4 1.11 2.20 -16 3 3 2.53 2.28 -16 3 2 2.30 2.14 -16 3 1 12.21 3.04 -16 3 0 0.79 1.78 -16 3 -1 1.83 1.75 16 -3 1 3.61 3.49 16 -3 1 -0.58 1.95 -16 3 -2 4.33 1.92 16 -3 2 3.73 3.33 16 -3 2 1.90 2.63 16 -3 3 6.68 4.37 16 -3 3 9.75 3.67 16 -3 4 12.92 4.28 16 -3 5 2.48 2.94 16 -3 6 16.14 5.41 16 -3 7 27.08 6.92 16 -3 8 -1.04 4.72 16 -3 9 -1.12 4.13 -16 2 4 -1.68 2.31 -16 2 3 7.23 2.83 16 -2 -3 6.75 3.19 -16 2 2 -0.48 1.85 16 -2 -2 -0.82 2.46 -16 2 1 4.88 2.29 16 -2 -1 6.11 3.96 -16 2 0 1.26 1.86 16 -2 0 1.84 2.78 16 -2 1 5.06 2.86 -16 2 -1 -0.80 1.61 16 -2 1 1.90 3.39 16 -2 2 3.98 2.72 -16 2 -2 1.53 1.93 16 -2 2 -0.97 3.14 16 -2 3 0.63 2.53 -16 2 -3 1.70 1.63 16 -2 3 1.97 3.19 16 -2 4 2.78 2.79 16 -2 4 3.97 3.56 16 -2 5 0.76 2.83 16 -2 5 1.00 2.63 16 -2 6 1.66 2.82 16 -2 7 7.24 4.36 16 -2 8 -1.96 4.58 16 -2 9 -3.18 5.32 16 -2 10 1.14 3.45 -16 1 4 6.33 3.08 -16 1 3 11.22 3.42 16 -1 -3 12.45 4.44 -16 1 2 -0.99 1.91 16 -1 -2 -0.89 2.85 -16 1 1 17.24 3.79 16 -1 -1 24.59 6.31 -16 1 0 30.47 4.85 16 -1 0 40.33 7.93 -16 1 -1 7.39 2.71 16 -1 1 7.07 4.36 -16 1 -2 1.28 1.65 16 -1 2 -1.02 2.92 16 -1 3 6.75 3.17 -16 1 -3 14.78 3.34 16 -1 3 12.38 4.88 16 -1 4 28.35 5.68 16 -1 4 31.94 7.19 16 -1 5 6.98 3.54 16 -1 5 14.39 4.99 16 -1 6 2.30 2.97 16 -1 7 -0.84 3.12 16 -1 7 -1.03 2.72 16 -1 8 13.75 5.24 16 -1 9 38.78 7.99 16 -1 10 16.12 5.79 16 -1 11 1.16 3.26 16 0 -4 22.96 5.64 -16 0 3 6.03 2.83 16 0 -3 9.20 4.37 -16 0 2 5.68 2.79 16 0 -2 14.67 4.91 -16 0 1 0.49 2.04 16 0 -1 2.05 3.29 -16 0 0 1.42 1.91 16 0 0 1.06 3.21 -16 0 -1 40.72 7.58 -16 0 -1 38.52 5.52 16 0 1 39.85 8.35 -16 0 -2 14.32 5.01 -16 0 -2 8.77 2.90 16 0 2 9.77 4.71 -16 0 -3 -0.90 1.81 16 0 3 -1.09 3.71 16 0 4 7.24 3.05 16 0 4 4.33 3.71 16 0 5 26.42 5.47 16 0 6 34.31 6.47 16 0 7 0.77 2.74 16 0 7 1.07 3.05 16 0 8 21.98 5.54 16 0 9 4.81 2.51 16 0 9 1.84 3.12 16 0 10 28.93 7.29 16 0 11 11.35 3.47 16 0 11 22.65 6.43 16 0 12 -0.63 2.01 16 0 13 20.26 4.98 16 1 -4 14.13 4.92 -16 -1 3 2.26 2.35 -16 -1 2 4.83 2.58 16 1 -2 4.24 3.92 -16 -1 1 2.06 2.41 16 1 -1 -1.10 2.89 -16 -1 0 -0.50 2.47 16 1 0 -1.13 3.43 -16 -1 -1 -0.49 1.99 16 1 1 2.30 3.49 -16 -1 -2 0.50 2.08 16 1 2 1.15 3.52 -16 -1 -3 1.48 1.91 16 1 3 2.30 3.93 16 1 4 -1.14 3.27 16 1 5 -1.65 2.35 16 1 6 -1.88 3.00 16 1 6 -1.12 3.44 16 1 7 -0.70 3.09 16 1 8 8.54 2.78 16 1 8 11.62 4.09 16 1 9 1.38 1.77 16 1 9 9.32 3.85 16 1 10 3.12 2.35 16 1 10 2.77 3.28 16 1 11 -0.58 2.03 16 1 11 4.01 3.70 16 1 12 1.09 3.26 16 1 13 3.48 3.02 16 2 -4 -1.03 2.65 16 2 -3 6.56 4.02 -16 -2 2 16.31 4.08 -16 -2 1 1.09 2.18 16 2 -1 8.34 4.93 -16 -2 0 0.53 2.05 -16 -2 0 0.86 3.19 16 2 0 -1.22 3.21 -16 -2 -1 14.23 4.87 -16 -2 -1 24.79 4.65 16 2 1 20.98 6.71 -16 -2 -2 2.49 3.47 -16 -2 -2 6.87 3.02 16 2 2 2.47 4.62 -16 -2 -3 11.67 3.62 16 2 3 13.52 5.50 16 2 6 17.73 4.23 16 2 6 15.46 5.95 16 2 7 12.15 3.12 16 2 7 14.58 4.17 16 2 8 11.12 3.16 16 2 8 12.79 4.13 16 2 9 -0.98 2.50 16 2 9 -0.79 2.06 16 2 10 3.78 2.51 16 2 10 6.05 3.45 16 2 11 4.72 2.35 16 2 11 3.77 3.33 16 2 12 1.93 2.64 16 2 12 7.18 4.08 16 2 13 -0.70 2.32 -16 -3 1 2.86 2.75 -16 -3 0 11.78 3.56 -16 -3 0 10.15 4.48 -16 -3 -1 1.65 3.31 -16 -3 -1 0.56 1.99 -16 -3 -2 15.43 4.93 -16 -3 -2 15.72 4.13 -16 -3 -3 47.37 6.71 16 3 6 -0.83 2.22 16 3 6 -0.48 2.11 16 3 7 15.02 3.54 16 3 7 7.43 3.22 16 3 8 32.24 5.97 16 3 9 2.09 2.37 16 3 9 -0.74 2.36 16 3 10 -0.57 2.17 16 3 10 -0.82 2.61 16 3 11 7.31 3.32 16 3 11 8.08 3.95 16 3 12 36.79 6.26 16 3 12 32.30 7.09 16 3 13 8.49 3.52 -16 -4 0 9.50 3.52 -16 -4 -1 9.63 4.16 -16 -4 -1 11.22 3.68 -16 -4 -2 0.79 2.93 -16 -4 -2 -0.60 2.72 -16 -4 -3 -0.60 2.40 16 4 6 -3.79 2.58 16 4 8 0.53 2.05 16 4 9 3.37 2.47 16 4 9 7.52 3.34 16 4 10 2.98 2.62 16 4 10 5.38 2.95 16 4 11 -1.27 2.77 16 4 11 0.85 2.85 16 4 12 5.42 2.87 16 4 12 2.79 3.27 -16 -5 0 21.63 5.57 -16 -5 -1 -2.32 3.50 -16 -5 -1 -1.26 2.52 -16 -5 -2 14.39 4.55 -16 -5 -2 11.31 3.87 16 5 5 4.88 2.65 16 5 7 4.47 2.53 16 5 8 -0.58 2.23 16 5 9 -0.60 2.48 16 5 10 4.43 3.22 16 5 10 3.62 3.17 16 5 11 -0.67 3.39 16 5 11 0.81 2.70 16 5 12 7.04 3.50 16 5 12 7.15 4.01 -16 -6 0 2.31 3.17 -16 -6 -1 18.48 5.05 16 6 5 12.08 3.78 16 6 6 2.33 2.69 16 6 7 4.28 2.68 16 6 8 0.63 2.32 16 6 9 16.95 4.71 16 6 10 14.87 4.52 16 6 11 3.52 2.88 -16 -7 0 0.73 2.68 -16 -7 -1 7.70 3.72 16 7 6 15.87 4.42 16 7 8 0.68 2.40 16 7 9 -0.70 2.78 16 7 10 -0.72 2.85 -16 -8 0 4.15 2.99 -16 -8 -1 0.66 2.39 16 8 6 6.88 3.41 16 8 7 -1.42 2.81 16 8 8 0.74 3.01 17 -6 3 3.90 3.39 17 -5 3 7.79 3.77 17 -5 4 27.78 6.47 17 -5 5 0.99 2.95 17 -4 4 6.74 3.79 17 -4 5 34.65 7.22 17 -4 6 20.62 5.77 17 -4 7 1.05 2.72 -17 3 3 -0.53 1.98 17 -3 4 1.53 3.13 17 -3 6 3.62 3.33 17 -3 7 -0.98 3.60 17 -3 8 3.18 3.55 -17 2 3 4.88 2.62 -17 2 2 21.38 4.42 -17 2 1 0.96 1.90 17 -2 -1 3.71 3.39 -17 2 0 15.17 3.57 17 -2 0 11.83 4.94 -17 2 -1 6.59 2.57 17 -2 1 6.19 3.96 17 -2 2 -1.06 3.20 17 -2 3 6.51 4.18 17 -2 5 31.98 6.35 17 -2 7 0.91 3.05 17 -2 8 1.98 3.31 17 -2 9 3.22 3.40 -17 1 2 8.00 3.10 17 -1 -2 5.63 3.83 -17 1 1 3.06 2.23 17 -1 -1 6.02 4.11 -17 1 0 4.92 2.52 17 -1 0 10.58 4.89 -17 1 -1 -0.48 2.15 17 -1 1 2.19 3.50 -17 1 -2 23.46 4.43 17 -1 2 51.69 9.38 17 -1 3 35.24 8.24 17 -1 6 3.06 2.81 17 -1 8 24.75 6.26 17 -1 9 -1.00 3.16 -17 0 2 -1.12 2.21 17 0 -2 1.03 3.75 -17 0 1 7.00 3.05 17 0 -1 10.96 5.06 -17 0 0 1.57 2.22 17 0 0 -1.14 3.84 -17 0 -1 3.07 2.18 17 0 1 -1.18 3.76 -17 0 -2 -0.50 1.86 17 0 2 -1.20 3.39 17 0 7 3.82 2.92 17 0 9 0.92 3.07 17 0 10 1.00 2.98 17 1 -2 3.40 3.57 -17 -1 1 16.46 4.22 17 1 -1 20.31 6.61 -17 -1 0 2.77 2.64 17 1 0 8.70 5.27 -17 -1 -1 -1.10 2.47 17 1 1 1.28 4.29 -17 -1 -2 -0.54 2.31 17 1 8 0.77 2.30 17 1 9 2.54 3.58 17 1 10 0.93 2.93 17 1 11 -1.01 3.01 -17 -2 0 10.56 3.78 -17 -2 -1 27.31 5.35 -17 -2 -2 6.39 3.04 17 2 10 34.02 6.77 17 2 11 6.69 3.77 -17 -3 -1 5.53 3.08 -17 -3 -2 -0.61 2.36 -17 -4 -2 1.94 2.84 -18 -1 -1 -0.60 2.17 -18 -2 -2 0.62 2.35 0 0 0 0.00 0.00 TITL Sjcm19ar19a_12_190_00 in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 11.832619 12.351096 13.991044 82.7902 77.2467 89.2509 ZERR 2.00 0.000223 0.000270 0.000302 0.0018 0.0017 0.0017 LATT 1 SFAC C H N O F S Fe I UNIT 80.00 80.00 10.00 4.00 6.00 2.00 2.00 6.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 43057 _olex2_exptl_crystal_mounting_method 'Paratone oil' _olex2_submission_original_sample_id Sjcm19ar19a_12_190_00 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 4.194 _oxdiff_exptl_absorpt_empirical_full_min 0.521 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I -0.08284(2) 0.23751(2) 0.38567(2) 0.03563(8) Uani 1 1 d . . . . . I3 I 0.28372(2) 0.05515(2) 0.60494(2) 0.04352(9) Uani 1 1 d . . . . . I2 I -0.00858(3) 0.42819(3) 0.74441(2) 0.05102(10) Uani 1 1 d . . . . . Fe04 Fe 0.51488(4) 0.36430(4) 0.78944(3) 0.02055(10) Uani 1 1 d . . . . . S1 S -0.20118(11) 0.29110(11) 0.19643(8) 0.0493(3) Uani 1 1 d . . . . . F3 F 0.1187(2) 0.0883(2) 0.45043(17) 0.0407(5) Uani 1 1 d . . . . . O1 O 0.62870(19) 0.4719(2) 0.73545(17) 0.0246(5) Uani 1 1 d . . . . . F1 F -0.1058(2) 0.3840(2) 0.55883(19) 0.0458(6) Uani 1 1 d . . . . . O3 O 0.59195(19) 0.3100(2) 0.88846(17) 0.0257(5) Uani 1 1 d . . . . . F2 F 0.1870(2) 0.2517(2) 0.71776(19) 0.0485(6) Uani 1 1 d . . . . . O4 O 0.9686(2) 0.0392(2) 0.8758(2) 0.0365(6) Uani 1 1 d . . . . . N3 N 0.5970(2) 0.2719(2) 0.6950(2) 0.0216(6) Uani 1 1 d . . . . . O2 O 0.6935(2) 0.8748(2) 0.8469(2) 0.0377(6) Uani 1 1 d . . . . . N4 N 0.4326(2) 0.4102(2) 0.6822(2) 0.0242(6) Uani 1 1 d . . . . . N2 N 0.3863(2) 0.2577(2) 0.8476(2) 0.0227(6) Uani 1 1 d . . . . . N1 N 0.4228(2) 0.4542(2) 0.8803(2) 0.0230(6) Uani 1 1 d . . . . . C25 C 0.6867(3) 0.2138(3) 0.7052(2) 0.0223(7) Uani 1 1 d . . . . . H25 H 0.723711 0.177119 0.651227 0.027 Uiso 1 1 calc R U . . . C23 C 0.8296(3) 0.1303(3) 0.7890(3) 0.0256(7) Uani 1 1 d . . . . . H23 H 0.861257 0.098134 0.730894 0.031 Uiso 1 1 calc R U . . . C18 C 0.6847(3) 0.2480(3) 0.8774(2) 0.0222(7) Uani 1 1 d . . . . . C34 C 0.4663(3) 0.3536(3) 0.6028(2) 0.0216(7) Uani 1 1 d . . . . . C7 C 0.5611(3) 0.6040(3) 0.8496(2) 0.0232(7) Uani 1 1 d . . . . . C24 C 0.7336(3) 0.2010(3) 0.7906(2) 0.0232(7) Uani 1 1 d . . . . . C8 C 0.4562(3) 0.5475(3) 0.8999(2) 0.0229(7) Uani 1 1 d . . . . . H8 H 0.407218 0.580229 0.951491 0.027 Uiso 1 1 calc R U . . . C19 C 0.7375(3) 0.2236(3) 0.9591(3) 0.0269(7) Uani 1 1 d . . . . . H19 H 0.707167 0.254434 1.018253 0.032 Uiso 1 1 calc R U . . . C9 C 0.3128(3) 0.4091(3) 0.9299(2) 0.0235(7) Uani 1 1 d . . . . . C17 C 0.2974(3) 0.3005(3) 0.9118(2) 0.0234(7) Uani 1 1 d . . . . . C26 C 0.5542(3) 0.2760(3) 0.6077(2) 0.0246(7) Uani 1 1 d . . . . . C21 C 0.8772(3) 0.1079(3) 0.8699(3) 0.0264(7) Uani 1 1 d . . . . . C6 C 0.5779(3) 0.7077(3) 0.8773(3) 0.0273(7) Uani 1 1 d . . . . . H6 H 0.523758 0.733428 0.930094 0.033 Uiso 1 1 calc R U . . . C16 C 0.3765(3) 0.1550(3) 0.8316(3) 0.0280(7) Uani 1 1 d . . . . . H16 H 0.437779 0.124922 0.787154 0.034 Uiso 1 1 calc R U . . . C1 C 0.6417(3) 0.5633(3) 0.7717(2) 0.0238(7) Uani 1 1 d . . . . . C20 C 0.8307(3) 0.1570(3) 0.9548(3) 0.0289(8) Uani 1 1 d . . . . . H20 H 0.864831 0.143493 1.010469 0.035 Uiso 1 1 calc R U . . . C13 C 0.1951(3) 0.2406(3) 0.9584(3) 0.0271(7) Uani 1 1 d . . . . . C27 C 0.5889(3) 0.2134(3) 0.5317(3) 0.0310(8) Uani 1 1 d . . . . . H27 H 0.646321 0.159464 0.535285 0.037 Uiso 1 1 calc R U . . . C4 C 0.6725(3) 0.7715(3) 0.8282(3) 0.0290(8) Uani 1 1 d . . . . . C2 C 0.7410(3) 0.6293(3) 0.7266(3) 0.0286(8) Uani 1 1 d . . . . . H2 H 0.798676 0.603412 0.676273 0.034 Uiso 1 1 calc R U . . . C33 C 0.3526(3) 0.4858(3) 0.6789(3) 0.0285(7) Uani 1 1 d . . . . . H33 H 0.328642 0.525441 0.733729 0.034 Uiso 1 1 calc R U . . . C12 C 0.1061(3) 0.2940(3) 1.0202(3) 0.0313(8) Uani 1 1 d . . . . . H12 H 0.036096 0.256039 1.052439 0.038 Uiso 1 1 calc R U . . . C30 C 0.4170(3) 0.3714(3) 0.5184(3) 0.0281(7) Uani 1 1 d . . . . . C28 C 0.5388(3) 0.2300(3) 0.4491(3) 0.0341(8) Uani 1 1 d . . . . . H28 H 0.562719 0.186409 0.397117 0.041 Uiso 1 1 calc R U . . . C36 C 0.0051(3) 0.2375(3) 0.5010(3) 0.0322(8) Uani 1 1 d . . . . . C32 C 0.3020(3) 0.5093(3) 0.5964(3) 0.0322(8) Uani 1 1 d . . . . . H32 H 0.245897 0.565062 0.595943 0.039 Uiso 1 1 calc R U . . . C41 C 0.0931(3) 0.1650(3) 0.5123(3) 0.0325(8) Uani 1 1 d . . . . . C38 C 0.0388(3) 0.3194(3) 0.6414(3) 0.0342(8) Uani 1 1 d . . . . . C10 C 0.2242(3) 0.4585(3) 0.9893(3) 0.0299(8) Uani 1 1 d . . . . . H10 H 0.232556 0.531902 1.000574 0.036 Uiso 1 1 calc R U . . . N5 N -0.3741(4) 0.1278(4) 0.2305(3) 0.0571(11) Uani 1 1 d . . . . . C3 C 0.7550(3) 0.7296(3) 0.7545(3) 0.0310(8) Uani 1 1 d . . . . . H3 H 0.822552 0.771863 0.723162 0.037 Uiso 1 1 calc R U . . . C37 C -0.0195(3) 0.3131(3) 0.5671(3) 0.0334(8) Uani 1 1 d . . . . . C11 C 0.1213(3) 0.3996(3) 1.0331(3) 0.0332(8) Uani 1 1 d . . . . . H11 H 0.060102 0.434795 1.073230 0.040 Uiso 1 1 calc R U . . . C29 C 0.4568(3) 0.3071(3) 0.4416(3) 0.0325(8) Uani 1 1 d . . . . . H29 H 0.426101 0.317657 0.383901 0.039 Uiso 1 1 calc R U . . . C35 C -0.3019(4) 0.1953(4) 0.2158(3) 0.0450(11) Uani 1 1 d . . . . . C15 C 0.2796(3) 0.0893(3) 0.8776(3) 0.0324(8) Uani 1 1 d . . . . . H15 H 0.276775 0.015601 0.865349 0.039 Uiso 1 1 calc R U . . . C14 C 0.1894(3) 0.1310(3) 0.9399(3) 0.0319(8) Uani 1 1 d . . . . . H14 H 0.123120 0.086845 0.970737 0.038 Uiso 1 1 calc R U . . . C40 C 0.1569(3) 0.1677(3) 0.5842(3) 0.0332(8) Uani 1 1 d . . . . . C31 C 0.3326(3) 0.4532(3) 0.5181(3) 0.0326(8) Uani 1 1 d . . . . . H31 H 0.297573 0.468624 0.463058 0.039 Uiso 1 1 calc R U . . . C39 C 0.1273(3) 0.2474(3) 0.6467(3) 0.0350(9) Uani 1 1 d . . . . . C5 C 0.6002(4) 0.9264(3) 0.9048(3) 0.0373(9) Uani 1 1 d . . . . . H5A H 0.532837 0.926714 0.874624 0.056 Uiso 1 1 calc R U . . . H5B H 0.622581 1.001610 0.908289 0.056 Uiso 1 1 calc R U . . . H5C H 0.580385 0.886495 0.971509 0.056 Uiso 1 1 calc R U . . . C22 C 0.9975(3) -0.0314(3) 0.8020(3) 0.0372(9) Uani 1 1 d . . . . . H22A H 1.022414 0.012007 0.737180 0.056 Uiso 1 1 calc R U . . . H22B H 0.929436 -0.075972 0.802274 0.056 Uiso 1 1 calc R U . . . H22C H 1.060461 -0.079084 0.815391 0.056 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.02814(13) 0.04144(16) 0.03880(15) -0.00868(11) -0.00876(10) 0.00477(10) I3 0.03718(15) 0.03482(16) 0.0613(2) -0.00267(13) -0.01884(13) 0.00619(11) I2 0.05814(19) 0.04466(18) 0.05202(19) -0.02012(14) -0.00819(14) 0.00272(14) Fe04 0.0208(2) 0.0218(2) 0.0193(2) -0.00448(18) -0.00416(17) 0.00297(18) S1 0.0568(7) 0.0579(7) 0.0371(6) -0.0141(5) -0.0150(5) 0.0222(6) F3 0.0450(13) 0.0396(13) 0.0400(13) -0.0127(10) -0.0108(10) 0.0103(10) O1 0.0218(11) 0.0300(13) 0.0216(11) -0.0055(10) -0.0028(9) 0.0018(10) F1 0.0424(13) 0.0462(15) 0.0536(15) -0.0138(12) -0.0176(11) 0.0179(11) O3 0.0262(12) 0.0324(14) 0.0200(11) -0.0070(10) -0.0064(9) 0.0060(10) F2 0.0597(16) 0.0433(15) 0.0517(15) -0.0072(12) -0.0310(13) 0.0024(12) O4 0.0322(13) 0.0385(16) 0.0442(16) -0.0081(13) -0.0189(12) 0.0108(11) N3 0.0231(13) 0.0233(14) 0.0182(13) -0.0028(11) -0.0040(10) 0.0019(11) O2 0.0346(14) 0.0296(15) 0.0467(17) -0.0085(12) -0.0014(12) -0.0097(12) N4 0.0219(13) 0.0260(16) 0.0250(14) -0.0029(12) -0.0063(11) 0.0000(11) N2 0.0247(13) 0.0233(15) 0.0215(13) -0.0055(11) -0.0069(11) 0.0008(11) N1 0.0219(13) 0.0239(15) 0.0219(14) -0.0027(11) -0.0023(11) 0.0015(11) C25 0.0225(15) 0.0243(17) 0.0210(15) -0.0082(13) -0.0039(12) 0.0060(13) C23 0.0221(16) 0.0273(18) 0.0273(17) -0.0063(14) -0.0037(13) 0.0045(13) C18 0.0225(15) 0.0252(17) 0.0203(15) -0.0031(13) -0.0072(12) -0.0024(13) C34 0.0202(15) 0.0217(17) 0.0222(16) -0.0010(13) -0.0042(12) -0.0013(12) C7 0.0210(15) 0.0252(17) 0.0235(16) -0.0017(13) -0.0058(12) 0.0012(13) C24 0.0202(15) 0.0257(18) 0.0241(16) -0.0039(13) -0.0056(13) 0.0016(13) C8 0.0246(16) 0.0225(17) 0.0201(15) -0.0038(13) -0.0010(12) 0.0012(13) C19 0.0317(18) 0.0298(19) 0.0223(16) -0.0055(14) -0.0113(14) 0.0020(15) C9 0.0211(15) 0.0256(17) 0.0233(16) -0.0042(13) -0.0033(12) -0.0002(13) C17 0.0261(16) 0.0247(17) 0.0210(16) -0.0033(13) -0.0085(13) 0.0041(13) C26 0.0245(16) 0.0302(19) 0.0195(15) -0.0042(14) -0.0051(13) 0.0004(14) C21 0.0216(16) 0.0274(19) 0.0317(18) -0.0035(15) -0.0093(14) 0.0016(13) C6 0.0259(17) 0.0282(19) 0.0273(17) -0.0031(14) -0.0052(14) 0.0007(14) C16 0.0329(18) 0.0258(18) 0.0258(17) -0.0060(14) -0.0062(14) 0.0010(14) C1 0.0210(15) 0.0278(18) 0.0238(16) -0.0020(14) -0.0081(13) 0.0017(13) C20 0.0303(18) 0.036(2) 0.0239(17) -0.0010(15) -0.0145(14) -0.0019(15) C13 0.0266(17) 0.0301(19) 0.0256(17) -0.0021(14) -0.0082(14) -0.0035(14) C27 0.0350(19) 0.034(2) 0.0262(18) -0.0079(15) -0.0104(15) 0.0058(16) C4 0.0264(17) 0.0283(19) 0.0336(19) -0.0036(15) -0.0095(15) -0.0039(14) C2 0.0207(16) 0.040(2) 0.0239(17) -0.0043(15) -0.0013(13) -0.0006(15) C33 0.0286(17) 0.0269(19) 0.0293(18) -0.0019(15) -0.0059(14) 0.0032(14) C12 0.0224(16) 0.036(2) 0.0336(19) -0.0084(16) -0.0003(14) -0.0040(15) C30 0.0280(17) 0.033(2) 0.0231(17) -0.0003(14) -0.0066(14) -0.0019(15) C28 0.044(2) 0.039(2) 0.0222(17) -0.0109(16) -0.0083(15) 0.0039(17) C36 0.0281(18) 0.035(2) 0.033(2) -0.0031(16) -0.0066(15) -0.0013(15) C32 0.0282(18) 0.032(2) 0.035(2) 0.0011(16) -0.0095(15) 0.0064(15) C41 0.0337(19) 0.029(2) 0.034(2) -0.0035(16) -0.0048(16) 0.0000(16) C38 0.039(2) 0.028(2) 0.037(2) -0.0088(16) -0.0065(16) -0.0016(16) C10 0.0267(17) 0.0291(19) 0.0326(19) -0.0087(15) -0.0009(14) 0.0000(14) N5 0.072(3) 0.059(3) 0.046(2) -0.023(2) -0.018(2) 0.023(2) C3 0.0227(16) 0.036(2) 0.0331(19) -0.0028(16) -0.0048(14) -0.0081(15) C37 0.0285(18) 0.029(2) 0.041(2) -0.0019(16) -0.0058(16) 0.0021(15) C11 0.0262(17) 0.037(2) 0.034(2) -0.0091(17) 0.0011(15) 0.0002(15) C29 0.038(2) 0.038(2) 0.0235(17) -0.0023(15) -0.0115(15) -0.0005(16) C35 0.064(3) 0.051(3) 0.026(2) -0.0185(19) -0.019(2) 0.035(2) C15 0.040(2) 0.0237(19) 0.035(2) -0.0035(15) -0.0115(16) -0.0075(15) C14 0.0322(19) 0.030(2) 0.034(2) -0.0012(16) -0.0101(15) -0.0094(15) C40 0.0299(18) 0.030(2) 0.040(2) 0.0004(16) -0.0093(16) 0.0016(15) C31 0.0343(19) 0.038(2) 0.0284(18) -0.0002(16) -0.0154(15) 0.0028(16) C39 0.037(2) 0.034(2) 0.036(2) 0.0011(17) -0.0135(16) 0.0012(16) C5 0.044(2) 0.025(2) 0.043(2) -0.0073(17) -0.0076(18) -0.0047(17) C22 0.034(2) 0.040(2) 0.039(2) -0.0072(18) -0.0088(16) 0.0138(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Fe04 O3 92.48(10) . . ? O1 Fe04 N3 88.11(11) . . ? O1 Fe04 N4 90.28(11) . . ? O1 Fe04 N2 176.23(11) . . ? O1 Fe04 N1 94.51(11) . . ? O3 Fe04 N3 94.03(11) . . ? O3 Fe04 N4 175.62(12) . . ? O3 Fe04 N2 89.66(11) . . ? O3 Fe04 N1 89.13(11) . . ? N3 Fe04 N4 82.64(12) . . ? N3 Fe04 N2 94.84(11) . . ? N4 Fe04 N2 87.78(11) . . ? N1 Fe04 N3 175.80(12) . . ? N1 Fe04 N4 94.05(12) . . ? N1 Fe04 N2 82.41(12) . . ? C1 O1 Fe04 126.0(2) . . ? C18 O3 Fe04 126.3(2) . . ? C21 O4 C22 116.5(3) . . ? C25 N3 Fe04 125.3(2) . . ? C25 N3 C26 120.5(3) . . ? C26 N3 Fe04 114.1(2) . . ? C4 O2 C5 116.5(3) . . ? C34 N4 Fe04 112.8(2) . . ? C33 N4 Fe04 128.7(2) . . ? C33 N4 C34 118.5(3) . . ? C17 N2 Fe04 112.9(2) . . ? C16 N2 Fe04 128.8(2) . . ? C16 N2 C17 118.3(3) . . ? C8 N1 Fe04 125.2(2) . . ? C8 N1 C9 120.1(3) . . ? C9 N1 Fe04 114.7(2) . . ? N3 C25 H25 117.5 . . ? N3 C25 C24 125.0(3) . . ? C24 C25 H25 117.5 . . ? C24 C23 H23 119.5 . . ? C21 C23 H23 119.5 . . ? C21 C23 C24 121.1(3) . . ? O3 C18 C24 124.8(3) . . ? O3 C18 C19 118.0(3) . . ? C24 C18 C19 117.2(3) . . ? N4 C34 C26 116.9(3) . . ? N4 C34 C30 122.5(3) . . ? C26 C34 C30 120.6(3) . . ? C6 C7 C8 116.1(3) . . ? C6 C7 C1 120.8(3) . . ? C1 C7 C8 123.0(3) . . ? C25 C24 C23 116.6(3) . . ? C18 C24 C25 123.3(3) . . ? C18 C24 C23 119.9(3) . . ? N1 C8 C7 124.7(3) . . ? N1 C8 H8 117.6 . . ? C7 C8 H8 117.6 . . ? C18 C19 H19 119.2 . . ? C20 C19 C18 121.5(3) . . ? C20 C19 H19 119.2 . . ? C17 C9 N1 112.8(3) . . ? C10 C9 N1 127.8(3) . . ? C10 C9 C17 119.3(3) . . ? N2 C17 C9 116.7(3) . . ? N2 C17 C13 122.4(3) . . ? C13 C17 C9 120.9(3) . . ? C34 C26 N3 113.3(3) . . ? C27 C26 N3 127.0(3) . . ? C27 C26 C34 119.7(3) . . ? O4 C21 C20 115.9(3) . . ? C23 C21 O4 125.1(3) . . ? C23 C21 C20 118.9(3) . . ? C7 C6 H6 119.9 . . ? C4 C6 C7 120.3(3) . . ? C4 C6 H6 119.9 . . ? N2 C16 H16 118.7 . . ? N2 C16 C15 122.6(3) . . ? C15 C16 H16 118.7 . . ? O1 C1 C7 125.1(3) . . ? O1 C1 C2 117.8(3) . . ? C2 C1 C7 117.0(3) . . ? C19 C20 C21 121.4(3) . . ? C19 C20 H20 119.3 . . ? C21 C20 H20 119.3 . . ? C17 C13 C12 118.0(3) . . ? C17 C13 C14 117.1(3) . . ? C14 C13 C12 125.0(3) . . ? C26 C27 H27 120.2 . . ? C26 C27 C28 119.5(3) . . ? C28 C27 H27 120.2 . . ? O2 C4 C6 124.5(3) . . ? O2 C4 C3 116.5(3) . . ? C6 C4 C3 119.0(3) . . ? C1 C2 H2 119.5 . . ? C3 C2 C1 121.0(3) . . ? C3 C2 H2 119.5 . . ? N4 C33 H33 119.0 . . ? N4 C33 C32 122.0(3) . . ? C32 C33 H33 119.0 . . ? C13 C12 H12 120.1 . . ? C11 C12 C13 119.9(3) . . ? C11 C12 H12 120.1 . . ? C29 C30 C34 117.7(3) . . ? C29 C30 C31 125.3(3) . . ? C31 C30 C34 117.0(3) . . ? C27 C28 H28 119.2 . . ? C29 C28 C27 121.6(3) . . ? C29 C28 H28 119.2 . . ? C41 C36 I1 122.1(3) . . ? C37 C36 I1 121.1(3) . . ? C37 C36 C41 116.7(4) . . ? C33 C32 H32 119.8 . . ? C31 C32 C33 120.5(3) . . ? C31 C32 H32 119.8 . . ? F3 C41 C36 118.7(3) . . ? F3 C41 C40 118.2(3) . . ? C36 C41 C40 123.1(4) . . ? C37 C38 I2 121.8(3) . . ? C39 C38 I2 121.1(3) . . ? C39 C38 C37 117.0(4) . . ? C9 C10 H10 120.3 . . ? C9 C10 C11 119.5(3) . . ? C11 C10 H10 120.3 . . ? C4 C3 H3 119.1 . . ? C2 C3 C4 121.7(3) . . ? C2 C3 H3 119.1 . . ? F1 C37 C36 118.1(4) . . ? F1 C37 C38 118.5(4) . . ? C38 C37 C36 123.4(4) . . ? C12 C11 C10 122.3(3) . . ? C12 C11 H11 118.8 . . ? C10 C11 H11 118.8 . . ? C30 C29 H29 119.6 . . ? C28 C29 C30 120.8(3) . . ? C28 C29 H29 119.6 . . ? N5 C35 S1 179.3(4) . . ? C16 C15 H15 120.0 . . ? C14 C15 C16 120.0(3) . . ? C14 C15 H15 120.0 . . ? C13 C14 H14 120.2 . . ? C15 C14 C13 119.6(3) . . ? C15 C14 H14 120.2 . . ? C41 C40 I3 123.1(3) . . ? C41 C40 C39 116.3(3) . . ? C39 C40 I3 120.5(3) . . ? C30 C31 H31 120.2 . . ? C32 C31 C30 119.6(3) . . ? C32 C31 H31 120.2 . . ? F2 C39 C38 118.7(4) . . ? F2 C39 C40 117.8(3) . . ? C38 C39 C40 123.4(4) . . ? O2 C5 H5A 109.5 . . ? O2 C5 H5B 109.5 . . ? O2 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? O4 C22 H22A 109.5 . . ? O4 C22 H22B 109.5 . . ? O4 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 C36 2.104(4) . ? I3 C40 2.076(4) . ? I2 C38 2.075(4) . ? Fe04 O1 1.870(2) . ? Fe04 O3 1.873(2) . ? Fe04 N3 1.943(3) . ? Fe04 N4 1.985(3) . ? Fe04 N2 1.987(3) . ? Fe04 N1 1.936(3) . ? S1 C35 1.645(6) . ? F3 C41 1.349(4) . ? O1 C1 1.318(4) . ? F1 C37 1.351(4) . ? O3 C18 1.321(4) . ? F2 C39 1.347(5) . ? O4 C21 1.377(4) . ? O4 C22 1.416(5) . ? N3 C25 1.297(4) . ? N3 C26 1.417(4) . ? O2 C4 1.371(4) . ? O2 C5 1.413(5) . ? N4 C34 1.368(4) . ? N4 C33 1.325(4) . ? N2 C17 1.371(4) . ? N2 C16 1.326(4) . ? N1 C8 1.303(4) . ? N1 C9 1.418(4) . ? C25 H25 0.9500 . ? C25 C24 1.416(5) . ? C23 H23 0.9500 . ? C23 C24 1.421(5) . ? C23 C21 1.368(5) . ? C18 C24 1.416(5) . ? C18 C19 1.419(4) . ? C34 C26 1.412(5) . ? C34 C30 1.422(5) . ? C7 C8 1.427(5) . ? C7 C6 1.413(5) . ? C7 C1 1.419(5) . ? C8 H8 0.9500 . ? C19 H19 0.9500 . ? C19 C20 1.362(5) . ? C9 C17 1.417(5) . ? C9 C10 1.373(5) . ? C17 C13 1.411(5) . ? C26 C27 1.379(5) . ? C21 C20 1.402(5) . ? C6 H6 0.9500 . ? C6 C4 1.376(5) . ? C16 H16 0.9500 . ? C16 C15 1.398(5) . ? C1 C2 1.418(5) . ? C20 H20 0.9500 . ? C13 C12 1.419(5) . ? C13 C14 1.414(5) . ? C27 H27 0.9500 . ? C27 C28 1.404(5) . ? C4 C3 1.400(5) . ? C2 H2 0.9500 . ? C2 C3 1.367(5) . ? C33 H33 0.9500 . ? C33 C32 1.412(5) . ? C12 H12 0.9500 . ? C12 C11 1.358(5) . ? C30 C29 1.410(5) . ? C30 C31 1.411(5) . ? C28 H28 0.9500 . ? C28 C29 1.362(5) . ? C36 C41 1.387(5) . ? C36 C37 1.380(6) . ? C32 H32 0.9500 . ? C32 C31 1.349(5) . ? C41 C40 1.388(5) . ? C38 C37 1.378(6) . ? C38 C39 1.374(5) . ? C10 H10 0.9500 . ? C10 C11 1.403(5) . ? N5 C35 1.169(6) . ? C3 H3 0.9500 . ? C11 H11 0.9500 . ? C29 H29 0.9500 . ? C15 H15 0.9500 . ? C15 C14 1.361(5) . ? C14 H14 0.9500 . ? C40 C39 1.389(6) . ? C31 H31 0.9500 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag I1 C36 C41 F3 -3.6(5) . . . . ? I1 C36 C41 C40 176.0(3) . . . . ? I1 C36 C37 F1 3.3(5) . . . . ? I1 C36 C37 C38 -177.3(3) . . . . ? I3 C40 C39 F2 2.9(5) . . . . ? I3 C40 C39 C38 -175.3(3) . . . . ? I2 C38 C37 F1 3.4(5) . . . . ? I2 C38 C37 C36 -176.0(3) . . . . ? I2 C38 C39 F2 -3.0(5) . . . . ? I2 C38 C39 C40 175.2(3) . . . . ? Fe04 O1 C1 C7 -10.1(5) . . . . ? Fe04 O1 C1 C2 173.0(2) . . . . ? Fe04 O3 C18 C24 -8.1(5) . . . . ? Fe04 O3 C18 C19 174.0(2) . . . . ? Fe04 N3 C25 C24 5.6(5) . . . . ? Fe04 N3 C26 C34 5.1(4) . . . . ? Fe04 N3 C26 C27 -174.6(3) . . . . ? Fe04 N4 C34 C26 -1.8(4) . . . . ? Fe04 N4 C34 C30 178.6(3) . . . . ? Fe04 N4 C33 C32 179.9(3) . . . . ? Fe04 N2 C17 C9 -2.9(4) . . . . ? Fe04 N2 C17 C13 177.3(3) . . . . ? Fe04 N2 C16 C15 -179.4(3) . . . . ? Fe04 N1 C8 C7 7.2(5) . . . . ? Fe04 N1 C9 C17 7.1(4) . . . . ? Fe04 N1 C9 C10 -171.9(3) . . . . ? F3 C41 C40 I3 -3.1(5) . . . . ? F3 C41 C40 C39 -179.6(3) . . . . ? O1 Fe04 O3 C18 -76.5(3) . . . . ? O1 C1 C2 C3 174.2(3) . . . . ? O3 Fe04 O1 C1 -76.6(3) . . . . ? O3 C18 C24 C25 -1.1(5) . . . . ? O3 C18 C24 C23 -176.3(3) . . . . ? O3 C18 C19 C20 177.5(3) . . . . ? O4 C21 C20 C19 -177.7(3) . . . . ? N3 Fe04 O1 C1 -170.6(3) . . . . ? N3 Fe04 O3 C18 11.8(3) . . . . ? N3 C25 C24 C23 177.6(3) . . . . ? N3 C25 C24 C18 2.2(6) . . . . ? N3 C26 C27 C28 -178.5(3) . . . . ? O2 C4 C3 C2 -177.2(3) . . . . ? N4 Fe04 O1 C1 106.8(3) . . . . ? N4 C34 C26 N3 -2.1(4) . . . . ? N4 C34 C26 C27 177.6(3) . . . . ? N4 C34 C30 C29 -178.9(3) . . . . ? N4 C34 C30 C31 1.7(5) . . . . ? N4 C33 C32 C31 1.2(6) . . . . ? N2 Fe04 O3 C18 106.6(3) . . . . ? N2 C17 C13 C12 -177.3(3) . . . . ? N2 C17 C13 C14 2.9(5) . . . . ? N2 C16 C15 C14 1.5(6) . . . . ? N1 Fe04 O1 C1 12.7(3) . . . . ? N1 Fe04 O3 C18 -171.0(3) . . . . ? N1 C9 C17 N2 -2.7(4) . . . . ? N1 C9 C17 C13 177.2(3) . . . . ? N1 C9 C10 C11 -179.3(3) . . . . ? C25 N3 C26 C34 -172.1(3) . . . . ? C25 N3 C26 C27 8.2(5) . . . . ? C23 C21 C20 C19 1.9(5) . . . . ? C18 C19 C20 C21 -1.2(6) . . . . ? C34 N4 C33 C32 -0.1(5) . . . . ? C34 C26 C27 C28 1.9(5) . . . . ? C34 C30 C29 C28 0.7(5) . . . . ? C34 C30 C31 C32 -0.5(5) . . . . ? C7 C6 C4 O2 177.1(3) . . . . ? C7 C6 C4 C3 -3.8(5) . . . . ? C7 C1 C2 C3 -2.9(5) . . . . ? C24 C23 C21 O4 178.8(3) . . . . ? C24 C23 C21 C20 -0.8(5) . . . . ? C24 C18 C19 C20 -0.6(5) . . . . ? C8 N1 C9 C17 -170.7(3) . . . . ? C8 N1 C9 C10 10.3(5) . . . . ? C8 C7 C6 C4 -175.5(3) . . . . ? C8 C7 C1 O1 1.7(5) . . . . ? C8 C7 C1 C2 178.5(3) . . . . ? C19 C18 C24 C25 176.8(3) . . . . ? C19 C18 C24 C23 1.6(5) . . . . ? C9 N1 C8 C7 -175.2(3) . . . . ? C9 C17 C13 C12 2.9(5) . . . . ? C9 C17 C13 C14 -177.0(3) . . . . ? C9 C10 C11 C12 1.0(6) . . . . ? C17 N2 C16 C15 -0.1(5) . . . . ? C17 C9 C10 C11 1.7(5) . . . . ? C17 C13 C12 C11 -0.2(5) . . . . ? C17 C13 C14 C15 -1.4(5) . . . . ? C26 N3 C25 C24 -177.5(3) . . . . ? C26 C34 C30 C29 1.6(5) . . . . ? C26 C34 C30 C31 -177.8(3) . . . . ? C26 C27 C28 C29 0.4(6) . . . . ? C21 C23 C24 C25 -176.5(3) . . . . ? C21 C23 C24 C18 -1.0(5) . . . . ? C6 C7 C8 N1 175.8(3) . . . . ? C6 C7 C1 O1 -174.3(3) . . . . ? C6 C7 C1 C2 2.6(5) . . . . ? C6 C4 C3 C2 3.5(6) . . . . ? C16 N2 C17 C9 177.7(3) . . . . ? C16 N2 C17 C13 -2.1(5) . . . . ? C16 C15 C14 C13 -0.7(6) . . . . ? C1 C7 C8 N1 -0.3(5) . . . . ? C1 C7 C6 C4 0.7(5) . . . . ? C1 C2 C3 C4 -0.1(6) . . . . ? C13 C12 C11 C10 -1.7(6) . . . . ? C27 C28 C29 C30 -1.7(6) . . . . ? C33 N4 C34 C26 178.2(3) . . . . ? C33 N4 C34 C30 -1.3(5) . . . . ? C33 C32 C31 C30 -0.8(6) . . . . ? C12 C13 C14 C15 178.7(4) . . . . ? C30 C34 C26 N3 177.4(3) . . . . ? C30 C34 C26 C27 -2.9(5) . . . . ? C36 C41 C40 I3 177.3(3) . . . . ? C36 C41 C40 C39 0.8(6) . . . . ? C41 C36 C37 F1 -179.1(3) . . . . ? C41 C36 C37 C38 0.3(6) . . . . ? C41 C40 C39 F2 179.5(3) . . . . ? C41 C40 C39 C38 1.3(6) . . . . ? C10 C9 C17 N2 176.5(3) . . . . ? C10 C9 C17 C13 -3.7(5) . . . . ? C37 C36 C41 F3 178.8(3) . . . . ? C37 C36 C41 C40 -1.6(6) . . . . ? C37 C38 C39 F2 179.4(3) . . . . ? C37 C38 C39 C40 -2.5(6) . . . . ? C29 C30 C31 C32 -179.9(4) . . . . ? C14 C13 C12 C11 179.6(4) . . . . ? C31 C30 C29 C28 -180.0(4) . . . . ? C39 C38 C37 F1 -179.0(3) . . . . ? C39 C38 C37 C36 1.6(6) . . . . ? C5 O2 C4 C6 -14.1(5) . . . . ? C5 O2 C4 C3 166.8(3) . . . . ? C22 O4 C21 C23 -15.0(5) . . . . ? C22 O4 C21 C20 164.6(3) . . . . ?