#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/34/2203432.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203432_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Luboradzki, Roman' 'Pakulski, Zbigniew' _publ_section_title ; (5-Methoxycarbonyl)pentyl \a-D-mannopyranoside ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o666 _journal_page_last o668 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1390 _cell_length_b 7.2320 _cell_length_c 33.9220 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.8811 _[local]_cod_data_source_file fl6092Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zp11_7 MERG4 run (regenerated PLATON/CIF) 19 MAR 2004' _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3324.82 3217.69 72.73 o 4 0 0 97.60 102.65 11.10 o 6 0 0 201.14 156.85 12.54 o 1 1 0 656.91 552.24 11.03 o 2 1 0 309.22 290.44 5.33 o 3 1 0 414.61 445.53 11.88 o 4 1 0 267.14 304.48 18.55 o 5 1 0 32.83 29.09 5.57 o 6 1 0 13.78 23.20 9.05 o 1 2 0 47.10 51.29 3.35 o 2 2 0 0.91 4.86 1.93 o 3 2 0 2299.86 2169.44 50.97 o 4 2 0 154.46 154.89 6.23 o 5 2 0 87.56 76.39 16.40 o 6 2 0 10.06 30.12 12.52 o 1 3 0 59.66 58.70 2.88 o 2 3 0 16.61 17.55 2.62 o 3 3 0 0.00 3.64 3.40 o 4 3 0 7.14 12.93 4.16 o 5 3 0 161.64 148.73 16.40 o 6 3 0 36.71 55.61 30.09 o 0 4 0 305.39 360.29 36.79 o 1 4 0 17.03 15.89 2.25 o 2 4 0 603.05 659.11 20.88 o 3 4 0 461.86 450.83 13.93 o 4 4 0 81.39 88.59 6.48 o 5 4 0 156.13 172.91 53.85 o 6 4 0 72.81 115.04 49.97 o 1 5 0 145.43 145.70 5.67 o 2 5 0 0.91 5.87 4.40 o 3 5 0 694.34 656.69 21.63 o 4 5 0 300.84 280.93 12.05 o 5 5 0 59.33 71.28 40.92 o 0 6 0 6419.44 6138.43 267.05 o 1 6 0 13.18 28.09 6.80 o 2 6 0 8.24 12.49 5.87 o 3 6 0 13.91 17.16 11.54 o 4 6 0 17.16 27.60 8.04 o 1 7 0 302.20 374.66 32.07 o 2 7 0 0.02 8.56 9.31 o 3 7 0 108.87 114.70 14.74 o 0 8 0 34.39 21.27 11.54 o 1 8 0 0.00 5.87 12.20 o 1 0 1 1363.95 1212.40 17.43 o 2 0 1 693.35 639.19 12.64 o 3 0 1 908.09 904.94 23.52 o 4 0 1 71.44 78.59 7.77 o 5 0 1 25.19 36.62 11.93 o 6 0 1 7.06 2.20 9.56 o 1 1 1 1985.13 1929.60 26.22 o 2 1 1 4232.21 4235.53 48.19 o 3 1 1 57.82 56.17 1.76 o 4 1 1 45.36 64.61 6.54 o 5 1 1 49.52 52.90 5.81 o 6 1 1 3.81 12.54 11.99 o 0 2 1 9016.12 8521.21 216.49 o 1 2 1 659.65 647.39 12.20 o 2 2 1 391.29 411.32 6.23 o 3 2 1 229.28 238.85 8.01 o 4 2 1 31.36 30.63 2.01 o 5 2 1 156.28 148.34 11.73 o 6 2 1 13.31 18.84 10.61 o 0 3 1 178.06 199.33 12.81 o 1 3 1 8922.70 8907.75 195.12 o 2 3 1 78.78 75.92 2.87 o 3 3 1 43.83 52.18 3.25 o 4 3 1 1.57 8.21 2.61 o 5 3 1 241.53 235.01 21.56 o 6 3 1 1.65 40.82 20.49 o 0 4 1 2923.68 2827.63 86.47 o 1 4 1 143.10 157.44 4.70 o 2 4 1 409.64 419.77 8.82 o 3 4 1 67.07 71.45 3.72 o 4 4 1 1.72 10.84 3.34 o 5 4 1 14.12 64.18 19.88 o 6 4 1 23.97 19.33 13.44 o 0 5 1 183.46 203.78 8.48 o 1 5 1 231.24 244.09 7.83 o 2 5 1 295.23 314.60 7.81 o 3 5 1 5.28 9.16 4.23 o 4 5 1 68.34 61.22 5.33 o 5 5 1 4.46 9.98 13.65 o 0 6 1 57.33 71.02 7.11 o 1 6 1 300.82 288.05 9.76 o 2 6 1 109.66 118.58 6.62 o 3 6 1 112.24 134.46 10.27 o 4 6 1 13.47 22.37 5.44 o 0 7 1 84.57 76.13 10.10 o 1 7 1 94.62 130.01 15.57 o 2 7 1 163.76 152.93 9.01 o 3 7 1 12.06 16.29 10.51 o 0 8 1 35.46 36.23 12.98 o 1 8 1 32.83 46.71 7.12 o 1 0 2 2936.50 2736.91 42.54 o 2 0 2 65.67 68.94 1.81 o 3 0 2 125.11 125.33 4.55 o 4 0 2 462.67 454.16 16.67 o 5 0 2 41.33 72.34 36.69 o 6 0 2 14.32 25.35 11.66 o 0 1 2 2231.37 2064.42 55.42 o 1 1 2 6478.31 6064.42 89.34 o 2 1 2 444.69 427.84 5.70 o 3 1 2 866.70 865.54 12.37 o 4 1 2 172.18 152.90 8.14 o 5 1 2 7.74 10.13 10.12 o 6 1 2 72.24 52.67 29.69 o 0 2 2 7950.53 7551.73 184.79 o 1 2 2 1924.52 1885.53 29.61 o 2 2 2 669.89 673.72 10.60 o 3 2 2 26.16 27.26 2.02 o 4 2 2 93.06 104.99 3.05 o 5 2 2 52.31 59.57 7.44 o 6 2 2 30.00 55.39 24.45 o 0 3 2 718.52 680.97 22.03 o 1 3 2 607.54 617.29 11.57 o 2 3 2 3061.02 3306.00 50.80 o 3 3 2 147.43 154.07 6.02 o 4 3 2 22.77 24.94 3.97 o 5 3 2 53.39 82.12 64.88 o 6 3 2 7.87 6.44 7.71 o 0 4 2 501.86 495.72 13.23 o 1 4 2 524.14 520.92 11.35 o 2 4 2 87.48 97.48 3.26 o 3 4 2 90.92 92.45 4.36 o 4 4 2 84.30 89.44 4.07 o 5 4 2 62.87 100.75 23.15 o 6 4 2 56.67 76.66 21.63 o 0 5 2 923.87 898.37 26.26 o 1 5 2 9.59 15.31 2.06 o 2 5 2 50.61 47.91 10.92 o 3 5 2 10.54 12.22 3.05 o 4 5 2 107.21 106.48 5.81 o 5 5 2 28.50 62.58 18.55 o 0 6 2 2331.88 2226.62 75.24 o 1 6 2 66.91 83.23 5.65 o 2 6 2 67.44 66.91 9.52 o 3 6 2 41.68 49.52 7.85 o 4 6 2 5.46 20.62 5.70 o 0 7 2 11.08 26.13 9.75 o 1 7 2 64.01 108.65 14.58 o 2 7 2 3.84 8.82 4.95 o 3 7 2 181.28 185.39 14.27 o 0 8 2 78.45 65.86 10.15 o 1 8 2 31.17 36.52 8.53 o 1 0 3 7258.08 6745.65 138.68 o 2 0 3 964.71 955.47 14.50 o 3 0 3 349.08 378.30 10.34 o 4 0 3 45.14 60.38 10.93 o 5 0 3 1.60 6.58 22.44 o 6 0 3 4.89 11.20 10.05 o 0 1 3 79.67 90.06 2.96 o 1 1 3 2717.92 2501.24 45.00 o 2 1 3 538.04 560.52 7.05 o 3 1 3 11.07 13.53 0.85 o 4 1 3 35.71 40.40 1.91 o 5 1 3 105.92 97.86 8.50 o 6 1 3 7.41 11.34 6.68 o 0 2 3 1049.93 1018.35 28.94 o 1 2 3 3015.17 2909.90 39.94 o 2 2 3 2003.98 2039.84 31.91 o 3 2 3 97.11 102.25 6.21 o 4 2 3 223.34 230.99 4.86 o 5 2 3 130.81 118.04 6.71 o 6 2 3 5.86 8.56 13.18 o 0 3 3 3.45 36.62 14.01 o 1 3 3 2309.87 2294.92 38.65 o 2 3 3 665.22 656.17 10.14 o 3 3 3 18.88 21.22 3.17 o 4 3 3 134.43 144.58 6.39 o 5 3 3 51.29 59.02 39.26 o 6 3 3 0.24 32.56 20.88 o 0 4 3 363.13 336.35 20.66 o 1 4 3 692.56 750.19 16.58 o 2 4 3 1080.71 1064.58 17.67 o 3 4 3 17.89 16.37 3.56 o 4 4 3 378.82 382.00 9.94 o 5 4 3 189.28 178.61 15.85 o 6 4 3 4.69 187.60 198.72 o 0 5 3 51.36 57.74 8.56 o 1 5 3 372.56 380.96 9.24 o 2 5 3 449.47 480.23 11.63 o 3 5 3 128.57 107.88 5.07 o 4 5 3 28.68 32.34 5.44 o 5 5 3 3.03 46.47 20.90 o 0 6 3 6.33 21.27 9.24 o 1 6 3 611.81 569.12 14.97 o 2 6 3 61.05 60.91 6.73 o 3 6 3 228.36 175.09 13.34 o 4 6 3 78.82 73.85 9.88 o 0 7 3 1.44 3.18 7.58 o 1 7 3 120.12 148.51 18.11 o 2 7 3 43.76 45.21 6.62 o 3 7 3 12.75 15.71 7.98 o 0 8 3 0.59 20.85 12.42 o 1 8 3 209.31 202.18 18.58 o 1 0 4 15.34 14.42 0.95 o 2 0 4 1752.11 1740.12 26.08 o 3 0 4 673.93 708.98 16.65 o 4 0 4 618.48 589.59 28.85 o 5 0 4 39.17 30.80 11.27 o 6 0 4 4.21 13.96 11.81 o 0 1 4 6873.21 6266.50 173.27 o 1 1 4 5712.35 5345.49 107.15 o 2 1 4 113.93 112.67 2.63 o 3 1 4 882.89 929.11 14.15 o 4 1 4 412.90 449.56 7.80 o 5 1 4 21.31 19.33 5.49 o 6 1 4 58.82 48.46 17.83 o 0 2 4 633.25 611.81 16.23 o 1 2 4 411.89 427.28 7.73 o 2 2 4 105.56 96.80 4.18 o 3 2 4 1716.63 1744.21 24.73 o 4 2 4 214.66 195.76 4.09 o 5 2 4 7.17 10.62 7.94 o 6 2 4 14.98 8.61 5.87 o 0 3 4 330.05 347.92 18.09 o 1 3 4 628.04 629.81 15.45 o 2 3 4 4112.51 4456.90 60.93 o 3 3 4 443.30 437.00 8.78 o 4 3 4 1487.68 1555.22 26.87 o 5 3 4 16.76 45.20 14.08 o 6 3 4 0.96 15.65 14.96 o 0 4 4 225.63 256.83 16.04 o 1 4 4 1062.97 1021.24 23.26 o 2 4 4 48.54 51.00 2.31 o 3 4 4 122.84 121.84 5.36 o 4 4 4 128.28 141.61 6.04 o 5 4 4 1.52 33.47 28.41 o 6 4 4 37.47 461.52 270.72 o 0 5 4 1919.92 1868.95 60.82 o 1 5 4 529.40 518.64 15.71 o 2 5 4 80.96 82.44 8.59 o 3 5 4 207.80 206.08 8.18 o 4 5 4 361.57 341.64 10.94 o 5 5 4 114.23 92.77 20.78 o 0 6 4 187.18 188.01 13.71 o 1 6 4 300.46 293.65 10.61 o 2 6 4 265.48 265.97 10.82 o 3 6 4 125.68 133.68 7.67 o 4 6 4 95.09 79.43 7.63 o 0 7 4 98.63 95.80 10.41 o 1 7 4 139.67 157.66 16.38 o 2 7 4 30.30 25.74 8.47 o 3 7 4 32.48 41.31 8.52 o 0 8 4 272.26 272.08 20.63 o 1 8 4 93.41 98.18 10.03 o 1 0 5 162.97 147.58 7.60 o 2 0 5 1212.91 1160.70 20.24 o 3 0 5 17.50 18.09 2.00 o 4 0 5 33.76 40.09 30.90 o 5 0 5 2.23 18.75 9.49 o 6 0 5 254.77 197.13 14.94 o 0 1 5 13.79 16.13 3.64 o 1 1 5 4280.39 3897.52 73.54 o 2 1 5 1686.24 1726.65 23.09 o 3 1 5 270.72 282.63 5.01 o 4 1 5 190.22 193.58 4.27 o 5 1 5 98.42 78.69 9.60 o 6 1 5 39.50 35.38 10.49 o 0 2 5 4349.83 4081.37 157.82 o 1 2 5 1785.04 1822.44 32.95 o 2 2 5 1437.25 1473.04 36.60 o 3 2 5 321.88 345.95 9.60 o 4 2 5 329.50 325.00 6.38 o 5 2 5 74.33 67.34 6.61 o 6 2 5 56.22 79.43 10.77 o 0 3 5 1649.55 1661.45 75.20 o 1 3 5 889.98 818.97 14.95 o 2 3 5 26.35 19.74 1.70 o 3 3 5 131.04 143.07 3.67 o 4 3 5 371.81 355.08 8.53 o 5 3 5 29.29 45.31 10.46 o 6 3 5 11.44 83.09 26.23 o 0 4 5 572.53 609.49 47.87 o 1 4 5 841.08 839.87 28.17 o 2 4 5 169.54 188.11 8.26 o 3 4 5 332.30 323.01 8.77 o 4 4 5 23.24 31.93 4.95 o 5 4 5 131.06 149.88 39.04 o 6 4 5 8.55 38.14 27.23 o 0 5 5 485.30 468.26 22.32 o 1 5 5 148.67 131.33 10.10 o 2 5 5 16.57 27.22 5.16 o 3 5 5 2.65 9.73 5.54 o 4 5 5 354.39 354.81 11.31 o 5 5 5 23.02 34.74 17.14 o 0 6 5 328.15 336.94 18.36 o 1 6 5 42.32 37.52 4.72 o 2 6 5 45.40 45.22 6.53 o 3 6 5 25.74 26.72 6.02 o 4 6 5 23.36 23.29 6.58 o 0 7 5 176.09 166.80 11.32 o 1 7 5 36.56 51.63 12.43 o 2 7 5 134.02 145.83 12.80 o 3 7 5 32.94 37.59 10.43 o 0 8 5 326.42 332.93 22.25 o 1 8 5 22.74 34.63 9.21 o 1 0 6 2276.99 2123.09 102.31 o 2 0 6 1571.57 1650.01 29.21 o 3 0 6 1970.18 2063.00 49.70 o 4 0 6 8.79 4.64 1.49 o 5 0 6 260.47 252.85 26.35 o 6 0 6 14.40 18.63 13.23 o 0 1 6 1081.79 1050.52 35.47 o 1 1 6 3230.02 3004.84 63.15 o 2 1 6 64.69 61.41 1.88 o 3 1 6 1067.07 1025.73 15.92 o 4 1 6 57.84 65.06 2.11 o 5 1 6 198.33 208.98 22.43 o 6 1 6 36.36 40.30 10.60 o 0 2 6 116.50 109.42 5.23 o 1 2 6 758.03 776.35 15.95 o 2 2 6 1682.01 1740.43 35.91 o 3 2 6 232.17 252.88 8.46 o 4 2 6 297.51 300.66 6.10 o 5 2 6 53.54 41.63 4.62 o 6 2 6 57.01 51.31 5.82 o 0 3 6 4363.69 4153.61 104.80 o 1 3 6 235.40 234.52 5.96 o 2 3 6 688.02 773.67 14.42 o 3 3 6 512.49 522.17 10.61 o 4 3 6 82.10 87.03 4.39 o 5 3 6 69.59 81.42 11.50 o 6 3 6 56.70 154.11 131.20 o 0 4 6 160.14 182.07 22.37 o 1 4 6 146.92 168.63 16.33 o 2 4 6 323.91 300.67 9.47 o 3 4 6 86.03 84.26 4.39 o 4 4 6 148.64 152.65 9.30 o 5 4 6 5.53 15.65 11.76 o 0 5 6 115.87 112.04 14.57 o 1 5 6 523.78 481.57 18.26 o 2 5 6 467.09 474.90 12.11 o 3 5 6 175.41 187.04 12.10 o 4 5 6 51.06 42.69 5.46 o 5 5 6 29.05 40.29 24.42 o 0 6 6 862.20 875.10 34.22 o 1 6 6 386.94 366.59 13.97 o 2 6 6 785.20 766.74 22.29 o 3 6 6 63.07 65.03 6.70 o 4 6 6 108.08 98.04 7.13 o 0 7 6 462.99 439.61 20.97 o 1 7 6 25.31 45.63 11.18 o 2 7 6 41.27 62.01 12.24 o 3 7 6 22.41 24.49 13.16 o 0 8 6 8.32 40.48 18.70 o 1 8 6 131.83 132.56 10.80 o 1 0 7 831.91 828.55 30.61 o 2 0 7 180.77 188.87 4.72 o 3 0 7 83.77 79.99 3.64 o 4 0 7 8.09 13.15 2.15 o 5 0 7 2.34 35.67 25.40 o 6 0 7 1.92 4.64 8.58 o 0 1 7 11567.46 10648.71 264.60 o 1 1 7 1313.20 1239.15 20.05 o 2 1 7 555.50 573.80 7.67 o 3 1 7 383.70 389.65 6.11 o 4 1 7 79.17 85.26 4.22 o 5 1 7 608.94 611.00 19.54 o 6 1 7 106.08 96.47 9.25 o 0 2 7 297.46 277.27 10.93 o 1 2 7 86.12 87.26 2.52 o 2 2 7 337.12 360.93 6.09 o 3 2 7 53.75 53.94 2.50 o 4 2 7 128.71 131.29 3.66 o 5 2 7 319.46 295.29 11.36 o 6 2 7 25.74 40.70 10.33 o 0 3 7 2.24 12.71 5.13 o 1 3 7 429.17 450.86 8.68 o 2 3 7 2587.36 2752.70 58.91 o 3 3 7 88.45 92.77 3.74 o 4 3 7 246.10 255.70 7.93 o 5 3 7 871.05 782.04 48.81 o 6 3 7 27.22 53.76 88.42 o 0 4 7 101.02 111.06 11.86 o 1 4 7 452.41 433.27 19.78 o 2 4 7 388.54 411.25 12.64 o 3 4 7 9.77 17.40 3.21 o 4 4 7 57.50 54.08 4.58 o 5 4 7 105.50 90.96 11.93 o 0 5 7 685.42 651.10 36.69 o 1 5 7 652.95 622.21 17.62 o 2 5 7 421.72 419.06 13.73 o 3 5 7 84.91 87.79 5.41 o 4 5 7 1.33 21.52 4.44 o 5 5 7 168.65 165.99 22.15 o 0 6 7 308.35 333.49 18.85 o 1 6 7 289.91 296.58 13.48 o 2 6 7 116.50 129.54 7.64 o 3 6 7 225.18 210.41 11.21 o 4 6 7 1.44 -1.55 8.30 o 0 7 7 545.01 573.75 25.47 o 1 7 7 27.19 33.38 7.32 o 2 7 7 205.09 224.08 17.53 o 3 7 7 190.16 174.25 12.78 o 0 8 7 327.87 348.50 25.69 o 1 0 8 1042.69 1048.49 70.87 o 2 0 8 6072.59 6398.39 170.10 o 3 0 8 499.93 504.10 11.93 o 4 0 8 9.02 8.56 2.20 o 5 0 8 143.06 159.19 30.00 o 6 0 8 152.40 94.58 11.86 o 0 1 8 621.71 606.41 13.10 o 1 1 8 329.12 338.48 6.30 o 2 1 8 137.08 124.12 2.68 o 3 1 8 197.75 201.63 4.23 o 4 1 8 227.37 213.81 8.74 o 5 1 8 443.86 438.85 15.97 o 6 1 8 203.74 166.86 15.19 o 0 2 8 757.96 710.65 21.68 o 1 2 8 1116.79 1085.18 19.02 o 2 2 8 582.35 584.98 12.91 o 3 2 8 39.91 53.77 2.31 o 4 2 8 198.68 197.57 4.66 o 5 2 8 31.00 38.54 11.29 o 6 2 8 15.02 22.98 7.35 o 0 3 8 26.55 22.73 1.64 o 1 3 8 420.77 431.45 9.65 o 2 3 8 317.76 295.12 14.28 o 3 3 8 196.15 203.26 5.83 o 4 3 8 79.99 68.77 4.10 o 5 3 8 54.89 69.32 8.57 o 6 3 8 66.22 71.88 10.91 o 0 4 8 47.17 51.51 8.97 o 1 4 8 554.87 532.22 28.72 o 2 4 8 428.61 430.72 14.63 o 3 4 8 16.99 17.92 3.13 o 4 4 8 336.84 318.10 8.47 o 5 4 8 52.48 59.89 12.83 o 0 5 8 226.91 205.57 22.42 o 1 5 8 270.86 271.57 19.19 o 2 5 8 42.95 41.23 6.33 o 3 5 8 219.01 220.49 8.04 o 4 5 8 38.72 43.15 5.17 o 5 5 8 5.14 -5.35 10.49 o 0 6 8 1552.09 1458.99 50.16 o 1 6 8 367.65 374.06 18.39 o 2 6 8 193.37 183.35 8.85 o 3 6 8 178.43 177.35 14.99 o 4 6 8 52.14 47.60 8.40 o 0 7 8 45.28 56.32 9.85 o 1 7 8 58.45 56.08 7.92 o 2 7 8 112.56 104.61 11.42 o 3 7 8 144.13 165.70 12.35 o 0 8 8 202.54 225.29 20.19 o 1 0 9 1688.81 1674.24 60.14 o 2 0 9 118.61 147.97 4.57 o 3 0 9 129.84 144.57 4.52 o 4 0 9 163.34 169.63 7.33 o 5 0 9 8.96 26.62 10.98 o 6 0 9 72.84 88.59 11.20 o 0 1 9 5940.98 5733.73 142.08 o 1 1 9 7.10 8.19 0.89 o 2 1 9 780.92 788.37 13.00 o 3 1 9 929.59 962.90 17.95 o 4 1 9 426.90 427.73 8.84 o 5 1 9 371.04 397.80 24.86 o 6 1 9 16.98 28.79 9.58 o 0 2 9 9.53 11.93 3.13 o 1 2 9 754.48 744.18 16.19 o 2 2 9 28.09 24.84 4.03 o 3 2 9 272.07 273.29 5.06 o 4 2 9 75.63 66.90 2.64 o 5 2 9 74.09 56.33 6.28 o 6 2 9 134.33 152.38 11.28 o 0 3 9 111.90 102.33 12.03 o 1 3 9 539.19 539.50 13.60 o 2 3 9 37.18 28.78 2.53 o 3 3 9 159.29 156.92 5.91 o 4 3 9 569.54 564.84 14.71 o 5 3 9 30.11 37.28 8.52 o 6 3 9 74.87 52.96 18.27 o 0 4 9 237.30 218.77 13.42 o 1 4 9 105.74 96.71 3.98 o 2 4 9 274.35 287.97 9.45 o 3 4 9 229.41 218.14 6.77 o 4 4 9 52.44 54.30 4.73 o 5 4 9 103.59 97.11 10.29 o 0 5 9 20.66 21.71 8.31 o 1 5 9 484.52 488.68 17.34 o 2 5 9 70.44 90.90 15.37 o 3 5 9 74.67 81.26 5.57 o 4 5 9 32.99 41.03 12.17 o 5 5 9 47.98 69.18 28.09 o 0 6 9 5.03 7.31 7.53 o 1 6 9 932.82 926.98 28.05 o 2 6 9 299.35 296.34 12.37 o 3 6 9 171.56 154.72 9.20 o 4 6 9 27.71 27.56 6.49 o 0 7 9 2.66 8.83 8.36 o 1 7 9 129.77 136.63 12.79 o 2 7 9 35.44 35.35 11.81 o 3 7 9 131.29 124.82 11.71 o 2 0 10 5578.08 5977.80 171.66 o 3 0 10 701.21 737.59 15.28 o 4 0 10 49.20 43.12 3.91 o 5 0 10 48.37 56.79 12.96 o 6 0 10 116.72 152.96 15.87 o 0 1 10 31.77 26.45 2.74 o 1 1 10 1154.62 1159.65 20.33 o 2 1 10 573.89 579.15 10.81 o 3 1 10 162.71 161.76 4.85 o 4 1 10 29.29 31.61 2.24 o 5 1 10 146.99 152.31 11.10 o 6 1 10 3.00 14.48 10.61 o 0 2 10 1149.00 1170.31 41.73 o 1 2 10 1149.16 1162.25 24.49 o 2 2 10 76.91 69.61 2.40 o 3 2 10 50.40 52.60 2.39 o 4 2 10 199.03 187.81 4.85 o 5 2 10 403.04 353.59 17.30 o 6 2 10 60.59 55.38 12.27 o 0 3 10 289.65 312.15 16.57 o 1 3 10 178.47 171.13 4.89 o 2 3 10 2090.85 2149.42 55.73 o 3 3 10 713.66 717.01 17.90 o 4 3 10 880.64 847.79 20.21 o 5 3 10 234.75 225.20 20.58 o 6 3 10 17.16 22.78 7.86 o 0 4 10 0.12 5.65 5.65 o 1 4 10 375.81 383.13 9.40 o 2 4 10 48.37 48.30 5.26 o 3 4 10 20.58 19.04 4.01 o 4 4 10 155.13 145.10 12.80 o 5 4 10 135.24 122.70 17.19 o 0 5 10 147.20 144.57 15.03 o 1 5 10 42.19 53.72 13.64 o 2 5 10 858.50 778.17 42.27 o 3 5 10 30.95 39.56 4.49 o 4 5 10 24.43 24.90 7.75 o 5 5 10 13.44 31.51 12.98 o 0 6 10 82.45 104.24 16.60 o 1 6 10 45.82 47.21 8.34 o 2 6 10 382.26 382.04 12.77 o 3 6 10 146.18 163.88 9.32 o 4 6 10 13.27 20.09 6.20 o 0 7 10 101.41 91.55 9.88 o 1 7 10 211.37 239.47 26.67 o 2 7 10 165.36 175.96 17.31 o 3 7 10 0.36 21.81 8.11 o 2 0 11 3959.98 4139.50 169.00 o 3 0 11 1258.42 1326.00 29.60 o 4 0 11 1.27 0.49 2.22 o 5 0 11 564.04 544.90 27.01 o 6 0 11 191.55 237.66 19.29 o 0 1 11 138.06 146.07 5.28 o 1 1 11 574.67 541.73 10.14 o 2 1 11 2270.35 2331.38 36.24 o 3 1 11 810.14 828.55 19.31 o 4 1 11 306.95 308.19 7.96 o 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516.76 14.97 o 2 3 19 13.47 19.55 4.72 o 3 3 19 77.14 73.58 5.20 o 4 3 19 485.67 475.85 34.09 o 5 3 19 12.07 21.27 13.98 o 0 4 19 8.49 20.97 11.47 o 1 4 19 76.15 78.18 5.05 o 2 4 19 74.27 71.53 12.65 o 3 4 19 114.92 120.09 12.25 o 4 4 19 94.74 103.35 8.04 o 5 4 19 11.03 13.07 8.12 o 0 5 19 0.80 9.97 12.93 o 1 5 19 896.22 847.53 32.01 o 2 5 19 116.69 124.92 33.60 o 3 5 19 42.10 54.23 19.46 o 4 5 19 64.68 63.73 8.97 o 0 6 19 0.11 9.02 8.53 o 1 6 19 102.77 95.30 17.98 o 2 6 19 635.31 604.00 36.96 o 3 6 19 184.15 164.38 14.22 o 0 7 19 0.53 43.95 21.56 o 1 7 19 107.73 98.91 15.41 o 4 0 20 0.00 3.18 5.84 o 5 0 20 0.10 12.71 8.80 o 0 1 20 7.74 8.09 5.16 o 1 1 20 1005.81 1015.39 27.37 o 2 1 20 20.46 19.58 5.67 o 3 1 20 335.79 340.39 15.01 o 4 1 20 161.57 160.18 10.43 o 5 1 20 43.22 53.69 12.26 o 0 2 20 200.86 216.47 17.01 o 1 2 20 545.71 519.93 22.14 o 2 2 20 613.17 632.52 25.51 o 3 2 20 1369.88 1341.99 60.72 o 4 2 20 179.90 152.39 9.48 o 5 2 20 4.02 14.69 9.03 o 0 3 20 553.30 492.25 20.12 o 1 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5.09 o 4 3 21 168.08 136.78 7.68 o 5 3 21 62.57 41.48 11.07 o 0 4 21 443.18 456.16 22.71 o 1 4 21 39.81 52.98 7.25 o 2 4 21 204.78 212.68 10.13 o 3 4 21 254.35 246.41 11.58 o 4 4 21 66.44 54.99 8.83 o 0 5 21 9.02 20.00 13.15 o 1 5 21 79.09 91.74 14.09 o 2 5 21 86.67 89.78 14.95 o 3 5 21 38.35 50.28 11.45 o 4 5 21 111.07 141.49 18.65 o 0 6 21 32.93 93.07 34.69 o 1 6 21 38.42 48.98 9.91 o 2 6 21 412.22 423.89 28.72 o 3 0 22 256.77 274.16 22.27 o 4 0 22 43.57 49.06 7.68 o 5 0 22 18.50 73.14 32.10 o 1 1 22 642.75 709.82 30.83 o 3 1 22 231.93 222.24 11.26 o 4 1 22 285.33 285.14 15.84 o 5 1 22 20.64 50.82 27.43 o 0 2 22 579.24 536.91 23.17 o 1 2 22 128.28 120.30 11.91 o 2 2 22 212.84 205.60 13.36 o 3 2 22 751.62 745.57 21.44 o 4 2 22 15.72 14.20 10.24 o 5 2 22 87.61 93.97 12.13 o 0 3 22 1458.58 1387.05 65.22 o 1 3 22 358.17 351.25 13.88 o 2 3 22 6.10 6.89 6.12 o 3 3 22 766.87 768.30 25.82 o 4 3 22 75.36 79.10 7.35 o 5 3 22 0.77 7.13 10.87 o 0 4 22 121.88 112.04 12.91 o 1 4 22 6.36 5.81 7.22 o 2 4 22 286.67 276.78 12.48 o 3 4 22 16.15 10.90 18.69 o 4 4 22 19.03 16.62 4.84 o 0 5 22 792.26 723.21 41.22 o 1 5 22 107.59 138.47 15.32 o 2 5 22 52.06 76.83 13.22 o 3 5 22 59.67 80.40 10.98 o 0 6 22 314.90 308.85 35.18 o 1 6 22 328.32 341.53 23.43 o 2 6 22 201.09 200.95 18.30 o 3 0 23 77.07 57.99 12.37 o 4 0 23 75.91 63.34 9.46 o 5 0 23 88.69 81.11 12.10 o 1 1 23 313.07 289.91 17.58 o 3 1 23 1.85 -0.06 2.31 o 4 1 23 65.29 96.57 24.26 o 5 1 23 9.88 8.56 9.78 o 0 2 23 420.59 373.46 29.02 o 1 2 23 282.88 266.03 23.64 o 2 2 23 272.91 314.13 63.02 o 3 2 23 388.79 372.85 20.53 o 4 2 23 207.45 210.53 9.97 o 5 2 23 22.60 20.27 9.02 o 0 3 23 66.52 45.20 6.94 o 1 3 23 123.43 128.07 10.41 o 2 3 23 156.29 147.66 7.52 o 3 3 23 54.48 59.15 10.77 o 4 3 23 61.65 71.55 9.27 o 0 4 23 727.70 710.65 40.02 o 1 4 23 7.67 43.18 12.76 o 2 4 23 220.90 229.01 11.52 o 3 4 23 275.29 280.78 16.77 o 4 4 23 84.71 79.43 8.01 o 0 5 23 1.59 10.27 13.93 o 1 5 23 23.57 44.27 18.70 o 2 5 23 277.63 272.71 17.61 o 3 5 23 36.44 39.96 14.36 o 0 6 23 64.94 78.86 23.88 o 1 6 23 54.58 55.49 9.31 o 2 6 23 173.13 176.95 16.02 o 4 0 24 203.57 207.82 13.98 o 5 0 24 37.79 20.97 6.31 o 0 1 24 150.29 152.96 18.95 o 4 1 24 43.66 58.70 11.27 o 5 1 24 88.92 91.21 9.66 o 0 2 24 154.41 141.93 11.17 o 1 2 24 857.09 769.49 27.16 o 2 2 24 224.79 225.76 13.62 o 3 2 24 687.81 643.15 38.06 o 4 2 24 129.09 143.63 8.43 o 5 2 24 5.57 16.24 7.66 o 0 3 24 79.80 71.02 11.86 o 1 3 24 509.57 494.89 24.39 o 2 3 24 60.78 60.53 9.81 o 3 3 24 39.70 35.10 5.38 o 4 3 24 148.55 142.69 19.04 o 0 4 24 1825.39 1757.13 104.87 o 1 4 24 344.66 313.33 15.36 o 2 4 24 87.84 88.02 6.71 o 3 4 24 272.19 245.00 14.98 o 4 4 24 1.67 16.32 21.06 o 0 5 24 56.56 70.75 10.27 o 1 5 24 3.86 5.66 12.45 o 2 5 24 273.54 295.87 111.77 o 3 5 24 56.09 43.70 7.38 o 0 6 24 427.07 396.78 33.00 o 1 6 24 229.82 217.77 44.47 o 3 0 25 155.36 186.30 49.94 o 4 0 25 58.03 115.70 26.23 o 5 0 25 8.98 29.60 11.91 o 0 1 25 30.45 68.67 10.63 o 2 1 25 353.48 398.64 31.22 o 4 1 25 18.75 2.20 14.67 o 5 1 25 40.49 34.86 7.79 o 0 2 25 169.33 178.29 18.80 o 1 2 25 460.25 474.71 20.46 o 2 2 25 68.14 66.40 9.58 o 3 2 25 150.03 144.57 17.28 o 4 2 25 3.74 2.70 6.34 o 5 2 25 133.58 118.25 157.64 o 0 3 25 0.04 8.56 10.98 o 1 3 25 464.55 419.58 23.74 o 2 3 25 7.06 18.74 15.80 o 3 3 25 36.83 43.73 7.24 o 4 3 25 62.86 63.03 5.95 o 0 4 25 11.92 13.49 11.03 o 1 4 25 60.66 57.62 11.97 o 2 4 25 99.93 98.63 7.33 o 3 4 25 202.92 228.13 23.15 o 4 4 25 22.42 38.40 11.57 o 0 5 25 0.31 -1.93 10.22 o 1 5 25 618.88 679.66 37.44 o 2 5 25 292.10 322.16 29.76 o 3 5 25 23.54 56.06 22.58 o 0 6 25 80.19 59.40 14.47 o 1 6 25 44.15 44.12 25.68 o 3 0 26 11.09 52.85 27.97 o 4 0 26 237.67 214.64 16.04 o 5 0 26 5.54 -6.82 10.19 o 0 1 26 286.41 267.46 14.84 o 2 1 26 443.29 436.34 23.52 o 4 1 26 35.47 30.70 6.23 o 5 1 26 13.00 18.99 10.23 o 0 2 26 107.06 97.96 9.90 o 1 2 26 883.82 898.37 54.37 o 2 2 26 115.66 106.17 17.41 o 3 2 26 375.56 359.77 13.40 o 4 2 26 88.31 82.97 8.52 o 0 3 26 25.22 34.00 14.59 o 1 3 26 166.22 168.88 14.89 o 2 3 26 136.28 150.86 24.49 o 3 3 26 84.24 91.16 9.27 o 4 3 26 8.02 13.54 6.18 o 0 4 26 168.78 164.77 23.27 o 1 4 26 983.68 1001.78 47.89 o 2 4 26 22.85 36.54 13.02 o 3 4 26 340.82 311.77 32.73 o 0 5 26 101.98 169.22 29.70 o 1 5 26 241.53 219.48 14.73 o 2 5 26 4.50 12.20 12.82 o 0 6 26 12.73 35.10 24.64 o 4 0 27 52.79 43.12 15.21 o 0 1 27 362.65 350.26 16.97 o 2 1 27 860.00 883.43 43.69 o 3 1 27 70.32 80.55 25.25 o 4 1 27 153.57 152.04 20.02 o 0 2 27 25.14 19.85 12.27 o 1 2 27 30.71 42.17 12.28 o 2 2 27 58.26 71.28 8.97 o 3 2 27 38.87 41.08 8.05 o 4 2 27 231.90 228.15 11.65 o 0 3 27 0.03 14.20 11.78 o 1 3 27 137.20 146.00 9.89 o 2 3 27 47.84 56.18 21.99 o 3 3 27 163.58 153.35 17.43 o 4 3 27 4.47 9.20 9.44 o 0 4 27 19.37 43.95 12.86 o 1 4 27 8.47 24.62 30.09 o 2 4 27 81.45 127.72 69.98 o 3 4 27 40.42 36.62 12.30 o 0 5 27 393.27 372.85 39.26 o 1 5 27 138.90 183.54 44.94 o 2 5 27 144.70 128.50 17.61 o 4 0 28 41.95 47.77 7.77 o 4 1 28 1.43 8.19 6.48 o 1 2 28 134.65 149.78 12.89 o 2 2 28 273.21 287.27 23.32 o 3 2 28 107.42 109.39 9.12 o 4 2 28 33.34 39.17 6.24 o 0 3 28 1084.07 1114.30 60.55 o 1 3 28 36.11 46.69 12.18 o 2 3 28 643.38 610.27 35.54 o 3 3 28 89.10 74.22 10.24 o 4 3 28 50.07 57.52 9.76 o 0 4 28 1.06 10.98 8.29 o 1 4 28 54.79 60.16 12.26 o 2 4 28 106.95 101.64 129.55 o 3 4 28 13.01 2.69 14.23 o 0 5 28 130.28 177.04 25.79 o 1 5 28 277.06 249.69 18.84 o 2 5 28 9.29 20.68 9.64 o 4 0 29 60.14 60.63 7.31 o 2 1 29 54.66 67.13 17.43 o 4 1 29 29.03 39.65 11.86 o 1 2 29 152.00 137.51 15.77 o 2 2 29 143.33 152.96 38.28 o 3 2 29 107.97 108.33 8.96 o 4 2 29 3.96 3.25 6.97 o 0 3 29 26.21 27.43 12.93 o 1 3 29 11.86 28.63 11.83 o 2 3 29 459.78 438.95 24.89 o 3 3 29 53.01 67.73 14.94 o 0 4 29 356.50 341.54 25.42 o 1 4 29 13.35 49.70 19.84 o 2 4 29 8.18 38.62 11.76 o 3 4 29 42.26 45.33 9.14 o 0 5 29 79.01 60.38 16.28 o 1 5 29 209.32 236.92 22.15 o 1 0 30 646.85 594.16 32.02 o 4 0 30 10.60 17.82 8.85 o 1 1 30 1489.74 1395.21 67.74 o 2 1 30 220.57 270.54 41.66 o 4 1 30 106.30 83.89 22.86 o 0 2 30 11.50 7.58 12.74 o 1 2 30 185.93 179.12 26.79 o 2 2 30 21.55 32.02 20.36 o 3 2 30 170.06 169.78 21.67 o 4 2 30 5.84 37.04 12.81 o 0 3 30 0.54 5.87 8.80 o 1 3 30 286.92 316.04 27.23 o 2 3 30 194.79 173.02 156.72 o 3 3 30 16.96 19.79 8.14 o 0 4 30 49.27 88.59 37.96 o 1 4 30 166.47 129.91 24.59 o 2 4 30 31.67 38.33 10.27 o 0 5 30 170.85 209.62 24.01 o 1 5 30 316.89 330.52 35.75 o 4 0 31 42.65 47.11 6.65 o 1 1 31 606.40 545.64 46.74 o 2 1 31 56.78 98.57 20.80 o 4 1 31 60.19 64.99 7.55 o 0 2 31 746.16 693.27 42.81 o 2 2 31 126.27 115.04 30.53 o 3 2 31 52.19 54.96 7.04 o 1 3 31 174.37 152.29 17.56 o 2 3 31 10.64 48.40 30.90 o 3 3 31 131.29 131.37 15.88 o 0 4 31 1141.57 1164.98 80.04 o 1 4 31 51.34 62.73 24.93 o 2 4 31 17.95 33.62 14.54 o 1 0 32 29.88 36.42 16.43 o 2 0 32 1.01 12.93 8.56 o 0 1 32 2.97 0.49 7.87 o 1 1 32 227.99 219.23 19.43 o 0 2 32 448.04 424.65 30.29 o 1 2 32 600.48 590.35 38.75 o 2 2 32 53.02 46.25 11.91 o 3 2 32 2.63 17.04 11.65 o 1 3 32 24.57 47.77 19.24 o 2 3 32 152.77 166.38 17.75 o 1 4 32 94.77 95.84 15.22 o 1 0 33 0.21 20.56 18.58 o 2 0 33 0.62 350.26 114.11 o 3 0 33 189.04 217.37 27.21 o 1 1 33 116.23 115.04 21.46 o 0 2 33 201.57 198.89 17.65 o 1 2 33 200.82 198.89 25.57 o 2 2 33 115.52 111.06 13.52 o 3 2 33 157.62 148.22 9.74 o 0 3 33 296.35 262.89 30.92 o 2 3 33 140.25 144.57 18.43 o 0 4 33 286.60 299.02 29.75 o 1 4 33 37.34 61.54 50.88 o 0 0 34 48.20 34.00 11.49 o 1 0 34 29.08 53.10 10.24 o 3 0 34 22.55 1.93 32.12 o 3 1 34 41.90 17.55 9.31 o 0 2 34 18.37 30.12 24.54 o 1 2 34 179.64 160.00 17.01 o 2 2 34 4.56 14.91 22.95 o 0 3 34 1.58 12.71 17.06 o 1 3 34 62.06 50.38 11.54 o 2 3 34 61.86 40.09 17.63 o 1 0 35 29.04 30.12 30.39 o 2 0 35 188.55 267.46 32.73 o 0 1 35 77.36 90.96 25.06 o 1 1 35 45.04 46.25 11.05 o 2 1 35 98.72 71.57 20.33 o 0 2 35 27.55 50.38 14.64 o 1 2 35 119.60 120.13 18.16 o 2 2 35 157.53 148.34 25.52 o 0 3 35 63.38 88.30 19.97 o 1 3 35 110.30 122.65 16.06 o 1 0 36 106.21 113.04 15.30 o 2 0 36 21.75 25.35 8.34 o 0 1 36 77.87 91.87 16.18 o 1 1 36 298.58 317.70 18.38 o 2 1 36 11.45 11.92 10.24 o 0 2 36 0.46 9.02 12.66 o 1 2 36 67.03 72.87 26.43 o 1 0 37 149.98 142.69 26.16 o 1 1 37 62.97 123.23 38.53 o 1 0 38 0.33 11.51 23.44 o 0 1 38 58.78 72.34 22.07 o