#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:01:32 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180944 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/24/2202407.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202407_Fobs loop_ _publ_author_name 'Jones, Peter G.' _publ_section_title ; N-Hydroxysuccinimide ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1951 _journal_page_last o1952 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.4266 _cell_length_b 7.2419 _cell_length_c 12.4454 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.7106 _cod_data_source_file bt6380Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' succoh in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 74.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 619.90 631.61 12.48 o 4 0 0 54.25 51.71 2.96 o 6 0 0 236.78 241.95 4.66 o 1 1 0 45.14 46.21 2.27 o 2 1 0 207.42 185.86 6.49 o 3 1 0 843.46 879.21 19.71 o 4 1 0 14.02 16.14 1.30 o 5 1 0 16.36 16.27 0.78 o 6 1 0 2.20 1.67 0.59 o 7 1 0 36.98 42.09 1.53 o 0 2 0 1422.65 2023.46 14.21 o 1 2 0 45.33 61.77 4.81 o 2 2 0 129.87 164.72 7.09 o 3 2 0 14.16 21.23 1.08 o 4 2 0 7.60 5.64 0.42 o 5 2 0 56.16 61.45 2.51 o 6 2 0 10.08 9.76 0.75 o 7 2 0 3.23 3.19 0.89 o 1 3 0 1.04 1.04 0.17 o 2 3 0 168.32 191.83 13.10 o 3 3 0 82.95 75.78 3.10 o 4 3 0 0.06 2.80 0.93 o 5 3 0 97.41 91.84 4.07 o 6 3 0 16.48 17.78 0.94 o 7 3 0 7.82 6.40 1.24 o 0 4 0 2168.39 3135.60 17.94 o 1 4 0 16.29 17.73 0.86 o 2 4 0 368.88 420.67 19.88 o 3 4 0 26.18 34.12 3.00 o 4 4 0 16.78 15.22 0.71 o 5 4 0 25.82 22.24 1.29 o 6 4 0 24.94 23.92 1.49 o 7 4 0 21.69 23.21 1.75 o 1 5 0 61.53 79.94 1.10 o 2 5 0 70.97 72.10 3.88 o 3 5 0 51.34 50.43 2.75 o 4 5 0 1.46 3.84 1.14 o 5 5 0 0.95 0.13 0.62 o 6 5 0 0.38 1.99 1.05 o 0 6 0 21.73 26.68 0.89 o 1 6 0 125.35 152.09 1.78 o 2 6 0 19.17 19.42 0.85 o 3 6 0 0.00 -0.24 0.43 o 4 6 0 27.91 28.49 1.15 o 5 6 0 20.61 15.99 1.07 o 6 6 0 0.02 1.14 1.11 o 1 7 0 79.73 88.33 1.13 o 2 7 0 132.93 129.09 3.80 o 3 7 0 7.02 5.20 0.84 o 4 7 0 2.13 2.64 0.95 o 5 7 0 86.18 85.34 2.40 o 0 8 0 0.00 -0.23 0.60 o 1 8 0 125.46 134.45 2.08 o 2 8 0 10.13 12.44 1.14 o 3 8 0 8.55 9.76 1.43 o 4 8 0 3.04 3.80 0.98 o 1 9 0 0.93 0.23 1.02 o 2 9 0 7.24 7.15 1.31 o 3 9 0 0.01 0.14 1.28 o 1 10 0 32.99 31.78 1.73 o 1 0 1 619.06 526.11 4.24 o 2 0 1 194.96 177.78 2.98 o 3 0 1 98.72 92.17 2.30 o 4 0 1 132.80 130.47 3.37 o 5 0 1 71.56 65.87 1.17 o 6 0 1 5.99 7.21 0.71 o 7 0 1 3.29 2.90 0.75 o 0 1 1 2.42 2.95 0.12 o 1 1 1 2411.16 2442.02 71.81 o 2 1 1 316.83 319.48 4.95 o 3 1 1 27.33 32.75 1.76 o 4 1 1 221.86 212.98 4.03 o 5 1 1 45.01 43.67 0.67 o 6 1 1 9.99 10.77 0.53 o 7 1 1 30.92 34.68 0.94 o 0 2 1 8.89 8.60 0.29 o 1 2 1 5621.55 6620.62 202.88 o 2 2 1 317.08 337.98 8.43 o 3 2 1 0.46 0.83 0.18 o 4 2 1 25.41 21.79 0.68 o 5 2 1 79.93 73.24 1.72 o 6 2 1 40.08 38.14 0.78 o 7 2 1 17.81 17.45 1.05 o 0 3 1 1.52 1.78 0.18 o 1 3 1 75.64 89.58 2.41 o 2 3 1 631.48 747.22 25.52 o 3 3 1 40.00 42.50 1.44 o 4 3 1 170.58 163.62 4.05 o 5 3 1 66.67 66.84 1.75 o 6 3 1 3.67 3.70 0.55 o 7 3 1 2.07 2.12 0.79 o 0 4 1 56.67 68.10 0.81 o 1 4 1 160.22 187.62 4.18 o 2 4 1 95.99 106.69 3.39 o 3 4 1 154.79 162.46 4.76 o 4 4 1 11.77 12.83 0.47 o 5 4 1 11.27 12.11 0.54 o 6 4 1 5.58 5.85 0.54 o 7 4 1 18.22 19.08 1.17 o 0 5 1 0.60 0.52 0.22 o 1 5 1 10.22 11.42 0.56 o 2 5 1 53.75 61.22 1.95 o 3 5 1 13.15 13.31 0.78 o 4 5 1 119.47 110.26 3.47 o 5 5 1 4.86 5.08 0.50 o 6 5 1 18.22 17.57 0.82 o 0 6 1 6.31 9.78 0.49 o 1 6 1 100.45 119.44 1.40 o 2 6 1 24.96 25.74 0.95 o 3 6 1 38.85 40.59 1.72 o 4 6 1 0.62 0.61 0.38 o 5 6 1 16.42 15.90 0.77 o 6 6 1 36.11 34.52 1.05 o 0 7 1 153.53 188.04 2.12 o 1 7 1 53.59 56.90 0.71 o 2 7 1 64.39 64.68 1.98 o 3 7 1 0.38 0.77 0.37 o 4 7 1 22.72 21.41 0.89 o 5 7 1 3.80 2.98 0.61 o 0 8 1 25.43 29.33 0.96 o 1 8 1 38.58 42.76 0.89 o 2 8 1 32.47 30.46 0.83 o 3 8 1 60.08 55.25 1.83 o 4 8 1 5.28 5.37 0.61 o 0 9 1 241.93 274.86 5.81 o 1 9 1 50.40 56.22 1.32 o 2 9 1 1.59 1.68 0.60 o 3 9 1 15.51 14.23 0.83 o 0 10 1 42.23 47.65 2.62 o 1 10 1 2.16 1.89 0.79 o 0 0 2 2423.54 2214.88 55.95 o 1 0 2 378.44 364.65 8.93 o 2 0 2 210.22 203.97 4.10 o 3 0 2 0.21 0.29 0.18 o 4 0 2 11.20 11.73 0.97 o 5 0 2 8.26 7.96 0.61 o 6 0 2 1.52 1.84 0.58 o 7 0 2 7.12 6.13 0.80 o 0 1 2 2144.38 2104.33 53.17 o 1 1 2 1085.62 1115.92 22.11 o 2 1 2 665.22 657.79 13.80 o 3 1 2 602.15 602.07 10.62 o 4 1 2 37.97 43.74 0.91 o 5 1 2 46.11 44.87 0.81 o 6 1 2 103.72 104.45 1.25 o 7 1 2 1.54 3.66 0.59 o 0 2 2 351.43 384.61 15.66 o 1 2 2 1477.66 1694.51 53.51 o 2 2 2 128.84 128.99 3.47 o 3 2 2 2.38 2.89 0.21 o 4 2 2 5.72 6.81 0.47 o 5 2 2 14.48 13.09 0.45 o 6 2 2 35.93 37.50 0.92 o 7 2 2 10.39 10.96 0.76 o 0 3 2 0.18 0.15 0.15 o 1 3 2 49.59 62.82 1.84 o 2 3 2 392.09 450.03 11.00 o 3 3 2 39.86 42.73 1.36 o 4 3 2 9.93 11.46 0.66 o 5 3 2 63.01 55.84 1.31 o 6 3 2 5.61 6.75 0.61 o 7 3 2 6.22 8.32 0.76 o 0 4 2 55.80 62.62 2.17 o 1 4 2 43.93 48.00 1.24 o 2 4 2 334.62 361.57 8.68 o 3 4 2 284.14 306.46 8.88 o 4 4 2 27.56 25.87 0.86 o 5 4 2 21.17 19.74 0.62 o 6 4 2 8.19 8.91 0.56 o 0 5 2 3.44 2.65 0.29 o 1 5 2 396.03 468.16 9.90 o 2 5 2 75.61 74.35 2.25 o 3 5 2 254.94 267.75 8.45 o 4 5 2 33.18 34.07 1.16 o 5 5 2 24.17 20.69 0.66 o 6 5 2 32.18 32.60 1.26 o 0 6 2 15.31 19.08 0.57 o 1 6 2 52.34 53.47 0.86 o 2 6 2 326.30 349.46 12.06 o 3 6 2 99.18 97.87 3.56 o 4 6 2 17.71 17.39 0.66 o 5 6 2 7.14 5.79 0.58 o 6 6 2 4.48 4.93 0.66 o 0 7 2 0.07 0.12 0.33 o 1 7 2 116.83 125.54 2.72 o 2 7 2 27.80 27.53 0.85 o 3 7 2 5.79 5.16 0.46 o 4 7 2 5.83 5.25 0.52 o 5 7 2 17.72 17.08 0.91 o 0 8 2 5.70 5.55 0.52 o 1 8 2 18.22 18.33 0.70 o 2 8 2 11.64 11.59 0.62 o 3 8 2 27.17 28.57 1.22 o 4 8 2 0.42 -0.18 0.57 o 0 9 2 59.01 68.76 1.62 o 1 9 2 11.32 11.81 0.81 o 2 9 2 23.97 22.62 0.96 o 3 9 2 9.31 10.03 0.88 o 0 10 2 13.21 15.98 1.93 o 1 10 2 8.61 10.46 1.01 o 1 0 3 26.27 17.98 0.94 o 2 0 3 407.08 411.49 8.82 o 3 0 3 27.49 29.10 1.16 o 4 0 3 35.98 29.62 1.11 o 5 0 3 39.97 38.93 1.01 o 6 0 3 18.78 17.62 0.92 o 7 0 3 16.87 20.65 1.28 o 0 1 3 19.70 17.63 0.73 o 1 1 3 302.67 279.30 6.63 o 2 1 3 282.57 280.77 4.26 o 3 1 3 59.79 54.22 1.37 o 4 1 3 83.10 75.69 1.63 o 5 1 3 20.21 19.34 0.54 o 6 1 3 2.95 3.35 0.48 o 7 1 3 30.12 32.52 1.12 o 0 2 3 193.76 212.53 7.98 o 1 2 3 172.14 178.70 6.97 o 2 2 3 167.89 186.87 5.50 o 3 2 3 55.41 52.51 0.98 o 4 2 3 329.65 321.66 5.54 o 5 2 3 56.00 50.62 1.02 o 6 2 3 17.94 20.56 0.81 o 7 2 3 4.71 5.94 0.71 o 0 3 3 163.51 191.15 8.83 o 1 3 3 60.04 63.92 2.36 o 2 3 3 1046.22 1197.48 28.71 o 3 3 3 361.54 372.32 8.05 o 4 3 3 98.88 88.80 1.83 o 5 3 3 16.11 15.75 0.58 o 6 3 3 15.33 15.87 0.71 o 7 3 3 67.89 76.49 1.38 o 0 4 3 584.95 685.35 24.02 o 1 4 3 258.70 292.17 8.50 o 2 4 3 239.22 282.99 9.80 o 3 4 3 3.92 4.16 0.34 o 4 4 3 178.57 157.04 3.44 o 5 4 3 22.67 22.13 0.70 o 6 4 3 11.25 11.83 0.65 o 0 5 3 17.59 18.69 0.85 o 1 5 3 68.88 74.58 1.86 o 2 5 3 166.99 171.16 5.19 o 3 5 3 222.46 230.03 7.01 o 4 5 3 42.79 40.43 1.38 o 5 5 3 6.41 6.34 0.48 o 6 5 3 9.66 9.57 0.70 o 0 6 3 46.90 58.64 2.09 o 1 6 3 0.34 0.71 0.22 o 2 6 3 145.73 139.94 4.71 o 3 6 3 40.76 41.48 1.41 o 4 6 3 54.90 58.86 1.47 o 5 6 3 6.30 7.06 0.62 o 6 6 3 7.31 7.26 0.71 o 0 7 3 38.21 43.45 2.04 o 1 7 3 90.82 98.41 2.49 o 2 7 3 28.45 31.89 1.54 o 3 7 3 9.23 9.66 0.50 o 4 7 3 3.51 2.29 0.47 o 5 7 3 0.75 0.53 0.54 o 0 8 3 13.20 13.17 0.75 o 1 8 3 116.75 121.97 1.97 o 2 8 3 57.40 55.72 1.03 o 3 8 3 32.21 31.00 0.91 o 4 8 3 39.38 34.77 1.21 o 0 9 3 0.60 0.37 0.78 o 1 9 3 2.84 2.58 0.54 o 2 9 3 3.81 4.39 0.57 o 3 9 3 38.73 36.45 1.14 o 0 10 3 9.06 7.28 1.59 o 0 0 4 38.03 43.86 0.61 o 1 0 4 126.42 118.67 4.38 o 2 0 4 620.15 617.22 16.07 o 3 0 4 335.50 308.39 9.11 o 4 0 4 36.55 34.72 0.90 o 5 0 4 332.70 335.94 6.53 o 6 0 4 19.80 21.35 1.15 o 7 0 4 6.62 8.08 0.99 o 0 1 4 1403.14 1468.56 58.51 o 1 1 4 283.56 265.81 5.69 o 2 1 4 396.11 391.52 7.38 o 3 1 4 78.91 77.30 1.15 o 4 1 4 2.35 2.10 0.24 o 5 1 4 159.19 154.95 2.15 o 6 1 4 25.29 26.25 0.79 o 7 1 4 0.85 0.31 0.65 o 0 2 4 203.80 200.48 3.11 o 1 2 4 54.62 59.63 2.51 o 2 2 4 71.19 66.14 2.20 o 3 2 4 79.58 77.88 1.50 o 4 2 4 29.87 32.34 1.07 o 5 2 4 27.94 25.23 0.98 o 6 2 4 40.28 43.03 1.00 o 7 2 4 7.03 9.23 0.78 o 0 3 4 1708.37 1929.46 61.28 o 1 3 4 147.45 169.28 5.04 o 2 3 4 88.64 83.60 2.14 o 3 3 4 278.34 275.44 7.15 o 4 3 4 11.24 10.07 0.44 o 5 3 4 22.93 20.70 0.66 o 6 3 4 10.71 11.57 0.63 o 7 3 4 0.68 1.76 0.68 o 0 4 4 16.31 18.28 0.87 o 1 4 4 91.65 108.60 2.97 o 2 4 4 118.37 127.26 3.76 o 3 4 4 428.70 404.52 11.76 o 4 4 4 3.79 4.37 0.37 o 5 4 4 62.86 67.33 1.63 o 6 4 4 13.94 13.79 0.69 o 0 5 4 343.40 357.55 18.06 o 1 5 4 102.93 110.68 3.28 o 2 5 4 21.92 21.72 0.64 o 3 5 4 52.47 48.60 1.29 o 4 5 4 50.47 47.69 1.16 o 5 5 4 15.92 15.91 0.64 o 6 5 4 30.35 31.51 0.94 o 0 6 4 149.62 156.46 5.86 o 1 6 4 30.57 33.80 0.96 o 2 6 4 24.76 23.16 0.56 o 3 6 4 190.16 178.67 5.70 o 4 6 4 14.68 15.44 0.61 o 5 6 4 1.61 1.12 0.47 o 0 7 4 112.89 127.56 6.74 o 1 7 4 25.04 25.97 0.67 o 2 7 4 55.32 57.16 1.79 o 3 7 4 3.38 4.13 0.43 o 4 7 4 122.90 115.36 2.72 o 5 7 4 9.50 8.37 0.67 o 0 8 4 7.55 8.09 0.66 o 1 8 4 36.51 37.87 1.30 o 2 8 4 23.53 21.24 0.72 o 3 8 4 16.44 16.84 0.80 o 4 8 4 11.68 10.04 0.72 o 0 9 4 45.01 46.00 1.44 o 1 9 4 2.99 3.13 0.57 o 2 9 4 3.27 3.71 0.67 o 3 9 4 8.07 7.16 0.68 o 1 0 5 146.13 140.64 3.98 o 2 0 5 3.30 2.87 0.23 o 3 0 5 63.29 56.81 1.90 o 4 0 5 65.59 52.56 1.70 o 5 0 5 9.57 13.23 0.85 o 6 0 5 53.12 52.62 1.49 o 7 0 5 1.41 2.53 1.54 o 0 1 5 9.44 7.57 0.44 o 1 1 5 1930.70 1947.99 35.73 o 2 1 5 139.95 138.58 2.92 o 3 1 5 109.38 107.08 2.39 o 4 1 5 79.98 75.10 1.50 o 5 1 5 52.49 45.61 0.77 o 6 1 5 44.72 45.49 1.12 o 7 1 5 2.32 2.24 0.70 o 0 2 5 282.82 272.11 6.47 o 1 2 5 184.19 196.93 5.72 o 2 2 5 32.99 33.83 0.79 o 3 2 5 18.77 18.96 0.47 o 4 2 5 559.59 538.21 7.96 o 5 2 5 25.82 24.59 0.63 o 6 2 5 101.57 106.36 1.43 o 7 2 5 4.49 4.93 0.79 o 0 3 5 126.34 145.37 3.77 o 1 3 5 462.15 492.02 12.40 o 2 3 5 24.17 26.77 0.94 o 3 3 5 57.06 56.01 1.67 o 4 3 5 129.14 115.30 2.98 o 5 3 5 21.08 19.87 0.63 o 6 3 5 28.84 28.84 1.02 o 0 4 5 20.78 19.43 0.78 o 1 4 5 4.67 4.75 0.26 o 2 4 5 30.97 36.28 1.08 o 3 4 5 37.31 37.18 0.88 o 4 4 5 26.46 22.81 0.70 o 5 4 5 6.51 7.03 0.49 o 6 4 5 25.10 24.72 0.91 o 0 5 5 63.05 69.07 4.21 o 1 5 5 362.22 393.03 9.02 o 2 5 5 49.10 47.14 1.55 o 3 5 5 23.62 24.17 0.61 o 4 5 5 14.29 15.36 0.58 o 5 5 5 13.70 13.81 0.60 o 6 5 5 17.91 17.29 0.75 o 0 6 5 48.13 56.99 2.90 o 1 6 5 41.90 44.29 1.24 o 2 6 5 67.95 63.45 1.74 o 3 6 5 58.74 53.26 1.52 o 4 6 5 38.43 39.07 0.81 o 5 6 5 30.00 31.27 0.82 o 0 7 5 35.81 31.31 1.21 o 1 7 5 28.02 26.31 0.69 o 2 7 5 44.16 42.41 1.23 o 3 7 5 1.99 2.48 0.44 o 4 7 5 63.81 60.37 1.11 o 5 7 5 45.57 44.31 1.05 o 0 8 5 3.73 3.39 0.56 o 1 8 5 9.74 10.34 0.55 o 2 8 5 26.05 24.76 0.83 o 3 8 5 13.72 13.03 0.72 o 4 8 5 10.66 10.30 0.75 o 0 9 5 34.33 31.81 1.30 o 1 9 5 63.45 67.39 1.19 o 2 9 5 9.35 10.99 0.76 o 0 0 6 341.06 336.34 7.76 o 1 0 6 13.96 12.08 0.83 o 2 0 6 1.73 1.54 0.23 o 3 0 6 87.29 89.64 2.91 o 4 0 6 57.82 53.35 1.02 o 5 0 6 554.51 554.27 4.70 o 6 0 6 65.46 64.08 1.62 o 7 0 6 6.20 5.48 1.24 o 0 1 6 151.08 134.02 4.30 o 1 1 6 161.83 159.49 3.69 o 2 1 6 873.29 897.06 9.94 o 3 1 6 13.21 13.92 0.48 o 4 1 6 66.00 62.90 1.03 o 5 1 6 10.40 9.86 0.52 o 6 1 6 5.01 5.28 0.66 o 7 1 6 16.22 17.69 1.13 o 0 2 6 17.39 14.98 0.59 o 1 2 6 175.13 195.03 6.61 o 2 2 6 52.09 50.56 1.36 o 3 2 6 209.62 194.72 4.61 o 4 2 6 4.54 4.45 0.43 o 5 2 6 104.56 95.61 1.70 o 6 2 6 3.40 3.42 0.62 o 7 2 6 7.74 9.18 0.87 o 0 3 6 623.78 667.87 13.05 o 1 3 6 93.52 94.93 2.93 o 2 3 6 27.23 25.52 0.78 o 3 3 6 114.13 119.22 3.69 o 4 3 6 0.83 0.44 0.31 o 5 3 6 15.79 16.06 0.60 o 6 3 6 2.68 2.30 0.52 o 0 4 6 21.34 15.84 0.73 o 1 4 6 3.10 2.92 0.34 o 2 4 6 67.70 66.79 2.45 o 3 4 6 89.66 79.61 2.45 o 4 4 6 18.19 17.84 0.59 o 5 4 6 36.57 34.95 0.76 o 6 4 6 26.39 28.16 0.89 o 0 5 6 0.20 0.28 0.37 o 1 5 6 15.23 16.23 0.51 o 2 5 6 139.32 131.97 3.41 o 3 5 6 123.21 112.84 3.11 o 4 5 6 9.82 9.42 0.50 o 5 5 6 32.43 30.92 0.78 o 6 5 6 22.93 23.83 0.82 o 0 6 6 3.76 3.91 0.49 o 1 6 6 45.45 42.88 1.37 o 2 6 6 14.27 12.79 0.53 o 3 6 6 36.86 35.72 0.97 o 4 6 6 48.68 48.03 1.24 o 5 6 6 16.95 15.79 0.74 o 0 7 6 230.73 233.81 10.65 o 1 7 6 59.74 59.96 1.73 o 2 7 6 16.08 14.46 0.63 o 3 7 6 27.98 24.87 0.78 o 4 7 6 9.07 8.30 0.66 o 0 8 6 1.37 1.34 0.53 o 1 8 6 3.20 1.96 0.43 o 2 8 6 45.10 42.67 1.38 o 3 8 6 8.69 8.51 0.72 o 0 9 6 1.77 1.80 0.72 o 1 9 6 22.08 19.70 0.93 o 2 9 6 16.63 16.47 0.91 o 1 0 7 20.84 29.54 0.91 o 2 0 7 462.40 417.98 11.29 o 3 0 7 249.95 234.98 6.38 o 4 0 7 47.74 44.01 1.05 o 5 0 7 14.03 14.42 1.32 o 6 0 7 7.98 10.44 2.19 o 7 0 7 8.67 10.04 1.41 o 0 1 7 35.02 32.50 0.73 o 1 1 7 76.68 78.22 1.58 o 2 1 7 155.16 146.90 3.94 o 3 1 7 43.67 39.86 0.95 o 4 1 7 201.92 189.60 2.58 o 5 1 7 3.96 3.70 0.49 o 6 1 7 45.78 46.30 1.17 o 0 2 7 0.41 0.93 0.20 o 1 2 7 204.81 217.93 4.87 o 2 2 7 54.62 51.89 1.70 o 3 2 7 24.78 20.48 0.58 o 4 2 7 102.56 98.69 2.13 o 5 2 7 41.41 39.69 0.83 o 6 2 7 13.90 13.63 0.84 o 0 3 7 284.54 260.88 8.28 o 1 3 7 109.14 110.93 2.79 o 2 3 7 102.70 108.55 3.24 o 3 3 7 74.43 67.73 2.17 o 4 3 7 35.53 35.05 0.77 o 5 3 7 7.56 6.44 0.47 o 6 3 7 2.86 2.07 0.59 o 0 4 7 1.14 0.77 0.36 o 1 4 7 35.56 36.58 1.07 o 2 4 7 310.14 307.31 10.13 o 3 4 7 53.74 49.68 1.18 o 4 4 7 66.46 60.67 1.32 o 5 4 7 11.07 10.91 0.57 o 6 4 7 17.51 17.56 0.79 o 0 5 7 44.23 38.00 2.03 o 1 5 7 85.32 80.35 2.04 o 2 5 7 46.71 49.64 1.43 o 3 5 7 21.32 18.22 0.59 o 4 5 7 20.42 18.60 0.69 o 5 5 7 6.40 6.87 0.54 o 0 6 7 8.76 7.08 0.58 o 1 6 7 78.79 74.67 2.14 o 2 6 7 69.92 68.86 2.11 o 3 6 7 42.53 42.29 1.40 o 4 6 7 21.30 20.44 0.76 o 5 6 7 9.80 11.03 0.64 o 0 7 7 24.19 24.74 0.98 o 1 7 7 3.42 4.00 0.44 o 2 7 7 3.67 3.94 0.61 o 3 7 7 55.51 56.86 1.13 o 4 7 7 38.98 37.06 0.97 o 0 8 7 13.57 11.82 0.95 o 1 8 7 63.97 61.43 1.44 o 2 8 7 39.44 37.42 0.99 o 3 8 7 20.79 19.83 0.88 o 0 9 7 0.21 0.01 0.66 o 1 9 7 20.77 19.97 0.89 o 0 0 8 144.52 149.62 3.41 o 1 0 8 1.86 2.57 0.27 o 2 0 8 12.71 13.30 0.62 o 3 0 8 0.00 -0.11 0.33 o 4 0 8 42.71 38.88 1.10 o 5 0 8 12.29 12.70 1.16 o 6 0 8 19.51 21.17 1.57 o 0 1 8 306.33 330.48 10.65 o 1 1 8 44.44 40.13 1.09 o 2 1 8 0.94 0.35 0.21 o 3 1 8 330.87 313.45 5.51 o 4 1 8 36.33 35.51 0.78 o 5 1 8 2.28 1.18 0.44 o 6 1 8 40.30 42.16 1.31 o 0 2 8 0.82 1.12 0.23 o 1 2 8 37.61 36.02 1.03 o 2 2 8 4.17 4.69 0.28 o 3 2 8 130.37 118.46 2.98 o 4 2 8 46.61 43.74 1.06 o 5 2 8 8.66 9.18 0.60 o 6 2 8 44.75 48.69 1.23 o 0 3 8 19.75 23.90 0.86 o 1 3 8 81.20 72.26 1.32 o 2 3 8 62.94 64.82 1.81 o 3 3 8 245.03 236.00 5.56 o 4 3 8 8.57 8.36 0.46 o 5 3 8 39.19 40.31 0.92 o 6 3 8 6.65 6.19 0.66 o 0 4 8 192.37 192.85 6.28 o 1 4 8 25.27 24.47 0.65 o 2 4 8 141.14 129.78 3.52 o 3 4 8 35.54 38.38 1.48 o 4 4 8 0.09 0.37 0.34 o 5 4 8 9.75 10.22 0.58 o 6 4 8 2.24 1.68 0.62 o 0 5 8 1.37 1.93 0.44 o 1 5 8 142.00 133.60 3.41 o 2 5 8 63.44 69.66 2.11 o 3 5 8 60.82 55.57 1.56 o 4 5 8 40.57 36.98 0.79 o 5 5 8 15.75 16.12 0.70 o 0 6 8 50.40 44.50 2.27 o 1 6 8 9.97 8.35 0.46 o 2 6 8 101.70 95.19 2.20 o 3 6 8 80.33 78.03 2.02 o 4 6 8 32.60 32.38 0.88 o 5 6 8 1.14 0.75 0.55 o 0 7 8 0.00 0.01 0.47 o 1 7 8 34.95 33.98 1.10 o 2 7 8 14.85 14.61 0.73 o 3 7 8 6.13 5.33 0.65 o 4 7 8 27.44 25.57 0.96 o 0 8 8 35.24 37.11 1.81 o 1 8 8 13.85 13.75 0.67 o 2 8 8 19.85 19.38 0.86 o 3 8 8 8.42 8.61 0.80 o 0 9 8 28.23 25.93 1.37 o 1 0 9 41.36 38.43 1.10 o 2 0 9 13.83 13.15 0.68 o 3 0 9 65.32 53.84 1.80 o 4 0 9 0.01 -0.38 0.55 o 5 0 9 15.17 17.85 2.25 o 6 0 9 0.19 1.13 1.54 o 0 1 9 147.37 134.28 2.60 o 1 1 9 142.35 133.79 2.91 o 2 1 9 31.93 29.59 0.94 o 3 1 9 18.23 16.16 0.49 o 4 1 9 85.71 79.21 1.62 o 5 1 9 16.65 17.68 0.75 o 6 1 9 20.15 22.76 1.15 o 0 2 9 19.55 20.40 0.85 o 1 2 9 464.75 465.80 9.70 o 2 2 9 93.01 85.12 2.41 o 3 2 9 17.87 15.93 0.47 o 4 2 9 9.51 10.77 0.49 o 5 2 9 1.31 0.84 0.50 o 6 2 9 3.38 3.31 0.71 o 0 3 9 16.33 14.64 0.72 o 1 3 9 141.81 132.56 2.66 o 2 3 9 253.50 240.51 4.69 o 3 3 9 28.09 24.00 0.60 o 4 3 9 41.45 41.39 0.90 o 5 3 9 13.23 13.00 0.71 o 6 3 9 19.40 19.46 0.90 o 0 4 9 151.41 142.39 4.88 o 1 4 9 69.74 71.19 1.96 o 2 4 9 22.15 15.86 0.54 o 3 4 9 5.03 5.78 0.39 o 4 4 9 13.32 13.61 0.57 o 5 4 9 32.17 29.57 0.79 o 0 5 9 67.81 64.15 2.17 o 1 5 9 13.00 14.51 0.54 o 2 5 9 69.09 62.39 1.74 o 3 5 9 38.41 35.34 1.05 o 4 5 9 46.57 46.94 1.18 o 5 5 9 5.66 5.39 0.59 o 0 6 9 30.09 27.41 0.96 o 1 6 9 91.68 94.55 2.44 o 2 6 9 1.11 0.97 0.39 o 3 6 9 26.19 24.15 0.89 o 4 6 9 1.89 2.26 0.56 o 0 7 9 0.41 0.21 0.52 o 1 7 9 13.24 14.48 0.66 o 2 7 9 11.74 11.13 0.68 o 3 7 9 0.70 0.26 0.57 o 0 8 9 2.88 2.63 0.66 o 1 8 9 25.53 23.73 0.99 o 2 8 9 0.09 0.04 0.59 o 0 0 10 950.56 951.32 40.00 o 1 0 10 53.17 48.43 1.86 o 2 0 10 228.27 221.79 5.71 o 3 0 10 60.79 52.81 2.02 o 4 0 10 50.79 52.31 1.36 o 5 0 10 12.88 15.39 1.33 o 6 0 10 12.04 13.44 1.45 o 0 1 10 351.91 343.93 9.19 o 1 1 10 13.43 13.40 0.41 o 2 1 10 14.52 12.90 0.43 o 3 1 10 71.38 63.81 0.98 o 4 1 10 3.94 3.74 0.39 o 5 1 10 50.15 53.39 1.21 o 6 1 10 10.39 12.22 0.99 o 0 2 10 5.43 5.47 0.49 o 1 2 10 92.82 86.77 1.92 o 2 2 10 109.97 102.78 2.27 o 3 2 10 27.08 22.06 0.68 o 4 2 10 34.73 34.00 0.83 o 5 2 10 0.98 1.10 0.52 o 6 2 10 0.80 1.60 0.78 o 0 3 10 15.85 15.74 0.74 o 1 3 10 11.02 9.07 0.43 o 2 3 10 20.35 18.60 0.62 o 3 3 10 12.86 12.24 0.48 o 4 3 10 29.25 25.90 0.74 o 5 3 10 40.36 40.31 0.93 o 0 4 10 142.16 132.21 3.69 o 1 4 10 123.00 109.86 2.65 o 2 4 10 170.47 173.42 3.05 o 3 4 10 1.49 1.98 0.37 o 4 4 10 26.67 25.64 0.72 o 5 4 10 26.24 27.34 0.87 o 0 5 10 7.00 5.98 0.60 o 1 5 10 22.98 19.28 0.65 o 2 5 10 2.82 2.84 0.42 o 3 5 10 4.30 3.14 0.56 o 4 5 10 1.91 1.70 0.49 o 5 5 10 30.77 29.37 1.06 o 0 6 10 36.67 38.21 1.26 o 1 6 10 3.34 3.02 0.41 o 2 6 10 18.00 17.92 0.70 o 3 6 10 2.39 1.86 0.52 o 4 6 10 2.56 2.09 0.57 o 0 7 10 25.12 25.27 1.58 o 1 7 10 39.30 37.31 0.90 o 2 7 10 15.61 15.00 0.76 o 3 7 10 5.35 4.88 0.65 o 0 8 10 10.37 11.31 1.05 o 1 8 10 0.60 0.53 0.49 o 1 0 11 308.81 301.97 7.72 o 2 0 11 73.71 68.62 2.37 o 3 0 11 28.54 23.88 0.90 o 4 0 11 3.80 2.61 0.68 o 5 0 11 10.33 11.65 1.27 o 0 1 11 4.11 4.28 0.42 o 1 1 11 86.09 77.98 1.61 o 2 1 11 53.59 49.70 1.49 o 3 1 11 25.56 23.87 0.59 o 4 1 11 32.84 34.11 0.80 o 5 1 11 1.43 1.71 0.61 o 0 2 11 200.08 175.46 5.85 o 1 2 11 324.64 315.62 4.06 o 2 2 11 45.30 42.74 0.84 o 3 2 11 1.60 1.86 0.40 o 4 2 11 4.01 5.16 0.46 o 5 2 11 12.41 15.84 0.88 o 0 3 11 36.72 34.92 1.49 o 1 3 11 27.15 26.44 0.62 o 2 3 11 32.16 31.24 0.87 o 3 3 11 17.43 17.77 0.61 o 4 3 11 24.05 23.62 0.75 o 5 3 11 0.60 -0.06 0.56 o 0 4 11 8.80 10.57 0.86 o 1 4 11 38.44 34.23 0.84 o 2 4 11 0.67 -0.24 0.36 o 3 4 11 23.90 22.28 0.78 o 4 4 11 0.89 0.40 0.49 o 5 4 11 2.83 2.78 0.57 o 0 5 11 19.94 20.64 0.94 o 1 5 11 27.57 28.99 0.88 o 2 5 11 1.74 1.65 0.42 o 3 5 11 8.24 8.36 0.63 o 4 5 11 12.64 12.75 0.83 o 0 6 11 58.40 57.40 1.68 o 1 6 11 18.94 17.85 0.71 o 2 6 11 0.35 0.20 0.43 o 3 6 11 5.71 4.84 0.62 o 0 7 11 21.74 20.50 1.04 o 1 7 11 0.39 0.29 0.51 o 2 7 11 22.85 21.90 0.91 o 0 0 12 464.17 412.93 5.17 o 1 0 12 62.87 62.12 2.10 o 2 0 12 4.43 5.69 0.59 o 3 0 12 15.54 16.77 0.85 o 4 0 12 1.84 2.70 0.72 o 5 0 12 15.28 18.00 1.50 o 0 1 12 38.66 38.24 0.98 o 1 1 12 10.40 10.17 0.46 o 2 1 12 69.79 63.97 1.45 o 3 1 12 72.85 68.70 1.76 o 4 1 12 28.03 29.69 0.82 o 5 1 12 5.39 5.44 0.72 o 0 2 12 68.30 60.51 1.31 o 1 2 12 33.58 34.45 0.83 o 2 2 12 56.01 53.64 1.24 o 3 2 12 53.38 57.99 1.16 o 4 2 12 1.56 1.47 0.43 o 5 2 12 13.74 15.19 0.90 o 0 3 12 3.72 4.57 0.55 o 1 3 12 19.17 17.68 0.59 o 2 3 12 37.55 33.33 0.72 o 3 3 12 1.10 1.59 0.51 o 4 3 12 4.07 5.14 0.55 o 5 3 12 0.46 -0.07 0.58 o 0 4 12 7.90 6.50 0.63 o 1 4 12 8.49 8.59 0.48 o 2 4 12 1.56 1.65 0.43 o 3 4 12 6.03 5.58 0.56 o 4 4 12 2.17 2.06 0.63 o 0 5 12 47.39 45.67 1.67 o 1 5 12 22.82 21.44 0.68 o 2 5 12 12.88 13.30 0.65 o 3 5 12 81.91 84.49 2.04 o 4 5 12 12.93 12.38 0.87 o 0 6 12 5.49 4.30 0.67 o 1 6 12 36.62 35.39 1.06 o 2 6 12 24.31 24.97 0.84 o 3 6 12 19.22 19.42 0.90 o 0 7 12 19.73 19.30 1.18 o 1 7 12 0.83 0.39 0.52 o 1 0 13 4.31 2.55 0.60 o 2 0 13 86.36 85.48 1.65 o 3 0 13 0.17 -0.46 0.52 o 4 0 13 0.01 0.64 0.83 o 5 0 13 36.70 46.28 2.03 o 0 1 13 4.89 5.70 0.69 o 1 1 13 113.75 109.45 2.47 o 2 1 13 4.23 4.53 0.45 o 3 1 13 3.63 4.20 0.44 o 4 1 13 0.21 -0.02 0.47 o 5 1 13 1.65 2.32 0.71 o 0 2 13 5.05 4.47 0.55 o 1 2 13 1.25 1.33 0.46 o 2 2 13 27.28 27.35 0.75 o 3 2 13 2.25 2.97 0.46 o 4 2 13 10.56 11.86 0.66 o 0 3 13 6.89 6.79 0.64 o 1 3 13 33.00 32.46 0.71 o 2 3 13 44.96 45.26 1.35 o 3 3 13 28.05 28.99 1.35 o 4 3 13 28.97 31.37 1.06 o 0 4 13 64.32 66.94 1.80 o 1 4 13 5.52 5.88 0.48 o 2 4 13 83.11 84.56 1.73 o 3 4 13 20.15 21.73 0.95 o 4 4 13 26.34 28.02 1.10 o 0 5 13 7.35 7.31 0.72 o 1 5 13 8.97 8.98 0.68 o 2 5 13 5.49 5.33 0.61 o 3 5 13 2.62 1.34 0.64 o 0 6 13 24.01 21.45 1.04 o 1 6 13 13.88 14.85 0.74 o 2 6 13 6.91 7.46 0.65 o 0 0 14 7.91 10.69 1.54 o 1 0 14 0.07 -0.27 0.56 o 2 0 14 21.17 25.22 1.15 o 3 0 14 4.66 5.59 0.70 o 4 0 14 0.50 1.55 0.81 o 0 1 14 18.96 22.09 1.06 o 1 1 14 6.01 5.87 0.53 o 2 1 14 31.28 28.54 0.85 o 3 1 14 0.87 0.93 0.47 o 4 1 14 10.81 13.20 0.77 o 0 2 14 5.17 5.90 0.76 o 1 2 14 62.62 61.93 1.01 o 2 2 14 3.04 3.26 0.48 o 3 2 14 0.16 0.65 0.56 o 4 2 14 18.23 22.39 1.05 o 0 3 14 47.03 47.02 1.49 o 1 3 14 10.16 11.30 0.60 o 2 3 14 14.26 16.42 0.78 o 3 3 14 27.78 30.33 0.93 o 4 3 14 23.50 23.54 1.19 o 0 4 14 18.18 19.95 0.96 o 1 4 14 12.89 12.78 0.60 o 2 4 14 1.12 0.22 0.51 o 3 4 14 69.82 77.38 1.34 o 0 5 14 26.88 29.05 1.14 o 1 5 14 9.96 10.33 0.61 o 2 5 14 39.55 41.54 1.10 o 0 6 14 0.67 0.34 0.66 o 1 0 15 3.18 3.63 0.88 o 2 0 15 10.87 15.07 1.27 o 3 0 15 0.11 0.69 0.75 o 0 1 15 32.14 32.27 1.27 o 1 1 15 46.14 51.68 1.16 o 2 1 15 0.60 0.59 0.53 o 3 1 15 10.20 11.79 0.81 o 0 2 15 1.04 0.07 0.65 o 1 2 15 2.05 2.25 0.62 o 2 2 15 10.52 12.66 0.71 o 3 2 15 19.84 20.91 0.99 o 0 3 15 8.80 8.26 0.90 o 1 3 15 45.36 47.77 0.98 o 2 3 15 20.64 22.66 0.82 o 3 3 15 1.69 0.98 0.63 o 0 4 15 33.22 32.70 2.23 o 1 4 15 2.55 2.17 0.51 o 2 4 15 1.30 0.25 0.55 o 0 5 15 16.97 18.67 1.06 o 1 5 15 22.78 23.72 0.98 o 0 0 16 4.75 6.60 1.54 o 1 0 16 0.12 -0.20 0.84 o 2 0 16 18.14 19.93 2.13 o 3 0 16 12.14 13.56 1.13 o 0 1 16 82.52 96.40 2.70 o 1 1 16 2.25 2.11 0.59 o 2 1 16 11.64 11.44 0.80 o 3 1 16 5.34 5.85 0.81 o 0 2 16 2.80 2.92 0.82 o 1 2 16 6.65 7.82 0.82 o 2 2 16 19.26 23.64 1.03 o 0 3 16 24.28 26.39 1.96 o 1 3 16 25.45 26.60 0.94 o 2 3 16 0.98 0.40 0.64 o 0 4 16 0.00 0.02 0.81 o 1 0 17 14.06 15.53 1.41 o 0 1 17 0.61 0.45 0.96 o 1 1 17 23.88 29.40 1.21 o 0 2 17 7.28 7.95 1.23 o 1 2 17 0.49 0.75 0.63 o