#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/23/2202368.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202368_Fobs loop_ _publ_author_name 'Xu, Tao' 'Yang, Shi-Yao' 'Xie, Zhao-Xiong' 'Ng, Seik Weng' _publ_section_title ; Bis(diisopropylammonium) dimethyldioxalatostannate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m870 _journal_page_last m872 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.128 _cell_angle_gamma 90.000 _cell_length_a 16.4714 _cell_length_b 14.0769 _cell_length_c 11.0443 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file bt6338Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 304.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 31863.69 34340.97 550.84 o 4 0 0 8517.15 9053.06 182.98 o 6 0 0 45772.55 47876.57 334.46 o 8 0 0 17793.77 18939.84 214.68 o 10 0 0 11873.96 13849.14 270.90 o 12 0 0 499.65 670.53 59.59 o 14 0 0 191.58 216.14 54.35 o 16 0 0 6157.23 6264.44 198.64 o 1 1 0 2141.99 2274.62 33.65 o 3 1 0 32141.39 35083.86 257.67 o 5 1 0 67.85 65.05 14.03 o 7 1 0 6855.81 7166.33 87.98 o 9 1 0 5364.39 5807.87 91.32 o 11 1 0 2020.41 2350.80 76.29 o 13 1 0 2487.71 2306.29 149.09 o 15 1 0 1502.41 1526.26 67.33 o 17 1 0 770.89 825.79 81.18 o 19 1 0 541.17 614.20 189.66 o 0 2 0 82548.95 79547.95 1296.77 o 2 2 0 16356.74 17585.77 144.73 o 4 2 0 119.54 124.50 16.08 o 6 2 0 25456.79 27817.94 208.54 o 8 2 0 3453.39 3413.85 71.65 o 10 2 0 2774.53 2780.49 78.78 o 12 2 0 4.49 32.73 18.36 o 14 2 0 14.54 62.44 23.93 o 16 2 0 1048.76 1011.68 73.01 o 18 2 0 76.80 77.71 65.08 o 1 3 0 11795.92 12390.72 98.33 o 3 3 0 6432.57 6334.68 100.70 o 5 3 0 61.80 53.57 14.23 o 7 3 0 16806.80 17143.02 144.59 o 9 3 0 35183.33 38592.56 456.77 o 11 3 0 6505.54 6241.81 372.12 o 13 3 0 4634.78 3992.96 398.94 o 15 3 0 4407.65 4553.33 132.48 o 17 3 0 2403.89 2500.42 137.58 o 19 3 0 1267.73 1331.88 241.34 o 0 4 0 2626.98 3008.10 72.83 o 2 4 0 23397.38 23842.97 261.23 o 4 4 0 10945.78 11445.26 225.63 o 6 4 0 5904.14 6513.60 85.27 o 8 4 0 1903.56 1694.68 52.50 o 10 4 0 1616.32 1571.79 80.55 o 12 4 0 4312.75 4408.21 116.71 o 14 4 0 2046.17 2073.91 102.27 o 16 4 0 269.41 354.95 61.70 o 18 4 0 1318.57 1535.35 148.83 o 1 5 0 4282.78 4398.09 99.72 o 3 5 0 314.28 291.90 20.93 o 5 5 0 2899.85 3193.63 57.68 o 7 5 0 582.88 556.17 30.86 o 9 5 0 1572.50 1535.67 83.34 o 11 5 0 144.24 166.31 31.74 o 13 5 0 117.90 138.38 38.88 o 15 5 0 120.01 166.16 47.19 o 17 5 0 126.42 187.47 51.21 o 0 6 0 25521.62 28111.85 251.48 o 2 6 0 12893.98 13789.72 215.48 o 4 6 0 4720.34 4091.98 66.13 o 6 6 0 5707.24 5228.04 77.84 o 8 6 0 10532.46 10557.40 187.08 o 10 6 0 2720.59 2705.17 86.91 o 12 6 0 2754.60 2583.91 106.74 o 14 6 0 958.20 888.34 72.45 o 16 6 0 769.31 737.80 81.65 o 18 6 0 1509.59 1685.10 122.97 o 1 7 0 8907.77 9484.33 112.22 o 3 7 0 7911.72 7949.90 99.56 o 5 7 0 17742.12 18937.35 151.30 o 7 7 0 6872.28 6767.53 126.98 o 9 7 0 4823.10 4648.83 109.17 o 11 7 0 4427.22 4228.19 134.00 o 13 7 0 1299.71 1229.28 80.77 o 15 7 0 2088.96 1994.50 126.54 o 17 7 0 326.36 393.44 63.16 o 0 8 0 451.15 490.83 44.86 o 2 8 0 6.46 36.08 15.44 o 4 8 0 347.75 323.24 26.36 o 6 8 0 135.10 161.85 28.75 o 8 8 0 136.74 140.07 34.77 o 10 8 0 11.61 16.24 25.44 o 12 8 0 160.91 197.12 43.28 o 14 8 0 25.37 61.52 35.35 o 16 8 0 0.28 46.56 32.82 o 1 9 0 10373.46 10942.12 138.89 o 3 9 0 3966.45 3910.52 182.61 o 5 9 0 2492.34 1850.67 240.59 o 7 9 0 4324.71 3870.66 121.20 o 9 9 0 4232.21 3864.35 128.66 o 11 9 0 876.96 904.08 71.90 o 13 9 0 578.53 562.70 59.51 o 15 9 0 986.99 951.13 92.40 o 0 10 0 6262.01 6942.82 157.65 o 2 10 0 3382.03 3242.21 77.53 o 4 10 0 5362.71 4807.02 333.95 o 6 10 0 5276.14 4948.84 139.34 o 8 10 0 924.95 870.14 66.84 o 10 10 0 1709.96 1559.86 89.26 o 12 10 0 1647.91 1647.82 97.03 o 14 10 0 593.38 658.03 78.44 o 1 11 0 96.07 136.88 30.47 o 3 11 0 590.53 573.55 51.60 o 5 11 0 12.25 6.79 23.64 o 7 11 0 48.74 69.87 33.02 o 9 11 0 82.69 122.91 38.92 o 11 11 0 46.31 79.18 34.54 o 13 11 0 393.82 422.64 66.52 o 0 12 0 1753.61 1730.59 148.88 o 2 12 0 845.71 852.56 63.74 o 4 12 0 226.27 194.75 43.21 o 6 12 0 714.84 705.17 62.18 o 8 12 0 796.64 744.68 66.65 o 10 12 0 464.29 480.75 58.45 o 12 12 0 293.60 321.23 54.73 o 1 13 0 579.34 672.08 72.95 o 3 13 0 2427.47 2474.99 107.03 o 5 13 0 963.16 974.53 74.35 o 7 13 0 680.88 674.01 64.47 o 9 13 0 693.73 754.27 70.51 o 11 13 0 542.81 614.64 66.63 o 0 14 0 635.91 669.58 146.31 o 2 14 0 537.98 580.58 73.72 o 4 14 0 534.67 583.53 62.36 o 6 14 0 368.43 449.64 56.63 o 8 14 0 11.98 56.95 32.85 o 10 14 0 77.20 136.41 41.50 o 1 15 0 122.19 177.66 73.48 o 3 15 0 106.26 171.48 72.69 o 5 15 0 47.26 61.54 34.50 o 7 15 0 85.46 140.47 41.38 o 0 16 0 496.68 660.32 155.30 o 2 16 0 501.99 683.81 111.25 o 4 16 0 820.61 879.23 121.04 o -19 1 1 1008.32 1205.81 122.67 o -17 1 1 2540.33 2470.67 137.44 o -15 1 1 6983.69 7178.46 158.79 o -13 1 1 2704.63 2670.54 88.61 o -11 1 1 3929.55 3747.64 85.22 o -9 1 1 15095.67 17112.12 156.22 o -7 1 1 9561.88 10234.61 106.85 o -5 1 1 15658.39 17178.34 169.34 o -3 1 1 45302.40 47795.88 374.45 o -1 1 1 8112.62 8411.01 100.92 o 1 1 1 64804.86 68270.24 395.69 o 3 1 1 80944.74 81503.34 1160.07 o 5 1 1 12136.29 13760.43 133.30 o 7 1 1 22261.61 26050.77 786.40 o 9 1 1 14154.03 15396.51 282.52 o 11 1 1 5779.85 5822.42 110.73 o 13 1 1 1104.33 944.41 57.35 o 15 1 1 158.18 250.45 42.71 o 17 1 1 775.50 923.78 113.67 o -18 2 1 1120.68 1225.05 103.59 o -16 2 1 1948.64 2103.08 125.65 o -14 2 1 2078.85 2180.58 77.27 o -12 2 1 4915.22 4770.50 101.63 o -10 2 1 8163.23 8378.97 121.93 o -8 2 1 18919.71 21041.03 198.81 o -6 2 1 48177.21 53982.59 239.05 o -4 2 1 25165.34 27337.92 276.83 o -2 2 1 27663.60 28496.26 135.21 o 0 2 1 80418.19 82142.37 376.11 o 2 2 1 3418.85 4063.41 83.63 o 4 2 1 5293.36 5265.65 78.51 o 6 2 1 4675.63 4744.86 71.01 o 8 2 1 3089.90 3187.65 67.20 o 10 2 1 8335.21 8983.96 123.04 o 12 2 1 4563.42 4531.66 105.42 o 14 2 1 2777.10 2779.85 101.30 o 16 2 1 3683.29 3886.47 146.98 o 18 2 1 1929.88 2073.69 128.34 o -19 3 1 145.70 178.50 87.06 o -17 3 1 28.41 91.86 38.97 o -15 3 1 45.75 106.07 30.35 o -13 3 1 338.77 395.56 35.70 o -11 3 1 16.30 34.50 16.92 o -9 3 1 43.65 46.35 17.47 o -7 3 1 374.88 370.68 26.73 o -5 3 1 1257.19 1343.64 38.67 o -3 3 1 8021.87 8291.89 109.33 o -1 3 1 532.90 547.78 22.93 o 1 3 1 111.77 170.69 15.06 o 3 3 1 283.18 604.71 243.05 o 5 3 1 37.79 84.08 15.28 o 7 3 1 481.65 654.92 32.97 o 9 3 1 697.50 702.08 39.34 o 11 3 1 45.45 61.11 20.43 o 13 3 1 1752.41 1685.63 77.51 o 15 3 1 1007.56 1087.25 80.94 o 17 3 1 59.18 154.02 44.01 o -18 4 1 485.56 513.53 116.14 o -16 4 1 656.04 729.90 85.34 o -14 4 1 1426.78 1361.87 75.97 o -12 4 1 2324.15 2230.28 81.63 o -10 4 1 2324.74 1859.79 137.05 o -8 4 1 15949.51 18000.88 246.03 o -6 4 1 16064.00 17586.89 140.71 o -4 4 1 854.80 686.93 29.20 o -2 4 1 3616.85 3325.82 63.33 o 0 4 1 8988.45 8820.54 82.38 o 2 4 1 7323.15 7207.98 72.09 o 4 4 1 317.02 280.28 24.67 o 6 4 1 4308.14 4544.38 78.22 o 8 4 1 4977.85 5097.88 84.83 o 10 4 1 3122.30 2636.16 198.19 o 12 4 1 1959.21 1877.88 86.36 o 14 4 1 1344.64 1248.59 82.28 o 16 4 1 1856.57 1830.76 104.98 o 18 4 1 1366.74 1479.34 112.92 o -17 5 1 1742.48 1788.48 158.56 o -15 5 1 2382.18 2314.98 127.82 o -13 5 1 3179.98 3113.01 102.17 o -11 5 1 5070.53 5053.95 127.50 o -9 5 1 7241.08 7233.74 109.52 o -7 5 1 2234.22 2485.81 64.38 o -5 5 1 4915.87 4619.96 80.63 o -3 5 1 4216.89 3891.72 64.73 o -1 5 1 8608.09 9111.69 103.14 o 1 5 1 5667.90 5025.38 67.68 o 3 5 1 32534.48 34962.36 341.36 o 5 5 1 19785.41 20645.28 180.27 o 7 5 1 13695.52 13838.69 257.68 o 9 5 1 17624.00 15932.25 1239.77 o 11 5 1 4908.30 4381.97 132.97 o 13 5 1 3637.38 3519.98 130.15 o 15 5 1 3371.91 3301.57 135.52 o 17 5 1 425.26 569.17 74.93 o -18 6 1 434.99 659.96 110.59 o -16 6 1 151.97 232.50 55.44 o -14 6 1 532.64 542.71 67.32 o -12 6 1 1981.35 2002.78 81.23 o -10 6 1 2138.71 2087.68 129.06 o -8 6 1 1745.29 1909.42 57.66 o -6 6 1 1549.97 1451.98 47.65 o -4 6 1 7781.99 8009.73 98.05 o -2 6 1 9110.96 9612.08 105.36 o 0 6 1 835.14 770.17 33.01 o 2 6 1 7275.28 7990.95 228.35 o 4 6 1 4197.90 4433.68 84.20 o 6 6 1 5683.16 6271.27 107.09 o 8 6 1 448.60 447.35 44.76 o 10 6 1 475.13 451.94 49.76 o 12 6 1 1007.51 975.14 71.26 o 14 6 1 34.27 57.35 32.83 o 16 6 1 1.52 49.77 31.46 o -17 7 1 381.80 482.15 94.13 o -15 7 1 380.02 422.65 63.57 o -13 7 1 493.51 444.05 60.61 o -11 7 1 420.44 348.95 39.80 o -9 7 1 721.99 628.38 45.74 o -7 7 1 1242.28 1163.02 45.64 o -5 7 1 20.77 49.33 15.72 o -3 7 1 5696.76 5890.17 89.22 o -1 7 1 228.51 138.18 21.86 o 1 7 1 2261.83 2230.48 55.81 o 3 7 1 5939.31 6196.27 132.79 o 5 7 1 2701.09 2922.61 76.95 o 7 7 1 2683.50 2026.68 269.41 o 9 7 1 3530.28 3130.64 111.90 o 11 7 1 553.76 511.70 54.94 o 13 7 1 1033.54 957.20 73.98 o 15 7 1 528.34 519.57 60.86 o 17 7 1 78.39 163.48 48.86 o -16 8 1 937.65 945.27 92.93 o -14 8 1 1204.38 1077.18 93.08 o -12 8 1 4294.58 3819.09 131.44 o -10 8 1 6525.16 5111.28 549.43 o -8 8 1 5735.72 5782.79 264.24 o -6 8 1 11761.42 11881.64 191.91 o -4 8 1 13306.46 12807.90 197.09 o -2 8 1 12392.16 12952.41 162.98 o 0 8 1 17739.16 19253.75 250.50 o 2 8 1 7949.78 8457.24 122.24 o 4 8 1 11228.44 11070.77 148.24 o 6 8 1 6215.14 5959.55 144.71 o 8 8 1 1725.29 1495.58 92.16 o 10 8 1 2811.33 2643.29 109.64 o 12 8 1 2798.59 2618.37 115.12 o 14 8 1 212.60 299.41 53.00 o 16 8 1 585.37 602.45 77.63 o -15 9 1 895.66 972.53 92.06 o -13 9 1 463.07 511.60 69.22 o -11 9 1 1273.69 1238.81 80.74 o -9 9 1 1921.79 1832.79 90.72 o -7 9 1 2054.09 1999.70 76.78 o -5 9 1 1709.43 1679.80 68.23 o -3 9 1 2080.36 2137.78 118.81 o -1 9 1 888.05 722.97 99.46 o 1 9 1 4991.26 5100.93 90.52 o 3 9 1 1625.66 1384.92 114.25 o 5 9 1 1648.87 1522.20 77.18 o 7 9 1 1995.51 1835.87 87.67 o 9 9 1 1605.79 1726.42 131.90 o 11 9 1 516.36 478.64 55.18 o 13 9 1 448.07 460.91 57.28 o 15 9 1 265.76 356.15 55.65 o -14 10 1 61.22 82.77 41.38 o -12 10 1 233.03 250.24 56.53 o -10 10 1 629.55 554.60 58.02 o -8 10 1 346.36 300.48 48.54 o -6 10 1 1160.47 1092.84 60.16 o -4 10 1 1355.68 1335.31 69.78 o -2 10 1 1241.11 1068.25 51.34 o 0 10 1 2059.84 1949.14 64.15 o 2 10 1 797.62 781.93 49.55 o 4 10 1 218.07 222.04 41.60 o 6 10 1 514.03 518.55 53.44 o 8 10 1 3.22 14.85 25.27 o 10 10 1 267.14 276.67 49.66 o 12 10 1 98.43 134.96 40.47 o 14 10 1 1.93 36.43 29.06 o -13 11 1 694.92 736.34 81.47 o -11 11 1 597.96 585.70 61.93 o -9 11 1 3009.95 2807.47 117.96 o -7 11 1 1777.89 1737.05 91.16 o -5 11 1 2634.16 2457.05 89.21 o -3 11 1 2691.16 2358.36 218.34 o -1 11 1 2735.16 2751.42 78.58 o 1 11 1 4034.59 3971.60 132.91 o 3 11 1 3825.21 3739.17 121.49 o 5 11 1 220.00 226.24 44.71 o 7 11 1 2497.30 2225.80 103.83 o 9 11 1 2182.16 2128.96 106.53 o 11 11 1 1100.27 1077.60 80.99 o 13 11 1 754.22 769.37 73.92 o -12 12 1 446.79 505.90 70.91 o -10 12 1 303.73 391.19 57.38 o -8 12 1 551.98 621.54 62.21 o -6 12 1 1523.83 1498.95 86.82 o -4 12 1 832.77 882.26 81.74 o -2 12 1 1747.83 1360.92 204.93 o 0 12 1 1803.25 1436.30 369.43 o 2 12 1 509.44 493.39 51.94 o 4 12 1 931.28 901.08 68.95 o 6 12 1 1036.63 998.81 74.10 o 8 12 1 302.10 353.27 54.35 o 10 12 1 889.45 843.67 74.11 o 12 12 1 306.01 378.94 58.49 o -11 13 1 4.12 36.48 33.24 o -9 13 1 31.54 51.92 31.20 o -7 13 1 147.20 178.79 43.23 o -5 13 1 1.46 32.48 29.20 o -3 13 1 54.36 53.92 30.38 o -1 13 1 5.78 8.38 30.07 o 1 13 1 165.36 169.03 42.90 o 3 13 1 94.70 114.57 37.06 o 5 13 1 23.90 31.99 30.92 o 7 13 1 4.69 29.73 30.05 o 9 13 1 150.75 165.71 44.45 o 11 13 1 6.24 40.29 29.11 o -10 14 1 202.98 265.04 59.54 o -8 14 1 532.93 552.69 61.31 o -6 14 1 518.80 569.98 61.54 o -4 14 1 379.05 457.43 55.17 o -2 14 1 866.51 869.81 109.68 o 0 14 1 883.18 1060.53 123.77 o 2 14 1 701.56 815.09 70.34 o 4 14 1 865.36 901.07 73.02 o 6 14 1 466.19 510.67 63.39 o 8 14 1 561.03 600.50 65.60 o 10 14 1 423.66 463.48 63.57 o -7 15 1 188.07 261.62 50.52 o -5 15 1 435.43 527.72 71.65 o -3 15 1 995.13 1048.59 127.89 o -1 15 1 468.73 524.25 98.60 o 1 15 1 509.18 633.79 105.82 o 3 15 1 678.35 747.98 85.79 o 5 15 1 1093.63 1134.81 84.20 o 7 15 1 424.78 544.93 64.47 o -4 16 1 104.07 139.04 63.70 o -2 16 1 21.75 49.22 52.85 o 0 16 1 1.62 10.92 46.51 o 2 16 1 0.15 29.42 53.92 o 4 16 1 1.13 28.67 38.24 o -18 0 2 2045.89 2172.40 166.58 o -16 0 2 6627.20 6664.95 262.51 o -14 0 2 14748.99 14824.01 354.25 o -12 0 2 5447.84 5614.35 151.77 o -10 0 2 20628.51 22695.74 577.37 o -8 0 2 58417.96 60865.53 392.48 o -6 0 2 46477.42 48578.50 1026.98 o -4 0 2 778.43 912.34 36.87 o -2 0 2 7153.35 7354.16 102.61 o 0 0 2 63491.31 63956.16 329.73 o 2 0 2 25044.64 27444.38 199.30 o 4 0 2 7087.54 8833.53 127.43 o 6 0 2 4032.63 3923.26 99.74 o 8 0 2 20684.84 23569.00 434.69 o 10 0 2 15359.43 16361.84 243.77 o 12 0 2 5132.40 5316.48 156.10 o 14 0 2 917.62 1025.10 80.92 o 16 0 2 2465.41 2368.89 229.71 o 18 0 2 1628.85 1742.93 203.15 o -19 1 2 318.93 489.49 70.28 o -17 1 2 639.53 710.98 79.64 o -15 1 2 769.28 785.90 67.89 o -13 1 2 577.56 623.31 42.29 o -11 1 2 704.72 749.48 41.79 o -9 1 2 3461.93 3531.48 74.69 o -7 1 2 8878.57 8616.52 98.52 o -5 1 2 10686.31 11833.90 101.87 o -3 1 2 42569.42 44674.68 440.16 o -1 1 2 1131.01 1306.55 28.95 o 1 1 2 23305.40 25708.67 274.90 o 3 1 2 7627.81 7972.00 114.49 o 5 1 2 3653.68 3997.03 85.41 o 7 1 2 2853.75 3076.82 66.85 o 9 1 2 3664.00 3867.15 82.40 o 11 1 2 1397.58 1367.07 56.30 o 13 1 2 1449.62 1515.34 73.56 o 15 1 2 366.16 399.91 52.02 o 17 1 2 468.66 578.76 98.13 o -18 2 2 242.68 308.48 62.45 o -16 2 2 1437.09 1399.06 104.68 o -14 2 2 6499.29 6293.77 143.23 o -12 2 2 819.15 914.86 48.85 o -10 2 2 1554.59 1671.22 58.27 o -8 2 2 16739.47 17879.48 166.58 o -6 2 2 399.82 331.15 23.56 o -4 2 2 5051.76 5908.99 69.67 o -2 2 2 11315.16 12219.91 104.70 o 0 2 2 4117.36 4207.62 52.82 o 2 2 2 27610.82 29997.96 218.06 o 4 2 2 1047.97 1284.88 37.15 o 6 2 2 262.43 265.24 24.60 o 8 2 2 4213.65 4655.99 84.87 o 10 2 2 443.14 483.95 36.77 o 12 2 2 867.32 907.61 63.74 o 14 2 2 70.33 95.00 36.67 o 16 2 2 95.78 164.50 44.71 o 18 2 2 413.91 577.04 98.59 o -19 3 2 485.31 578.24 105.34 o -17 3 2 2483.06 2410.91 140.38 o -15 3 2 2354.07 2307.26 128.47 o -13 3 2 455.26 537.19 57.91 o -11 3 2 3314.99 3362.94 82.46 o -9 3 2 10154.63 10999.09 130.89 o -7 3 2 14582.94 14769.81 133.98 o -5 3 2 12670.25 13222.03 175.77 o -3 3 2 9672.59 9153.17 93.15 o -1 3 2 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