#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200891.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200891_Fobs loop_ _publ_author_name 'Sridhar, B.' 'Srinivasan, N.' 'Rajaram, R. K.' _publ_section_title ; Bis(L-tyrosinium) sulfate monohydrate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o211 _journal_page_last o214 _journal_volume 58 _journal_year 2002 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.510 _cell_angle_gamma 90.000 _cell_length_a 13.4730 _cell_length_b 6.1340 _cell_length_c 13.7850 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.8416 _[local]_cod_data_source_file cv6082Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' L-TYROSINE SULPHATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 142.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -1 0 1335.84 1510.98 17.97 o 2 -1 0 4327.22 4710.13 45.20 o 3 -1 0 8610.99 8791.17 78.68 o 4 -1 0 2925.03 3040.32 9.97 o 5 -1 0 480.75 480.32 4.36 o 6 -1 0 106.35 99.52 1.28 o 7 -1 0 506.94 485.34 4.58 o 8 -1 0 352.42 357.30 3.48 o 9 -1 0 980.78 971.85 8.60 o 10 -1 0 129.67 130.15 2.06 o 11 -1 0 19.36 18.27 1.12 o 12 -1 0 58.07 55.15 1.70 o 13 -1 0 8.58 9.12 1.14 o 14 -1 0 24.55 20.65 1.49 o 1 0 0 32.84 37.10 0.26 o 2 0 0 1.38 7.41 0.29 o 3 0 0 347.22 343.97 2.85 o 4 0 0 2739.12 2813.44 9.23 o 5 0 0 18.61 20.99 0.71 o 6 0 0 75.76 58.38 1.04 o 7 0 0 86.04 97.67 1.37 o 8 0 0 329.48 334.94 3.38 o 9 0 0 135.76 126.71 1.80 o 10 0 0 290.63 310.83 3.08 o 11 0 0 0.50 -1.62 1.62 o 12 0 0 134.19 138.07 2.44 o 13 0 0 8.35 10.02 1.14 o 14 0 0 9.91 13.98 1.29 o 15 0 0 3.20 0.27 1.92 o 1 1 0 1300.72 1429.10 15.68 o 2 1 0 4330.39 4633.62 42.92 o 3 1 0 8661.26 8815.54 80.08 o 4 1 0 2929.04 3181.81 10.57 o 5 1 0 471.28 492.39 4.62 o 6 1 0 104.38 107.74 1.38 o 7 1 0 492.34 458.54 4.61 o 8 1 0 350.03 381.83 3.74 o 9 1 0 974.80 1042.81 9.29 o 10 1 0 126.33 134.32 2.16 o 11 1 0 17.36 21.71 1.17 o 12 1 0 59.31 57.80 1.74 o 13 1 0 7.95 9.33 1.12 o 14 1 0 25.93 25.34 1.54 o 0 2 0 6891.79 7631.81 68.88 o 1 2 0 562.03 614.52 6.46 o 2 2 0 87.49 102.60 1.94 o 3 2 0 751.66 867.78 5.90 o 4 2 0 135.22 151.83 1.51 o 5 2 0 709.42 780.18 6.38 o 6 2 0 225.74 220.42 2.17 o 7 2 0 267.96 297.40 3.01 o 8 2 0 96.53 92.60 1.61 o 9 2 0 78.97 74.15 1.69 o 10 2 0 226.40 233.15 2.91 o 11 2 0 7.61 6.15 0.97 o 12 2 0 73.80 75.61 1.94 o 13 2 0 106.55 103.62 2.54 o 14 2 0 11.11 13.21 1.37 o 1 3 0 789.37 832.40 5.17 o 2 3 0 127.38 128.20 1.77 o 3 3 0 1051.81 1152.02 8.13 o 4 3 0 43.04 47.41 1.11 o 5 3 0 66.92 82.09 1.39 o 6 3 0 108.68 103.61 1.65 o 7 3 0 246.39 240.56 2.54 o 8 3 0 274.89 290.84 3.10 o 9 3 0 612.24 642.84 6.39 o 10 3 0 19.35 20.32 1.26 o 11 3 0 14.44 15.68 1.23 o 12 3 0 0.69 0.24 1.82 o 13 3 0 6.55 7.60 1.27 o 0 4 0 1603.66 1698.60 11.04 o 1 4 0 295.53 328.77 2.31 o 2 4 0 34.85 38.65 0.80 o 3 4 0 774.48 829.43 8.08 o 4 4 0 89.11 100.38 1.71 o 5 4 0 5.11 5.40 0.85 o 6 4 0 1055.92 1113.00 10.24 o 7 4 0 202.04 219.13 2.86 o 8 4 0 116.41 120.71 2.27 o 9 4 0 6.01 7.49 1.05 o 10 4 0 33.49 37.97 1.59 o 11 4 0 17.36 20.10 1.46 o 12 4 0 52.12 55.74 2.16 o 1 5 0 186.10 206.67 1.89 o 2 5 0 58.55 62.00 2.47 o 3 5 0 570.45 637.80 6.28 o 4 5 0 277.61 287.92 3.27 o 5 5 0 238.72 253.70 3.18 o 6 5 0 56.97 59.55 1.75 o 7 5 0 90.73 94.92 2.17 o 8 5 0 15.83 18.07 1.33 o 9 5 0 69.95 76.38 2.29 o 10 5 0 11.89 14.03 1.49 o 0 6 0 341.75 377.25 4.03 o 1 6 0 27.25 29.95 1.66 o 2 6 0 11.93 13.04 0.84 o 3 6 0 13.75 14.05 1.26 o 4 6 0 308.92 342.33 3.97 o 5 6 0 12.63 14.34 1.41 o 6 6 0 23.10 19.40 1.54 o 7 6 0 19.68 20.38 1.51 o 8 6 0 2.87 3.36 1.23 o 1 7 0 18.54 21.31 1.12 o 2 7 0 5.88 4.67 1.11 o 3 7 0 25.99 31.22 1.86 o 4 7 0 6.77 7.46 1.32 o -15 -1 1 1.96 2.16 1.89 o -14 -1 1 28.38 24.59 1.67 o -13 -1 1 44.82 41.13 1.58 o -12 -1 1 121.82 121.74 2.22 o -11 -1 1 202.40 181.20 2.50 o -10 -1 1 570.45 533.29 5.21 o -9 -1 1 653.64 629.95 5.93 o -8 -1 1 167.01 159.68 1.81 o -7 -1 1 1377.78 1372.15 8.58 o -6 -1 1 108.85 121.52 1.35 o -5 -1 1 313.93 312.52 3.05 o -4 -1 1 6074.84 6054.38 60.18 o -3 -1 1 6407.20 6668.82 58.10 o -2 -1 1 2440.47 2423.83 20.95 o -1 -1 1 2936.16 2847.07 19.76 o 0 -1 1 1432.17 1423.71 5.85 o 1 -1 1 11729.04 12446.31 397.41 o 2 -1 1 2239.93 2374.00 30.17 o 3 -1 1 776.38 786.94 4.85 o 4 -1 1 32.41 28.42 0.70 o 5 -1 1 1164.39 1220.34 7.20 o 6 -1 1 1135.90 1186.59 7.76 o 7 -1 1 222.01 215.68 2.13 o 8 -1 1 109.90 108.21 1.59 o 9 -1 1 70.10 72.24 1.58 o 10 -1 1 151.68 147.06 2.21 o 11 -1 1 25.30 24.13 1.24 o 12 -1 1 19.39 21.69 1.26 o 13 -1 1 79.59 83.91 2.31 o 14 -1 1 3.69 -0.53 2.13 o -15 0 1 9.47 9.25 1.33 o -14 0 1 8.03 6.17 1.24 o -13 0 1 277.44 294.27 3.57 o -12 0 1 3.70 1.25 1.69 o -11 0 1 11.28 14.04 1.00 o -10 0 1 10.95 8.83 0.89 o -9 0 1 123.66 123.15 1.76 o -8 0 1 183.99 181.22 1.94 o -7 0 1 636.21 674.04 6.03 o -6 0 1 111.87 93.01 1.22 o -5 0 1 79.70 60.95 0.94 o -4 0 1 20310.89 18931.96 123.43 o -3 0 1 2207.65 2364.24 23.13 o -2 0 1 139.53 176.59 6.93 o -1 0 1 610.38 596.79 10.62 o 0 0 1 798.80 835.46 30.92 o 1 0 1 346.12 376.99 6.69 o 2 0 1 50.50 53.79 0.47 o 3 0 1 2068.28 2288.43 7.67 o 4 0 1 909.04 955.27 5.67 o 5 0 1 725.13 823.95 5.86 o 6 0 1 541.92 529.51 5.24 o 7 0 1 252.07 247.28 2.57 o 8 0 1 71.90 65.65 1.31 o 9 0 1 69.39 73.31 1.48 o 10 0 1 408.30 441.20 4.61 o 11 0 1 5.81 5.90 0.96 o 12 0 1 57.84 61.81 1.79 o 13 0 1 219.22 200.38 3.12 o 14 0 1 41.94 43.48 1.93 o -15 1 1 1.95 1.59 1.78 o -14 1 1 26.99 26.94 1.59 o -13 1 1 44.59 42.87 1.56 o -12 1 1 120.07 125.32 2.28 o -11 1 1 200.67 189.95 2.63 o -10 1 1 571.56 550.80 5.46 o -9 1 1 653.90 669.11 6.27 o -8 1 1 168.39 169.53 1.95 o -7 1 1 1388.24 1410.00 8.99 o -6 1 1 113.35 127.17 1.44 o -5 1 1 306.07 299.80 3.09 o -4 1 1 6038.41 5661.60 59.91 o -3 1 1 6358.51 6107.54 56.05 o -2 1 1 2425.37 2315.54 48.32 o -1 1 1 2976.66 2760.90 43.32 o 0 1 1 1435.41 1354.35 14.23 o 1 1 1 11734.38 11470.28 106.06 o 2 1 1 2251.56 2327.12 12.83 o 3 1 1 770.33 813.31 5.05 o 4 1 1 31.16 31.44 0.75 o 5 1 1 1142.37 1332.57 7.80 o 6 1 1 1142.52 1314.10 8.43 o 7 1 1 217.96 229.29 2.28 o 8 1 1 108.52 108.05 1.68 o 9 1 1 69.20 73.82 1.63 o 10 1 1 151.17 154.51 2.37 o 11 1 1 27.14 28.05 1.28 o 12 1 1 19.44 23.62 1.31 o 13 1 1 76.33 80.92 2.21 o 14 1 1 3.58 4.27 1.15 o -14 2 1 56.36 53.06 2.09 o -13 2 1 130.86 130.86 2.58 o -12 2 1 12.83 11.51 1.14 o -11 2 1 36.12 33.20 1.41 o -10 2 1 137.25 129.12 2.18 o -9 2 1 47.05 55.55 1.45 o -8 2 1 360.77 360.95 3.46 o -7 2 1 2290.18 2226.92 12.11 o -6 2 1 398.26 403.15 4.22 o -5 2 1 456.52 391.45 3.91 o -4 2 1 89.46 106.34 1.28 o -3 2 1 403.44 377.70 3.40 o -2 2 1 562.12 605.09 8.37 o -1 2 1 131.34 142.22 1.02 o 0 2 1 4113.40 4228.51 29.86 o 1 2 1 323.29 346.41 2.63 o 2 2 1 41.12 62.72 0.68 o 3 2 1 586.05 665.36 5.32 o 4 2 1 19.63 24.96 0.77 o 5 2 1 614.26 732.43 6.38 o 6 2 1 528.14 615.16 5.43 o 7 2 1 129.30 137.34 1.83 o 8 2 1 15.80 18.30 0.91 o 9 2 1 104.05 100.09 1.93 o 10 2 1 520.30 548.73 5.36 o 11 2 1 10.05 12.29 1.09 o 12 2 1 32.84 42.28 1.63 o 13 2 1 15.57 18.38 1.43 o 14 2 1 1.60 3.29 1.09 o -14 3 1 7.55 5.21 1.34 o -13 3 1 36.68 32.21 1.79 o -12 3 1 90.00 84.07 2.15 o -11 3 1 27.25 30.70 1.41 o -10 3 1 546.98 549.78 5.59 o -9 3 1 207.15 208.85 2.76 o -8 3 1 87.55 86.43 1.78 o -7 3 1 185.86 171.88 2.16 o -6 3 1 129.19 131.44 1.82 o -5 3 1 46.75 48.72 1.14 o -4 3 1 150.78 132.57 1.64 o -3 3 1 207.58 226.33 2.24 o -2 3 1 381.73 369.72 2.77 o -1 3 1 1249.45 1365.00 24.58 o 0 3 1 274.67 313.43 2.26 o 1 3 1 402.34 433.21 8.49 o 2 3 1 965.07 1126.29 8.32 o 3 3 1 39.38 40.05 0.99 o 4 3 1 208.06 250.78 2.53 o 5 3 1 206.71 204.63 2.17 o 6 3 1 10.47 9.95 0.86 o 7 3 1 214.63 228.30 2.67 o 8 3 1 7.95 9.63 0.97 o 9 3 1 156.39 175.84 2.62 o 10 3 1 19.02 17.66 1.23 o 11 3 1 24.49 29.23 1.46 o 12 3 1 5.15 5.38 1.16 o 13 3 1 17.57 21.36 1.55 o -12 4 1 67.20 61.95 2.20 o -11 4 1 101.24 107.63 2.58 o -10 4 1 188.96 192.13 3.00 o -9 4 1 36.65 37.12 1.53 o -8 4 1 10.34 11.85 1.14 o -7 4 1 823.62 826.38 7.94 o -6 4 1 10.78 8.30 0.99 o -5 4 1 78.49 78.89 1.68 o -4 4 1 64.78 61.42 1.43 o -3 4 1 1154.02 1192.03 9.56 o -2 4 1 130.58 142.87 1.33 o -1 4 1 107.44 105.58 1.15 o 0 4 1 779.71 867.26 5.60 o 1 4 1 56.02 65.82 0.94 o 2 4 1 201.80 218.52 1.73 o 3 4 1 622.04 622.10 6.14 o 4 4 1 332.75 355.94 3.65 o 5 4 1 84.25 85.56 1.78 o 6 4 1 385.21 412.60 4.21 o 7 4 1 48.49 59.86 1.67 o 8 4 1 93.52 91.11 2.06 o 9 4 1 9.56 10.25 1.13 o 10 4 1 293.81 313.51 3.89 o 11 4 1 43.42 45.85 1.96 o 12 4 1 36.40 45.36 2.02 o -11 5 1 11.41 12.69 1.41 o -10 5 1 34.54 35.31 1.77 o -9 5 1 96.58 93.06 2.51 o -8 5 1 228.28 228.60 3.26 o -7 5 1 259.90 256.73 3.35 o -6 5 1 203.50 205.74 2.95 o -5 5 1 248.37 258.81 3.15 o -4 5 1 42.18 48.05 1.55 o -3 5 1 289.29 305.24 3.29 o -2 5 1 7.40 8.04 0.74 o -1 5 1 29.70 28.91 0.89 o 0 5 1 407.25 425.83 3.01 o 1 5 1 402.37 433.42 3.06 o 2 5 1 706.64 756.92 5.38 o 3 5 1 429.12 439.80 4.50 o 4 5 1 116.99 122.46 2.30 o 5 5 1 0.16 0.20 1.51 o 6 5 1 0.24 1.37 1.71 o 7 5 1 56.70 62.43 1.85 o 8 5 1 1.44 2.62 1.67 o 9 5 1 150.28 164.06 3.19 o 10 5 1 30.87 38.75 1.85 o -8 6 1 11.16 13.10 1.38 o -7 6 1 108.87 119.70 2.79 o -6 6 1 25.60 27.34 1.56 o -5 6 1 8.88 9.39 1.20 o -4 6 1 81.89 87.95 2.16 o -3 6 1 9.52 7.75 1.13 o -2 6 1 28.64 31.97 1.11 o -1 6 1 55.53 53.61 1.26 o 0 6 1 438.00 456.93 4.03 o 1 6 1 53.13 55.13 2.68 o 2 6 1 121.47 127.16 3.96 o 3 6 1 4.61 3.67 1.91 o 4 6 1 25.01 24.19 1.49 o 5 6 1 26.94 31.70 1.61 o 6 6 1 72.23 78.03 2.35 o 7 6 1 26.30 24.68 1.62 o 8 6 1 3.88 5.11 1.31 o -4 7 1 44.04 44.80 2.10 o -3 7 1 104.23 107.84 2.74 o -2 7 1 2.64 3.07 1.40 o -1 7 1 0.09 0.51 1.19 o 0 7 1 15.14 17.64 1.06 o 1 7 1 19.13 23.90 2.03 o 2 7 1 95.62 104.03 1.96 o 3 7 1 59.25 63.91 2.26 o -15 -1 2 17.76 17.54 1.49 o -14 -1 2 33.12 33.36 1.62 o -13 -1 2 37.56 39.21 1.58 o -12 -1 2 39.09 41.47 1.44 o -11 -1 2 2.41 1.82 0.90 o -10 -1 2 183.06 174.01 2.29 o -9 -1 2 8.54 8.47 0.74 o -8 -1 2 758.63 724.96 6.68 o -7 -1 2 609.11 576.25 5.52 o -6 -1 2 1522.71 1476.95 8.11 o -5 -1 2 849.29 902.02 5.83 o -4 -1 2 1041.84 961.08 5.59 o -3 -1 2 1346.07 1320.93 6.11 o -2 -1 2 1884.88 1966.14 13.07 o -1 -1 2 1477.95 1311.39 6.83 o 0 -1 2 725.73 744.91 3.42 o 1 -1 2 3792.24 3781.49 88.52 o 2 -1 2 5046.30 5071.84 87.65 o 3 -1 2 812.82 836.49 5.36 o 4 -1 2 70.71 78.76 1.07 o 5 -1 2 2329.33 2472.08 10.80 o 6 -1 2 134.17 142.88 1.60 o 7 -1 2 52.29 50.02 1.13 o 8 -1 2 311.34 326.45 3.28 o 9 -1 2 183.05 187.79 2.42 o 10 -1 2 1.49 2.10 0.86 o 11 -1 2 140.72 136.57 2.39 o 12 -1 2 80.30 78.10 1.99 o 13 -1 2 31.16 32.39 1.65 o 14 -1 2 1.33 3.78 1.15 o -15 0 2 41.70 42.66 1.88 o -14 0 2 2.24 2.84 1.09 o -13 0 2 148.34 152.33 2.62 o -12 0 2 161.78 158.49 2.49 o -11 0 2 10.89 10.63 1.02 o -10 0 2 351.14 384.12 3.76 o -9 0 2 537.43 533.00 5.44 o -8 0 2 1736.91 1884.94 10.77 o -7 0 2 2543.10 2763.66 12.08 o -6 0 2 887.17 1008.33 6.68 o -5 0 2 173.03 224.39 2.29 o -4 0 2 3727.87 3635.44 36.33 o -3 0 2 1645.23 1558.81 5.95 o -2 0 2 39.04 27.80 0.39 o -1 0 2 693.33 656.34 3.39 o 0 0 2 318.63 330.85 4.21 o 1 0 2 4695.54 4917.75 124.27 o 2 0 2 182.68 197.64 2.82 o 3 0 2 1064.58 1066.92 5.74 o 4 0 2 31.85 30.77 0.76 o 5 0 2 2865.81 2856.95 11.55 o 6 0 2 20.99 26.76 0.83 o 7 0 2 400.34 382.11 3.97 o 8 0 2 16.25 15.01 0.88 o 9 0 2 95.16 100.12 1.82 o 10 0 2 694.25 729.82 7.36 o 11 0 2 48.46 44.14 1.54 o 12 0 2 0.22 -0.43 1.62 o 13 0 2 34.19 32.66 1.74 o 14 0 2 14.91 18.05 1.52 o -15 1 2 18.68 18.68 1.43 o -14 1 2 32.47 28.57 1.68 o -13 1 2 37.96 36.61 1.57 o -12 1 2 39.68 44.29 1.51 o -11 1 2 2.04 1.74 1.62 o -10 1 2 188.02 189.03 2.43 o -9 1 2 8.00 6.69 0.78 o -8 1 2 741.54 724.59 6.97 o -7 1 2 611.15 591.39 5.80 o -6 1 2 1507.17 1436.51 8.28 o -5 1 2 848.64 854.63 5.91 o -4 1 2 1020.63 913.54 5.56 o -3 1 2 1346.09 1219.46 5.84 o -2 1 2 1897.07 1925.68 56.76 o -1 1 2 1479.77 1270.02 27.39 o 0 1 2 716.52 699.70 10.50 o 1 1 2 3788.46 3620.10 25.79 o 2 1 2 5065.18 4720.20 100.79 o 3 1 2 806.98 791.65 5.37 o 4 1 2 64.89 76.23 1.10 o 5 1 2 2324.51 2636.10 11.57 o 6 1 2 126.83 150.75 1.69 o 7 1 2 53.93 59.74 1.20 o 8 1 2 309.40 348.41 3.51 o 9 1 2 178.57 197.59 2.53 o 10 1 2 1.75 0.18 1.54 o 11 1 2 140.49 149.26 2.50 o 12 1 2 78.79 82.21 2.05 o 13 1 2 31.29 29.62 1.67 o 14 1 2 1.10 -1.33 1.94 o -15 2 2 3.96 4.83 1.22 o -14 2 2 39.40 37.42 1.82 o -13 2 2 7.97 6.33 1.12 o -12 2 2 135.10 132.29 2.42 o -11 2 2 146.42 138.48 2.38 o -10 2 2 361.99 317.78 3.21 o -9 2 2 533.76 462.48 4.46 o -8 2 2 83.33 92.32 1.56 o -7 2 2 225.01 218.81 2.14 o -6 2 2 544.23 533.44 4.78 o -5 2 2 131.45 120.17 1.43 o -4 2 2 958.46 920.34 6.41 o -3 2 2 1540.18 1420.62 7.53 o -2 2 2 471.47 424.46 14.60 o -1 2 2 8.71 6.34 0.44 o 0 2 2 2247.31 2160.93 38.92 o 1 2 2 563.84 563.14 3.33 o 2 2 2 1984.20 2231.31 67.06 o 3 2 2 530.10 542.58 5.07 o 4 2 2 120.10 135.22 1.54 o 5 2 2 193.47 213.25 2.12 o 6 2 2 166.78 206.43 2.12 o 7 2 2 103.34 116.49 1.73 o 8 2 2 27.85 25.98 1.16 o 9 2 2 51.63 55.33 1.56 o 10 2 2 134.53 146.85 2.41 o 11 2 2 61.98 68.03 1.91 o 12 2 2 4.88 5.79 1.16 o 13 2 2 6.78 4.28 1.28 o -14 3 2 172.44 163.03 3.30 o -13 3 2 25.46 28.94 1.74 o -12 3 2 107.47 101.83 2.32 o -11 3 2 37.84 37.17 1.49 o -10 3 2 190.01 187.27 2.76 o -9 3 2 41.95 40.45 1.44 o -8 3 2 3.04 3.65 0.83 o -7 3 2 17.12 16.89 0.88 o -6 3 2 969.93 942.60 8.29 o -5 3 2 272.70 254.32 2.57 o -4 3 2 722.23 720.88 6.67 o -3 3 2 190.72 191.59 1.87 o -2 3 2 886.60 897.48 8.06 o -1 3 2 3185.97 3309.99 25.96 o 0 3 2 927.22 952.90 10.59 o 1 3 2 1075.13 1147.51 24.58 o 2 3 2 222.24 227.26 5.59 o 3 3 2 588.66 677.72 6.61 o 4 3 2 66.75 64.57 1.28 o 5 3 2 60.93 70.21 1.39 o 6 3 2 1.63 0.23 1.36 o 7 3 2 133.63 148.89 2.27 o 8 3 2 112.36 115.88 2.12 o 9 3 2 7.77 7.45 0.98 o 10 3 2 7.55 7.15 1.09 o 11 3 2 118.35 119.55 2.54 o 12 3 2 46.93 55.03 2.03 o -13 4 2 76.78 74.85 2.48 o -12 4 2 40.18 42.88 1.89 o -11 4 2 89.89 93.12 2.40 o -10 4 2 166.50 174.84 2.83 o -9 4 2 180.23 190.39 2.86 o -8 4 2 43.87 44.62 1.54 o -7 4 2 1128.92 1118.11 10.48 o -6 4 2 79.75 68.31 1.66 o -5 4 2 344.41 324.81 3.33 o -4 4 2 66.40 62.63 1.40 o -3 4 2 330.12 330.71 3.40 o -2 4 2 129.73 114.81 1.58 o -1 4 2 485.72 487.45 4.66 o 0 4 2 107.56 120.99 1.24 o 1 4 2 8.47 6.24 2.16 o 2 4 2 311.18 341.24 9.99 o 3 4 2 155.66 162.51 2.13 o 4 4 2 77.18 77.40 1.70 o 5 4 2 225.56 255.72 2.94 o 6 4 2 80.30 91.11 1.95 o 7 4 2 210.15 222.63 2.97 o 8 4 2 25.51 27.23 1.35 o 9 4 2 7.38 8.28 1.14 o 10 4 2 219.64 246.33 3.73 o 11 4 2 69.54 84.43 2.44 o -11 5 2 4.15 2.73 1.26 o -10 5 2 99.65 99.79 2.56 o -9 5 2 13.70 10.73 1.24 o -8 5 2 3.88 1.92 1.89 o -7 5 2 54.11 55.26 1.75 o -6 5 2 170.30 164.96 2.66 o -5 5 2 18.50 13.59 1.20 o -4 5 2 284.53 296.09 3.33 o -3 5 2 20.65 19.71 1.21 o -2 5 2 540.02 530.66 3.66 o -1 5 2 210.62 221.19 3.09 o 0 5 2 160.70 173.44 2.72 o 1 5 2 34.65 33.70 1.16 o 2 5 2 247.11 266.02 2.21 o 3 5 2 23.48 24.14 1.26 o 4 5 2 58.03 57.40 1.69 o 5 5 2 96.20 104.55 2.20 o 6 5 2 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