#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/08/2200886.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200886_Fobs loop_ _publ_author_name 'Subha Nandhini, M.' 'Krishnakumar, R. V.' 'Natarajan, S.' _publ_section_title ; Dichlorobis(DL-alanine)zinc(II) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m127 _journal_page_last m129 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.300 _cell_angle_gamma 90.000 _cell_length_a 9.9960 _cell_length_b 13.6220 _cell_length_c 8.6160 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.8323 _[local]_cod_data_source_file ci6103Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DLALAZN IN P21/n P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 175.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10753.81 9375.58 43.53 o 2 0 0 30785.13 29410.92 700.46 o 3 0 0 2835.98 2095.58 115.87 o 4 0 0 2329.29 2038.39 134.29 o 5 0 0 28573.74 28067.33 2438.29 o 6 0 0 6.22 14.55 0.99 o 7 0 0 6288.79 5953.65 719.61 o 8 0 0 887.58 733.92 101.10 o 9 0 0 1530.77 1382.07 227.25 o 10 0 0 990.83 926.01 179.09 o 11 0 0 205.71 218.11 5.27 o 12 0 0 528.29 540.42 6.43 o 1 1 0 1463.67 1509.04 75.06 o 2 1 0 1159.22 1093.34 20.35 o 3 1 0 448.87 376.13 10.66 o 4 1 0 2468.57 2477.90 171.40 o 5 1 0 147.57 191.50 7.58 o 6 1 0 3312.30 3127.87 404.10 o 7 1 0 331.24 340.41 68.22 o 8 1 0 34.66 45.67 9.46 o 9 1 0 109.20 166.78 9.67 o 10 1 0 3.84 5.23 1.41 o 11 1 0 322.73 363.78 6.81 o 0 2 0 3592.61 4221.57 40.60 o 1 2 0 277.07 296.95 1.59 o 2 2 0 5715.93 6056.24 254.38 o 3 2 0 1476.44 1397.77 58.32 o 4 2 0 12016.72 12627.23 254.88 o 5 2 0 5567.61 5491.50 379.63 o 6 2 0 338.70 325.74 34.12 o 7 2 0 560.70 531.41 101.20 o 8 2 0 164.00 137.76 21.21 o 9 2 0 757.63 737.65 118.33 o 10 2 0 684.21 634.92 122.29 o 11 2 0 165.98 190.58 4.93 o 1 3 0 22712.08 27045.07 115.41 o 2 3 0 170.80 179.52 3.26 o 3 3 0 308.05 278.82 5.22 o 4 3 0 3935.76 3951.41 183.74 o 5 3 0 401.29 392.65 21.55 o 6 3 0 8565.97 8628.70 940.52 o 7 3 0 65.57 65.82 10.43 o 8 3 0 922.85 937.06 146.80 o 9 3 0 3.58 7.84 1.10 o 10 3 0 878.93 889.98 151.23 o 11 3 0 1087.04 1074.75 201.58 o 0 4 0 4318.12 4775.50 11.50 o 1 4 0 1391.64 1503.25 17.60 o 2 4 0 5768.87 6442.20 111.51 o 3 4 0 3612.81 3816.70 97.47 o 4 4 0 1226.77 1173.50 29.46 o 5 4 0 2.80 9.41 1.67 o 6 4 0 1008.93 978.18 77.92 o 7 4 0 1005.91 961.66 120.91 o 8 4 0 604.04 630.07 109.49 o 9 4 0 429.67 465.51 69.79 o 10 4 0 0.86 12.32 2.36 o 11 4 0 720.60 740.41 132.05 o 1 5 0 1960.32 1882.11 9.42 o 2 5 0 8447.93 9039.57 14.69 o 3 5 0 2330.09 2266.28 7.72 o 4 5 0 2683.36 2520.31 62.10 o 5 5 0 2586.15 2695.24 131.47 o 6 5 0 563.23 799.67 79.55 o 7 5 0 101.20 123.23 13.82 o 8 5 0 1137.05 1232.52 158.15 o 9 5 0 2242.11 2401.94 385.70 o 10 5 0 722.68 757.15 133.10 o 11 5 0 248.66 229.30 37.22 o 0 6 0 1040.68 1112.10 7.34 o 1 6 0 24.28 27.49 4.08 o 2 6 0 405.25 395.78 24.23 o 3 6 0 2325.90 2406.52 18.66 o 4 6 0 8025.42 8548.89 216.20 o 5 6 0 150.58 145.70 10.44 o 6 6 0 52.10 51.73 6.61 o 7 6 0 1179.16 1247.84 121.16 o 8 6 0 174.12 189.12 17.49 o 9 6 0 283.26 308.43 41.94 o 10 6 0 40.44 46.79 3.22 o 11 6 0 45.27 53.86 9.11 o 1 7 0 10031.92 11259.13 40.54 o 2 7 0 38.88 35.84 2.74 o 3 7 0 6374.69 6995.82 56.10 o 4 7 0 6446.98 6788.92 28.62 o 5 7 0 0.69 35.29 20.38 o 6 7 0 3141.99 3088.52 175.24 o 7 7 0 20.89 21.27 3.51 o 8 7 0 1701.93 1670.42 136.23 o 9 7 0 330.30 325.63 41.58 o 10 7 0 0.32 4.59 1.13 o 0 8 0 2216.96 2439.91 13.72 o 1 8 0 165.56 210.48 3.00 o 2 8 0 2026.25 2008.87 9.18 o 3 8 0 1591.74 1603.94 21.71 o 4 8 0 63.24 75.93 15.10 o 5 8 0 27.09 27.29 1.99 o 6 8 0 210.96 211.35 9.02 o 7 8 0 74.64 87.35 4.93 o 8 8 0 58.92 66.97 3.88 o 9 8 0 58.63 64.57 5.41 o 10 8 0 55.50 61.25 9.98 o 1 9 0 3762.26 3822.26 21.05 o 2 9 0 80.99 61.59 6.44 o 3 9 0 287.05 249.63 12.82 o 4 9 0 450.07 453.60 5.32 o 5 9 0 129.15 147.79 22.07 o 6 9 0 776.57 764.48 11.80 o 7 9 0 286.66 276.87 18.01 o 8 9 0 477.31 466.21 18.75 o 9 9 0 21.61 17.60 1.11 o 10 9 0 17.64 22.95 2.26 o 0 10 0 5126.32 5062.15 24.01 o 1 10 0 612.68 686.29 8.62 o 2 10 0 4954.35 4966.26 17.42 o 3 10 0 1906.22 1881.77 41.39 o 4 10 0 820.26 864.96 66.78 o 5 10 0 1495.41 1511.39 10.63 o 6 10 0 181.31 184.52 8.17 o 7 10 0 3821.56 3713.23 78.40 o 8 10 0 167.66 165.18 4.13 o 9 10 0 37.50 41.55 1.37 o 1 11 0 22.17 23.16 1.23 o 2 11 0 1059.38 1006.27 21.16 o 3 11 0 348.65 348.99 18.35 o 4 11 0 23.83 26.82 2.48 o 5 11 0 1278.15 1220.97 17.78 o 6 11 0 2.55 15.94 3.46 o 7 11 0 132.69 132.47 2.74 o 8 11 0 1.50 2.56 1.16 o 0 12 0 91.98 98.95 2.99 o 1 12 0 35.44 43.56 1.50 o 2 12 0 323.75 320.06 5.13 o 3 12 0 401.69 412.21 6.59 o 4 12 0 77.40 74.09 1.85 o 5 12 0 306.44 282.05 4.67 o 6 12 0 5.76 5.58 1.38 o 7 12 0 512.62 490.97 13.68 o 8 12 0 205.16 221.11 3.15 o 1 13 0 37.89 37.80 3.86 o 2 13 0 90.47 95.84 2.05 o 3 13 0 0.89 40.34 19.80 o 4 13 0 13.48 25.48 9.18 o 5 13 0 0.61 18.89 5.78 o 6 13 0 0.45 7.20 0.98 o 7 13 0 340.70 376.32 4.49 o 0 14 0 138.19 159.94 4.51 o 1 14 0 1339.42 1241.01 9.74 o 2 14 0 0.13 20.15 10.75 o 3 14 0 492.46 477.80 5.84 o 4 14 0 880.96 862.74 10.15 o 5 14 0 338.88 355.80 5.90 o 6 14 0 155.09 175.68 2.89 o 1 15 0 88.81 86.01 1.86 o 2 15 0 530.16 502.80 20.78 o 3 15 0 431.32 439.75 5.62 o 4 15 0 133.62 129.76 2.87 o 0 16 0 2112.41 1980.68 13.46 o 1 16 0 83.41 77.93 2.97 o 2 16 0 29.05 34.85 3.35 o -11 1 1 194.41 223.04 5.21 o -10 1 1 77.41 75.16 2.67 o -9 1 1 0.21 6.10 1.98 o -8 1 1 2091.05 1980.45 16.34 o -7 1 1 15.06 18.45 1.32 o -6 1 1 4310.95 3810.47 17.77 o -5 1 1 186.93 198.12 3.54 o -4 1 1 1851.14 1493.93 9.48 o -3 1 1 10974.39 11747.65 118.86 o -2 1 1 61.95 45.81 1.26 o -1 1 1 10540.51 9909.05 79.68 o 0 1 1 38.09 39.92 1.02 o 1 1 1 11254.65 10208.35 81.27 o 2 1 1 7584.25 6652.42 14.62 o 3 1 1 218.92 216.68 2.99 o 4 1 1 86.62 73.64 1.95 o 5 1 1 805.35 655.97 6.88 o 6 1 1 6395.32 5303.38 22.30 o 7 1 1 485.21 383.91 6.84 o 8 1 1 311.36 254.12 6.21 o 9 1 1 52.49 49.30 2.11 o 10 1 1 144.70 112.24 3.44 o 11 1 1 1419.80 1102.99 11.09 o -11 2 1 387.00 462.14 7.51 o -10 2 1 301.24 316.98 7.37 o -9 2 1 1624.95 1695.58 16.44 o -8 2 1 674.73 740.54 10.40 o -7 2 1 574.80 595.98 8.33 o -6 2 1 3662.04 4128.95 21.09 o -5 2 1 2532.32 2666.18 12.68 o -4 2 1 1393.68 1321.10 8.01 o -3 2 1 13913.99 13000.08 124.21 o -2 2 1 12.37 28.06 0.82 o -1 2 1 164.06 192.60 2.14 o 0 2 1 1302.62 1267.02 4.97 o 1 2 1 509.20 491.71 3.43 o 2 2 1 6099.25 5681.07 13.33 o 3 2 1 44.15 67.42 1.80 o 4 2 1 1015.55 927.33 7.19 o 5 2 1 5817.02 4578.97 18.49 o 6 2 1 854.56 707.88 8.22 o 7 2 1 104.09 83.48 2.45 o 8 2 1 837.77 606.31 9.21 o 9 2 1 3.21 7.74 1.42 o 10 2 1 10.64 27.63 1.83 o 11 2 1 47.70 35.31 1.88 o -11 3 1 259.36 290.38 5.67 o -10 3 1 1180.95 1377.33 13.89 o -9 3 1 466.97 532.06 9.56 o -8 3 1 624.07 706.45 11.01 o -7 3 1 135.47 132.59 3.64 o -6 3 1 36.23 59.02 1.74 o -5 3 1 3950.88 4272.90 16.66 o -4 3 1 1237.29 1180.65 7.84 o -3 3 1 5642.83 5493.92 15.42 o -2 3 1 2136.14 1885.25 7.84 o -1 3 1 363.49 247.32 2.68 o 0 3 1 837.57 882.36 4.61 o 1 3 1 3020.58 2713.53 8.62 o 2 3 1 6738.01 6518.22 15.61 o 3 3 1 15588.71 15159.40 146.03 o 4 3 1 9923.54 9161.49 23.37 o 5 3 1 50.32 45.56 1.37 o 6 3 1 535.49 446.47 6.52 o 7 3 1 1650.42 1278.47 12.24 o 8 3 1 971.98 733.56 10.13 o 9 3 1 786.35 585.26 9.44 o 10 3 1 515.27 400.65 7.48 o 11 3 1 24.31 23.10 1.60 o -11 4 1 117.96 120.81 3.57 o -10 4 1 1312.15 1619.77 15.73 o -9 4 1 947.85 1129.79 13.67 o -8 4 1 364.66 414.38 7.77 o -7 4 1 62.41 60.92 2.09 o -6 4 1 207.86 267.10 5.04 o -5 4 1 3489.90 3494.33 16.01 o -4 4 1 2818.89 2542.56 11.99 o -3 4 1 4434.62 4389.05 14.23 o -2 4 1 19.29 9.38 0.60 o -1 4 1 3414.54 3597.60 10.90 o 0 4 1 3729.27 3639.43 10.99 o 1 4 1 20254.92 22599.44 161.89 o 2 4 1 2373.01 2212.54 9.65 o 3 4 1 4780.93 4601.37 15.15 o 4 4 1 5295.19 4956.02 18.05 o 5 4 1 2898.19 2636.81 14.72 o 6 4 1 402.88 864.39 9.31 o 7 4 1 3183.80 2699.92 18.29 o 8 4 1 2403.02 1851.49 16.16 o 9 4 1 1813.84 1414.69 14.41 o 10 4 1 976.52 739.91 9.96 o 11 4 1 7.45 8.08 1.29 o -11 5 1 0.40 6.34 1.86 o -10 5 1 12.60 12.06 1.69 o -9 5 1 174.75 195.98 5.68 o -8 5 1 0.62 16.32 1.61 o -7 5 1 61.84 68.68 2.22 o -6 5 1 303.84 312.84 5.74 o -5 5 1 77.53 96.14 2.71 o -4 5 1 406.30 486.23 5.73 o -3 5 1 10.98 20.52 0.88 o -2 5 1 348.70 400.21 4.39 o -1 5 1 1818.43 1899.84 8.91 o 0 5 1 4859.37 5246.07 15.02 o 1 5 1 688.69 716.36 5.66 o 2 5 1 34.27 37.47 1.14 o 3 5 1 1245.32 1218.48 8.54 o 4 5 1 1043.66 1009.20 8.53 o 5 5 1 51.35 31.38 1.27 o 6 5 1 45.10 30.43 1.48 o 7 5 1 584.32 486.43 7.89 o 8 5 1 1670.88 1354.77 14.10 o 9 5 1 555.15 443.25 8.21 o 10 5 1 4.89 6.08 1.82 o 11 5 1 122.63 105.30 2.83 o -11 6 1 243.58 250.27 4.75 o -10 6 1 279.32 294.55 5.85 o -9 6 1 380.86 416.91 7.46 o -8 6 1 1696.94 1835.59 15.71 o -7 6 1 2225.96 2393.10 17.17 o -6 6 1 600.05 672.95 8.64 o -5 6 1 270.84 241.70 4.79 o -4 6 1 1147.46 1206.53 9.62 o -3 6 1 5430.33 5153.04 18.39 o -2 6 1 5490.80 5262.28 17.41 o -1 6 1 352.61 359.63 4.31 o 0 6 1 2329.06 2368.61 11.16 o 1 6 1 1278.72 1386.04 8.50 o 2 6 1 9288.22 9721.11 24.81 o 3 6 1 9483.95 9922.27 26.69 o 4 6 1 897.32 814.06 8.12 o 5 6 1 2059.45 1863.79 13.39 o 6 6 1 60.25 57.85 2.04 o 7 6 1 2345.26 2050.42 16.64 o 8 6 1 986.27 799.99 10.81 o 9 6 1 1172.70 1016.94 11.94 o 10 6 1 423.07 365.86 6.52 o 11 6 1 73.32 56.27 1.89 o -10 7 1 479.91 471.92 6.88 o -9 7 1 285.35 297.33 6.16 o -8 7 1 3.06 3.03 2.02 o -7 7 1 2.11 8.27 1.56 o -6 7 1 13.48 25.75 1.69 o -5 7 1 878.30 787.22 9.13 o -4 7 1 3343.12 3433.30 17.29 o -3 7 1 1268.37 1262.15 9.84 o -2 7 1 2428.15 2396.65 12.81 o -1 7 1 1135.68 1174.70 8.65 o 0 7 1 12.50 18.48 0.87 o 1 7 1 9.11 20.52 0.99 o 2 7 1 717.77 618.19 6.67 o 3 7 1 4078.38 3979.77 18.15 o 4 7 1 392.82 431.60 6.41 o 5 7 1 552.62 564.59 7.91 o 6 7 1 359.63 316.94 6.50 o 7 7 1 1388.33 1238.73 13.18 o 8 7 1 0.47 -0.36 1.03 o 9 7 1 41.08 28.11 1.89 o 10 7 1 295.83 273.41 5.50 o -10 8 1 31.78 26.41 1.63 o -9 8 1 5.88 6.16 1.85 o -8 8 1 133.47 123.95 3.97 o -7 8 1 4238.26 4352.57 24.36 o -6 8 1 192.93 195.89 5.34 o -5 8 1 1319.31 1421.40 12.89 o -4 8 1 10.55 9.45 1.17 o -3 8 1 1846.07 1820.25 12.88 o -2 8 1 11480.90 12043.70 33.17 o -1 8 1 1234.05 1291.83 10.25 o 0 8 1 1921.95 1930.63 12.19 o 1 8 1 2944.28 2960.62 15.60 o 2 8 1 3647.01 3560.84 17.63 o 3 8 1 308.04 269.80 5.20 o 4 8 1 50.02 54.80 1.86 o 5 8 1 826.95 824.47 10.04 o 6 8 1 747.91 779.58 10.44 o 7 8 1 831.50 769.04 10.60 o 8 8 1 250.99 238.87 6.02 o 9 8 1 49.16 45.62 2.03 o 10 8 1 5.01 7.88 1.25 o -9 9 1 128.97 124.59 3.71 o -8 9 1 1107.39 1022.17 11.19 o -7 9 1 440.83 428.73 7.91 o -6 9 1 1735.78 1672.86 15.00 o -5 9 1 61.55 66.48 2.25 o -4 9 1 202.11 206.73 5.13 o -3 9 1 467.01 387.84 6.56 o -2 9 1 889.77 930.74 9.68 o -1 9 1 5930.71 5789.29 23.87 o 0 9 1 16.10 24.77 1.37 o 1 9 1 685.85 677.67 8.25 o 2 9 1 137.31 142.01 3.96 o 3 9 1 177.24 193.39 4.97 o 4 9 1 966.04 979.13 11.20 o 5 9 1 32.37 43.55 1.98 o 6 9 1 407.77 389.40 7.69 o 7 9 1 848.83 770.27 10.61 o 8 9 1 1341.13 1234.80 12.88 o 9 9 1 214.97 208.17 5.04 o -9 10 1 36.65 34.88 1.72 o -8 10 1 32.09 35.79 1.89 o -7 10 1 197.03 176.85 5.18 o -6 10 1 161.41 147.39 4.24 o -5 10 1 335.64 321.96 6.85 o -4 10 1 435.27 381.34 7.29 o -3 10 1 253.11 278.94 6.10 o -2 10 1 1700.37 1661.26 14.28 o -1 10 1 243.43 233.75 5.46 o 0 10 1 3323.53 3251.85 19.61 o 1 10 1 0.05 23.89 1.55 o 2 10 1 1103.01 1139.81 11.81 o 3 10 1 309.51 301.29 6.48 o 4 10 1 324.93 346.73 7.11 o 5 10 1 718.92 744.65 10.65 o 6 10 1 317.10 309.81 6.86 o 7 10 1 593.28 579.60 9.19 o 8 10 1 128.12 129.62 3.69 o 9 10 1 1.38 4.99 1.52 o -8 11 1 817.48 796.52 8.72 o -7 11 1 218.54 195.59 5.34 o -6 11 1 2359.83 2297.44 17.61 o -5 11 1 65.46 61.36 2.35 o -4 11 1 1283.71 1212.08 13.32 o -3 11 1 9.12 30.65 1.80 o -2 11 1 2107.60 1939.93 16.53 o -1 11 1 3948.67 3694.21 22.43 o 0 11 1 504.36 518.24 8.69 o 1 11 1 3348.57 3303.63 21.17 o 2 11 1 56.50 54.32 2.21 o 3 11 1 3381.04 3212.22 21.81 o 4 11 1 3209.80 3166.07 21.64 o 5 11 1 65.65 67.48 2.47 o 6 11 1 1087.59 1071.94 12.25 o 7 11 1 319.79 342.99 6.77 o 8 11 1 1290.23 1256.75 11.26 o -8 12 1 26.30 19.23 1.57 o -7 12 1 597.67 546.71 7.60 o -6 12 1 131.81 114.56 3.21 o -5 12 1 222.79 194.11 5.54 o -4 12 1 1121.58 1035.06 12.30 o -3 12 1 30.48 43.50 2.19 o -2 12 1 1185.31 1081.43 12.84 o -1 12 1 996.51 945.53 12.00 o 0 12 1 207.53 196.81 5.69 o 1 12 1 1307.20 1193.04 13.50 o 2 12 1 154.69 154.56 4.44 o 3 12 1 8.59 26.37 1.79 o 4 12 1 787.69 747.85 10.67 o 5 12 1 80.35 96.86 2.96 o 6 12 1 141.95 133.82 3.94 o 7 12 1 219.66 232.52 5.20 o 8 12 1 129.55 127.16 3.48 o -7 13 1 96.43 108.56 2.87 o -6 13 1 292.30 307.28 5.98 o -5 13 1 440.84 403.30 7.34 o -4 13 1 2051.19 1989.54 16.74 o -3 13 1 1484.26 1411.15 14.38 o -2 13 1 664.78 612.93 9.86 o -1 13 1 371.13 357.64 7.83 o 0 13 1 117.44 131.36 3.90 o 1 13 1 936.88 844.10 11.58 o 2 13 1 1245.78 1129.76 13.13 o 3 13 1 1967.43 1954.82 17.31 o 4 13 1 671.41 632.09 9.60 o 5 13 1 843.22 902.62 10.99 o 6 13 1 771.91 791.17 9.38 o 7 13 1 300.29 308.96 5.28 o -6 14 1 219.75 221.33 4.47 o -5 14 1 142.92 140.78 4.14 o -4 14 1 7.02 17.32 1.79 o -3 14 1 2516.75 2343.65 17.80 o -2 14 1 130.23 125.95 3.64 o -1 14 1 1090.91 1019.19 12.21 o 0 14 1 455.67 418.10 7.97 o 1 14 1 13.44 9.88 2.96 o 2 14 1 3013.89 2850.68 20.09 o 3 14 1 579.10 576.72 8.98 o 4 14 1 894.95 897.20 10.48 o 5 14 1 0.13 2.09 1.61 o 6 14 1 124.37 139.43 3.64 o -4 15 1 409.69 417.75 6.47 o -3 15 1 214.49 229.19 5.16 o -2 15 1 63.42 62.83 2.38 o -1 15 1 208.75 193.55 5.19 o 0 15 1 124.58 129.43 3.88 o 1 15 1 1187.64 1095.26 11.59 o 2 15 1 302.05 294.90 6.00 o 3 15 1 3.75 2.53 1.73 o 4 15 1 25.47 37.52 1.89 o -2 16 1 469.10 431.76 6.08 o -1 16 1 488.86 474.29 6.55 o 0 16 1 1067.03 1029.83 9.67 o 1 16 1 187.28 181.02 4.26 o 2 16 1 919.92 841.69 8.03 o -11 0 2 362.70 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869.31 844.10 9.22 o 2 9 8 104.79 86.10 2.63 o 3 9 8 582.19 594.48 7.33 o -2 10 8 34.28 41.23 1.77 o -1 10 8 66.84 65.70 2.10 o 0 10 8 471.48 458.78 6.09 o 1 10 8 120.90 119.05 3.54 o 2 10 8 1540.76 1568.26 10.99 o -5 1 9 587.06 473.95 6.90 o -4 1 9 696.39 617.19 8.48 o -3 1 9 62.09 48.51 2.32 o -2 1 9 1343.16 1280.91 13.12 o -1 1 9 1397.95 1394.65 13.69 o 0 1 9 39.28 42.44 2.38 o 1 1 9 1674.79 1656.48 14.93 o 2 1 9 5.90 11.20 1.79 o 3 1 9 2437.45 2450.34 16.99 o 4 1 9 389.80 370.65 6.41 o 5 1 9 95.41 100.67 2.85 o -5 2 9 464.68 447.78 6.71 o -4 2 9 47.93 35.85 1.99 o -3 2 9 352.42 302.96 6.36 o -2 2 9 39.52 49.47 2.40 o -1 2 9 6.59 5.96 2.36 o 0 2 9 484.75 545.77 8.73 o 1 2 9 924.53 906.59 11.02 o 2 2 9 24.62 30.56 2.02 o 3 2 9 347.53 371.93 6.89 o 4 2 9 673.31 670.14 8.42 o 5 2 9 120.29 134.95 3.68 o -5 3 9 334.50 292.81 5.42 o -4 3 9 179.00 182.73 4.72 o -3 3 9 277.49 289.70 6.08 o -2 3 9 553.72 584.29 8.84 o -1 3 9 709.40 650.21 9.33 o 0 3 9 446.51 485.39 8.23 o 1 3 9 169.54 163.18 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123.46 106.05 3.01 o 0 8 9 298.07 278.24 4.88 o -3 0 10 172.12 137.76 3.43 o -2 0 10 120.73 102.65 2.88 o -1 0 10 1242.19 1124.00 9.83 o 0 0 10 2669.09 2517.74 14.79 o 1 0 10 3.15 8.94 1.58 o 2 0 10 1373.55 1241.81 9.77 o 3 0 10 61.85 77.50 2.36 o -3 1 10 87.77 71.90 2.06 o -2 1 10 4.17 10.63 1.43 o -1 1 10 18.19 32.71 1.86 o 0 1 10 133.57 112.16 3.10 o 1 1 10 1.06 2.88 1.64 o 2 1 10 118.49 116.05 3.41 o -2 2 10 718.42 600.70 6.98 o -1 2 10 112.97 111.03 2.99 o 0 2 10 775.40 680.41 7.64 o 1 2 10 70.56 68.83 2.22 o 2 2 10 33.59 41.55 1.72 o -2 3 10 462.90 423.34 5.69 o -1 3 10 546.85 520.53 6.49 o 0 3 10 24.13 39.07 1.77 o 1 3 10 561.40 548.78 6.48 o 2 3 10 0.05 1.63 1.31 o -1 4 10 22.78 20.71 1.55 o 0 4 10 1.65 8.06 1.24 o