#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/08/2200841.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200841_Fobs loop_ _publ_author_name 'Jones, Peter G.' 'Hopf, Henning' 'Hillmer, J\"org' _publ_section_title ; 4,13-Diacetyl-[2.2]paracyclophane ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o300 _journal_page_last o302 _journal_volume 58 _journal_year 2002 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 119.340 _cell_angle_gamma 90.000 _cell_length_a 15.8270 _cell_length_b 9.4420 _cell_length_c 11.4230 _exptl_crystal_F_000 624.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file bt6113Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sinx in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 231.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5438.68 5403.80 71.84 o 6 0 0 732.56 753.71 8.94 o 8 0 0 41.88 39.89 2.41 o 10 0 0 2113.86 2186.58 22.00 o 12 0 0 2110.85 2219.32 26.39 o 14 0 0 4.39 5.30 3.03 o 16 0 0 24.74 38.84 4.36 o 3 1 0 5630.36 5896.13 162.43 o 5 1 0 3373.88 3300.80 93.02 o 7 1 0 70.18 66.99 2.32 o 9 1 0 233.25 223.49 3.54 o 11 1 0 105.53 102.46 2.99 o 13 1 0 19.66 16.21 3.26 o 15 1 0 31.99 31.25 2.77 o 17 1 0 6.32 8.61 2.69 o 0 2 0 569.04 651.13 16.36 o 2 2 0 1664.52 1488.51 8.66 o 4 2 0 5106.83 5350.79 19.84 o 6 2 0 13271.79 14509.71 121.15 o 8 2 0 31.87 51.83 1.89 o 10 2 0 425.20 466.56 12.84 o 12 2 0 6.37 -0.75 1.70 o 14 2 0 1.16 3.09 3.28 o 16 2 0 37.93 36.95 3.19 o 1 3 0 149.41 156.13 1.99 o 3 3 0 164.21 211.27 3.66 o 5 3 0 27.08 32.56 1.47 o 7 3 0 145.87 137.35 2.69 o 9 3 0 64.02 69.37 2.39 o 11 3 0 117.13 123.45 7.64 o 13 3 0 345.93 323.98 5.55 o 15 3 0 112.95 125.47 4.21 o 17 3 0 15.60 15.20 2.92 o 0 4 0 2812.22 3292.09 43.11 o 2 4 0 2402.95 2406.51 47.67 o 4 4 0 63.17 47.30 1.68 o 6 4 0 0.99 -0.13 1.18 o 8 4 0 199.14 152.52 3.18 o 10 4 0 54.41 65.00 2.62 o 12 4 0 261.96 218.65 4.60 o 14 4 0 17.32 9.31 2.27 o 16 4 0 29.52 28.42 3.04 o 1 5 0 2468.83 2786.38 15.12 o 3 5 0 5.44 15.95 9.54 o 5 5 0 249.96 201.13 3.30 o 7 5 0 427.53 372.46 11.61 o 9 5 0 265.39 241.05 7.75 o 11 5 0 69.96 55.23 2.75 o 13 5 0 6.76 1.74 2.46 o 15 5 0 3.54 5.60 3.02 o 0 6 0 1529.32 1828.38 35.31 o 2 6 0 712.79 764.56 8.40 o 4 6 0 1082.49 1025.45 12.52 o 6 6 0 1883.63 1836.23 18.98 o 8 6 0 803.43 791.95 8.96 o 10 6 0 0.36 1.38 1.80 o 12 6 0 11.91 -1.11 1.99 o 14 6 0 53.21 57.19 3.48 o 1 7 0 100.15 122.43 4.58 o 3 7 0 75.70 59.87 2.40 o 5 7 0 3343.47 3317.59 37.37 o 7 7 0 1365.58 1276.30 10.07 o 9 7 0 8.85 7.98 2.01 o 11 7 0 109.66 111.87 3.91 o 13 7 0 4.35 1.45 6.11 o 0 8 0 150.64 123.55 4.71 o 2 8 0 418.35 360.10 7.42 o 4 8 0 63.27 63.82 3.92 o 6 8 0 1017.11 1025.80 12.94 o 8 8 0 230.45 246.87 5.07 o 10 8 0 36.24 35.68 2.84 o 12 8 0 17.32 13.37 2.74 o 1 9 0 964.51 881.13 12.07 o 3 9 0 1.41 -1.80 2.68 o 5 9 0 114.01 107.46 5.20 o 7 9 0 59.05 51.27 4.49 o 9 9 0 0.99 -1.69 3.34 o 11 9 0 274.30 307.92 9.29 o 0 10 0 137.71 118.47 5.59 o 2 10 0 48.23 60.01 4.49 o 4 10 0 0.14 -2.73 3.00 o 6 10 0 2.26 -0.32 3.15 o 8 10 0 3.62 1.23 3.58 o 10 10 0 0.79 -2.48 3.66 o 1 11 0 0.43 0.69 3.28 o 3 11 0 66.13 86.65 5.53 o 5 11 0 92.39 118.81 6.40 o 7 11 0 199.64 234.98 8.52 o 0 12 0 0.19 -2.30 3.55 o 2 12 0 0.03 -3.60 3.60 o -17 1 1 18.18 20.09 2.82 o -15 1 1 3.10 3.44 2.67 o -13 1 1 1503.59 1554.60 13.38 o -11 1 1 1840.34 1703.01 10.34 o -9 1 1 7.44 13.79 2.51 o -7 1 1 2119.42 2326.20 12.77 o -5 1 1 2592.04 2726.48 46.39 o -3 1 1 485.41 521.11 5.43 o 1 1 1 10530.58 9766.85 165.45 o 3 1 1 4324.55 4473.17 45.61 o 5 1 1 119.69 143.83 4.69 o 7 1 1 72.45 88.13 2.99 o 9 1 1 50.34 27.38 2.57 o 11 1 1 491.19 517.75 12.46 o 13 1 1 19.29 15.51 2.28 o 15 1 1 15.13 10.70 2.55 o 17 1 1 236.61 258.23 6.29 o -18 2 1 27.10 24.62 3.16 o -16 2 1 37.52 48.63 3.22 o -14 2 1 70.10 73.56 3.18 o -12 2 1 183.60 173.63 3.82 o -10 2 1 10.52 3.87 1.39 o -8 2 1 25.67 26.17 1.51 o -6 2 1 747.28 708.34 10.10 o -4 2 1 1653.52 1619.37 12.29 o -2 2 1 2776.27 2702.04 121.47 o 0 2 1 5253.04 5006.23 57.57 o 2 2 1 717.63 633.59 4.63 o 4 2 1 103.28 88.14 2.32 o 6 2 1 299.61 329.38 3.69 o 8 2 1 0.63 2.87 1.24 o 10 2 1 1.21 -1.43 1.43 o 12 2 1 134.02 127.03 3.63 o 14 2 1 3.73 0.40 2.13 o 16 2 1 45.00 41.79 3.40 o -17 3 1 34.59 45.88 3.41 o -15 3 1 7.25 2.28 2.15 o -13 3 1 5.69 12.39 2.08 o -11 3 1 63.50 58.15 2.47 o -9 3 1 0.23 1.73 1.23 o -7 3 1 689.95 835.18 9.82 o -5 3 1 1118.54 1322.44 21.70 o -3 3 1 2198.47 2162.30 38.41 o -1 3 1 19.18 19.74 0.93 o 1 3 1 125.90 116.93 1.83 o 3 3 1 647.63 642.66 12.21 o 5 3 1 4.42 6.82 1.12 o 7 3 1 4.91 -1.64 1.64 o 9 3 1 276.98 309.30 12.26 o 11 3 1 0.12 0.44 1.63 o 13 3 1 29.44 30.00 2.58 o 15 3 1 51.96 69.34 3.61 o -16 4 1 2.09 1.26 2.32 o -14 4 1 1.15 -1.56 2.00 o -12 4 1 197.29 156.03 7.40 o -10 4 1 123.25 123.50 5.89 o -8 4 1 477.95 479.64 12.21 o -6 4 1 683.54 626.19 12.23 o -4 4 1 476.78 448.30 4.29 o -2 4 1 21.35 17.60 1.17 o 0 4 1 374.75 517.56 5.58 o 2 4 1 0.37 2.24 1.20 o 4 4 1 7.04 3.15 1.05 o 6 4 1 156.24 173.91 3.14 o 8 4 1 13.50 13.61 1.66 o 10 4 1 38.40 32.60 2.24 o 12 4 1 3.07 2.03 1.95 o 14 4 1 5.22 0.31 2.21 o 16 4 1 20.13 12.01 2.88 o -17 5 1 2.83 2.61 2.56 o -15 5 1 1.90 0.99 2.28 o -13 5 1 999.32 899.00 18.41 o -11 5 1 736.62 610.02 6.98 o -9 5 1 60.30 42.83 2.26 o -7 5 1 1.66 -1.16 1.61 o -5 5 1 4.25 2.70 2.44 o -3 5 1 1691.71 1771.95 40.17 o -1 5 1 3362.59 3674.24 25.39 o 1 5 1 2606.01 3015.72 35.99 o 3 5 1 94.16 68.82 2.05 o 5 5 1 61.84 48.19 3.43 o 7 5 1 196.12 213.94 3.86 o 9 5 1 1.17 -1.04 1.62 o 11 5 1 67.53 58.64 2.95 o 13 5 1 8.54 12.71 2.43 o 15 5 1 18.94 14.02 2.79 o -16 6 1 5.45 6.63 2.64 o -14 6 1 10.12 7.91 3.05 o -12 6 1 16.85 11.42 2.20 o -10 6 1 0.14 -0.57 2.40 o -8 6 1 254.72 238.73 4.30 o -6 6 1 2463.40 2345.09 46.71 o -4 6 1 179.64 173.29 3.56 o -2 6 1 44.24 22.24 1.52 o 0 6 1 82.56 72.89 1.55 o 2 6 1 275.84 257.92 5.12 o 4 6 1 13.91 17.26 1.95 o 6 6 1 257.83 253.29 4.28 o 8 6 1 19.17 6.05 5.68 o 10 6 1 39.94 33.27 2.50 o 12 6 1 148.38 155.04 8.17 o 14 6 1 14.43 21.22 4.82 o -15 7 1 23.48 19.81 3.01 o -13 7 1 0.00 -2.17 2.17 o -11 7 1 24.01 20.77 2.50 o -9 7 1 374.79 358.63 11.01 o -7 7 1 3809.34 3572.50 104.65 o -5 7 1 2243.51 2233.06 65.64 o -3 7 1 399.14 382.96 7.21 o -1 7 1 31.04 45.58 2.11 o 1 7 1 110.17 90.52 2.69 o 3 7 1 652.73 630.57 17.37 o 5 7 1 6.58 5.52 1.78 o 7 7 1 578.77 573.36 13.60 o 9 7 1 100.74 84.19 5.24 o 11 7 1 99.20 105.51 3.98 o 13 7 1 5.71 8.88 2.63 o -14 8 1 62.84 72.64 6.89 o -12 8 1 338.23 403.77 14.65 o -10 8 1 28.67 24.91 2.60 o -8 8 1 16.38 9.89 2.19 o -6 8 1 288.06 282.67 7.51 o -4 8 1 2.20 6.29 2.53 o -2 8 1 517.67 533.98 8.81 o 0 8 1 168.10 132.31 4.79 o 2 8 1 318.68 295.86 6.90 o 4 8 1 7.86 5.70 2.59 o 6 8 1 6.42 6.78 2.88 o 8 8 1 54.84 54.64 5.34 o 10 8 1 58.36 58.34 4.32 o 12 8 1 0.03 -0.49 2.45 o -11 9 1 16.96 19.91 4.27 o -9 9 1 135.53 136.19 6.29 o -7 9 1 19.55 19.01 3.50 o -5 9 1 42.65 34.08 3.70 o -3 9 1 564.71 548.12 9.80 o -1 9 1 57.55 43.56 3.75 o 1 9 1 95.78 83.43 4.62 o 3 9 1 91.55 91.16 4.83 o 5 9 1 1.64 5.62 2.94 o 7 9 1 2.54 4.63 3.23 o 9 9 1 24.61 26.57 4.30 o 11 9 1 105.38 119.25 6.64 o -10 10 1 65.00 58.26 5.36 o -8 10 1 171.36 178.20 7.21 o -6 10 1 115.89 133.22 6.22 o -4 10 1 46.05 45.97 4.36 o -2 10 1 37.20 52.35 4.33 o 0 10 1 57.93 34.94 2.80 o 2 10 1 44.57 54.25 4.43 o 4 10 1 76.97 72.08 4.97 o 6 10 1 40.97 30.90 4.30 o 8 10 1 78.81 89.28 5.85 o -7 11 1 37.12 41.32 4.91 o -5 11 1 178.69 204.59 7.71 o -3 11 1 45.84 38.14 4.49 o -1 11 1 16.25 9.39 3.64 o 1 11 1 49.67 46.42 4.60 o 3 11 1 49.65 37.02 4.56 o 5 11 1 70.18 74.87 5.62 o 7 11 1 1.25 -1.37 3.78 o -4 12 1 57.14 77.20 5.90 o -2 12 1 61.73 61.43 5.52 o 0 12 1 111.86 116.35 4.66 o 2 12 1 75.95 73.10 5.71 o -18 0 2 57.59 61.52 5.15 o -16 0 2 1079.70 1199.10 16.85 o -14 0 2 1069.39 1080.80 13.00 o -12 0 2 7175.28 7529.63 41.73 o -10 0 2 2310.32 2134.67 16.26 o -8 0 2 41.36 11.43 1.71 o -6 0 2 4145.44 4249.55 32.56 o -4 0 2 12905.92 11631.49 159.11 o -2 0 2 719.98 542.71 6.03 o 0 0 2 11654.29 11440.60 128.17 o 2 0 2 524.56 666.67 6.70 o 4 0 2 1752.65 1413.26 13.30 o 6 0 2 2482.98 2940.48 24.91 o 8 0 2 1401.75 1462.68 15.86 o 10 0 2 2269.77 2148.99 23.48 o 12 0 2 1861.23 1896.11 22.72 o 14 0 2 62.75 41.29 4.34 o 16 0 2 2.33 2.18 3.75 o -19 1 2 22.40 19.98 5.84 o -17 1 2 33.60 40.76 3.62 o -15 1 2 48.00 40.30 2.73 o -13 1 2 299.57 304.46 7.68 o -11 1 2 445.14 461.76 5.35 o -9 1 2 588.80 558.34 8.81 o -7 1 2 20.68 14.80 1.21 o -5 1 2 2468.97 2500.85 18.67 o -3 1 2 2526.66 2598.31 44.53 o -1 1 2 187.00 184.23 1.72 o 1 1 2 2368.22 2441.81 32.83 o 3 1 2 4300.26 4080.62 23.64 o 5 1 2 1044.56 1002.78 8.20 o 7 1 2 78.66 74.25 2.18 o 9 1 2 4.41 5.54 1.52 o 11 1 2 57.21 62.42 2.78 o 13 1 2 3.24 3.03 4.95 o 15 1 2 5.30 0.14 2.42 o -18 2 2 432.09 552.29 13.60 o -16 2 2 274.71 317.64 5.97 o -14 2 2 0.60 -1.80 1.80 o -12 2 2 9.06 14.74 6.16 o -10 2 2 1888.75 2101.42 38.58 o -8 2 2 59.53 75.31 2.06 o -6 2 2 10992.83 11192.66 113.30 o -4 2 2 436.23 522.74 4.21 o -2 2 2 1374.74 1369.88 40.98 o 0 2 2 7526.15 7741.27 152.09 o 2 2 2 322.14 335.48 5.19 o 4 2 2 403.89 436.64 4.12 o 6 2 2 186.79 221.32 4.81 o 8 2 2 182.94 174.37 3.37 o 10 2 2 404.84 426.49 11.05 o 12 2 2 35.69 35.92 4.39 o 14 2 2 262.24 289.46 5.90 o 16 2 2 153.63 185.14 8.15 o -17 3 2 39.31 41.52 6.20 o -15 3 2 38.05 31.30 2.65 o -13 3 2 35.90 38.15 2.45 o -11 3 2 33.97 35.80 2.14 o -9 3 2 4.72 11.46 1.39 o -7 3 2 213.14 223.40 3.52 o -5 3 2 1294.31 1386.23 39.70 o -3 3 2 1695.25 1773.13 40.75 o -1 3 2 3639.26 3927.63 31.10 o 1 3 2 579.29 545.11 8.71 o 3 3 2 142.36 103.60 3.16 o 5 3 2 312.92 358.84 4.05 o 7 3 2 0.19 -0.97 1.18 o 9 3 2 7.22 7.49 3.45 o 11 3 2 146.19 123.73 5.48 o 13 3 2 141.85 144.20 4.32 o 15 3 2 82.36 109.03 9.23 o -18 4 2 30.78 31.81 3.25 o -16 4 2 7.72 1.17 2.28 o -14 4 2 130.19 98.49 3.57 o -12 4 2 254.58 163.28 5.10 o -10 4 2 15.52 21.86 1.84 o -8 4 2 0.63 -1.13 1.13 o -6 4 2 166.37 177.60 2.91 o -4 4 2 17.60 9.31 1.14 o -2 4 2 22.54 20.93 2.32 o 0 4 2 928.29 931.83 13.87 o 2 4 2 301.24 277.51 3.52 o 4 4 2 315.90 390.63 4.31 o 6 4 2 11.03 13.62 1.52 o 8 4 2 35.69 30.82 2.07 o 10 4 2 742.33 694.28 12.62 o 12 4 2 53.99 32.41 2.70 o 14 4 2 6.20 1.34 2.36 o -17 5 2 0.01 -1.53 2.38 o -15 5 2 155.82 150.13 4.52 o -13 5 2 79.46 72.64 3.22 o -11 5 2 322.36 273.96 4.77 o -9 5 2 33.29 26.44 1.95 o -7 5 2 100.64 101.89 2.64 o -5 5 2 108.65 97.14 4.15 o -3 5 2 93.76 88.80 2.20 o -1 5 2 88.11 116.46 3.27 o 1 5 2 139.25 142.43 3.61 o 3 5 2 51.80 64.90 2.10 o 5 5 2 1286.01 1233.09 9.14 o 7 5 2 396.30 373.11 5.13 o 9 5 2 2.86 4.58 1.88 o 11 5 2 97.77 87.26 3.49 o 13 5 2 96.66 86.22 3.84 o -16 6 2 8.78 8.17 4.97 o -14 6 2 32.61 28.84 2.81 o -12 6 2 138.94 103.81 3.61 o -10 6 2 94.70 95.20 3.19 o -8 6 2 778.13 702.37 18.83 o -6 6 2 305.93 255.88 4.05 o -4 6 2 61.58 46.45 1.96 o -2 6 2 561.36 616.55 15.90 o 0 6 2 48.10 58.43 1.49 o 2 6 2 154.57 155.35 3.14 o 4 6 2 688.31 645.65 6.62 o 6 6 2 908.39 869.12 7.78 o 8 6 2 83.03 78.03 3.04 o 10 6 2 26.38 24.25 2.68 o 12 6 2 123.86 111.77 4.16 o 14 6 2 68.69 91.64 4.33 o -15 7 2 33.79 31.35 4.01 o -13 7 2 20.16 20.96 2.65 o -11 7 2 318.52 318.26 8.01 o -9 7 2 217.38 202.50 4.39 o -7 7 2 576.88 555.64 6.73 o -5 7 2 1567.95 1505.87 39.16 o -3 7 2 35.37 26.31 3.07 o -1 7 2 491.71 436.50 17.51 o 1 7 2 177.83 205.39 3.81 o 3 7 2 469.55 493.70 5.85 o 5 7 2 196.31 185.40 4.08 o 7 7 2 98.54 86.85 3.26 o 9 7 2 12.23 5.74 2.16 o 11 7 2 137.52 151.61 4.71 o 13 7 2 33.53 38.22 3.38 o -14 8 2 195.28 237.18 6.68 o -12 8 2 173.33 190.70 7.86 o -10 8 2 12.88 14.23 3.57 o -8 8 2 377.57 399.81 19.30 o -6 8 2 341.69 355.73 7.97 o -4 8 2 153.30 168.19 5.48 o -2 8 2 252.74 265.61 6.49 o 0 8 2 144.69 132.73 3.54 o 2 8 2 106.47 109.24 4.74 o 4 8 2 495.63 517.45 9.98 o 6 8 2 21.27 19.29 3.29 o 8 8 2 10.34 7.90 2.28 o 10 8 2 26.75 31.36 3.03 o 12 8 2 142.80 179.62 10.76 o -13 9 2 137.01 155.95 7.48 o -11 9 2 497.15 551.64 11.62 o -9 9 2 0.01 -2.13 3.12 o -7 9 2 2.47 1.42 2.97 o -5 9 2 331.22 346.75 8.17 o -3 9 2 86.21 95.42 4.80 o -1 9 2 53.47 60.79 4.11 o 1 9 2 52.08 44.12 3.81 o 3 9 2 10.55 5.41 2.97 o 5 9 2 68.25 57.96 4.48 o 7 9 2 24.80 25.79 3.99 o 9 9 2 336.01 367.94 9.86 o -10 10 2 9.04 4.80 3.70 o -8 10 2 20.97 17.55 4.02 o -6 10 2 0.35 0.15 3.12 o -4 10 2 9.86 4.75 3.20 o -2 10 2 115.75 122.68 5.76 o 0 10 2 6.56 3.15 2.19 o 2 10 2 71.84 76.80 5.03 o 4 10 2 36.68 36.76 4.25 o 6 10 2 0.01 2.80 3.47 o 8 10 2 66.10 64.74 5.59 o -7 11 2 13.66 13.42 4.22 o -5 11 2 68.38 67.49 5.35 o -3 11 2 1.83 -1.43 3.38 o -1 11 2 11.34 14.58 3.81 o 1 11 2 10.58 11.46 3.67 o 3 11 2 1.02 0.21 3.49 o 5 11 2 169.95 191.82 7.85 o -4 12 2 9.51 2.47 3.95 o -2 12 2 0.08 1.16 3.79 o 0 12 2 14.26 9.31 3.19 o -19 1 3 126.72 134.99 4.83 o -17 1 3 0.12 -2.13 2.13 o 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86.34 3.06 o -11 3 3 2.30 3.61 1.48 o -9 3 3 337.46 348.75 5.60 o -7 3 3 2384.64 2435.56 69.58 o -5 3 3 23.34 6.31 1.07 o -3 3 3 3916.36 4098.96 123.63 o -1 3 3 474.18 507.89 8.11 o 1 3 3 149.98 231.06 6.80 o 3 3 3 2021.10 2111.60 12.63 o 5 3 3 1276.38 1527.38 10.35 o 7 3 3 147.75 132.04 3.21 o 9 3 3 75.64 58.24 2.67 o 11 3 3 31.71 27.68 2.48 o 13 3 3 5.57 6.95 2.73 o -18 4 3 9.58 8.38 2.70 o -16 4 3 15.83 14.63 2.50 o -14 4 3 43.62 30.20 2.73 o -12 4 3 25.79 15.13 1.95 o -10 4 3 221.55 209.94 3.80 o -8 4 3 245.71 233.30 9.60 o -6 4 3 284.61 291.73 3.65 o -4 4 3 6.90 9.58 2.47 o -2 4 3 210.29 254.05 3.33 o 0 4 3 1088.81 1066.05 5.38 o 2 4 3 88.10 61.90 1.93 o 4 4 3 177.50 177.87 3.19 o 6 4 3 5.90 1.58 1.37 o 8 4 3 110.55 93.21 3.04 o 10 4 3 18.35 11.69 2.11 o 12 4 3 56.63 51.07 4.04 o 14 4 3 9.19 4.54 2.60 o -17 5 3 69.02 58.95 4.63 o -15 5 3 80.00 83.11 3.62 o -13 5 3 164.78 161.02 7.94 o -11 5 3 297.44 237.57 4.43 o -9 5 3 289.50 278.09 4.34 o -7 5 3 882.52 890.81 17.07 o -5 5 3 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