#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/06/2200655.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200655_Fobs loop_ _publ_author_name 'van Albada, Gerard A.' 'Mutikainen, Ilpo' 'Turpeinen, Urho' 'Reedijk, Jan' _publ_section_title ; catena-Poly[[dicyanamidobis(3-hydroxypyridine-N)copper(II)]-\m-dicyanamido] ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m421 _journal_page_last m423 _journal_volume 57 _journal_year 2001 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.2660 _cell_length_b 13.9250 _cell_length_c 30.3270 _exptl_crystal_F_000 1560.00 _reflns_d_resolution_high 0.8380 _[local]_cod_data_source_file cv6054Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 359.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 39496.32 37089.98 127.10 o 4 0 0 84371.40 82253.50 293.51 o 6 0 0 23932.93 21287.60 208.15 o 8 0 0 2424.46 2552.50 67.32 o 2 1 0 129181.70 120306.43 979.64 o 4 1 0 10791.06 10258.19 112.29 o 6 1 0 12949.26 12434.24 164.26 o 8 1 0 4124.27 3487.44 85.63 o 0 2 0 4638.92 4137.21 34.47 o 2 2 0 81.30 81.59 13.46 o 4 2 0 4829.51 4682.77 83.21 o 6 2 0 195.47 234.00 33.39 o 8 2 0 393.51 346.02 29.35 o 2 3 0 16823.52 16181.26 99.09 o 4 3 0 46.03 88.05 22.35 o 6 3 0 318.67 310.21 35.28 o 8 3 0 110.64 9.69 47.12 o 2 4 0 1783.31 1787.74 47.66 o 4 4 0 14886.52 13172.60 137.33 o 6 4 0 23.39 17.23 33.12 o 8 4 0 3664.95 3251.28 77.28 o 2 5 0 53210.14 50426.58 201.15 o 4 5 0 1270.97 1495.58 48.74 o 6 5 0 3936.97 3687.51 104.75 o 8 5 0 192.25 200.07 25.85 o 0 6 0 45136.36 43088.99 179.07 o 2 6 0 1175.62 1171.63 35.81 o 4 6 0 7570.98 7711.08 119.29 o 6 6 0 6407.77 5921.45 125.21 o 8 6 0 151.26 150.32 18.17 o 2 7 0 2031.43 2248.48 62.74 o 4 7 0 0.64 -37.97 50.89 o 6 7 0 682.97 771.49 36.62 o 0 8 0 7066.23 6343.68 89.94 o 2 8 0 2938.69 3002.46 74.86 o 4 8 0 407.04 433.00 31.24 o 6 8 0 217.74 324.21 32.04 o 2 9 0 7286.43 6373.84 109.60 o 4 9 0 33.31 11.58 30.16 o 6 9 0 4519.62 4307.93 101.25 o 0 10 0 1252.41 1170.56 35.28 o 2 10 0 11.10 39.05 23.70 o 4 10 0 1247.53 1205.29 38.78 o 6 10 0 38.61 115.25 26.66 o 2 11 0 1950.36 1874.72 54.13 o 4 11 0 178.55 184.73 30.16 o 6 11 0 13.69 28.01 23.43 o 0 12 0 325.51 354.64 27.20 o 2 12 0 65.33 105.56 25.31 o 4 12 0 288.09 291.09 29.62 o 2 13 0 505.34 539.10 30.43 o 4 13 0 225.51 219.73 27.20 o 0 14 0 881.76 1053.42 33.66 o 2 14 0 1.61 23.43 23.43 o 4 14 0 827.57 890.78 30.16 o 2 15 0 1162.41 1108.62 32.85 o 0 16 0 552.60 508.67 25.58 o 2 16 0 323.77 322.15 16.48 o 1 1 1 7504.61 8535.61 48.20 o 2 1 1 48276.63 45150.05 142.72 o 3 1 1 70.41 100.44 18.04 o 4 1 1 5711.92 5465.56 86.71 o 5 1 1 4135.92 3949.52 91.02 o 6 1 1 1412.48 1287.42 39.58 o 7 1 1 378.06 327.98 34.47 o 8 1 1 449.13 399.07 30.16 o 0 2 1 36965.92 29934.43 81.59 o 1 2 1 15146.09 14001.71 68.67 o 2 2 1 5429.35 5753.15 59.24 o 3 2 1 23114.91 22034.85 134.10 o 4 2 1 26763.58 25177.07 170.72 o 5 2 1 24.17 97.75 25.31 o 6 2 1 271.91 302.13 33.93 o 7 2 1 2839.37 2616.86 80.78 o 8 2 1 1152.75 1017.61 34.47 o 1 3 1 36710.99 34817.54 118.75 o 2 3 1 13719.38 11852.33 86.98 o 3 3 1 2713.03 2824.74 63.28 o 4 3 1 166.92 358.14 23.16 o 5 3 1 7690.45 7323.86 120.64 o 6 3 1 1668.83 1653.91 46.59 o 7 3 1 323.94 352.76 35.01 o 8 3 1 155.16 178.26 26.93 o 0 4 1 6708.04 6467.28 59.24 o 1 4 1 15003.81 13274.12 86.17 o 2 4 1 302.71 302.13 16.70 o 3 4 1 2203.86 2095.26 60.05 o 4 4 1 381.33 331.21 23.97 o 5 4 1 293.11 323.94 28.54 o 6 4 1 582.14 517.02 36.89 o 7 4 1 2024.82 1937.19 52.24 o 8 4 1 147.11 106.37 25.58 o 1 5 1 11730.23 11592.47 90.21 o 2 5 1 50.98 94.25 19.12 o 3 5 1 1841.47 2039.79 60.86 o 4 5 1 1807.50 2019.32 59.24 o 5 5 1 823.81 743.21 36.35 o 6 5 1 251.81 209.77 33.12 o 7 5 1 102.42 62.47 31.24 o 8 5 1 9.64 16.16 41.74 o 0 6 1 6015.00 5483.33 70.01 o 1 6 1 3101.51 2600.97 56.82 o 2 6 1 0.08 -25.85 37.70 o 3 6 1 7720.94 7437.49 103.94 o 4 6 1 7236.42 7094.43 115.79 o 5 6 1 0.75 67.59 26.66 o 6 6 1 383.80 395.03 34.47 o 7 6 1 1286.46 1154.94 38.51 o 8 6 1 401.73 398.88 19.44 o 1 7 1 4930.71 4355.32 73.51 o 2 7 1 18785.18 19172.68 149.99 o 3 7 1 2171.21 1981.63 59.24 o 4 7 1 521.41 513.78 29.08 o 5 7 1 3294.82 3185.57 83.75 o 6 7 1 3090.41 3246.97 85.63 o 7 7 1 0.40 4.58 47.66 o 0 8 1 6433.31 5421.13 84.55 o 1 8 1 3754.12 3448.39 72.17 o 2 8 1 362.89 352.22 22.08 o 3 8 1 4448.19 4372.02 95.86 o 4 8 1 1192.74 1114.82 36.08 o 5 8 1 45.46 73.78 30.43 o 6 8 1 695.11 623.92 36.62 o 7 8 1 956.21 872.20 31.77 o 1 9 1 766.45 781.45 23.97 o 2 9 1 359.82 290.82 23.43 o 3 9 1 788.05 748.87 31.24 o 4 9 1 490.87 487.66 33.66 o 5 9 1 633.30 661.89 35.81 o 6 9 1 11.58 61.66 27.47 o 7 9 1 7.52 0.00 40.12 o 0 10 1 2389.01 2406.82 62.20 o 1 10 1 233.36 224.31 21.81 o 2 10 1 966.17 967.79 30.70 o 3 10 1 173.69 145.41 27.20 o 4 10 1 2044.79 2061.06 64.09 o 5 10 1 200.21 269.82 30.70 o 6 10 1 498.60 507.32 30.16 o 1 11 1 267.92 263.62 24.77 o 2 11 1 2931.29 2735.34 77.28 o 3 11 1 19.66 -8.08 53.86 o 4 11 1 392.76 345.49 32.85 o 5 11 1 204.42 262.28 29.35 o 6 11 1 218.33 237.77 26.12 o 0 12 1 3407.88 3435.20 93.17 o 1 12 1 18.94 4.04 43.89 o 2 12 1 195.62 182.57 26.66 o 3 12 1 782.90 796.53 33.39 o 4 12 1 970.79 1069.04 35.28 o 5 12 1 1461.35 1302.77 40.93 o 1 13 1 824.91 859.81 32.04 o 2 13 1 287.50 259.32 29.35 o 3 13 1 12.90 20.47 46.32 o 4 13 1 218.23 246.12 27.20 o 5 13 1 473.91 407.96 26.12 o 0 14 1 2411.33 2254.68 68.94 o 1 14 1 87.92 88.32 24.77 o 2 14 1 12.39 47.39 22.62 o 3 14 1 71.68 9.42 42.55 o 4 14 1 316.11 331.48 24.77 o 1 15 1 104.63 121.18 22.89 o 2 15 1 192.98 253.12 24.24 o 3 15 1 141.56 116.06 21.27 o 0 16 1 1964.03 1838.91 49.82 o 1 16 1 526.71 482.55 25.04 o 2 16 1 258.28 243.10 15.68 o 0 0 2 473.25 484.16 14.00 o 1 0 2 13214.51 12790.76 56.55 o 2 0 2 137.82 218.65 12.66 o 3 0 2 22828.63 21261.48 126.56 o 4 0 2 1080.05 1136.09 33.93 o 5 0 2 705.82 811.07 28.81 o 6 0 2 3230.76 2866.75 81.05 o 7 0 2 685.57 697.70 35.28 o 8 0 2 49.76 94.79 26.93 o 1 1 2 15469.07 15697.90 65.17 o 2 1 2 17992.90 18389.35 94.52 o 3 1 2 7161.18 6685.67 79.44 o 4 1 2 9695.07 9458.16 108.25 o 5 1 2 14614.74 14010.60 154.57 o 6 1 2 93.72 -54.66 63.55 o 7 1 2 49.52 34.20 31.51 o 8 1 2 854.25 618.80 32.04 o 0 2 2 16196.81 13326.36 58.16 o 1 2 2 2647.10 2383.39 37.43 o 2 2 2 8418.59 9479.71 74.05 o 3 2 2 3960.65 3979.95 67.32 o 4 2 2 2049.32 1980.28 54.13 o 5 2 2 1634.05 1522.24 46.05 o 6 2 2 1300.75 1240.57 40.93 o 7 2 2 66.40 126.83 31.51 o 8 2 2 48.02 82.13 27.47 o 1 3 2 6417.14 5782.23 54.39 o 2 3 2 4320.49 4335.67 58.97 o 3 3 2 3271.18 3574.68 67.86 o 4 3 2 234.54 285.71 23.16 o 5 3 2 855.27 792.49 31.24 o 6 3 2 1212.57 1064.19 40.66 o 7 3 2 1194.12 1139.59 40.93 o 8 3 2 43.09 38.51 26.39 o 0 4 2 1731.54 1536.51 36.35 o 1 4 2 196.57 82.94 12.66 o 2 4 2 355.06 335.79 17.50 o 3 4 2 10637.27 9401.35 101.79 o 4 4 2 28.16 113.91 22.35 o 5 4 2 2083.05 2047.06 62.20 o 6 4 2 1035.81 1008.18 39.05 o 7 4 2 5640.23 4926.19 116.06 o 8 4 2 692.40 545.02 29.35 o 1 5 2 37947.68 31663.74 145.14 o 2 5 2 289.86 287.86 19.39 o 3 5 2 5334.20 4982.47 83.75 o 4 5 2 841.76 901.01 29.89 o 5 5 2 5806.31 5472.02 112.56 o 6 5 2 16.51 -63.01 63.01 o 7 5 2 162.61 201.15 33.12 o 8 5 2 221.56 167.22 26.66 o 0 6 2 1771.06 1670.34 46.32 o 1 6 2 5001.38 4315.74 66.51 o 2 6 2 73.15 79.17 17.77 o 3 6 2 3903.95 3549.10 78.63 o 4 6 2 8.27 4.58 53.32 o 5 6 2 29.38 81.05 29.62 o 6 6 2 0.68 -61.66 61.66 o 7 6 2 1103.26 989.87 36.62 o 8 6 2 47.87 52.30 36.76 o 1 7 2 37.37 51.70 15.89 o 2 7 2 894.38 1107.55 31.77 o 3 7 2 127.81 190.11 22.89 o 4 7 2 54.09 13.19 53.86 o 5 7 2 73.22 189.84 34.20 o 6 7 2 191.69 157.26 33.66 o 7 7 2 0.06 -49.55 49.55 o 0 8 2 4576.88 4731.77 79.17 o 1 8 2 12876.64 11732.77 123.87 o 2 8 2 680.94 762.06 25.04 o 3 8 2 1019.54 866.54 29.89 o 4 8 2 49.25 64.09 29.35 o 5 8 2 237.67 218.39 33.12 o 6 8 2 108.27 137.33 32.31 o 7 8 2 1059.01 1007.64 32.04 o 1 9 2 105.31 84.28 19.12 o 2 9 2 906.07 823.46 28.01 o 3 9 2 200.78 196.04 27.74 o 4 9 2 87.33 121.98 31.77 o 5 9 2 1542.08 1356.09 42.82 o 6 9 2 218.43 207.88 30.97 o 7 9 2 296.77 238.31 25.31 o 0 10 2 113.28 246.66 21.81 o 1 10 2 2540.95 2247.40 63.55 o 2 10 2 2.44 25.04 23.16 o 3 10 2 5023.47 5166.93 112.29 o 4 10 2 29.94 5.92 56.01 o 5 10 2 933.64 948.13 38.24 o 6 10 2 140.57 179.07 27.47 o 1 11 2 1736.43 1605.71 49.28 o 2 11 2 6.44 31.51 25.31 o 3 11 2 344.44 339.56 30.16 o 4 11 2 1.22 4.04 53.86 o 5 11 2 824.99 783.06 33.93 o 6 11 2 0.43 -28.27 40.12 o 0 12 2 752.37 727.05 30.70 o 1 12 2 31.71 -47.93 47.93 o 2 12 2 391.64 397.19 28.01 o 3 12 2 458.19 406.61 30.43 o 4 12 2 45.54 16.70 26.93 o 5 12 2 181.66 233.47 26.12 o 1 13 2 2376.91 2328.46 65.17 o 2 13 2 2.00 -4.04 45.78 o 3 13 2 168.82 128.72 27.47 o 4 13 2 2.90 14.27 42.55 o 5 13 2 1391.48 1221.18 37.97 o 0 14 2 7.18 -37.97 44.97 o 1 14 2 3258.13 3159.18 89.94 o 2 14 2 16.39 15.35 23.70 o 3 14 2 3034.56 2852.74 78.63 o 4 14 2 0.03 -36.89 36.89 o 1 15 2 905.75 850.11 31.24 o 2 15 2 171.02 130.60 23.16 o 3 15 2 608.06 568.72 26.12 o 0 16 2 1.45 -34.20 34.20 o 1 16 2 792.99 735.13 26.66 o 2 16 2 61.59 76.29 19.39 o 1 1 3 6700.64 6153.84 45.78 o 3 1 3 2139.46 1926.69 53.05 o 4 1 3 138.79 150.26 20.73 o 5 1 3 3832.76 3675.39 90.48 o 6 1 3 1211.85 1159.52 37.16 o 7 1 3 671.79 629.84 36.89 o 8 1 3 488.17 451.31 31.24 o 1 2 3 20382.28 17520.65 79.71 o 2 2 3 3873.57 3816.49 52.51 o 3 2 3 9275.31 8637.13 96.94 o 4 2 3 296.02 243.97 21.27 o 5 2 3 1852.29 1871.49 57.36 o 6 2 3 1095.38 1010.60 39.05 o 7 2 3 4499.72 4042.42 106.90 o 8 2 3 470.91 515.40 29.35 o 1 3 3 6741.29 5461.52 54.66 o 2 3 3 4299.11 3787.68 55.74 o 3 3 3 4363.36 4511.50 73.24 o 4 3 3 4002.63 4146.63 83.75 o 5 3 3 4072.28 3873.85 95.59 o 6 3 3 23.89 -13.73 60.59 o 7 3 3 475.88 521.06 35.28 o 8 3 3 1355.50 1199.91 35.28 o 0 4 3 5456.12 4797.75 53.59 o 1 4 3 21995.32 20091.73 105.83 o 2 4 3 1578.24 1516.85 40.93 o 3 4 3 5377.87 5665.10 82.94 o 4 4 3 1492.21 1576.63 49.28 o 5 4 3 172.63 151.33 28.01 o 6 4 3 3.94 29.89 61.93 o 7 4 3 1991.77 1829.21 56.55 o 8 4 3 20.00 8.89 43.08 o 1 5 3 46.07 34.20 13.73 o 2 5 3 7.45 3.23 40.66 o 3 5 3 3589.37 3506.02 72.71 o 4 5 3 4.55 -53.59 53.59 o 5 5 3 21.87 -31.51 59.24 o 6 5 3 294.09 301.86 35.01 o 7 5 3 84.64 52.78 30.70 o 8 5 3 158.35 133.83 25.85 o 0 6 3 115.56 77.55 14.54 o 1 6 3 109.88 194.42 16.96 o 2 6 3 2555.26 2365.89 61.13 o 3 6 3 1014.21 795.18 26.39 o 4 6 3 432.30 364.87 28.27 o 5 6 3 278.30 313.71 32.04 o 6 6 3 7.09 26.12 59.78 o 7 6 3 489.52 491.97 32.58 o 8 6 3 671.42 650.77 34.20 o 1 7 3 2449.23 1937.73 55.74 o 2 7 3 2973.81 2363.19 66.78 o 3 7 3 1582.16 1434.99 42.55 o 4 7 3 181.12 161.03 27.74 o 5 7 3 1745.76 1685.69 51.70 o 6 7 3 4068.51 4189.99 108.25 o 7 7 3 15.17 -10.77 50.89 o 0 8 3 10649.49 9793.96 110.67 o 1 8 3 1594.90 1323.51 42.55 o 2 8 3 1822.49 1846.18 56.28 o 3 8 3 2624.36 2342.46 68.94 o 4 8 3 412.02 430.04 32.31 o 5 8 3 16.45 29.62 31.77 o 6 8 3 2168.49 2076.14 60.86 o 7 8 3 485.51 554.45 30.16 o 1 9 3 110.49 43.89 19.12 o 2 9 3 1715.25 1764.59 53.86 o 3 9 3 1069.92 1026.22 33.66 o 4 9 3 0.13 -28.81 30.97 o 5 9 3 60.04 36.08 30.43 o 6 9 3 4.73 75.40 28.54 o 7 9 3 74.83 116.90 34.60 o 0 10 3 4916.56 4443.65 94.52 o 1 10 3 16.61 26.12 20.73 o 2 10 3 678.44 641.96 29.08 o 3 10 3 13.74 65.97 26.39 o 4 10 3 6.91 -30.16 58.70 o 5 10 3 143.92 138.14 30.43 o 6 10 3 264.13 232.12 28.54 o 1 11 3 1114.19 1005.76 31.24 o 2 11 3 3588.44 3408.00 95.59 o 3 11 3 45.81 31.24 26.93 o 4 11 3 643.70 636.31 34.74 o 5 11 3 277.63 323.40 29.62 o 6 11 3 332.53 299.71 26.93 o 0 12 3 2124.69 2014.75 60.05 o 1 12 3 336.17 242.62 26.93 o 2 12 3 7.43 2.15 48.74 o 3 12 3 1338.66 1285.81 39.05 o 4 12 3 1076.70 1087.35 36.62 o 5 12 3 1134.52 1142.82 34.20 o 1 13 3 2912.26 2704.10 77.01 o 2 13 3 450.33 497.09 30.43 o 3 13 3 170.34 185.53 26.93 o 4 13 3 525.15 472.85 29.62 o 5 13 3 1299.70 1249.68 60.05 o 0 14 3 35.44 -16.96 43.89 o 1 14 3 393.56 454.27 30.43 o 2 14 3 193.11 160.49 24.77 o 3 14 3 124.85 135.72 23.43 o 4 14 3 170.22 162.11 23.43 o 1 15 3 22.65 24.24 22.89 o 2 15 3 1277.42 1255.65 37.16 o 3 15 3 17.15 24.24 20.20 o 0 16 3 2196.05 2086.11 54.66 o 1 16 3 83.12 71.90 21.27 o 2 16 3 171.09 170.15 26.93 o 0 0 4 27060.27 27845.09 74.32 o 1 0 4 72.86 -21.00 22.35 o 3 0 4 320.97 368.10 17.50 o 4 0 4 6550.92 6296.02 90.75 o 5 0 4 1.84 -39.58 49.01 o 6 0 4 2449.32 2382.31 69.74 o 7 0 4 235.58 216.23 32.58 o 8 0 4 3205.10 2821.24 78.63 o 1 1 4 8.84 145.41 9.96 o 3 1 4 14.97 44.43 16.70 o 4 1 4 1060.17 972.37 28.54 o 5 1 4 37.36 -27.74 50.09 o 6 1 4 2824.49 2636.78 80.25 o 7 1 4 31.63 30.70 31.24 o 8 1 4 1001.52 1144.17 35.01 o 0 2 4 3660.36 2692.52 36.08 o 1 2 4 4036.59 4088.74 44.97 o 2 2 4 3573.15 3765.87 53.05 o 3 2 4 4984.42 5910.14 78.90 o 4 2 4 1276.73 1205.56 35.01 o 5 2 4 268.42 297.55 26.39 o 6 2 4 9.67 9.96 31.77 o 7 2 4 897.34 913.93 39.05 o 8 2 4 3.09 0.00 44.97 o 1 3 4 5658.18 5414.13 55.47 o 2 3 4 958.75 933.32 27.20 o 3 3 4 302.51 323.40 19.66 o 4 3 4 537.15 545.29 24.77 o 5 3 4 429.78 494.94 28.81 o 6 3 4 148.49 196.04 33.39 o 7 3 4 24.54 60.32 31.24 o 8 3 4 128.00 160.49 26.93 o 0 4 4 1860.13 1967.89 40.12 o 1 4 4 243.62 215.69 13.46 o 2 4 4 61.65 72.71 16.96 o 3 4 4 137.76 159.14 19.66 o 4 4 4 14049.26 13961.59 142.99 o 5 4 4 77.88 98.83 29.08 o 6 4 4 2642.35 2521.80 75.94 o 7 4 4 220.90 166.95 34.47 o 8 4 4 1135.12 1097.58 35.28 o 1 5 4 1.59 23.43 14.00 o 2 5 4 23488.40 19971.10 134.37 o 3 5 4 156.32 176.65 20.73 o 4 5 4 1894.99 2011.79 63.55 o 5 5 4 0.23 14.27 57.36 o 6 5 4 3192.16 3307.83 88.05 o 7 5 4 229.81 180.96 32.31 o 8 5 4 631.06 518.95 21.48 o 1 6 4 3951.28 3932.55 66.78 o 2 6 4 49.56 59.51 17.50 o 3 6 4 437.72 509.48 24.24 o 4 6 4 2833.29 2690.64 72.17 o 5 6 4 182.05 26.12 64.36 o 6 6 4 2960.52 3126.33 85.90 o 7 6 4 203.94 175.57 31.51 o 8 6 4 744.92 631.81 20.92 o 1 7 4 191.26 297.28 17.23 o 2 7 4 3214.18 2972.04 70.82 o 3 7 4 28.68 18.31 23.16 o 4 7 4 167.89 149.99 29.89 o 5 7 4 440.24 444.31 36.89 o 6 7 4 158.61 224.31 33.93 o 7 7 4 29.67 72.71 28.81 o 0 8 4 90.58 221.62 18.04 o 1 8 4 1370.56 1389.48 39.05 o 2 8 4 33.61 66.51 19.93 o 3 8 4 2806.62 2805.89 83.48 o 4 8 4 1371.03 1293.89 37.70 o 5 8 4 10.13 48.74 32.31 o 6 8 4 1.20 -29.08 32.58 o 7 8 4 307.81 279.24 29.08 o 1 9 4 88.94 100.98 20.20 o 2 9 4 6407.26 5544.19 104.21 o 3 9 4 91.42 100.44 27.47 o 4 9 4 1142.02 1046.69 38.51 o 5 9 4 192.35 190.92 31.77 o 6 9 4 1799.53 1878.49 55.47 o 7 9 4 0.08 32.50 40.66 o 0 10 4 2424.64 2069.41 65.17 o 1 10 4 787.15 732.71 25.85 o 2 10 4 302.27 309.94 26.12 o 3 10 4 3.74 11.58 28.01 o 4 10 4 1546.47 1435.80 45.51 o 5 10 4 10.27 -13.19 54.39 o 6 10 4 327.80 325.02 29.08 o 1 11 4 46.46 65.70 22.62 o 2 11 4 1514.36 1362.82 39.58 o 3 11 4 225.97 220.81 28.81 o 4 11 4 53.76 64.90 28.54 o 5 11 4 93.75 124.14 27.20 o 6 11 4 257.00 256.35 25.58 o 0 12 4 515.12 503.01 29.08 o 1 12 4 560.66 465.58 29.35 o 2 12 4 53.47 73.24 25.58 o 3 12 4 1482.68 1397.83 39.58 o 4 12 4 34.58 19.93 26.66 o 5 12 4 9.17 -44.16 44.16 o 1 13 4 1626.78 1460.84 43.08 o 2 13 4 3457.89 3068.17 91.82 o 3 13 4 10.47 11.31 24.50 o 4 13 4 231.93 208.15 27.20 o 5 13 4 497.26 466.51 52.91 o 0 14 4 3956.51 3656.54 95.32 o 1 14 4 36.20 50.36 23.70 o 2 14 4 288.76 249.08 26.39 o 3 14 4 22.35 -18.31 39.05 o 4 14 4 1506.55 1565.86 48.47 o 1 15 4 157.92 126.29 23.70 o 2 15 4 459.70 511.36 25.58 o 3 15 4 7.21 -25.04 32.85 o 0 16 4 132.00 175.30 21.54 o 1 16 4 322.24 319.60 17.02 o 2 16 4 351.80 274.71 17.64 o 1 1 5 1643.64 1995.63 34.74 o 2 1 5 132.70 266.86 12.93 o 3 1 5 1778.05 1684.88 44.43 o 4 1 5 328.25 332.83 21.00 o 5 1 5 1165.22 1129.09 32.31 o 6 1 5 642.52 641.42 36.08 o 7 1 5 2279.07 2195.16 65.97 o 8 1 5 307.89 313.44 29.62 o 0 2 5 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4 28 52.01 97.75 23.97 o 4 4 28 1448.40 1444.14 42.28 o 5 4 28 261.50 286.78 22.35 o 1 5 28 3021.35 2874.29 86.17 o 2 5 28 1300.30 1309.24 39.85 o 3 5 28 256.33 278.17 26.93 o 4 5 28 0.41 51.16 21.00 o 0 6 28 1678.33 1679.76 53.05 o 1 6 28 863.39 819.96 30.70 o 2 6 28 212.56 211.92 25.04 o 3 6 28 1786.04 1663.07 50.09 o 4 6 28 498.24 466.12 26.12 o 1 7 28 611.75 628.23 28.01 o 2 7 28 11.33 -21.81 39.85 o 3 7 28 55.19 33.39 21.27 o 4 7 28 63.30 32.31 20.73 o 0 8 28 120.70 110.94 22.62 o 1 8 28 287.55 319.10 24.50 o 2 8 28 163.72 135.99 22.62 o 3 8 28 1321.28 1292.81 39.31 o 1 9 28 235.83 262.01 23.16 o 2 9 28 1843.09 1622.68 47.12 o 0 10 28 302.78 362.18 22.08 o 1 10 28 102.99 112.29 19.93 o 1 1 29 1185.40 1133.13 36.35 o 2 1 29 3672.82 3601.61 95.32 o 3 1 29 299.31 282.20 27.20 o 4 1 29 35.99 78.09 22.35 o 5 1 29 511.98 455.62 24.77 o 0 2 29 11381.51 11071.42 156.45 o 1 2 29 311.78 263.89 28.27 o 2 2 29 417.61 419.54 29.08 o 3 2 29 1743.64 1668.18 54.13 o 4 2 29 2131.50 2071.30 59.24 o 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2382.85 67.32 o 3 1 30 361.24 311.56 26.93 o 4 1 30 1.13 -11.85 36.89 o 0 2 30 420.80 402.84 27.47 o 1 2 30 115.20 138.41 25.85 o 2 2 30 158.21 176.92 24.77 o 3 2 30 147.02 177.72 24.24 o 4 2 30 687.63 688.55 29.35 o 1 3 30 666.68 631.46 29.35 o 2 3 30 2330.70 2082.61 62.74 o 3 3 30 1.33 -30.70 40.12 o 4 3 30 115.78 135.45 22.89 o 0 4 30 2513.34 2313.11 67.32 o 1 4 30 1959.81 1694.84 48.20 o 2 4 30 61.79 -31.77 45.51 o 3 4 30 1256.49 1127.47 36.08 o 4 4 30 3250.46 2941.07 67.86 o 1 5 30 482.49 412.81 26.66 o 2 5 30 5197.84 4857.26 97.21 o 3 5 30 78.32 44.16 21.81 o 4 5 30 919.65 920.67 28.54 o 0 6 30 1847.04 1710.73 50.09 o 1 6 30 142.53 197.11 23.70 o 2 6 30 473.03 497.63 25.58 o 3 6 30 157.64 190.11 22.62 o 1 7 30 115.01 52.51 21.81 o 2 7 30 203.14 181.76 22.89 o 3 7 30 0.13 0.00 31.51 o 0 8 30 809.40 761.79 28.01 o 1 8 30 64.01 87.25 20.73 o 2 8 30 1.22 -9.42 30.16 o 1 9 30 259.52 241.00 20.20 o 1 1 31 925.66 996.06 32.58 o 2 1 31 220.34 223.50 25.04 o 3 1 31 1343.45 1216.87 36.08 o 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