#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/06/2200634.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200634_Fobs loop_ _publ_author_name 'Wild, Kirstie Y.' 'Therrien, Bruno' 'Plieger, Paul G.' 'Officer, David L.' 'Burrell, Anthony K.' _publ_section_title ; [5,15-Bis(4-pyridyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato]zinc(II) chloroform solvate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m478 _journal_page_last m479 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.837 _cell_angle_gamma 90.000 _cell_length_a 17.8146 _cell_length_b 13.1650 _cell_length_c 20.2171 _exptl_crystal_F_000 1952.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file ci6042Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kw8 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 420.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7.76 3.18 19.08 o 4 0 0 1569.47 1836.84 99.40 o 6 0 0 66.65 213.11 55.66 o 8 0 0 50.16 -3.18 51.69 o 10 0 0 34843.29 33107.66 851.63 o 12 0 0 749.36 885.82 82.70 o 14 0 0 1344.23 1653.95 98.60 o 16 0 0 55.94 -16.70 69.18 o 18 0 0 989.63 726.78 87.47 o 20 0 0 503.21 621.03 88.26 o 22 0 0 17.57 -103.37 89.85 o 1 1 0 27217.10 26895.80 414.28 o 2 1 0 3899.82 3543.27 69.18 o 3 1 0 5965.02 7250.35 193.23 o 4 1 0 3455.27 3431.15 87.47 o 5 1 0 12416.42 12535.04 269.56 o 6 1 0 1048.42 979.65 47.71 o 7 1 0 57.94 148.70 35.78 o 8 1 0 2435.90 2830.01 86.67 o 9 1 0 3669.04 3486.82 100.99 o 10 1 0 293.88 303.75 45.32 o 11 1 0 4287.68 4733.64 135.18 o 12 1 0 697.39 609.89 49.30 o 13 1 0 1311.03 1265.91 98.60 o 14 1 0 836.87 614.67 53.28 o 15 1 0 2415.58 2170.02 120.87 o 16 1 0 2518.84 2595.43 94.63 o 17 1 0 42.36 47.71 75.54 o 18 1 0 900.11 791.19 62.82 o 19 1 0 301.00 333.18 54.87 o 20 1 0 43.67 -59.64 42.94 o 21 1 0 573.56 475.51 81.11 o 22 1 0 88.53 102.58 83.49 o 23 1 0 8.47 51.69 139.15 o 0 2 0 5106.57 4199.29 130.41 o 1 2 0 6340.53 5163.83 97.01 o 2 2 0 7672.18 7097.68 116.89 o 3 2 0 176412.44 175491.42 2678.13 o 4 2 0 61242.13 60678.56 1049.62 o 5 2 0 554.58 615.46 34.99 o 6 2 0 21746.73 20370.64 524.81 o 7 2 0 6280.05 5267.20 163.01 o 8 2 0 103.15 248.89 45.32 o 9 2 0 149.63 336.36 129.61 o 10 2 0 297.95 376.11 59.64 o 11 2 0 197.00 161.42 38.17 o 12 2 0 671.34 987.60 63.61 o 13 2 0 5137.80 5406.35 264.79 o 14 2 0 913.93 966.93 81.90 o 15 2 0 523.10 580.47 64.41 o 16 2 0 63.50 78.72 95.42 o 17 2 0 727.61 805.51 80.31 o 18 2 0 155.24 135.18 59.64 o 19 2 0 497.96 481.87 67.59 o 20 2 0 183.24 71.57 93.83 o 21 2 0 538.59 416.67 98.60 o 22 2 0 155.43 88.26 46.12 o 1 3 0 10080.15 9783.76 178.91 o 2 3 0 21220.14 20424.71 359.42 o 3 3 0 103974.63 103465.81 1584.77 o 4 3 0 25539.18 24753.61 389.63 o 5 3 0 923.52 575.70 27.04 o 6 3 0 946.00 811.07 40.55 o 7 3 0 10351.31 10918.47 208.33 o 8 3 0 7915.02 7849.11 182.09 o 9 3 0 56.89 -4.77 27.83 o 10 3 0 114.67 90.65 32.60 o 11 3 0 101.43 91.44 46.91 o 12 3 0 7347.30 7230.47 230.60 o 13 3 0 241.64 152.67 60.43 o 14 3 0 423.58 457.22 98.60 o 15 3 0 145.33 153.47 64.41 o 16 3 0 179.32 135.18 42.94 o 17 3 0 18.11 27.83 59.64 o 18 3 0 1488.32 1280.22 74.75 o 19 3 0 32.97 32.60 46.12 o 20 3 0 46.82 6.36 108.14 o 21 3 0 286.59 74.75 46.12 o 22 3 0 883.21 937.50 84.29 o 0 4 0 8235.45 8315.08 221.85 o 1 4 0 1223.22 1230.13 40.55 o 2 4 0 46.83 21.47 25.45 o 3 4 0 13864.13 13346.91 244.12 o 4 4 0 333.07 364.19 31.01 o 5 4 0 546.78 722.81 30.22 o 6 4 0 4352.83 5027.85 95.42 o 7 4 0 7221.88 7553.31 135.18 o 8 4 0 1534.33 1526.72 64.41 o 9 4 0 12.30 -13.52 31.01 o 10 4 0 354.74 295.80 35.78 o 11 4 0 99.35 125.64 42.14 o 12 4 0 6.68 22.26 43.73 o 13 4 0 3365.10 3625.97 149.49 o 14 4 0 274.66 198.79 56.46 o 15 4 0 70.06 74.75 85.88 o 16 4 0 998.08 894.57 76.34 o 17 4 0 2345.64 2507.96 110.53 o 18 4 0 368.27 520.84 95.42 o 19 4 0 0.65 24.65 58.84 o 20 4 0 855.80 903.31 68.38 o 21 4 0 146.01 209.13 67.59 o 22 4 0 49.09 188.46 82.70 o 1 5 0 4986.43 4642.99 98.60 o 2 5 0 2865.83 2941.33 70.77 o 3 5 0 4689.00 4821.11 103.37 o 4 5 0 9178.00 9095.14 176.53 o 5 5 0 11113.29 12150.18 229.80 o 6 5 0 18147.63 17848.37 291.83 o 7 5 0 8879.88 8619.63 152.67 o 8 5 0 489.51 495.39 34.19 o 9 5 0 40.01 84.29 38.96 o 10 5 0 673.93 874.69 65.20 o 11 5 0 532.88 585.24 61.23 o 12 5 0 22.85 13.52 38.96 o 13 5 0 35.24 -0.80 63.61 o 14 5 0 679.18 740.30 74.75 o 15 5 0 1991.42 2068.23 100.99 o 16 5 0 343.02 353.85 66.00 o 17 5 0 272.27 297.39 66.79 o 18 5 0 104.49 276.72 66.79 o 19 5 0 1112.55 952.61 75.54 o 20 5 0 1.94 21.47 62.02 o 21 5 0 39.04 58.84 58.84 o 0 6 0 9107.69 9584.97 259.23 o 1 6 0 1330.64 1505.26 50.89 o 2 6 0 1118.19 1174.46 44.53 o 3 6 0 129.55 137.56 31.01 o 4 6 0 6640.40 6390.77 134.38 o 5 6 0 3772.39 3637.90 100.19 o 6 6 0 2444.67 2458.66 70.77 o 7 6 0 3.45 -5.57 55.66 o 8 6 0 84.31 212.31 43.73 o 9 6 0 3522.98 3601.32 96.22 o 10 6 0 6537.77 6282.63 169.37 o 11 6 0 83.93 48.51 46.91 o 12 6 0 643.16 624.21 64.41 o 13 6 0 1850.62 1752.55 107.35 o 14 6 0 667.94 642.50 89.06 o 15 6 0 274.88 221.06 56.46 o 16 6 0 1399.99 1211.04 85.08 o 17 6 0 621.24 671.12 98.60 o 18 6 0 6.19 -18.29 112.12 o 19 6 0 92.10 318.07 82.70 o 20 6 0 545.69 565.37 192.43 o 21 6 0 5.20 26.24 86.67 o 1 7 0 1426.85 1386.77 52.48 o 2 7 0 7322.65 6836.86 142.34 o 3 7 0 276.83 378.50 36.58 o 4 7 0 4836.79 4332.08 102.58 o 5 7 0 97.50 7.95 27.83 o 6 7 0 163.21 187.66 34.99 o 7 7 0 327.57 321.25 41.35 o 8 7 0 3642.38 3988.57 104.17 o 9 7 0 2084.78 2386.30 101.78 o 10 7 0 172.37 150.29 42.14 o 11 7 0 1906.98 1968.84 93.83 o 12 7 0 17.67 -22.26 42.94 o 13 7 0 92.50 108.14 60.43 o 14 7 0 11.47 11.93 62.02 o 15 7 0 656.21 760.98 70.77 o 16 7 0 1200.80 1090.18 211.51 o 17 7 0 165.18 131.20 80.31 o 18 7 0 375.76 419.85 90.65 o 19 7 0 234.22 118.48 85.08 o 20 7 0 1.20 11.13 91.44 o 0 8 0 4556.06 4844.17 156.65 o 1 8 0 4858.65 5268.00 118.48 o 2 8 0 1796.62 2169.22 69.18 o 3 8 0 1722.57 1646.80 61.23 o 4 8 0 36.26 112.91 44.53 o 5 8 0 573.40 475.51 46.91 o 6 8 0 469.37 560.59 47.71 o 7 8 0 3096.90 3072.53 90.65 o 8 8 0 1.96 18.29 33.40 o 9 8 0 1674.06 1688.14 72.36 o 10 8 0 27.97 18.29 47.71 o 11 8 0 626.81 694.98 57.25 o 12 8 0 1218.99 1289.76 80.31 o 13 8 0 1398.38 1426.53 85.08 o 14 8 0 65.08 47.71 73.16 o 15 8 0 354.29 217.88 74.75 o 16 8 0 93.88 113.71 68.38 o 17 8 0 480.78 423.03 81.90 o 18 8 0 89.17 196.41 77.13 o 19 8 0 5.11 -38.96 100.19 o 1 9 0 70.14 16.70 54.87 o 2 9 0 6117.09 6176.87 139.15 o 3 9 0 404.44 461.99 61.23 o 4 9 0 233.30 217.08 44.53 o 5 9 0 4524.99 4644.58 116.09 o 6 9 0 1763.69 1968.84 74.75 o 7 9 0 1079.76 1063.94 60.43 o 8 9 0 150.17 168.58 41.35 o 9 9 0 72.12 -10.34 141.54 o 10 9 0 3.88 34.19 45.32 o 11 9 0 286.81 429.39 64.41 o 12 9 0 3282.87 3416.05 157.44 o 13 9 0 366.98 208.33 94.63 o 14 9 0 889.35 753.82 132.79 o 15 9 0 513.38 644.09 248.09 o 16 9 0 605.47 597.97 99.40 o 17 9 0 11.99 161.42 78.72 o 18 9 0 128.12 58.05 76.34 o 0 10 0 2517.31 2337.00 117.69 o 1 10 0 499.39 617.85 49.30 o 2 10 0 202.84 150.29 70.77 o 3 10 0 923.69 929.55 57.25 o 4 10 0 2103.13 2115.15 76.34 o 5 10 0 407.19 413.49 49.30 o 6 10 0 218.08 190.84 77.13 o 7 10 0 666.21 659.20 68.38 o 8 10 0 56.46 31.81 51.69 o 9 10 0 59.44 62.82 46.12 o 10 10 0 1683.66 1585.57 113.71 o 11 10 0 158.51 89.06 65.20 o 12 10 0 21.31 -34.19 52.48 o 13 10 0 1281.61 1107.67 107.35 o 14 10 0 337.09 357.03 77.93 o 15 10 0 27.28 34.19 133.59 o 16 10 0 2.43 102.58 108.94 o 17 10 0 28.07 -111.32 69.18 o 1 11 0 2402.09 2384.71 105.76 o 2 11 0 0.99 -0.80 45.32 o 3 11 0 1064.38 1242.05 61.23 o 4 11 0 1720.79 1760.50 73.16 o 5 11 0 513.87 477.90 77.93 o 6 11 0 753.91 795.17 66.79 o 7 11 0 78.61 77.93 89.06 o 8 11 0 394.75 351.46 61.23 o 9 11 0 2662.67 2747.31 140.74 o 10 11 0 106.33 163.80 75.54 o 11 11 0 474.07 545.49 100.19 o 12 11 0 2.02 -6.36 69.18 o 13 11 0 270.50 530.38 95.42 o 14 11 0 15.49 -6.36 66.79 o 15 11 0 363.25 315.68 93.03 o 16 11 0 34.13 155.85 85.88 o 0 12 0 12.73 169.37 89.85 o 1 12 0 19.03 24.65 78.72 o 2 12 0 584.15 696.57 83.49 o 3 12 0 195.07 169.37 46.12 o 4 12 0 250.14 240.14 48.51 o 5 12 0 1174.17 1043.26 75.54 o 6 12 0 270.16 374.52 54.07 o 7 12 0 821.00 976.47 97.01 o 8 12 0 1447.36 1459.93 108.14 o 9 12 0 61.28 90.65 67.59 o 10 12 0 761.72 847.65 137.56 o 11 12 0 18.66 54.87 87.47 o 12 12 0 58.97 -6.36 173.35 o 13 12 0 392.10 405.54 123.25 o 14 12 0 449.90 480.28 100.19 o 15 12 0 282.91 109.73 73.95 o 1 13 0 1079.49 1153.00 75.54 o 2 13 0 534.98 555.82 66.00 o 3 13 0 249.83 222.65 67.59 o 4 13 0 1385.55 1417.79 85.88 o 5 13 0 6.82 -38.96 50.10 o 6 13 0 703.78 581.27 86.67 o 7 13 0 149.58 136.77 76.34 o 8 13 0 417.19 433.37 85.88 o 9 13 0 121.47 237.76 94.63 o 10 13 0 48.27 -34.19 61.23 o 11 13 0 32.06 -34.19 67.59 o 12 13 0 424.37 425.42 162.21 o 13 13 0 14.66 135.18 89.85 o 14 13 0 88.78 -82.70 67.59 o 0 14 0 402.54 435.75 108.94 o 1 14 0 148.49 260.02 75.54 o 2 14 0 243.29 202.77 58.05 o 3 14 0 11.76 165.40 101.78 o 4 14 0 4.61 -3.18 120.07 o 5 14 0 16.81 -45.32 57.25 o 6 14 0 0.69 28.63 92.24 o 7 14 0 691.35 468.35 195.61 o 8 14 0 1.80 -36.58 85.88 o 9 14 0 314.91 267.97 76.34 o 10 14 0 133.03 267.18 89.06 o 11 14 0 375.16 529.58 111.32 o 12 14 0 80.16 235.37 78.72 o 13 14 0 121.09 113.71 114.50 o 1 15 0 1658.92 1306.46 135.18 o 2 15 0 39.97 -28.63 85.88 o 4 15 0 560.07 543.90 113.71 o 5 15 0 148.16 334.77 98.60 o 6 15 0 17.28 12.72 81.90 o 7 15 0 1.14 -38.96 124.84 o 8 15 0 55.72 76.34 77.93 o 9 15 0 407.79 520.84 88.26 o 10 15 0 5.19 -186.07 93.03 o 11 15 0 147.02 -13.52 94.63 o 2 16 0 4.71 14.31 92.24 o 3 16 0 10.07 -99.40 94.63 o 4 16 0 807.53 830.16 150.29 o 5 16 0 7.16 -146.31 89.06 o 6 16 0 57.82 192.43 140.74 o 7 16 0 38.85 239.35 123.25 o 8 16 0 57.86 -21.47 100.19 o -23 0 1 386.99 529.58 130.41 o -21 0 1 110.02 -44.53 63.61 o -19 0 1 980.94 856.40 102.58 o -17 0 1 593.64 549.46 81.11 o -15 0 1 5.69 43.73 58.84 o -13 0 1 6410.89 6535.49 219.47 o -11 0 1 4.07 39.76 49.30 o -9 0 1 10211.56 10189.30 289.44 o -7 0 1 333.58 410.31 47.71 o -5 0 1 2622.37 2792.63 96.22 o -3 0 1 13364.64 10996.39 284.67 o -1 0 1 10882.84 11106.92 225.83 o 1 0 1 148823.94 129331.86 3103.54 o 3 0 1 1507.34 1694.51 81.90 o 5 0 1 2687.10 3199.76 147.11 o 7 0 1 1880.57 1803.44 108.94 o 9 0 1 6578.24 7168.45 174.14 o 11 0 1 6492.43 6883.78 213.90 o 13 0 1 225.64 260.82 116.89 o 15 0 1 1299.37 1401.09 93.83 o 17 0 1 3200.69 3350.05 155.06 o 19 0 1 35.03 151.88 79.52 o 21 0 1 268.25 423.03 89.06 o 23 0 1 498.48 117.69 95.42 o -23 1 1 36.41 26.24 121.66 o -22 1 1 10.27 -93.03 79.52 o -21 1 1 47.78 120.87 64.41 o -20 1 1 72.75 100.99 58.84 o -19 1 1 874.66 969.31 78.72 o -18 1 1 678.68 682.26 64.41 o -17 1 1 23.69 -50.10 42.94 o -16 1 1 3.09 -23.86 47.71 o -15 1 1 933.58 960.56 76.34 o -14 1 1 2579.21 2473.77 91.44 o -13 1 1 47.98 11.93 34.19 o -12 1 1 320.50 301.37 46.12 o -11 1 1 13207.67 13059.86 260.02 o -10 1 1 5576.04 6493.35 166.99 o -9 1 1 6002.79 6254.80 157.44 o -8 1 1 8146.65 8279.30 194.82 o -7 1 1 266.58 183.68 50.89 o -6 1 1 59.35 50.10 28.63 o -5 1 1 2044.92 1754.14 58.84 o -4 1 1 5389.64 6162.56 173.35 o -3 1 1 1907.63 2457.87 73.95 o -2 1 1 17362.47 18392.26 372.93 o -1 1 1 43670.84 41152.39 818.23 o 0 1 1 11856.91 11249.26 198.00 o 1 1 1 2893.01 2880.90 49.30 o 2 1 1 7844.29 7845.14 142.34 o 3 1 1 18845.65 16303.35 289.44 o 4 1 1 703.86 1061.55 41.35 o 5 1 1 2756.17 3070.94 82.70 o 6 1 1 11152.77 10574.16 287.06 o 7 1 1 1922.39 2025.30 67.59 o 8 1 1 1581.43 1962.48 86.67 o 9 1 1 10169.27 9604.85 280.69 o 10 1 1 3432.73 3509.08 128.02 o 11 1 1 9.53 149.49 38.17 o 12 1 1 3025.93 3018.46 102.58 o 13 1 1 81.61 34.99 44.53 o 14 1 1 1931.79 2003.03 88.26 o 15 1 1 33.26 38.96 35.78 o 16 1 1 1162.86 1083.82 68.38 o 17 1 1 490.74 520.84 54.07 o 18 1 1 7.96 76.34 42.94 o 19 1 1 1357.77 1459.93 81.11 o 20 1 1 58.72 129.61 194.02 o 21 1 1 125.02 298.19 60.43 o 22 1 1 705.50 844.47 76.34 o 23 1 1 89.83 113.71 76.34 o -22 2 1 158.30 206.74 71.57 o -21 2 1 16.72 34.19 63.61 o -20 2 1 545.62 708.50 93.03 o -19 2 1 65.54 100.19 58.05 o -18 2 1 41.32 11.13 44.53 o -17 2 1 0.81 14.31 64.41 o -16 2 1 3384.40 3290.41 129.61 o -15 2 1 86.15 37.37 95.42 o -14 2 1 87.36 100.19 52.48 o -13 2 1 2428.95 2377.56 100.19 o -12 2 1 1137.85 1326.34 86.67 o -11 2 1 12.97 110.53 73.16 o -10 2 1 2528.06 2681.31 154.26 o -9 2 1 491.40 429.39 54.87 o -8 2 1 600.02 629.77 60.43 o -7 2 1 493.30 535.15 51.69 o -6 2 1 35216.72 32562.97 823.00 o -5 2 1 2142.90 2255.89 67.59 o -4 2 1 53088.27 52968.60 918.42 o -3 2 1 68155.09 67457.38 1342.25 o -2 2 1 75005.76 75017.04 1281.02 o -1 2 1 3602.15 3781.82 74.75 o 0 2 1 1379.04 1355.76 35.78 o 1 2 1 1628.55 1378.03 31.01 o 2 2 1 7243.21 6695.32 111.32 o 3 2 1 2973.34 3692.76 68.38 o 4 2 1 25118.29 21572.14 383.27 o 5 2 1 2165.10 1991.90 53.28 o 6 2 1 4360.88 4993.66 120.87 o 7 2 1 2180.30 2136.62 68.38 o 8 2 1 3917.06 5033.42 129.61 o 9 2 1 553.91 557.41 46.91 o 10 2 1 7.81 10.34 33.40 o 11 2 1 5356.94 5846.08 187.66 o 12 2 1 14.86 -13.52 82.70 o 13 2 1 634.60 658.40 74.75 o 14 2 1 4821.74 4916.53 147.90 o 15 2 1 6.71 9.54 31.81 o 16 2 1 1375.86 1390.75 77.13 o 17 2 1 17.57 -75.54 49.30 o 18 2 1 126.78 93.03 57.25 o 19 2 1 3.62 -42.94 53.28 o 20 2 1 1225.94 1179.24 74.75 o 21 2 1 210.53 201.18 64.41 o 22 2 1 83.03 140.74 124.84 o -22 3 1 0.20 52.48 54.07 o -21 3 1 640.66 586.83 63.61 o -20 3 1 105.87 50.89 58.05 o -19 3 1 216.03 259.23 61.23 o -18 3 1 9.35 116.89 106.55 o -17 3 1 511.63 500.16 80.31 o -16 3 1 5.15 -55.66 45.32 o -15 3 1 799.38 791.99 59.64 o -14 3 1 39.98 -10.34 52.48 o -13 3 1 1429.28 1473.45 100.19 o -12 3 1 115.40 206.74 62.82 o -11 3 1 1708.90 1514.00 124.84 o -10 3 1 331.70 357.03 64.41 o -9 3 1 3591.56 3971.07 178.91 o -8 3 1 6705.14 6658.75 164.60 o -7 3 1 17867.93 18418.50 334.77 o -6 3 1 1104.96 1013.05 36.58 o -5 3 1 7807.12 8484.45 143.93 o -4 3 1 4764.74 5040.58 91.44 o 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