#------------------------------------------------------------------------------ #$Date: 2021-07-16 08:08:54 +0300 (Fri, 16 Jul 2021) $ #$Revision: 267585 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/10/88/2108835.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2108835 _cell_angle_alpha 90.000 _cell_angle_beta 105.485 _cell_angle_gamma 90.000 _cell_length_a 12.1709 _cell_length_b 14.5397 _cell_length_c 8.2078 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.7488 _cod_data_source_file xk5079KB02_RTsup2.hkl _cod_data_source_block KB02_RT _shelx_title ' KB02_RT in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 390.90 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3940.25 4225.15 95.36 o 2 0 0 62955.35 61798.68 1108.02 o 3 0 0 152799.91 144276.23 2473.44 o 4 0 0 1382.91 1649.81 30.53 o 5 0 0 43012.28 41183.22 818.67 o 6 0 0 30390.35 30247.31 619.11 o 7 0 0 792.81 643.10 15.80 o 8 0 0 22171.82 21169.07 733.70 o 9 0 0 2123.36 2130.07 43.26 o 10 0 0 1183.16 1167.20 28.04 o 11 0 0 5162.17 5246.25 100.05 o 12 0 0 71.01 57.04 7.17 o 13 0 0 447.29 527.11 16.74 o 14 0 0 518.19 511.91 23.45 o 15 0 0 44.42 18.72 9.80 o 1 1 0 10369.61 10255.77 163.18 o 2 1 0 9176.52 9642.22 126.77 o 3 1 0 3917.59 3688.76 47.88 o 4 1 0 21879.39 22228.19 276.66 o 5 1 0 668.73 687.88 10.75 o 6 1 0 4886.95 5081.04 68.19 o 7 1 0 5955.79 5997.20 78.55 o 8 1 0 54.22 49.82 5.94 o 9 1 0 1725.09 1787.18 25.70 o 10 1 0 331.52 324.18 9.25 o 11 1 0 6.45 5.98 3.89 o 12 1 0 665.81 715.93 13.57 o 13 1 0 5.06 -0.89 3.75 o 14 1 0 26.24 34.31 6.31 o 15 1 0 103.34 113.47 9.51 o 0 2 0 3292.84 3295.19 115.09 o 1 2 0 866.55 864.70 16.97 o 2 2 0 482.47 515.28 8.90 o 3 2 0 781.67 802.90 12.46 o 4 2 0 54.35 70.19 4.25 o 5 2 0 41.10 37.29 3.19 o 6 2 0 6.95 18.86 3.00 o 7 2 0 1002.11 1023.84 15.94 o 8 2 0 4.56 6.55 3.73 o 9 2 0 7.51 6.80 3.49 o 10 2 0 467.62 463.56 10.45 o 11 2 0 85.32 80.50 5.26 o 12 2 0 112.15 116.27 6.62 o 13 2 0 117.90 107.15 6.14 o 14 2 0 0.06 -0.59 5.97 o 15 2 0 56.11 54.71 8.03 o 1 3 0 27563.25 28646.03 440.66 o 2 3 0 41697.63 42979.87 586.41 o 3 3 0 7455.12 7187.52 102.05 o 4 3 0 15258.54 14676.06 183.57 o 5 3 0 8564.26 8626.83 112.81 o 6 3 0 4760.54 4213.73 55.85 o 7 3 0 6220.57 5963.81 105.85 o 8 3 0 1475.69 1421.81 21.88 o 9 3 0 4263.59 4101.68 54.36 o 10 3 0 1691.94 1651.01 24.40 o 11 3 0 325.77 369.10 9.70 o 12 3 0 172.28 169.71 7.36 o 13 3 0 553.59 509.91 11.38 o 14 3 0 217.35 224.26 20.16 o 15 3 0 33.55 31.06 7.26 o 0 4 0 59783.80 57351.36 1208.54 o 1 4 0 15703.13 15846.18 236.84 o 2 4 0 34774.59 34148.86 492.54 o 3 4 0 46825.77 46219.42 615.47 o 4 4 0 1273.93 1453.72 20.44 o 5 4 0 35294.57 34873.34 454.25 o 6 4 0 14926.43 14975.32 187.84 o 7 4 0 780.97 770.10 29.48 o 8 4 0 9163.08 9343.98 121.56 o 9 4 0 3489.03 3440.54 46.26 o 10 4 0 1030.91 995.01 16.43 o 11 4 0 1905.27 1951.37 29.19 o 12 4 0 246.40 241.39 11.08 o 13 4 0 307.74 341.12 10.16 o 14 4 0 329.46 359.41 25.19 o 15 4 0 0.02 2.68 6.34 o 1 5 0 24.65 26.11 2.97 o 2 5 0 88.04 81.96 4.31 o 3 5 0 26.64 43.70 3.15 o 4 5 0 380.54 395.38 7.67 o 5 5 0 1851.34 1867.89 26.17 o 6 5 0 34.47 50.65 4.64 o 7 5 0 259.57 297.26 9.60 o 8 5 0 889.38 867.03 14.34 o 9 5 0 28.49 45.22 4.20 o 10 5 0 11.27 15.46 3.88 o 11 5 0 71.75 85.06 5.30 o 12 5 0 143.53 147.42 9.67 o 13 5 0 61.18 62.51 5.96 o 14 5 0 0.21 -5.76 6.16 o 15 5 0 13.40 9.41 6.59 o 0 6 0 5858.62 6176.78 118.98 o 1 6 0 1448.77 1474.06 25.80 o 2 6 0 0.02 3.28 2.65 o 3 6 0 565.81 626.29 12.73 o 4 6 0 50.97 48.15 3.52 o 5 6 0 218.31 222.41 6.47 o 6 6 0 79.34 88.90 9.94 o 7 6 0 59.08 71.57 4.69 o 8 6 0 292.63 259.91 10.15 o 9 6 0 529.88 554.24 11.03 o 10 6 0 33.02 28.58 4.27 o 11 6 0 13.19 9.98 3.93 o 12 6 0 94.71 123.27 6.57 o 13 6 0 4.81 1.89 5.32 o 14 6 0 2.16 11.28 6.49 o 1 7 0 42624.38 43890.22 739.50 o 2 7 0 17301.69 17810.84 251.90 o 3 7 0 828.29 819.96 14.51 o 4 7 0 25609.23 25884.49 330.50 o 5 7 0 3875.14 3674.20 115.63 o 6 7 0 2457.75 2332.82 34.51 o 7 7 0 8590.07 8284.85 111.04 o 8 7 0 689.34 685.43 12.20 o 9 7 0 2264.68 2155.10 30.72 o 10 7 0 1846.84 1697.99 24.86 o 11 7 0 42.34 32.95 4.50 o 12 7 0 750.80 728.73 14.14 o 13 7 0 289.01 235.76 17.33 o 14 7 0 0.96 0.23 6.33 o 0 8 0 1620.64 1319.84 28.69 o 1 8 0 4820.03 4958.04 82.89 o 2 8 0 6011.59 5776.16 77.41 o 3 8 0 5230.25 5272.39 81.64 o 4 8 0 415.43 428.79 19.87 o 5 8 0 5704.95 5606.96 84.44 o 6 8 0 3468.55 3537.89 47.23 o 7 8 0 358.12 405.14 9.21 o 8 8 0 1468.78 1496.09 23.05 o 9 8 0 1262.52 1301.96 20.83 o 10 8 0 280.71 332.49 12.35 o 11 8 0 411.20 440.59 10.89 o 12 8 0 216.37 213.29 9.36 o 13 8 0 177.91 208.68 19.28 o 14 8 0 61.72 67.52 8.71 o 1 9 0 3090.83 2980.46 94.96 o 2 9 0 461.36 443.84 23.03 o 3 9 0 42.71 57.18 7.50 o 4 9 0 4312.87 4271.72 67.09 o 5 9 0 18.09 31.47 4.07 o 6 9 0 172.42 192.43 11.14 o 7 9 0 930.61 921.09 15.80 o 8 9 0 6.74 10.29 4.00 o 9 9 0 50.67 54.97 5.01 o 10 9 0 49.77 57.60 5.23 o 11 9 0 288.99 251.21 10.10 o 12 9 0 78.52 72.13 8.69 o 13 9 0 4.72 3.77 6.56 o 0 10 0 172.06 190.60 15.42 o 1 10 0 237.14 282.41 9.78 o 2 10 0 159.90 176.24 8.81 o 3 10 0 283.34 310.95 8.20 o 4 10 0 3.60 8.49 3.81 o 5 10 0 71.15 57.18 4.85 o 6 10 0 17.50 14.54 3.86 o 7 10 0 0.31 2.16 3.53 o 8 10 0 18.88 6.41 3.82 o 9 10 0 43.89 28.32 4.59 o 10 10 0 15.05 9.72 4.16 o 11 10 0 0.02 2.93 5.21 o 12 10 0 10.77 3.85 6.49 o 13 10 0 4.05 6.50 6.53 o 1 11 0 7223.87 7302.93 100.74 o 2 11 0 2888.82 2857.10 39.72 o 3 11 0 57.29 69.10 4.85 o 4 11 0 9452.04 9353.83 131.36 o 5 11 0 753.97 762.05 14.54 o 6 11 0 796.27 777.41 14.25 o 7 11 0 2864.17 2872.43 39.96 o 8 11 0 168.79 170.06 10.52 o 9 11 0 221.52 225.19 10.64 o 10 11 0 542.94 541.24 12.76 o 11 11 0 124.82 87.87 10.56 o 12 11 0 148.64 132.41 13.21 o 0 12 0 101.78 85.78 7.42 o 1 12 0 452.17 473.00 9.70 o 2 12 0 329.76 368.15 8.79 o 3 12 0 69.06 90.18 5.45 o 4 12 0 113.10 126.59 8.83 o 5 12 0 802.81 786.10 15.83 o 6 12 0 38.09 41.79 4.63 o 7 12 0 54.42 59.06 4.99 o 8 12 0 0.59 4.03 3.88 o 9 12 0 152.00 133.05 6.62 o 10 12 0 20.02 25.91 6.95 o 11 12 0 7.94 14.31 6.82 o 12 12 0 24.64 17.39 7.02 o 1 13 0 2883.92 2707.23 38.38 o 2 13 0 1913.39 1932.83 27.48 o 3 13 0 412.84 415.25 9.81 o 4 13 0 2137.35 2090.88 33.33 o 5 13 0 116.16 129.87 9.36 o 6 13 0 154.12 143.29 6.67 o 7 13 0 908.01 929.90 16.03 o 8 13 0 9.91 11.75 4.12 o 9 13 0 242.31 305.90 16.61 o 10 13 0 228.48 178.61 18.54 o 11 13 0 38.85 37.89 7.38 o 0 14 0 7.00 17.67 5.96 o 1 14 0 241.75 293.75 13.00 o 2 14 0 90.56 96.78 5.54 o 3 14 0 95.48 99.30 5.57 o 4 14 0 119.26 122.69 6.71 o 5 14 0 21.22 20.08 5.16 o 6 14 0 104.57 89.35 5.86 o 7 14 0 79.02 72.23 5.83 o 8 14 0 0.01 -3.05 5.88 o 9 14 0 225.65 195.99 13.54 o 10 14 0 1.50 0.38 6.30 o 1 15 0 411.96 376.27 9.84 o 2 15 0 606.34 608.46 12.20 o 3 15 0 64.24 64.92 5.17 o 4 15 0 125.59 123.94 7.25 o 5 15 0 555.86 553.84 13.50 o 6 15 0 93.78 104.73 7.81 o 7 15 0 135.85 106.34 9.94 o 8 15 0 133.64 131.46 13.98 o 9 15 0 38.22 43.67 7.85 o 0 16 0 1996.95 2040.35 43.60 o 1 16 0 140.98 166.36 8.60 o 2 16 0 574.97 598.25 12.50 o 3 16 0 809.63 843.20 15.30 o 4 16 0 78.85 80.70 7.31 o 5 16 0 656.12 721.57 23.84 o 6 16 0 381.47 372.53 41.55 o 7 16 0 23.78 37.42 7.83 o 8 16 0 225.17 219.04 21.03 o 1 17 0 434.98 491.10 26.73 o 2 17 0 546.13 590.41 29.33 o 3 17 0 204.87 123.54 16.05 o 4 17 0 260.44 263.38 31.91 o 5 17 0 220.61 196.54 14.63 o 6 17 0 189.01 184.94 16.60 o 7 17 0 203.62 260.49 16.48 o 0 18 0 120.27 135.89 21.06 o 1 18 0 1.77 1.38 6.62 o 2 18 0 3.23 5.67 7.60 o 3 18 0 68.41 67.17 8.68 o 4 18 0 23.95 18.11 7.46 o 5 18 0 2.14 -1.06 6.82 o 1 19 0 34.77 35.03 7.42 o 2 19 0 46.33 42.48 7.79 o 3 19 0 9.47 9.31 7.29 o -15 1 1 74.91 95.81 9.26 o -14 1 1 43.87 52.02 6.70 o -13 1 1 691.77 690.55 13.46 o -12 1 1 482.23 491.47 11.06 o -11 1 1 24.00 19.48 4.09 o -10 1 1 4808.76 4842.52 65.18 o -9 1 1 963.66 906.79 15.87 o -8 1 1 1903.19 2017.11 79.01 o -7 1 1 6149.31 6045.09 83.14 o -6 1 1 7500.74 7102.11 116.20 o -5 1 1 9499.68 9867.02 171.83 o -4 1 1 14683.10 14106.04 215.58 o -3 1 1 5951.84 5874.94 77.35 o -2 1 1 19718.02 20713.76 269.49 o -1 1 1 3615.19 4072.69 54.53 o 0 1 1 193.82 213.45 4.92 o 1 1 1 944.55 1000.31 20.80 o 2 1 1 34642.67 35890.04 489.99 o 3 1 1 3955.31 3671.45 46.53 o 4 1 1 6671.85 6379.72 82.19 o 5 1 1 17959.85 18103.14 241.90 o 6 1 1 3022.32 2850.64 39.72 o 7 1 1 6100.57 6139.32 88.91 o 8 1 1 3489.73 3556.37 62.38 o 9 1 1 1321.53 1257.90 19.45 o 10 1 1 2011.61 1984.00 27.76 o 11 1 1 335.31 310.08 11.02 o 12 1 1 347.90 372.59 9.98 o 13 1 1 548.32 571.61 12.97 o 14 1 1 8.38 15.64 5.33 o 15 1 1 64.16 77.30 7.42 o -15 2 1 4.95 3.26 6.60 o -14 2 1 14.12 15.20 7.06 o -13 2 1 36.33 37.82 4.82 o -12 2 1 39.65 29.23 4.50 o -11 2 1 379.06 341.24 11.42 o -10 2 1 1416.62 1418.48 24.31 o -9 2 1 88.82 103.69 5.79 o -8 2 1 1093.79 1117.42 20.64 o -7 2 1 769.17 762.89 13.64 o -6 2 1 18.91 15.40 3.24 o -5 2 1 2067.44 2310.07 37.82 o -4 2 1 64.89 77.03 6.40 o -3 2 1 278.96 307.41 5.83 o -2 2 1 931.06 943.14 13.48 o -1 2 1 796.57 841.82 11.85 o 0 2 1 327.38 280.12 4.86 o 1 2 1 4088.83 4181.45 61.07 o 2 2 1 1525.61 1563.47 20.36 o 3 2 1 1114.88 1130.12 15.74 o 4 2 1 0.72 5.94 2.00 o 5 2 1 1113.71 1277.37 17.75 o 6 2 1 142.67 152.22 5.61 o 7 2 1 2.03 -1.17 2.81 o 8 2 1 94.17 92.72 5.28 o 9 2 1 18.36 23.87 3.67 o 10 2 1 649.20 658.75 11.94 o 11 2 1 121.68 104.65 5.37 o 12 2 1 6.07 2.11 3.71 o 13 2 1 41.30 30.43 4.63 o 14 2 1 3.82 -0.65 5.47 o 15 2 1 12.25 11.31 5.60 o -15 3 1 69.17 81.92 9.19 o -14 3 1 11.10 4.03 11.97 o -13 3 1 412.43 429.36 10.92 o -12 3 1 204.99 197.39 7.37 o -11 3 1 55.61 62.11 4.86 o -10 3 1 2036.59 2101.41 29.34 o -9 3 1 234.63 242.04 7.44 o -8 3 1 1323.69 1378.54 22.44 o -7 3 1 3524.08 3411.40 62.41 o -6 3 1 0.18 8.64 3.32 o -5 3 1 6160.05 6606.17 103.93 o -4 3 1 2150.87 2012.78 31.14 o -3 3 1 169.31 160.53 4.67 o -2 3 1 9612.33 10058.52 131.52 o -1 3 1 7854.14 8164.95 112.39 o 0 3 1 1993.77 2196.17 29.45 o 1 3 1 11386.63 11621.72 147.82 o 2 3 1 6958.17 7285.48 89.27 o 3 3 1 101.27 137.81 4.67 o 4 3 1 2921.51 2896.25 42.57 o 5 3 1 2514.14 2612.26 33.67 o 6 3 1 13.76 42.51 3.27 o 7 3 1 2282.51 2237.38 37.48 o 8 3 1 737.85 786.39 14.06 o 9 3 1 47.50 53.14 4.27 o 10 3 1 1295.06 1316.34 20.21 o 11 3 1 176.11 166.20 9.82 o 12 3 1 248.61 263.87 13.47 o 13 3 1 137.16 164.76 8.51 o 14 3 1 21.23 18.82 7.22 o 15 3 1 25.07 24.00 10.34 o -15 4 1 0.24 6.00 6.64 o -14 4 1 153.52 145.95 20.12 o -13 4 1 63.34 76.21 5.63 o -12 4 1 10.51 25.76 4.36 o -11 4 1 2268.57 2153.40 31.01 o -10 4 1 72.38 86.11 5.11 o -9 4 1 41.61 46.98 4.27 o -8 4 1 7116.40 6819.22 99.10 o -7 4 1 334.58 324.33 24.23 o -6 4 1 3285.28 3473.12 52.91 o -5 4 1 12212.17 12313.63 175.02 o -4 4 1 547.89 522.18 9.43 o -3 4 1 19600.91 20276.62 333.87 o -2 4 1 15544.69 15160.09 206.40 o -1 4 1 0.46 9.75 2.13 o 0 4 1 42532.78 43511.72 547.24 o 1 4 1 6552.81 6687.21 87.98 o 2 4 1 1465.90 1454.77 21.06 o 3 4 1 23288.83 23067.84 294.04 o 4 4 1 1370.94 1472.43 19.79 o 5 4 1 5598.28 5462.06 68.38 o 6 4 1 5716.77 5609.27 71.86 o 7 4 1 147.67 208.26 9.77 o 8 4 1 3543.84 3474.19 48.47 o 9 4 1 706.99 667.53 11.79 o 10 4 1 374.80 384.01 8.94 o 11 4 1 2566.45 2420.35 34.27 o 12 4 1 69.46 57.61 4.81 o 13 4 1 2.07 6.55 4.30 o 14 4 1 165.87 179.33 16.02 o -15 5 1 261.75 283.41 24.17 o -14 5 1 16.51 33.60 10.67 o -13 5 1 26.00 21.27 4.65 o -12 5 1 1170.83 1276.95 20.63 o -11 5 1 1.09 5.89 3.79 o -10 5 1 585.03 625.64 11.77 o -9 5 1 3323.86 3471.34 47.75 o -8 5 1 101.60 93.99 5.54 o -7 5 1 10764.70 10845.90 182.85 o -6 5 1 3854.02 3788.28 51.99 o -5 5 1 985.47 1096.67 17.79 o -4 5 1 23775.08 23494.53 330.96 o -3 5 1 6851.47 6753.49 99.56 o -2 5 1 7476.07 7328.77 104.50 o -1 5 1 48949.12 47443.72 630.16 o 0 5 1 272.15 261.29 5.38 o 1 5 1 19447.63 18819.48 234.83 o 2 5 1 21034.07 20136.79 245.71 o 3 5 1 256.60 313.75 6.21 o 4 5 1 23731.14 22846.88 291.07 o 5 5 1 5675.54 5728.43 71.75 o 6 5 1 179.37 149.69 8.22 o 7 5 1 10706.72 10640.51 161.53 o 8 5 1 587.58 615.52 11.83 o 9 5 1 647.60 676.97 12.24 o 10 5 1 2002.93 2077.15 29.74 o 11 5 1 31.82 22.95 4.04 o 12 5 1 420.91 489.32 10.97 o 13 5 1 149.90 127.06 8.99 o 14 5 1 5.75 2.10 6.90 o -15 6 1 87.76 76.94 8.85 o -14 6 1 46.49 38.18 7.70 o -13 6 1 115.50 125.78 8.48 o -12 6 1 318.97 272.87 8.48 o -11 6 1 190.83 178.08 10.33 o -10 6 1 935.30 920.70 15.76 o -9 6 1 852.68 805.79 14.39 o -8 6 1 0.26 -1.34 3.72 o -7 6 1 1612.10 1678.27 28.13 o -6 6 1 1761.03 1721.40 81.47 o -5 6 1 774.01 891.50 14.55 o -4 6 1 2283.29 2406.41 34.55 o -3 6 1 468.57 485.50 9.40 o -2 6 1 1046.19 1085.30 16.37 o -1 6 1 3304.90 3547.53 49.17 o 0 6 1 840.41 975.91 14.15 o 1 6 1 1195.56 1188.59 20.03 o 2 6 1 0.64 -0.02 2.20 o 3 6 1 64.92 82.42 3.64 o 4 6 1 460.31 461.00 8.15 o 5 6 1 126.72 153.93 5.33 o 6 6 1 26.41 27.83 4.39 o 7 6 1 76.28 105.84 6.38 o 8 6 1 0.21 1.74 3.26 o 9 6 1 31.55 21.42 3.83 o 10 6 1 160.45 156.14 6.80 o 11 6 1 12.14 11.03 3.80 o 12 6 1 22.02 13.20 4.13 o 13 6 1 62.99 60.49 7.24 o 14 6 1 12.78 6.12 6.17 o -14 7 1 155.96 175.47 12.37 o -13 7 1 0.81 3.23 10.03 o -12 7 1 4.04 2.82 4.06 o -11 7 1 304.14 349.76 10.24 o -10 7 1 15.76 6.18 3.82 o -9 7 1 244.11 226.70 10.06 o -8 7 1 283.29 306.12 8.86 o -7 7 1 137.77 161.63 6.51 o -6 7 1 2391.65 2285.44 33.77 o -5 7 1 71.85 86.70 14.19 o -4 7 1 44.30 43.74 3.59 o -3 7 1 4020.16 4072.43 59.95 o -2 7 1 55.54 74.60 4.85 o -1 7 1 0.97 0.75 2.52 o 0 7 1 1211.12 1256.88 20.16 o 1 7 1 671.75 684.27 10.86 o 2 7 1 2729.72 2961.41 39.03 o 3 7 1 32.64 38.30 3.22 o 4 7 1 0.82 3.13 2.75 o 5 7 1 892.03 849.55 26.53 o 6 7 1 602.90 599.87 11.34 o 7 7 1 7.47 13.53 3.62 o 8 7 1 306.90 271.18 11.80 o 9 7 1 344.46 359.97 8.93 o 10 7 1 39.33 27.44 4.17 o 11 7 1 0.13 6.62 3.85 o 12 7 1 7.71 6.99 4.15 o 13 7 1 44.87 31.36 6.70 o 14 7 1 45.14 44.24 7.15 o -14 8 1 269.53 279.43 14.62 o -13 8 1 314.43 262.81 26.08 o -12 8 1 11.99 5.84 5.01 o -11 8 1 1294.07 1234.39 19.67 o -10 8 1 1529.14 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3.59 3.31 o -3 10 2 18.12 21.05 3.60 o -2 10 2 255.92 267.79 11.71 o -1 10 2 49.87 43.50 4.10 o 0 10 2 192.21 212.84 7.82 o 1 10 2 362.47 376.84 9.39 o 2 10 2 0.63 0.16 2.97 o 3 10 2 56.20 59.23 4.12 o 4 10 2 137.05 144.49 5.92 o 5 10 2 23.26 32.90 4.18 o 6 10 2 32.50 31.24 4.14 o 7 10 2 22.44 21.86 3.97 o 8 10 2 15.54 15.48 3.78 o 9 10 2 44.20 28.18 4.23 o 10 10 2 3.97 4.78 3.68 o 11 10 2 12.52 14.41 5.02 o 12 10 2 29.38 13.85 5.36 o -13 11 2 27.75 20.36 7.87 o -12 11 2 314.12 283.02 17.39 o -11 11 2 9.13 2.04 10.22 o -10 11 2 505.03 514.97 11.27 o -9 11 2 864.35 838.95 15.26 o -8 11 2 12.23 14.97 4.03 o -7 11 2 2951.08 2945.33 46.06 o -6 11 2 1489.58 1463.31 25.27 o -5 11 2 6.01 8.28 4.02 o -4 11 2 10632.87 10605.01 132.24 o -3 11 2 864.27 898.33 14.93 o -2 11 2 1288.20 1313.49 19.89 o -1 11 2 7806.64 7678.92 105.67 o 0 11 2 112.90 145.49 7.59 o 1 11 2 2673.94 2602.67 38.38 o 2 11 2 3848.05 4030.35 60.50 o 3 11 2 39.27 44.60 4.49 o 4 11 2 3671.17 3670.54 51.43 o 5 11 2 1449.47 1445.12 22.38 o 6 11 2 19.60 26.23 3.84 o 7 11 2 1711.88 1675.18 24.99 o 8 11 2 237.27 202.79 6.96 o 9 11 2 1.06 5.26 3.84 o 10 11 2 335.13 316.58 14.92 o 11 11 2 137.91 114.88 8.17 o -12 12 2 8.77 7.69 7.19 o -11 12 2 0.46 6.26 7.33 o -10 12 2 0.01 2.23 8.17 o -9 12 2 116.47 90.32 5.81 o -8 12 2 14.38 26.34 4.36 o -7 12 2 76.42 74.19 6.08 o -6 12 2 2.53 5.89 4.25 o -5 12 2 332.44 299.47 12.37 o -4 12 2 72.16 67.09 4.96 o -3 12 2 179.46 228.24 9.09 o -2 12 2 121.18 129.42 6.61 o -1 12 2 51.02 53.11 4.46 o 0 12 2 8.25 5.94 3.36 o 1 12 2 375.85 417.22 9.04 o 2 12 2 260.76 278.53 11.53 o 3 12 2 1.78 6.15 3.46 o 4 12 2 239.95 251.72 9.29 o 5 12 2 128.77 144.21 6.66 o 6 12 2 317.18 304.64 9.46 o 7 12 2 26.91 19.73 4.10 o 8 12 2 1.61 7.68 4.08 o 9 12 2 67.99 55.58 5.46 o 10 12 2 14.70 15.60 4.88 o 11 12 2 41.69 49.77 7.26 o -12 13 2 61.18 80.02 9.09 o -11 13 2 32.91 37.87 7.99 o -10 13 2 105.49 106.47 12.76 o -9 13 2 258.34 301.49 24.14 o -8 13 2 4.49 6.04 3.99 o -7 13 2 639.02 669.70 13.21 o -6 13 2 732.57 785.30 17.35 o -5 13 2 408.33 413.88 10.38 o -4 13 2 1461.84 1392.07 22.07 o -3 13 2 543.36 543.65 11.20 o -2 13 2 831.49 824.68 14.56 o -1 13 2 2832.71 2666.98 37.03 o 0 13 2 277.96 277.61 10.11 o 1 13 2 2346.61 2183.58 31.83 o 2 13 2 1822.55 1766.09 29.13 o 3 13 2 44.80 50.26 4.53 o 4 13 2 1551.93 1532.23 22.82 o 5 13 2 361.69 363.62 10.06 o 6 13 2 121.84 130.85 6.04 o 7 13 2 536.66 575.36 11.88 o 8 13 2 82.38 69.73 5.84 o 9 13 2 95.39 101.18 7.30 o 10 13 2 222.66 187.03 10.78 o -11 14 2 15.69 4.15 6.59 o -10 14 2 1.11 -0.16 6.83 o -9 14 2 400.50 357.65 20.11 o -8 14 2 5.12 1.43 7.01 o -7 14 2 3.65 4.80 4.07 o -6 14 2 571.06 569.47 14.13 o -5 14 2 24.56 30.59 5.18 o -4 14 2 93.10 103.77 5.87 o -3 14 2 229.66 253.64 11.63 o -2 14 2 108.45 133.77 6.69 o -1 14 2 148.72 143.29 6.43 o 0 14 2 45.69 63.62 4.92 o 1 14 2 191.54 235.77 8.13 o 2 14 2 129.41 136.00 7.88 o 3 14 2 8.34 10.02 3.78 o 4 14 2 229.46 291.36 10.86 o 5 14 2 215.50 213.43 10.52 o 6 14 2 0.63 4.43 3.79 o 7 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316.95 19.41 o 5 16 2 296.17 339.08 18.53 o 6 16 2 356.70 372.64 17.18 o 7 16 2 35.15 24.34 7.00 o -7 17 2 120.24 129.04 10.68 o -6 17 2 316.01 287.12 25.53 o -5 17 2 41.57 41.81 9.36 o -4 17 2 91.83 63.01 11.28 o -3 17 2 588.24 633.36 19.89 o -2 17 2 137.12 125.24 9.84 o -1 17 2 494.04 469.71 16.61 o 0 17 2 139.60 153.62 16.39 o 1 17 2 260.92 270.07 15.18 o 2 17 2 531.43 522.62 15.36 o 3 17 2 0.95 -4.44 5.17 o 4 17 2 244.67 214.40 19.17 o 5 17 2 385.24 361.54 21.76 o 6 17 2 51.00 46.62 6.63 o -5 18 2 17.45 23.68 8.20 o -4 18 2 99.34 95.57 12.80 o -3 18 2 196.86 206.32 15.62 o -2 18 2 0.05 -1.13 6.65 o -1 18 2 83.43 95.71 9.12 o 0 18 2 251.58 282.39 27.98 o 1 18 2 72.86 73.90 10.39 o 2 18 2 13.40 10.86 6.12 o 3 18 2 65.84 56.64 7.05 o 4 18 2 0.22 -2.65 5.70 o -2 19 2 14.52 11.80 9.10 o -1 19 2 69.92 78.89 9.89 o 0 19 2 30.05 21.15 7.17 o -16 1 3 34.09 23.55 12.82 o -15 1 3 42.65 44.75 8.39 o -14 1 3 164.93 196.96 13.50 o -13 1 3 820.44 787.01 14.33 o -12 1 3 329.41 342.85 9.14 o -11 1 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107.04 o -1 3 3 4907.08 4927.04 74.24 o 0 3 3 782.87 884.21 15.46 o 1 3 3 1808.84 1713.35 29.72 o 2 3 3 8400.43 8992.13 130.97 o 3 3 3 26.87 18.52 2.31 o 4 3 3 2293.55 2283.34 33.98 o 5 3 3 1318.90 1373.62 20.53 o 6 3 3 61.58 57.58 3.88 o 7 3 3 978.84 983.73 22.09 o 8 3 3 521.91 538.02 12.01 o 9 3 3 108.48 125.18 6.03 o 10 3 3 351.61 347.88 8.68 o 11 3 3 215.74 211.50 8.89 o 12 3 3 121.38 127.07 6.89 o 13 3 3 67.83 53.24 5.45 o -15 4 3 0.09 -3.77 9.00 o -14 4 3 1.53 -0.36 10.40 o -13 4 3 145.34 151.49 7.13 o -12 4 3 122.05 164.60 7.23 o -11 4 3 570.23 527.98 11.15 o -10 4 3 596.95 623.47 11.95 o -9 4 3 195.71 237.93 9.41 o -8 4 3 4114.30 4004.51 53.98 o -7 4 3 911.97 855.63 24.33 o -6 4 3 9.27 23.82 3.07 o -5 4 3 11035.19 10715.41 137.93 o -4 4 3 2711.38 2630.22 33.71 o -3 4 3 3569.96 3685.99 48.30 o -2 4 3 12635.47 12466.00 167.07 o -1 4 3 1717.49 1589.23 24.54 o 0 4 3 3594.79 3549.68 51.13 o 1 4 3 10251.90 10127.92 147.44 o 2 4 3 2593.75 2548.81 46.43 o 3 4 3 11546.80 11420.22 171.38 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76.27 o -6 8 3 1184.07 1199.59 18.79 o -5 8 3 6601.23 6416.73 96.21 o -4 8 3 6453.54 6349.41 108.36 o -3 8 3 2290.94 2321.95 41.81 o -2 8 3 19797.72 19157.30 279.11 o -1 8 3 2147.29 2153.17 31.35 o 0 8 3 6412.72 6326.05 86.68 o 1 8 3 21569.56 20959.48 296.26 o 2 8 3 1.82 11.92 3.22 o 3 8 3 8991.58 8955.89 136.23 o 4 8 3 9436.34 9393.75 138.78 o 5 8 3 62.45 68.23 6.14 o 6 8 3 8446.66 8221.94 112.77 o 7 8 3 2467.65 2454.78 36.54 o 8 8 3 833.03 857.28 15.37 o 9 8 3 2141.93 2082.83 34.01 o 10 8 3 126.76 111.09 6.65 o 11 8 3 295.94 309.15 11.87 o 12 8 3 388.07 351.72 19.93 o -14 9 3 69.28 71.24 9.52 o -13 9 3 171.10 129.31 12.35 o -12 9 3 204.61 244.49 24.35 o -11 9 3 637.86 650.09 13.18 o -10 9 3 269.47 235.79 12.54 o -9 9 3 1293.26 1320.05 20.34 o -8 9 3 1989.16 1983.39 30.08 o -7 9 3 51.26 69.83 4.80 o -6 9 3 3727.43 3808.96 53.84 o -5 9 3 1018.37 965.87 16.71 o -4 9 3 1835.65 1762.33 26.23 o -3 9 3 3737.16 3641.58 68.52 o -2 9 3 687.35 684.12 12.63 o -1 9 3 6557.65 6113.20 86.16 o 0 9 3 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