#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2100009.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2100009_Fobs loop_ _publ_author_name 'Peresypkina, Eugenia V.' 'Bushuev, Mark B.' 'Virovets, Alexander V.' 'Krivopalov, Victor P.' 'Lavrenova, Ludmila G.' 'Larionov, Stanislav V.' _publ_section_title ; Three differently coloured concomitant polymorphs: synthesis, structure and packing analysis of (4-(3',5'-dimethyl-1H-pyrazol-1'-yl)-6-methyl-2-phenylpyrimidine)dichlorocopper(II) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 164 _journal_page_last 173 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6899 _cell_length_b 14.9843 _cell_length_c 19.2115 _exptl_crystal_F_000 1624.00 _reflns_d_resolution_high 0.6640 _[local]_cod_data_source_file av50232egsup4.hkl _[local]_cod_data_source_block 2eg #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2EG in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 463.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 42162.36 43322.89 843.53 o 4 0 0 91071.70 92757.38 1798.29 o 6 0 0 118891.80 130324.47 3095.04 o 8 0 0 4966.65 4325.18 108.95 o 10 0 0 4048.14 4256.71 156.63 o 12 0 0 4929.80 4665.04 175.16 o 14 0 0 15.24 51.62 43.02 o 16 0 0 1098.69 1243.30 83.83 o 2 1 0 1556.48 1580.74 25.14 o 4 1 0 20516.19 22438.24 308.92 o 6 1 0 1972.88 2028.91 43.97 o 8 1 0 1722.60 1832.17 46.41 o 10 1 0 10341.20 10293.60 206.20 o 12 1 0 366.92 343.58 27.53 o 14 1 0 240.34 196.63 31.17 o 16 1 0 306.16 341.02 64.64 o 0 2 0 18738.48 19333.26 463.36 o 2 2 0 26353.42 27972.77 543.21 o 4 2 0 19280.62 19684.73 297.03 o 6 2 0 9108.25 9432.23 186.59 o 8 2 0 5168.61 5201.51 106.00 o 10 2 0 250.30 304.33 17.56 o 12 2 0 140.97 96.97 18.75 o 14 2 0 29.72 15.66 26.72 o 16 2 0 32.48 -9.65 37.27 o 2 3 0 1883.86 2005.76 36.62 o 4 3 0 2444.44 2390.49 49.29 o 6 3 0 35.55 24.11 9.12 o 8 3 0 4200.34 4320.67 103.94 o 10 3 0 27.31 16.61 14.04 o 12 3 0 1953.41 1782.86 47.31 o 14 3 0 93.79 113.46 30.34 o 16 3 0 51.28 24.23 39.47 o 0 4 0 74444.04 74383.50 1766.41 o 2 4 0 25882.44 25823.93 434.25 o 4 4 0 45.27 17.27 5.33 o 6 4 0 28260.64 28882.22 689.39 o 8 4 0 2168.93 2239.01 50.03 o 10 4 0 8122.94 8359.52 168.79 o 12 4 0 3947.14 4281.67 93.43 o 14 4 0 317.93 275.83 26.49 o 16 4 0 1238.27 1222.99 57.90 o 2 5 0 10964.42 9902.97 167.85 o 4 5 0 1.80 -6.22 6.22 o 6 5 0 19028.04 19183.49 459.46 o 8 5 0 1914.26 1814.02 64.75 o 10 5 0 575.42 487.17 21.25 o 12 5 0 1718.45 1737.59 47.14 o 14 5 0 5.11 33.64 24.08 o 16 5 0 338.21 524.02 77.43 o 0 6 0 28737.10 27147.07 646.73 o 2 6 0 34650.63 38277.92 743.63 o 4 6 0 11423.33 11523.33 277.19 o 6 6 0 12062.63 11017.14 393.00 o 8 6 0 7691.05 8118.20 198.80 o 10 6 0 7068.06 7098.91 145.43 o 12 6 0 2742.00 2995.70 88.04 o 14 6 0 2969.47 3202.18 112.12 o 16 6 0 2640.24 2986.93 136.11 o 2 7 0 4182.88 4720.76 115.20 o 4 7 0 2095.25 2760.77 69.79 o 6 7 0 4052.97 3872.58 97.48 o 8 7 0 996.16 1073.49 43.35 o 10 7 0 1160.37 1090.02 39.70 o 12 7 0 0.52 3.02 19.23 o 14 7 0 198.50 206.77 28.27 o 16 7 0 0.52 -29.12 52.94 o 0 8 0 632.00 757.98 32.43 o 2 8 0 639.60 954.51 43.90 o 4 8 0 11.83 4.72 8.73 o 6 8 0 241.46 230.53 14.60 o 8 8 0 3931.57 4195.68 107.37 o 10 8 0 134.80 133.88 23.82 o 12 8 0 245.92 248.86 24.45 o 14 8 0 578.79 550.55 35.09 o 16 8 0 19.39 -23.60 53.61 o 2 9 0 595.18 617.28 33.97 o 4 9 0 6279.91 6824.86 283.36 o 6 9 0 55.37 69.94 12.72 o 8 9 0 634.33 662.95 28.62 o 10 9 0 87.85 103.03 24.49 o 12 9 0 129.74 142.18 24.83 o 14 9 0 14.43 2.32 28.23 o 0 10 0 10579.58 8937.41 305.75 o 2 10 0 5318.21 5303.65 130.48 o 4 10 0 6527.63 6142.89 150.83 o 6 10 0 7881.64 8257.52 202.23 o 8 10 0 501.55 463.18 40.15 o 10 10 0 2025.54 2253.41 66.86 o 12 10 0 221.00 157.41 26.54 o 14 10 0 184.25 157.09 31.87 o 2 11 0 509.75 472.21 19.02 o 4 11 0 68.19 82.18 12.94 o 6 11 0 376.95 311.24 25.81 o 8 11 0 117.21 97.43 19.13 o 10 11 0 513.73 449.81 31.88 o 12 11 0 424.64 383.11 34.30 o 14 11 0 10.46 24.20 44.96 o 0 12 0 13074.00 12135.23 414.29 o 2 12 0 16278.55 16910.00 406.27 o 4 12 0 10213.35 9673.44 235.77 o 6 12 0 1557.89 1489.61 94.86 o 8 12 0 7431.81 7761.13 193.16 o 10 12 0 492.61 451.92 31.10 o 12 12 0 83.71 97.55 29.77 o 2 13 0 634.99 707.11 60.11 o 4 13 0 411.82 326.55 30.00 o 6 13 0 618.00 638.26 28.48 o 8 13 0 690.94 655.58 30.46 o 10 13 0 81.98 48.96 25.49 o 12 13 0 59.65 15.86 30.90 o 0 14 0 215.11 169.64 24.49 o 2 14 0 1635.51 1918.57 54.36 o 4 14 0 19.80 7.57 16.54 o 6 14 0 15.45 7.85 18.72 o 8 14 0 123.04 173.16 34.63 o 10 14 0 248.59 255.84 29.94 o 12 14 0 69.47 77.65 54.71 o 2 15 0 71.23 56.74 17.62 o 4 15 0 10.45 9.74 22.17 o 6 15 0 21.87 -21.73 21.73 o 8 15 0 904.12 920.98 41.55 o 10 15 0 39.90 73.46 48.09 o 0 16 0 59.07 34.19 26.25 o 2 16 0 1580.55 1610.85 50.19 o 4 16 0 606.39 554.59 42.13 o 6 16 0 7.56 -6.27 22.48 o 10 16 0 857.25 791.29 67.94 o 2 17 0 0.13 -2.54 33.64 o 4 17 0 476.47 443.22 28.51 o 6 17 0 166.73 94.30 49.75 o 8 17 0 80.51 98.83 52.06 o 0 18 0 3.45 6.84 32.21 o 2 18 0 496.95 534.03 37.28 o 4 18 0 4.16 0.48 25.75 o 6 18 0 499.31 414.51 53.83 o 8 18 0 462.78 497.01 58.90 o 2 19 0 24.61 33.70 29.89 o 4 19 0 21.79 16.11 28.93 o 6 19 0 152.95 186.19 52.94 o 0 20 0 11.74 -12.35 43.90 o 2 20 0 409.83 362.17 34.63 o 4 20 0 157.32 147.80 51.62 o 6 20 0 18.55 63.75 56.03 o 2 21 0 63.27 93.96 35.01 o 4 21 0 2.28 75.00 55.15 o 0 22 0 166.05 255.90 58.46 o 2 22 0 420.54 508.70 67.50 o 1 1 1 19180.57 18749.91 304.87 o 2 1 1 6326.36 6259.28 67.11 o 3 1 1 164.93 180.46 3.14 o 4 1 1 327.40 293.49 5.61 o 5 1 1 1635.88 1909.86 24.82 o 6 1 1 3044.23 3604.93 57.40 o 7 1 1 1903.59 1891.47 27.44 o 8 1 1 68.10 77.69 7.46 o 9 1 1 755.73 717.28 16.63 o 10 1 1 63.40 37.50 13.78 o 11 1 1 217.68 190.58 13.72 o 12 1 1 150.29 114.59 16.98 o 13 1 1 171.18 193.11 24.45 o 14 1 1 61.05 45.33 20.75 o 15 1 1 141.91 127.05 24.70 o 16 1 1 21.47 -18.60 27.14 o 17 1 1 172.64 146.04 69.49 o 0 2 1 7632.18 7822.59 158.99 o 1 2 1 81846.42 81409.77 1035.39 o 2 2 1 1396.28 1601.81 19.99 o 3 2 1 1181.65 949.01 12.34 o 4 2 1 1253.77 1054.09 12.88 o 5 2 1 64158.90 65580.98 899.77 o 6 2 1 3169.09 3180.70 50.96 o 7 2 1 9120.32 9012.46 126.49 o 8 2 1 46.51 45.56 7.34 o 9 2 1 4786.18 4989.20 72.79 o 10 2 1 1220.06 1144.56 23.11 o 11 2 1 5196.39 5774.58 84.86 o 12 2 1 1111.63 1036.04 29.15 o 13 2 1 1282.15 1277.42 43.95 o 14 2 1 57.32 53.90 20.50 o 15 2 1 1427.26 1554.21 44.80 o 16 2 1 74.42 53.22 28.48 o 17 2 1 835.53 855.05 77.87 o 1 3 1 969.26 906.78 11.71 o 2 3 1 13045.00 13784.94 176.03 o 3 3 1 232.47 215.47 4.68 o 4 3 1 728.29 713.60 11.45 o 5 3 1 736.11 899.60 17.65 o 6 3 1 854.61 923.87 20.03 o 7 3 1 3788.74 3962.33 68.64 o 8 3 1 193.04 202.16 8.98 o 9 3 1 1676.76 1570.71 29.66 o 10 3 1 143.56 129.65 11.06 o 11 3 1 60.54 52.00 11.17 o 12 3 1 54.84 39.17 12.56 o 13 3 1 263.94 260.82 18.36 o 14 3 1 0.06 -15.63 17.62 o 15 3 1 261.96 340.54 27.67 o 16 3 1 70.96 72.81 28.72 o 17 3 1 11.27 -59.12 65.52 o 0 4 1 89233.47 92194.94 1787.51 o 1 4 1 90845.37 89758.95 1139.54 o 2 4 1 10349.77 10819.88 129.31 o 3 4 1 14939.29 14572.84 174.03 o 4 4 1 161.53 117.20 6.99 o 5 4 1 18760.98 18543.33 280.12 o 6 4 1 81.28 57.61 9.12 o 7 4 1 18947.77 19447.08 329.77 o 8 4 1 478.60 468.41 13.05 o 9 4 1 5363.68 5322.86 84.76 o 10 4 1 2234.26 2099.95 38.67 o 11 4 1 2653.57 2700.41 51.55 o 12 4 1 69.33 89.77 14.19 o 13 4 1 721.09 808.32 22.64 o 14 4 1 254.27 252.27 20.63 o 15 4 1 945.02 996.38 38.13 o 16 4 1 61.86 66.06 29.24 o 17 4 1 227.65 252.37 68.83 o 1 5 1 3353.57 3578.85 46.68 o 2 5 1 518.09 409.04 7.71 o 3 5 1 58.88 85.68 6.47 o 4 5 1 508.04 748.24 14.36 o 5 5 1 591.85 674.66 15.57 o 6 5 1 136.82 135.78 8.34 o 7 5 1 187.63 179.95 10.13 o 8 5 1 52.06 75.59 14.43 o 9 5 1 8.63 10.73 9.11 o 10 5 1 983.44 944.44 37.49 o 11 5 1 275.27 254.36 13.94 o 12 5 1 77.94 52.04 13.69 o 13 5 1 42.96 27.86 15.06 o 14 5 1 21.71 30.77 17.55 o 15 5 1 0.53 2.57 22.57 o 16 5 1 0.12 32.29 28.64 o 17 5 1 511.15 529.66 68.83 o 0 6 1 1248.68 1551.11 51.75 o 1 6 1 923.57 535.26 17.23 o 2 6 1 501.98 336.68 8.17 o 3 6 1 1421.60 1502.96 25.01 o 4 6 1 756.06 822.12 30.38 o 5 6 1 6512.07 6210.94 107.18 o 6 6 1 558.19 467.63 18.66 o 7 6 1 74.22 100.63 8.58 o 8 6 1 174.91 172.49 11.13 o 9 6 1 6.18 15.34 11.56 o 10 6 1 3.38 19.60 11.80 o 11 6 1 844.09 911.11 22.11 o 12 6 1 4.57 6.60 13.75 o 13 6 1 10.81 16.23 15.30 o 14 6 1 82.35 123.34 19.35 o 15 6 1 116.40 140.54 24.17 o 16 6 1 3.18 73.57 33.31 o 1 7 1 904.14 884.16 17.67 o 2 7 1 27.00 29.33 4.86 o 3 7 1 1085.11 858.56 17.91 o 4 7 1 4615.47 4930.34 99.30 o 5 7 1 201.84 117.47 7.61 o 6 7 1 23.79 8.63 11.02 o 7 7 1 103.11 113.98 9.65 o 8 7 1 281.15 282.65 12.77 o 9 7 1 226.95 229.82 15.28 o 10 7 1 1.82 -8.12 11.41 o 11 7 1 22.92 33.08 12.52 o 12 7 1 60.27 59.43 14.24 o 13 7 1 233.60 234.14 17.79 o 14 7 1 0.53 8.32 18.71 o 15 7 1 64.14 105.39 22.57 o 16 7 1 6.62 -38.97 38.97 o 0 8 1 728.51 1063.01 30.25 o 1 8 1 39501.83 40166.65 675.95 o 2 8 1 5557.61 4746.86 82.20 o 3 8 1 12978.06 13085.27 222.14 o 4 8 1 1040.41 1192.57 24.18 o 5 8 1 11628.72 10953.32 186.85 o 6 8 1 426.40 391.97 23.52 o 7 8 1 9592.41 10040.89 172.92 o 8 8 1 29.36 52.56 10.03 o 9 8 1 5404.23 5540.18 99.09 o 10 8 1 210.06 199.62 15.36 o 11 8 1 2847.19 2804.28 57.87 o 12 8 1 162.18 109.83 15.38 o 13 8 1 478.34 493.02 21.44 o 14 8 1 37.19 17.21 19.58 o 15 8 1 1231.07 1218.67 33.01 o 16 8 1 74.33 -17.43 55.37 o 1 9 1 88.99 99.62 13.37 o 2 9 1 20.22 2.73 6.43 o 3 9 1 2.06 1.91 6.34 o 4 9 1 746.22 626.46 25.52 o 5 9 1 74.62 35.98 11.40 o 6 9 1 328.08 288.25 11.90 o 7 9 1 111.10 143.24 11.15 o 8 9 1 3.23 -10.82 10.82 o 9 9 1 69.96 100.19 13.34 o 10 9 1 248.12 204.44 20.43 o 11 9 1 18.07 17.97 14.60 o 12 9 1 19.09 10.07 15.01 o 13 9 1 2.19 -12.13 17.46 o 14 9 1 19.65 -6.28 20.11 o 15 9 1 3.93 -24.56 38.47 o 0 10 1 43.12 31.29 22.61 o 1 10 1 4387.10 4856.29 84.71 o 2 10 1 19.52 75.65 8.85 o 3 10 1 8726.17 9050.91 155.19 o 4 10 1 1033.21 1012.60 22.54 o 5 10 1 844.26 803.46 20.15 o 6 10 1 132.33 164.82 15.64 o 7 10 1 2041.60 1962.51 39.33 o 8 10 1 280.62 218.40 14.42 o 9 10 1 2493.14 2440.07 59.61 o 10 10 1 97.59 128.77 15.45 o 11 10 1 14.04 -2.00 16.15 o 12 10 1 20.11 -0.14 17.02 o 13 10 1 260.41 221.70 20.03 o 14 10 1 18.33 29.28 24.46 o 15 10 1 145.36 108.98 56.47 o 1 11 1 534.30 541.84 15.28 o 2 11 1 2.46 2.38 8.00 o 3 11 1 13.41 3.34 8.03 o 4 11 1 227.54 261.30 15.57 o 5 11 1 4.46 -10.76 10.76 o 6 11 1 931.79 839.14 24.77 o 7 11 1 52.78 34.96 11.46 o 8 11 1 15.11 18.39 12.55 o 9 11 1 39.26 16.50 14.32 o 10 11 1 7.42 0.50 14.51 o 11 11 1 11.79 -1.24 16.80 o 12 11 1 8.16 4.78 17.92 o 13 11 1 4.60 -8.37 19.08 o 14 11 1 6.56 29.39 27.10 o 0 12 1 962.56 1024.09 62.76 o 1 12 1 663.49 685.50 21.21 o 2 12 1 272.71 297.63 21.08 o 3 12 1 715.21 735.41 29.59 o 4 12 1 154.77 197.79 11.94 o 5 12 1 1124.71 1171.28 27.19 o 6 12 1 744.94 685.95 19.87 o 7 12 1 307.09 297.06 15.56 o 8 12 1 146.54 197.69 15.68 o 9 12 1 2029.40 2075.16 44.40 o 10 12 1 9.22 16.95 16.71 o 11 12 1 741.66 788.60 27.25 o 12 12 1 77.01 91.95 20.90 o 13 12 1 7.24 -14.63 24.72 o 1 13 1 88.30 90.80 11.14 o 2 13 1 19.03 20.90 10.09 o 3 13 1 105.39 67.61 13.63 o 4 13 1 17.30 7.64 10.14 o 5 13 1 26.14 0.14 11.32 o 6 13 1 18.65 -6.22 11.44 o 7 13 1 0.30 -0.31 12.96 o 8 13 1 107.56 128.99 15.52 o 9 13 1 11.53 45.08 21.27 o 10 13 1 61.86 46.08 22.35 o 11 13 1 1.36 -5.88 18.79 o 12 13 1 0.04 2.45 26.45 o 13 13 1 3.29 -63.97 63.97 o 0 14 1 513.92 472.81 22.53 o 1 14 1 1530.51 1597.26 33.14 o 2 14 1 482.81 385.99 32.11 o 3 14 1 4187.35 4287.75 89.70 o 4 14 1 616.26 575.23 18.49 o 5 14 1 1027.01 993.29 26.94 o 6 14 1 21.13 -12.33 13.14 o 7 14 1 1269.89 1287.41 45.21 o 8 14 1 257.21 259.51 18.28 o 9 14 1 2154.97 2408.92 50.77 o 10 14 1 25.61 37.26 18.56 o 11 14 1 327.78 339.46 29.84 o 12 14 1 51.08 16.05 40.14 o 1 15 1 0.55 4.93 11.36 o 2 15 1 29.25 35.30 12.58 o 3 15 1 51.13 53.71 12.47 o 4 15 1 0.93 14.21 12.83 o 5 15 1 79.93 85.45 14.28 o 6 15 1 0.04 -14.68 14.68 o 7 15 1 190.41 160.11 17.73 o 8 15 1 21.00 18.38 17.30 o 9 15 1 1.60 3.70 20.17 o 10 15 1 18.19 33.47 26.70 o 11 15 1 15.28 -38.04 38.41 o 0 16 1 150.36 116.68 22.94 o 1 16 1 231.70 192.69 14.77 o 2 16 1 9.55 22.04 13.77 o 3 16 1 76.46 103.76 14.65 o 4 16 1 5.26 8.48 14.31 o 5 16 1 79.27 55.71 15.51 o 6 16 1 143.73 117.42 17.64 o 7 16 1 1018.49 1033.54 35.19 o 8 16 1 38.16 75.44 19.26 o 9 16 1 2.23 21.78 25.02 o 10 16 1 68.77 112.95 41.10 o 1 17 1 6.44 -5.60 14.81 o 2 17 1 3.03 -4.46 14.53 o 3 17 1 4.52 -0.76 15.41 o 4 17 1 38.92 60.24 16.83 o 5 17 1 162.86 111.45 18.10 o 6 17 1 3.29 1.65 16.97 o 7 17 1 10.41 16.41 34.39 o 8 17 1 35.67 46.81 25.84 o 9 17 1 13.75 20.13 39.70 o 0 18 1 11.60 9.30 23.74 o 1 18 1 113.00 121.49 17.36 o 2 18 1 52.34 46.58 16.77 o 3 18 1 486.18 488.06 21.20 o 4 18 1 27.86 38.16 18.25 o 5 18 1 183.48 190.54 20.48 o 6 18 1 13.12 18.34 24.73 o 7 18 1 154.57 173.49 27.21 o 8 18 1 39.35 75.45 46.00 o 9 18 1 106.77 89.12 56.69 o 1 19 1 12.87 29.65 18.23 o 2 19 1 9.17 16.33 19.36 o 3 19 1 95.43 80.24 19.98 o 4 19 1 31.23 44.19 20.04 o 5 19 1 0.06 -3.11 25.77 o 6 19 1 2.09 2.16 31.94 o 7 19 1 0.25 25.16 37.07 o 0 20 1 206.73 176.48 30.41 o 1 20 1 496.59 474.72 26.39 o 2 20 1 45.91 49.75 21.30 o 3 20 1 324.81 386.14 36.02 o 4 20 1 11.88 4.03 25.79 o 5 20 1 151.45 91.98 35.48 o 6 20 1 31.43 29.89 40.24 o 1 21 1 3.27 33.31 28.08 o 2 21 1 5.10 17.55 27.64 o 3 21 1 29.32 54.92 29.36 o 4 21 1 7.92 16.20 38.91 o 0 22 1 8.62 36.40 55.59 o 1 22 1 28.38 44.95 36.52 o 2 22 1 0.06 38.83 60.00 o 0 0 2 111304.96 101353.38 3431.88 o 1 0 2 16218.21 17316.63 292.46 o 2 0 2 12102.44 11842.11 178.80 o 3 0 2 20436.16 20358.25 306.74 o 4 0 2 3105.72 2735.56 39.37 o 5 0 2 31247.86 31488.04 474.55 o 6 0 2 55497.98 57925.44 1125.17 o 7 0 2 373.49 222.08 11.22 o 8 0 2 4952.22 5264.69 107.11 o 9 0 2 568.92 526.34 27.87 o 10 0 2 10658.63 10414.68 208.37 o 11 0 2 3888.60 3665.25 144.23 o 12 0 2 3224.76 3367.49 93.67 o 13 0 2 156.89 154.61 26.98 o 14 0 2 533.58 523.34 37.58 o 15 0 2 13.85 1.61 32.69 o 16 0 2 986.91 951.42 53.69 o 17 0 2 478.85 633.34 79.20 o 1 1 2 906.17 901.24 10.81 o 2 1 2 5923.77 6190.66 69.99 o 3 1 2 2966.11 2838.75 31.13 o 4 1 2 1620.07 1710.46 18.73 o 5 1 2 5803.20 5895.80 71.68 o 6 1 2 824.31 757.42 19.91 o 7 1 2 2495.49 2619.36 36.44 o 8 1 2 185.73 151.30 10.77 o 9 1 2 625.90 558.65 15.23 o 10 1 2 655.13 581.07 17.05 o 11 1 2 14.91 8.59 12.14 o 12 1 2 510.85 475.36 27.14 o 13 1 2 0.40 -9.06 17.88 o 14 1 2 8.01 -5.21 19.41 o 15 1 2 7.63 -18.79 24.10 o 16 1 2 190.12 267.41 29.50 o 17 1 2 597.85 686.51 74.12 o 0 2 2 27895.89 27527.13 465.49 o 1 2 2 780.54 853.80 11.69 o 2 2 2 8066.16 8060.60 91.02 o 3 2 2 13622.95 13809.12 155.47 o 4 2 2 3534.03 3584.38 39.38 o 5 2 2 2176.82 1903.15 26.53 o 6 2 2 3539.93 3286.55 52.48 o 7 2 2 1227.16 1198.75 20.81 o 8 2 2 315.12 308.42 12.09 o 9 2 2 216.16 169.80 13.09 o 10 2 2 1657.16 1648.75 29.27 o 11 2 2 144.51 106.47 12.93 o 12 2 2 655.70 648.27 23.50 o 13 2 2 55.23 36.55 15.58 o 14 2 2 504.04 544.10 30.76 o 15 2 2 11.20 15.85 23.76 o 16 2 2 326.23 332.32 31.13 o 17 2 2 38.81 61.99 67.06 o 1 3 2 1624.96 1648.19 20.50 o 2 3 2 6613.36 6763.48 81.33 o 3 3 2 4039.07 3842.37 44.14 o 4 3 2 4781.75 4953.34 64.30 o 5 3 2 2792.49 2898.32 45.97 o 6 3 2 223.02 269.31 7.82 o 7 3 2 6877.92 6732.85 116.70 o 8 3 2 193.74 147.11 9.21 o 9 3 2 87.14 100.14 13.30 o 10 3 2 1376.62 1358.14 25.99 o 11 3 2 1455.99 1355.56 27.25 o 12 3 2 150.52 151.96 21.85 o 13 3 2 189.58 220.32 18.45 o 14 3 2 64.03 71.75 18.35 o 15 3 2 104.64 133.07 25.12 o 16 3 2 176.81 199.75 30.56 o 17 3 2 30.95 -31.77 58.90 o 0 4 2 215060.28 217643.06 3653.28 o 1 4 2 3281.11 3556.67 46.13 o 2 4 2 12043.67 11989.45 143.22 o 3 4 2 8138.48 8350.97 100.26 o 4 4 2 7613.76 7341.59 102.01 o 5 4 2 4521.13 4392.45 68.29 o 6 4 2 24186.86 24620.12 371.87 o 7 4 2 458.15 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27096.10 28229.68 476.57 o 1 2 3 1258.32 1213.98 17.64 o 2 2 3 3254.51 2826.88 34.43 o 3 2 3 3014.87 2942.13 32.30 o 4 2 3 12923.51 12087.98 144.62 o 5 2 3 14318.53 14344.28 183.68 o 6 2 3 17470.70 17243.37 220.81 o 7 2 3 2749.90 2561.02 42.42 o 8 2 3 1647.72 1493.71 25.39 o 9 2 3 1842.00 1897.13 31.58 o 10 2 3 4379.16 4482.19 73.27 o 11 2 3 2581.55 2651.74 47.56 o 12 2 3 4851.62 4864.54 80.85 o 13 2 3 682.47 677.83 22.83 o 14 2 3 184.88 225.44 20.18 o 15 2 3 876.76 947.24 35.35 o 16 2 3 557.01 521.86 32.34 o 17 2 3 79.28 75.00 61.11 o 1 3 3 132.67 182.58 4.04 o 2 3 3 482.20 473.31 11.08 o 3 3 3 750.47 762.62 10.15 o 4 3 3 787.74 768.55 12.86 o 5 3 3 137.53 146.33 6.12 o 6 3 3 105.51 181.14 8.86 o 7 3 3 340.48 413.05 11.64 o 8 3 3 6.39 7.16 7.59 o 9 3 3 210.94 177.65 11.88 o 10 3 3 219.69 176.29 11.27 o 11 3 3 28.08 34.98 11.55 o 12 3 3 612.92 612.24 20.77 o 13 3 3 38.39 51.20 15.88 o 14 3 3 132.20 139.75 19.57 o 15 3 3 2.70 1.49 24.54 o 16 3 3 149.49 141.64 31.20 o 17 3 3 109.62 45.66 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3 5005.82 5139.05 71.84 o 2 6 3 7.62 5.30 5.07 o 3 6 3 503.27 672.85 13.08 o 4 6 3 85.17 45.26 4.96 o 5 6 3 3836.09 4213.22 65.73 o 6 6 3 3408.14 3460.72 55.20 o 7 6 3 149.99 119.48 9.02 o 8 6 3 459.39 469.28 13.57 o 9 6 3 35.64 12.27 9.80 o 10 6 3 160.21 173.89 16.42 o 11 6 3 98.30 134.34 13.03 o 12 6 3 260.14 247.50 15.75 o 13 6 3 79.54 84.19 16.35 o 14 6 3 123.64 154.36 19.23 o 15 6 3 31.87 46.58 22.02 o 16 6 3 105.18 69.43 39.61 o 1 7 3 1733.12 1967.37 31.76 o 2 7 3 434.74 403.03 11.93 o 3 7 3 602.34 733.31 14.36 o 4 7 3 6.18 12.94 7.36 o 5 7 3 1.06 2.82 6.73 o 6 7 3 1229.41 1301.67 44.39 o 7 7 3 0.65 6.56 8.11 o 8 7 3 21.63 23.06 11.78 o 9 7 3 80.68 74.14 11.30 o 10 7 3 114.70 98.35 12.63 o 11 7 3 0.13 -13.09 13.09 o 12 7 3 651.47 662.21 20.54 o 13 7 3 9.39 11.79 16.50 o 14 7 3 16.12 13.72 18.54 o 15 7 3 46.42 11.31 27.33 o 16 7 3 58.63 37.28 56.47 o 0 8 3 349.15 235.58 19.85 o 1 8 3 10766.07 10660.40 209.09 o 2 8 3 8020.83 8048.02 137.60 o 3 8 3 6811.92 6819.86 116.97 o 4 8 3 10163.53 10033.27 171.24 o 5 8 3 6600.03 6581.75 113.82 o 6 8 3 3228.42 3326.95 60.34 o 7 8 3 3449.82 3419.21 62.29 o 8 8 3 1107.02 1063.77 25.78 o 9 8 3 5156.99 5500.14 98.31 o 10 8 3 2330.02 2513.73 45.62 o 11 8 3 1316.85 1333.03 61.86 o 12 8 3 992.18 1024.82 25.62 o 13 8 3 287.51 328.49 19.89 o 14 8 3 330.64 306.71 24.31 o 15 8 3 264.92 298.35 28.47 o 1 9 3 1001.03 853.28 18.53 o 2 9 3 213.35 222.28 12.60 o 3 9 3 8.30 5.01 6.61 o 4 9 3 220.81 304.24 10.72 o 5 9 3 323.83 411.37 12.98 o 6 9 3 444.40 369.87 23.47 o 7 9 3 70.23 88.35 10.18 o 8 9 3 77.42 52.09 10.84 o 9 9 3 5.37 29.81 12.43 o 10 9 3 332.59 340.19 16.23 o 11 9 3 73.61 65.17 15.20 o 12 9 3 48.76 67.65 16.96 o 13 9 3 0.11 2.81 17.81 o 14 9 3 86.75 67.29 23.62 o 15 9 3 9.32 6.12 38.53 o 0 10 3 77.62 68.83 17.32 o 1 10 3 193.91 192.00 21.37 o 2 10 3 2677.17 2128.45 49.90 o 3 10 3 4141.16 4666.47 81.92 o 4 10 3 2623.28 2582.11 47.87 o 5 10 3 60.11 29.75 8.54 o 6 10 3 87.30 83.19 11.81 o 7 10 3 713.14 733.12 29.29 o 8 10 3 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0 14 10333.25 11386.43 274.99 o 6 0 14 136.19 116.33 38.61 o 7 0 14 5762.96 5746.66 142.99 o 8 0 14 456.49 450.35 18.45 o 9 0 14 1712.49 1739.52 43.10 o 10 0 14 532.67 492.16 46.55 o 11 0 14 2652.21 2813.10 120.45 o 12 0 14 745.04 837.62 61.11 o 13 0 14 33.32 11.91 45.66 o 14 0 14 172.61 142.73 55.15 o 1 1 14 470.52 456.58 10.49 o 2 1 14 1420.41 1346.74 21.72 o 3 1 14 801.40 734.88 14.20 o 4 1 14 1714.77 1643.70 39.60 o 5 1 14 366.30 395.33 13.10 o 6 1 14 219.66 228.35 14.21 o 7 1 14 146.40 114.66 10.15 o 8 1 14 996.00 848.73 24.02 o 9 1 14 368.38 353.39 16.99 o 10 1 14 881.58 811.69 25.29 o 11 1 14 32.71 20.71 26.36 o 12 1 14 23.13 16.78 40.48 o 13 1 14 178.78 136.00 37.75 o 14 1 14 3.44 16.07 39.46 o 0 2 14 990.30 891.58 44.01 o 1 2 14 4003.91 3926.85 56.17 o 2 2 14 209.28 283.72 9.96 o 3 2 14 3033.88 2818.02 51.03 o 4 2 14 357.91 293.65 15.68 o 5 2 14 1707.85 1683.57 33.44 o 6 2 14 9.50 16.90 8.92 o 7 2 14 211.77 216.77 12.70 o 8 2 14 11.25 1.67 14.08 o 9 2 14 282.94 287.60 27.31 o 10 2 14 110.33 73.35 16.34 o 11 2 14 36.79 48.26 21.60 o 12 2 14 801.21 811.36 42.88 o 13 2 14 35.91 13.53 36.80 o 14 2 14 76.52 54.86 42.23 o 1 3 14 2594.83 2894.13 51.79 o 2 3 14 587.31 578.99 32.83 o 3 3 14 216.75 186.65 8.18 o 4 3 14 79.77 93.55 7.32 o 5 3 14 10.90 22.36 7.65 o 6 3 14 464.94 482.00 22.19 o 7 3 14 776.57 807.11 42.52 o 8 3 14 1593.27 1485.40 39.17 o 9 3 14 20.60 0.61 16.32 o 10 3 14 67.79 45.32 19.97 o 11 3 14 1.25 11.15 18.62 o 12 3 14 65.19 27.84 29.54 o 13 3 14 89.12 106.61 34.52 o 14 3 14 12.14 -55.15 55.15 o 0 4 14 6699.16 7119.18 172.89 o 1 4 14 4131.73 4098.94 64.22 o 2 4 14 5470.39 5286.71 107.02 o 3 4 14 16.44 1.14 9.38 o 4 4 14 2361.24 2344.42 51.79 o 5 4 14 3146.59 3372.80 71.91 o 6 4 14 914.45 962.20 44.52 o 7 4 14 1210.17 1209.93 34.11 o 8 4 14 97.98 97.56 16.03 o 9 4 14 752.56 846.27 30.36 o 10 4 14 11.80 19.38 19.14 o 11 4 14 2138.21 2278.62 70.19 o 12 4 14 41.55 86.01 27.42 o 13 4 14 157.03 145.70 39.30 o 14 4 14 12.03 -6.40 57.80 o 1 5 14 15.16 -1.65 5.97 o 2 5 14 369.97 346.90 14.20 o 3 5 14 97.40 110.58 11.46 o 4 5 14 0.23 0.20 15.65 o 5 5 14 414.11 533.50 19.79 o 6 5 14 2349.82 2295.22 52.92 o 7 5 14 765.16 890.06 29.39 o 8 5 14 115.85 103.51 16.70 o 9 5 14 65.61 82.34 31.00 o 10 5 14 0.32 -19.72 19.72 o 11 5 14 316.52 341.54 26.43 o 12 5 14 121.22 114.08 22.71 o 13 5 14 237.16 265.47 33.01 o 0 6 14 4451.06 4545.58 91.64 o 1 6 14 1269.47 1252.27 30.86 o 2 6 14 1516.29 1387.35 33.65 o 3 6 14 1479.49 1423.81 35.14 o 4 6 14 5902.91 6180.14 125.88 o 5 6 14 3626.42 3791.00 94.00 o 6 6 14 1038.61 1121.35 44.67 o 7 6 14 1040.42 1092.92 33.32 o 8 6 14 48.73 49.90 17.28 o 9 6 14 2715.26 2920.77 90.79 o 10 6 14 11.41 -13.01 20.84 o 11 6 14 1012.66 1027.46 38.40 o 12 6 14 123.26 106.83 26.99 o 13 6 14 819.74 883.82 43.65 o 1 7 14 203.91 213.41 12.43 o 2 7 14 1287.01 1315.84 40.96 o 3 7 14 71.68 40.19 11.41 o 4 7 14 1149.97 1169.25 63.82 o 5 7 14 792.63 755.40 33.26 o 6 7 14 533.05 607.09 23.36 o 7 7 14 156.37 138.20 26.96 o 8 7 14 2.08 9.73 16.94 o 9 7 14 177.84 227.41 40.55 o 10 7 14 442.57 443.95 28.27 o 11 7 14 5.57 -0.77 24.78 o 12 7 14 160.22 169.86 29.32 o 13 7 14 6.46 0.80 33.06 o 0 8 14 872.30 829.14 28.78 o 1 8 14 133.31 90.68 11.87 o 2 8 14 3695.59 3894.32 81.88 o 3 8 14 851.65 795.48 25.81 o 4 8 14 2713.59 2747.65 61.30 o 5 8 14 310.77 308.65 18.17 o 6 8 14 2.24 4.19 15.50 o 7 8 14 505.77 507.35 27.86 o 8 8 14 14.51 19.54 18.52 o 9 8 14 140.16 138.68 21.96 o 10 8 14 8.57 4.46 22.95 o 11 8 14 4.06 -8.38 25.17 o 12 8 14 23.68 65.88 29.68 o 13 8 14 229.57 243.75 49.08 o 1 9 14 216.93 167.32 22.28 o 2 9 14 0.22 -12.10 12.10 o 3 9 14 125.62 118.73 14.64 o 4 9 14 1340.84 1388.53 37.65 o 5 9 14 37.99 45.58 15.97 o 6 9 14 191.87 182.28 18.51 o 7 9 14 250.62 293.78 22.66 o 8 9 14 327.88 387.33 25.35 o 9 9 14 52.74 72.34 23.08 o 10 9 14 104.52 124.48 37.35 o 11 9 14 9.22 33.56 26.88 o 12 9 14 30.66 15.80 32.15 o 13 9 14 65.32 95.93 48.34 o 0 10 14 687.98 619.01 39.27 o 1 10 14 1529.66 1555.96 49.06 o 2 10 14 33.44 16.26 13.35 o 3 10 14 1125.34 1179.97 35.31 o 4 10 14 66.69 54.27 18.62 o 5 10 14 2052.52 2206.45 53.78 o 6 10 14 4.84 3.82 18.16 o 7 10 14 208.16 250.02 22.23 o 8 10 14 187.32 214.49 23.71 o 9 10 14 473.18 518.06 30.23 o 10 10 14 379.53 418.39 31.58 o 11 10 14 87.31 47.63 29.70 o 12 10 14 169.55 199.01 47.18 o 13 10 14 147.07 180.01 71.25 o 1 11 14 1.04 -18.64 18.64 o 2 11 14 348.66 332.88 23.00 o 3 11 14 71.08 75.76 16.58 o 4 11 14 0.27 -7.00 16.53 o 5 11 14 3.90 10.91 17.54 o 6 11 14 242.66 199.51 21.11 o 7 11 14 54.26 55.72 20.59 o 8 11 14 452.01 445.02 28.41 o 9 11 14 48.62 60.73 25.80 o 10 11 14 254.32 249.21 30.71 o 11 11 14 1.26 -14.49 31.11 o 12 11 14 42.81 77.94 47.03 o 0 12 14 613.37 650.33 42.80 o 1 12 14 1374.47 1468.54 49.21 o 2 12 14 10.26 -12.30 19.03 o 3 12 14 1904.72 1957.79 60.52 o 4 12 14 46.83 22.83 22.93 o 5 12 14 176.50 197.39 20.78 o 6 12 14 8.83 16.76 42.48 o 7 12 14 1381.79 1480.85 46.51 o 8 12 14 2.82 0.36 24.28 o 9 12 14 230.45 215.46 29.19 o 10 12 14 364.94 389.06 57.49 o 11 12 14 177.16 99.27 47.01 o 1 13 14 6.22 31.71 22.30 o 2 13 14 427.96 412.83 27.53 o 3 13 14 16.72 23.05 25.70 o 4 13 14 271.87 279.63 27.63 o 5 13 14 40.24 31.17 28.35 o 6 13 14 166.14 242.32 28.77 o 7 13 14 291.72 287.64 31.23 o 8 13 14 88.00 61.26 26.60 o 9 13 14 1.68 -19.29 28.41 o 10 13 14 129.65 199.35 49.86 o 11 13 14 0.03 -54.49 72.80 o 0 14 14 0.76 -29.34 29.34 o 1 14 14 19.05 24.20 21.50 o 2 14 14 129.40 183.13 37.17 o 3 14 14 41.93 16.88 25.43 o 4 14 14 0.82 12.99 25.53 o 5 14 14 19.36 8.14 25.57 o 6 14 14 0.09 -4.99 28.64 o 7 14 14 14.29 22.49 30.96 o 8 14 14 0.13 43.22 33.17 o 9 14 14 8.73 8.38 58.02 o 1 15 14 31.73 52.96 24.10 o 2 15 14 42.12 54.32 27.14 o 3 15 14 13.77 -25.69 25.69 o 4 15 14 11.60 9.11 28.02 o 5 15 14 77.50 46.85 30.03 o 6 15 14 77.80 65.21 33.65 o 7 15 14 35.84 7.79 35.08 o 8 15 14 105.04 81.62 58.68 o 0 16 14 215.96 234.06 42.58 o 1 16 14 262.64 251.78 32.21 o 2 16 14 307.65 309.96 32.06 o 3 16 14 318.05 292.91 31.74 o 4 16 14 208.72 141.75 31.10 o 5 16 14 103.65 102.01 35.39 o 6 16 14 140.34 140.85 67.72 o 7 16 14 391.09 371.05 59.34 o 1 17 14 1.98 -12.79 28.62 o 2 17 14 3.51 -28.27 52.28 o 3 17 14 32.50 13.24 30.71 o 4 17 14 63.95 55.81 33.98 o 5 17 14 34.30 -5.07 54.49 o 0 18 14 65.90 28.90 49.86 o 1 18 14 38.11 71.16 32.05 o 1 1 15 1598.61 1610.34 28.03 o 2 1 15 97.47 67.34 6.90 o 3 1 15 103.49 108.39 7.77 o 4 1 15 5.43 8.58 7.32 o 5 1 15 160.06 173.55 10.87 o 6 1 15 1997.98 1742.48 32.56 o 7 1 15 664.36 618.89 24.10 o 8 1 15 2.08 -3.18 14.09 o 9 1 15 278.16 273.42 18.66 o 10 1 15 5.84 -3.86 25.04 o 11 1 15 11.03 -23.67 27.61 o 12 1 15 83.51 110.62 32.98 o 13 1 15 101.52 82.25 38.68 o 0 2 15 2010.53 1978.76 45.49 o 1 2 15 1.32 3.57 5.84 o 2 2 15 4819.42 5135.27 89.17 o 3 2 15 1561.91 1388.44 30.89 o 4 2 15 2008.47 2049.26 38.73 o 5 2 15 0.98 7.03 7.95 o 6 2 15 5615.55 5887.32 120.22 o 7 2 15 25.51 26.88 13.36 o 8 2 15 1586.51 1619.46 41.75 o 9 2 15 52.90 67.97 17.22 o 10 2 15 2853.96 3119.72 72.19 o 11 2 15 270.22 197.64 31.53 o 12 2 15 364.46 297.94 70.59 o 13 2 15 226.02 205.90 39.02 o 1 3 15 645.14 637.76 16.61 o 2 3 15 1702.56 1818.79 34.76 o 3 3 15 363.06 382.10 18.08 o 4 3 15 8.94 40.02 8.59 o 5 3 15 85.45 75.50 12.18 o 6 3 15 143.30 154.60 14.47 o 7 3 15 873.64 894.27 32.28 o 8 3 15 0.23 -13.20 15.35 o 9 3 15 401.73 385.37 21.97 o 10 3 15 18.50 43.04 19.64 o 11 3 15 0.01 -27.98 27.98 o 12 3 15 305.54 319.64 70.26 o 13 3 15 111.16 86.35 37.21 o 0 4 15 13605.83 14778.92 354.94 o 1 4 15 140.35 142.81 7.47 o 2 4 15 1369.80 1519.65 35.78 o 3 4 15 1067.26 973.02 26.53 o 4 4 15 1034.75 1120.24 30.53 o 5 4 15 105.01 102.01 13.24 o 6 4 15 3786.05 3770.66 80.53 o 7 4 15 5.52 15.68 14.64 o 8 4 15 2107.99 2210.70 53.44 o 9 4 15 3.36 -3.38 18.21 o 10 4 15 1327.68 1282.85 61.37 o 11 4 15 19.59 21.55 29.48 o 12 4 15 667.28 681.91 43.18 o 13 4 15 24.30 27.27 36.99 o 1 5 15 2003.72 1933.13 36.79 o 2 5 15 0.28 -1.97 9.78 o 3 5 15 97.05 74.09 11.53 o 4 5 15 574.39 554.59 39.41 o 5 5 15 926.29 912.29 34.19 o 6 5 15 57.76 53.37 13.99 o 7 5 15 64.54 38.49 15.78 o 8 5 15 17.01 26.44 17.42 o 9 5 15 94.21 73.83 21.02 o 10 5 15 19.28 16.90 20.17 o 11 5 15 50.73 53.89 25.45 o 12 5 15 0.08 -19.79 27.65 o 13 5 15 20.13 11.24 59.89 o 0 6 15 6026.95 6212.30 152.58 o 1 6 15 727.14 694.20 21.81 o 2 6 15 130.16 52.64 16.29 o 3 6 15 18.99 21.02 11.20 o 4 6 15 425.90 394.25 17.70 o 5 6 15 307.27 318.08 22.83 o 6 6 15 768.92 725.40 25.13 o 7 6 15 10.96 -0.46 16.15 o 8 6 15 310.84 316.01 24.67 o 9 6 15 272.96 281.19 23.15 o 10 6 15 12.71 31.48 21.90 o 11 6 15 197.67 205.79 40.71 o 12 6 15 191.53 178.50 30.19 o 13 6 15 186.63 231.19 66.84 o 1 7 15 516.63 468.57 17.20 o 2 7 15 45.95 8.31 11.68 o 3 7 15 330.05 330.35 19.65 o 4 7 15 323.40 293.04 17.02 o 5 7 15 472.17 499.35 20.71 o 6 7 15 1.93 27.38 15.32 o 7 7 15 246.28 224.83 19.39 o 8 7 15 314.79 367.65 25.41 o 9 7 15 447.15 509.68 49.94 o 10 7 15 88.57 114.29 23.92 o 11 7 15 34.83 11.60 25.55 o 12 7 15 96.47 86.67 29.91 o 13 7 15 33.15 10.61 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