#------------------------------------------------------------------------------
#$Date: 2025-02-05 05:03:59 +0200 (Wed, 05 Feb 2025) $
#$Revision: 297594 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/33/2023373.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023373
loop_
_publ_author_name
'Upmann, Daniel'
'Jones, Peter G.'
_publ_section_title
;
Crystal structures of six complexes of phosphane chalcogenides R 1 R 2 R
3PE (R = tert-butyl or isopropyl, E = S or Se) with the metal halides MX
2 (M = Pd or Pt, X = Cl or Br), two halochalcogenylphosphonium
derivatives ( t Bu2 iPrPEBr)2[Pd2Br6] and one hydrolysis product
;
_journal_coeditor_code YZ2063
_journal_issue 3
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi 10.1107/S2056989025000805
_journal_volume 81
_journal_year 2025
_chemical_formula_iupac '[Pd Cl2 (C11 H25 P1 Se1)2]'
_chemical_formula_moiety 'C22 H50 Cl2 P2 Pd Se2'
_chemical_formula_sum 'C22 H50 Cl2 P2 Pd Se2'
_chemical_formula_weight 711.78
_chemical_name_systematic
;
(Di-tert-butylisopropylphosphine
selenide-\kSe)dichloridopalladium(II)
;
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2ybc'
_space_group_name_H-M_alt 'P 1 21/c 1'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary direct
_atom_sites_solution_secondary difmap
_audit_creation_method SHELXL2019/3
_cell_angle_alpha 90
_cell_angle_beta 117.306(3)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 15.3744(4)
_cell_length_b 13.2969(2)
_cell_length_c 16.0503(3)
_cell_measurement_reflns_used 15039
_cell_measurement_temperature 100(2)
_cell_measurement_theta_max 30.8273
_cell_measurement_theta_min 2.1330
_cell_volume 2915.57(13)
_computing_cell_refinement
;
CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2012)
;
_computing_data_collection
;
CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2012)
;
_computing_data_reduction
;
CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2012)
;
_computing_molecular_graphics
;
Bruker XP, Version 5.1 (Bruker, 1998)
;
_computing_publication_material
;
publCIF (Westrip, 2010)
;
_computing_structure_refinement
;
SHELXL2019/3 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS-97 (Sheldrick, 2008)
;
_diffrn_ambient_temperature 100(2)
_diffrn_detector_area_resol_mean 16.1419
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type 'Oxford Diffraction Xcalibur, Eos'
_diffrn_measurement_method '\w scans'
_diffrn_radiation_monochromator graphite
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0912
_diffrn_reflns_av_unetI/netI 0.0340
_diffrn_reflns_limit_h_max 20
_diffrn_reflns_limit_h_min -20
_diffrn_reflns_limit_k_max 17
_diffrn_reflns_limit_k_min -17
_diffrn_reflns_limit_l_max 21
_diffrn_reflns_limit_l_min -21
_diffrn_reflns_number 134870
_diffrn_reflns_theta_full 28.000
_diffrn_reflns_theta_max 28.281
_diffrn_reflns_theta_min 2.137
_diffrn_source 'Enhance (Mo) X-ray Source'
_exptl_absorpt_coefficient_mu 3.435
_exptl_absorpt_correction_T_max 1.00000
_exptl_absorpt_correction_T_min 0.71342
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2012)
;
_exptl_crystal_colour 'dichroic red orange'
_exptl_crystal_density_diffrn 1.622
_exptl_crystal_density_method 'not measured'
_exptl_crystal_description plate
_exptl_crystal_F_000 1440
_exptl_crystal_size_max 0.200
_exptl_crystal_size_mid 0.100
_exptl_crystal_size_min 0.020
_refine_diff_density_max 1.353
_refine_diff_density_min -0.783
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.041
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 278
_refine_ls_number_reflns 7231
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.041
_refine_ls_R_factor_all 0.0477
_refine_ls_R_factor_gt 0.0321
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0234P)^2^+4.2293P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0629
_refine_ls_wR_factor_ref 0.0679
_reflns_number_gt 5841
_reflns_number_total 7231
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file yz2063.cif
_cod_data_source_block 2
_cod_original_cell_volume 2915.56(12)
_cod_original_sg_symbol_H-M 'P 21/c'
_cod_database_code 2023373
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.547
_shelx_estimated_absorpt_t_max 0.934
_shelx_hkl_file
;
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0 0 3 140.412 98.0027
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0 0 3-172.878 110.320
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0 0 3-58.7416 67.4159
0 0 3 32.1312 72.6693
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0 0 3-46.9867 62.2300
0 0 3-19.5189 45.4804
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_shelx_hkl_checksum 57621
_shelx_res_file
;
TITL Dana in P2(1)/c
shelx.res
created by SHELXL-2019/3 at 11:49:45 on 28-Jan-2025
CELL 0.71073 15.3744 13.2969 16.0503 90.000 117.306 90.000
ZERR 4.00 0.0004 0.0002 0.0003 0.000 0.003 0.000
LATT 1
SYMM - X, 1/2 + Y, 1/2 - Z
SFAC C H P CL SE PD
UNIT 88 200 8 8 8 4
MERG 2
SHEL 999 0.75
CONF 2.5
HTAB C11 Se1
HTAB C12 Se1
HTAB C21 Cl1
HTAB C21 Se1
HTAB C3 Cl2
HTAB C31 Se1
HTAB C41 Se2
HTAB C43 Se2
HTAB C5 Cl1
EQIV $1 -x+1, -y+1, -z+1
HTAB C51 Cl1_$1
HTAB C52 Cl1
HTAB C52 Se2
HTAB C62 Se2
HTAB C62 Cl1
EQIV $2 x, -y+3/2, z-1/2
HTAB C63 Se1_$2
HTAB C63 Pd1_$2
FMAP 2
PLAN 10
SIZE 0.020 0.100 0.200
ACTA 56.00
BOND $H
L.S. 6
TEMP -173.00
WGHT 0.023400 4.229300
FVAR 0.92035
PD1 6 0.216307 0.753496 0.434743 11.00000 0.01474 0.01251 =
0.01476 0.00004 0.00538 0.00092
CL1 4 0.271191 0.592165 0.433004 11.00000 0.02292 0.01529 =
0.03197 0.00041 0.01028 0.00385
CL2 4 0.169156 0.914558 0.451749 11.00000 0.02087 0.01515 =
0.02674 -0.00215 0.01145 0.00094
SE1 5 0.083715 0.676802 0.456218 11.00000 0.01708 0.01778 =
0.01473 0.00452 0.00516 -0.00054
SE2 5 0.347015 0.849362 0.423225 11.00000 0.02171 0.01730 =
0.02555 -0.00411 0.01387 -0.00316
P1 3 -0.053824 0.711070 0.332089 11.00000 0.01485 0.01147 =
0.01288 0.00052 0.00561 -0.00031
P2 3 0.436308 0.771694 0.368856 11.00000 0.01796 0.02415 =
0.01875 0.00274 0.00841 0.00482
C1 1 -0.143295 0.619865 0.340799 11.00000 0.01928 0.01386 =
0.01956 -0.00021 0.00813 -0.00355
C11 1 -0.121944 0.513404 0.318242 11.00000 0.02429 0.01435 =
0.03054 0.00147 0.01182 -0.00328
AFIX 137
H11A 2 -0.160709 0.464688 0.332998 11.00000 -1.50000
H11B 2 -0.052156 0.498536 0.355833 11.00000 -1.50000
H11C 2 -0.139325 0.508954 0.251481 11.00000 -1.50000
AFIX 0
C12 1 -0.130067 0.618799 0.442164 11.00000 0.03124 0.02429 =
0.02787 0.00210 0.01903 -0.00563
AFIX 137
H12A 2 -0.176767 0.571550 0.446459 11.00000 -1.50000
H12B 2 -0.141840 0.686386 0.459183 11.00000 -1.50000
H12C 2 -0.063198 0.597785 0.485175 11.00000 -1.50000
AFIX 0
C13 1 -0.250295 0.647951 0.275364 11.00000 0.02012 0.02545 =
0.03332 0.00128 0.01325 -0.00299
AFIX 137
H13A 2 -0.260177 0.651640 0.210622 11.00000 -1.50000
H13B 2 -0.265127 0.713400 0.293923 11.00000 -1.50000
H13C 2 -0.293788 0.596718 0.279834 11.00000 -1.50000
AFIX 0
C2 1 -0.041650 0.694332 0.221200 11.00000 0.01890 0.01913 =
0.01427 0.00128 0.00707 0.00076
C21 1 0.021475 0.602474 0.228002 11.00000 0.02247 0.02651 =
0.01962 -0.00265 0.00988 0.00240
AFIX 137
H21A 2 0.031078 0.598683 0.171795 11.00000 -1.50000
H21B 2 -0.011447 0.541326 0.232944 11.00000 -1.50000
H21C 2 0.085160 0.608671 0.283618 11.00000 -1.50000
AFIX 0
C22 1 0.009228 0.787954 0.207374 11.00000 0.02397 0.02210 =
0.01689 0.00202 0.01064 -0.00095
AFIX 137
H22A 2 0.070588 0.800034 0.264343 11.00000 -1.50000
H22B 2 -0.033787 0.846468 0.194614 11.00000 -1.50000
H22C 2 0.023270 0.776957 0.154365 11.00000 -1.50000
AFIX 0
C23 1 -0.142569 0.680888 0.135097 11.00000 0.02114 0.02643 =
0.01689 0.00012 0.00679 0.00009
AFIX 137
H23A 2 -0.134537 0.679690 0.077960 11.00000 -1.50000
H23B 2 -0.185338 0.736972 0.131925 11.00000 -1.50000
H23C 2 -0.171914 0.617463 0.140730 11.00000 -1.50000
AFIX 0
C3 1 -0.086072 0.844832 0.336460 11.00000 0.01995 0.01272 =
0.02030 0.00069 0.01014 0.00070
AFIX 13
H3 2 -0.029117 0.883940 0.339530 11.00000 -1.20000
AFIX 0
C31 1 -0.091163 0.871588 0.427067 11.00000 0.03475 0.02013 =
0.02762 -0.00371 0.01713 0.00246
AFIX 137
H31A 2 -0.088046 0.944789 0.435029 11.00000 -1.50000
H31B 2 -0.035950 0.840529 0.480612 11.00000 -1.50000
H31C 2 -0.152747 0.846544 0.423459 11.00000 -1.50000
AFIX 0
C32 1 -0.175862 0.888350 0.251488 11.00000 0.02469 0.01864 =
0.02797 0.00338 0.01116 0.00334
AFIX 137
H32A 2 -0.235194 0.854274 0.244931 11.00000 -1.50000
H32B 2 -0.168594 0.877950 0.194552 11.00000 -1.50000
H32C 2 -0.180919 0.960508 0.260924 11.00000 -1.50000
AFIX 0
C4 1 0.537160 0.867529 0.389935 11.00000 0.02699 0.02989 =
0.03909 0.00863 0.01769 0.00238
C41 1 0.607310 0.866703 0.493988 11.00000 0.02608 0.04011 =
0.04819 0.00266 0.00703 -0.00673
AFIX 137
H41A 2 0.655858 0.920298 0.508305 11.00000 -1.50000
H41B 2 0.640662 0.801528 0.511255 11.00000 -1.50000
H41C 2 0.570742 0.877751 0.529645 11.00000 -1.50000
AFIX 0
C42 1 0.594407 0.843028 0.334871 11.00000 0.03780 0.04375 =
0.06207 0.01149 0.03293 0.00655
AFIX 137
H42A 2 0.645149 0.894025 0.348349 11.00000 -1.50000
H42B 2 0.549428 0.842777 0.267542 11.00000 -1.50000
H42C 2 0.625043 0.776703 0.353712 11.00000 -1.50000
AFIX 0
C43 1 0.495052 0.974103 0.362934 11.00000 0.03637 0.02849 =
0.04621 0.00635 0.02189 -0.00308
AFIX 137
H43A 2 0.453950 0.989210 0.393325 11.00000 -1.50000
H43B 2 0.455536 0.978337 0.294732 11.00000 -1.50000
H43C 2 0.548795 1.022783 0.383513 11.00000 -1.50000
AFIX 0
C5 1 0.490760 0.654210 0.431711 11.00000 0.02794 0.02559 =
0.03215 0.00622 0.01343 0.00497
AFIX 13
H5 2 0.438287 0.602317 0.402417 11.00000 -1.20000
AFIX 0
C51 1 0.579143 0.612741 0.421025 11.00000 0.03490 0.03381 =
0.05095 0.01596 0.01950 0.01944
AFIX 137
H51A 2 0.636018 0.656369 0.454863 11.00000 -1.50000
H51B 2 0.563010 0.611008 0.354459 11.00000 -1.50000
H51C 2 0.594383 0.544578 0.446984 11.00000 -1.50000
AFIX 0
C52 1 0.515214 0.655561 0.535593 11.00000 0.03606 0.04141 =
0.03054 0.01502 0.01154 0.00448
AFIX 137
H52A 2 0.535191 0.588088 0.562099 11.00000 -1.50000
H52B 2 0.457333 0.676426 0.541816 11.00000 -1.50000
H52C 2 0.568761 0.703035 0.569321 11.00000 -1.50000
AFIX 0
C6 1 0.360080 0.743570 0.241499 11.00000 0.03083 0.03400 =
0.02259 -0.00139 0.01162 0.00491
C61 1 0.408675 0.670851 0.202640 11.00000 0.04622 0.04919 =
0.03402 -0.00641 0.02007 0.01395
AFIX 137
H61A 2 0.419072 0.606082 0.234969 11.00000 -1.50000
H61B 2 0.471833 0.698348 0.212523 11.00000 -1.50000
H61C 2 0.366455 0.661231 0.135372 11.00000 -1.50000
AFIX 0
C62 1 0.262837 0.698255 0.226352 11.00000 0.03018 0.04343 =
0.02922 -0.01129 0.00875 -0.00939
AFIX 137
H62A 2 0.222619 0.683661 0.159586 11.00000 -1.50000
H62B 2 0.228373 0.746102 0.247212 11.00000 -1.50000
H62C 2 0.275005 0.635872 0.262518 11.00000 -1.50000
AFIX 0
C63 1 0.336825 0.842815 0.185060 11.00000 0.04392 0.04364 =
0.02173 0.00486 0.01312 0.00977
AFIX 137
H63A 2 0.289663 0.829621 0.119645 11.00000 -1.50000
H63B 2 0.397166 0.870319 0.187677 11.00000 -1.50000
H63C 2 0.308914 0.891380 0.212100 11.00000 -1.50000
AFIX 0
HKLF 4
REM Dana in P2(1)/c
REM wR2 = 0.0679, GooF = S = 1.041, Restrained GooF = 1.041 for all data
REM R1 = 0.0321 for 5841 Fo > 4sig(Fo) and 0.0477 for all 7231 data
REM 278 parameters refined using 0 restraints
END
WGHT 0.0234 4.2290
REM Highest difference peak 1.353, deepest hole -0.783, 1-sigma level 0.106
Q1 1 0.3861 0.8125 0.4742 11.00000 0.05 1.35
Q2 1 0.4238 0.7158 0.3663 11.00000 0.05 0.74
Q3 1 0.3473 0.6582 0.4215 11.00000 0.05 0.59
Q4 1 0.4303 0.9241 0.2599 11.00000 0.05 0.58
Q5 1 0.2904 0.5964 0.4882 11.00000 0.05 0.57
Q6 1 0.2161 0.7614 0.3632 11.00000 0.05 0.53
Q7 1 0.3302 0.6839 0.2400 11.00000 0.05 0.52
Q8 1 0.0199 0.7244 0.4003 11.00000 0.05 0.52
Q9 1 0.2228 0.7530 0.5072 11.00000 0.05 0.49
Q10 1 0.0830 0.8272 0.4528 11.00000 0.05 0.49
;
_shelx_res_checksum 24924
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pd Pd1 0.21631(2) 0.75350(2) 0.43474(2) 0.01454(6) Uani d 1 . .
Cl Cl1 0.27119(6) 0.59216(5) 0.43300(6) 0.02429(16) Uani d 1 . .
Cl Cl2 0.16916(5) 0.91456(5) 0.45175(5) 0.02071(15) Uani d 1 . .
Se Se1 0.08372(2) 0.67680(2) 0.45622(2) 0.01735(7) Uani d 1 . .
Se Se2 0.34701(2) 0.84936(2) 0.42322(2) 0.02034(7) Uani d 1 . .
P P1 -0.05382(5) 0.71107(5) 0.33209(5) 0.01336(14) Uani d 1 . .
P P2 0.43631(6) 0.77169(6) 0.36886(5) 0.02029(17) Uani d 1 . .
C C1 -0.1433(2) 0.6199(2) 0.3408(2) 0.0179(6) Uani d 1 . .
C C11 -0.1219(2) 0.5134(2) 0.3182(2) 0.0234(7) Uani d 1 . .
H H11A -0.160709 0.464688 0.332998 0.035 Uiso calc 1 . .
H H11B -0.052156 0.498536 0.355833 0.035 Uiso calc 1 . .
H H11C -0.139325 0.508954 0.251481 0.035 Uiso calc 1 . .
C C12 -0.1301(2) 0.6188(2) 0.4422(2) 0.0257(7) Uani d 1 . .
H H12A -0.176767 0.571550 0.446459 0.039 Uiso calc 1 . .
H H12B -0.141840 0.686386 0.459183 0.039 Uiso calc 1 . .
H H12C -0.063198 0.597785 0.485175 0.039 Uiso calc 1 . .
C C13 -0.2503(2) 0.6480(2) 0.2754(2) 0.0259(7) Uani d 1 . .
H H13A -0.260177 0.651640 0.210622 0.039 Uiso calc 1 . .
H H13B -0.265127 0.713400 0.293923 0.039 Uiso calc 1 . .
H H13C -0.293788 0.596718 0.279834 0.039 Uiso calc 1 . .
C C2 -0.0416(2) 0.6943(2) 0.2212(2) 0.0176(6) Uani d 1 . .
C C21 0.0215(2) 0.6025(2) 0.2280(2) 0.0228(7) Uani d 1 . .
H H21A 0.031078 0.598683 0.171795 0.034 Uiso calc 1 . .
H H21B -0.011447 0.541326 0.232944 0.034 Uiso calc 1 . .
H H21C 0.085160 0.608671 0.283618 0.034 Uiso calc 1 . .
C C22 0.0092(2) 0.7880(2) 0.2074(2) 0.0205(6) Uani d 1 . .
H H22A 0.070588 0.800034 0.264343 0.031 Uiso calc 1 . .
H H22B -0.033787 0.846468 0.194614 0.031 Uiso calc 1 . .
H H22C 0.023270 0.776957 0.154365 0.031 Uiso calc 1 . .
C C23 -0.1426(2) 0.6809(2) 0.1351(2) 0.0222(6) Uani d 1 . .
H H23A -0.134537 0.679690 0.077960 0.033 Uiso calc 1 . .
H H23B -0.185338 0.736972 0.131925 0.033 Uiso calc 1 . .
H H23C -0.171914 0.617463 0.140730 0.033 Uiso calc 1 . .
C C3 -0.0861(2) 0.8448(2) 0.3365(2) 0.0173(6) Uani d 1 . .
H H3 -0.029117 0.883940 0.339530 0.021 Uiso calc 1 . .
C C31 -0.0912(3) 0.8716(2) 0.4271(2) 0.0264(7) Uani d 1 . .
H H31A -0.088046 0.944789 0.435029 0.040 Uiso calc 1 . .
H H31B -0.035950 0.840529 0.480612 0.040 Uiso calc 1 . .
H H31C -0.152747 0.846544 0.423459 0.040 Uiso calc 1 . .
C C32 -0.1759(2) 0.8883(2) 0.2515(2) 0.0241(7) Uani d 1 . .
H H32A -0.235194 0.854274 0.244931 0.036 Uiso calc 1 . .
H H32B -0.168594 0.877950 0.194552 0.036 Uiso calc 1 . .
H H32C -0.180919 0.960508 0.260924 0.036 Uiso calc 1 . .
C C4 0.5372(3) 0.8675(3) 0.3899(3) 0.0310(8) Uani d 1 . .
C C41 0.6073(3) 0.8667(3) 0.4940(3) 0.0420(10) Uani d 1 . .
H H41A 0.655858 0.920298 0.508305 0.063 Uiso calc 1 . .
H H41B 0.640662 0.801528 0.511255 0.063 Uiso calc 1 . .
H H41C 0.570742 0.877751 0.529645 0.063 Uiso calc 1 . .
C C42 0.5944(3) 0.8430(3) 0.3349(3) 0.0440(10) Uani d 1 . .
H H42A 0.645149 0.894025 0.348349 0.066 Uiso calc 1 . .
H H42B 0.549428 0.842777 0.267542 0.066 Uiso calc 1 . .
H H42C 0.625043 0.776703 0.353712 0.066 Uiso calc 1 . .
C C43 0.4951(3) 0.9741(3) 0.3629(3) 0.0359(8) Uani d 1 . .
H H43A 0.453950 0.989210 0.393325 0.054 Uiso calc 1 . .
H H43B 0.455536 0.978337 0.294732 0.054 Uiso calc 1 . .
H H43C 0.548795 1.022783 0.383513 0.054 Uiso calc 1 . .
C C5 0.4908(3) 0.6542(3) 0.4317(2) 0.0287(7) Uani d 1 . .
H H5 0.438287 0.602317 0.402417 0.034 Uiso calc 1 . .
C C51 0.5791(3) 0.6127(3) 0.4210(3) 0.0400(9) Uani d 1 . .
H H51A 0.636018 0.656369 0.454863 0.060 Uiso calc 1 . .
H H51B 0.563010 0.611008 0.354459 0.060 Uiso calc 1 . .
H H51C 0.594383 0.544578 0.446984 0.060 Uiso calc 1 . .
C C52 0.5152(3) 0.6556(3) 0.5356(2) 0.0375(9) Uani d 1 . .
H H52A 0.535191 0.588088 0.562099 0.056 Uiso calc 1 . .
H H52B 0.457333 0.676426 0.541816 0.056 Uiso calc 1 . .
H H52C 0.568761 0.703035 0.569321 0.056 Uiso calc 1 . .
C C6 0.3601(3) 0.7436(3) 0.2415(2) 0.0294(7) Uani d 1 . .
C C61 0.4087(3) 0.6709(3) 0.2026(3) 0.0425(10) Uani d 1 . .
H H61A 0.419072 0.606082 0.234969 0.064 Uiso calc 1 . .
H H61B 0.471833 0.698348 0.212523 0.064 Uiso calc 1 . .
H H61C 0.366455 0.661231 0.135372 0.064 Uiso calc 1 . .
C C62 0.2628(3) 0.6983(3) 0.2264(3) 0.0362(9) Uani d 1 . .
H H62A 0.222619 0.683661 0.159586 0.054 Uiso calc 1 . .
H H62B 0.228373 0.746102 0.247212 0.054 Uiso calc 1 . .
H H62C 0.275005 0.635872 0.262518 0.054 Uiso calc 1 . .
C C63 0.3368(3) 0.8428(3) 0.1851(2) 0.0372(9) Uani d 1 . .
H H63A 0.289663 0.829621 0.119645 0.056 Uiso calc 1 . .
H H63B 0.397166 0.870319 0.187677 0.056 Uiso calc 1 . .
H H63C 0.308914 0.891380 0.212100 0.056 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Pd1 0.01474(11) 0.01251(10) 0.01476(11) 0.00092(8) 0.00538(9) 0.00004(8)
Cl1 0.0229(4) 0.0153(3) 0.0320(4) 0.0039(3) 0.0103(3) 0.0004(3)
Cl2 0.0209(4) 0.0151(3) 0.0267(4) 0.0009(3) 0.0115(3) -0.0021(3)
Se1 0.01708(15) 0.01778(14) 0.01473(14) -0.00054(11) 0.00516(12) 0.00452(11)
Se2 0.02171(16) 0.01730(15) 0.02555(17) -0.00316(12) 0.01387(14) -0.00411(12)
P1 0.0149(4) 0.0115(3) 0.0129(3) -0.0003(3) 0.0056(3) 0.0005(3)
P2 0.0180(4) 0.0242(4) 0.0187(4) 0.0048(3) 0.0084(3) 0.0027(3)
C1 0.0193(15) 0.0139(14) 0.0196(15) -0.0036(11) 0.0081(13) -0.0002(11)
C11 0.0243(17) 0.0143(14) 0.0305(18) -0.0033(12) 0.0118(15) 0.0015(12)
C12 0.0312(18) 0.0243(16) 0.0279(17) -0.0056(13) 0.0190(16) 0.0021(13)
C13 0.0201(16) 0.0254(16) 0.0333(18) -0.0030(13) 0.0133(15) 0.0013(14)
C2 0.0189(15) 0.0191(15) 0.0143(14) 0.0008(11) 0.0071(12) 0.0013(11)
C21 0.0225(16) 0.0265(17) 0.0196(16) 0.0024(13) 0.0099(14) -0.0026(13)
C22 0.0240(16) 0.0221(15) 0.0169(15) -0.0010(12) 0.0106(13) 0.0020(12)
C23 0.0211(16) 0.0264(16) 0.0169(15) 0.0001(13) 0.0068(13) 0.0001(12)
C3 0.0200(15) 0.0127(13) 0.0203(15) 0.0007(11) 0.0101(13) 0.0007(11)
C31 0.0347(19) 0.0201(16) 0.0276(17) 0.0025(14) 0.0171(16) -0.0037(13)
C32 0.0247(17) 0.0186(15) 0.0280(17) 0.0033(13) 0.0112(15) 0.0034(13)
C4 0.0270(18) 0.0299(18) 0.039(2) 0.0024(14) 0.0177(17) 0.0086(15)
C41 0.026(2) 0.040(2) 0.048(2) -0.0067(16) 0.0070(18) 0.0027(18)
C42 0.038(2) 0.044(2) 0.062(3) 0.0066(18) 0.033(2) 0.011(2)
C43 0.036(2) 0.0285(19) 0.046(2) -0.0031(15) 0.0219(19) 0.0064(16)
C5 0.0279(18) 0.0256(17) 0.0322(19) 0.0050(14) 0.0134(16) 0.0062(14)
C51 0.035(2) 0.034(2) 0.051(2) 0.0194(17) 0.0195(19) 0.0160(18)
C52 0.036(2) 0.041(2) 0.031(2) 0.0045(17) 0.0115(17) 0.0150(16)
C6 0.0308(18) 0.0340(19) 0.0226(17) 0.0049(15) 0.0116(15) -0.0014(14)
C61 0.046(2) 0.049(2) 0.034(2) 0.0139(19) 0.0201(19) -0.0064(18)
C62 0.030(2) 0.043(2) 0.0292(19) -0.0094(17) 0.0088(16) -0.0113(16)
C63 0.044(2) 0.044(2) 0.0217(18) 0.0098(18) 0.0131(17) 0.0049(16)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
Cl1 Pd1 Cl2 . . 174.61(3) y
Cl1 Pd1 Se1 . . 86.97(2) y
Cl2 Pd1 Se1 . . 92.46(2) y
Cl1 Pd1 Se2 . . 99.50(2) y
Cl2 Pd1 Se2 . . 80.81(2) y
Se1 Pd1 Se2 . . 172.772(14) y
P1 Se1 Pd1 . . 107.78(2) y
P2 Se2 Pd1 . . 117.93(3) y
C3 P1 C2 . . 107.01(13) ?
C3 P1 C1 . . 113.37(13) ?
C2 P1 C1 . . 112.67(13) ?
C3 P1 Se1 . . 109.18(10) y
C2 P1 Se1 . . 111.22(9) y
C1 P1 Se1 . . 103.40(10) y
C5 P2 C6 . . 109.22(16) ?
C5 P2 C4 . . 109.91(16) ?
C6 P2 C4 . . 112.17(16) ?
C5 P2 Se2 . . 113.08(11) ?
C6 P2 Se2 . . 109.66(11) ?
C4 P2 Se2 . . 102.73(11) ?
C11 C1 C13 . . 109.9(2) ?
C11 C1 C12 . . 107.5(2) ?
C13 C1 C12 . . 107.7(3) ?
C11 C1 P1 . . 109.5(2) ?
C13 C1 P1 . . 112.4(2) ?
C12 C1 P1 . . 109.6(2) ?
C1 C11 H11A . . 109.5 ?
C1 C11 H11B . . 109.5 ?
H11A C11 H11B . . 109.5 ?
C1 C11 H11C . . 109.5 ?
H11A C11 H11C . . 109.5 ?
H11B C11 H11C . . 109.5 ?
C1 C12 H12A . . 109.5 ?
C1 C12 H12B . . 109.5 ?
H12A C12 H12B . . 109.5 ?
C1 C12 H12C . . 109.5 ?
H12A C12 H12C . . 109.5 ?
H12B C12 H12C . . 109.5 ?
C1 C13 H13A . . 109.5 ?
C1 C13 H13B . . 109.5 ?
H13A C13 H13B . . 109.5 ?
C1 C13 H13C . . 109.5 ?
H13A C13 H13C . . 109.5 ?
H13B C13 H13C . . 109.5 ?
C21 C2 C22 . . 107.9(2) ?
C21 C2 C23 . . 108.4(2) ?
C22 C2 C23 . . 109.5(2) ?
C21 C2 P1 . . 111.1(2) ?
C22 C2 P1 . . 108.51(19) ?
C23 C2 P1 . . 111.4(2) ?
C2 C21 H21A . . 109.5 ?
C2 C21 H21B . . 109.5 ?
H21A C21 H21B . . 109.5 ?
C2 C21 H21C . . 109.5 ?
H21A C21 H21C . . 109.5 ?
H21B C21 H21C . . 109.5 ?
C2 C22 H22A . . 109.5 ?
C2 C22 H22B . . 109.5 ?
H22A C22 H22B . . 109.5 ?
C2 C22 H22C . . 109.5 ?
H22A C22 H22C . . 109.5 ?
H22B C22 H22C . . 109.5 ?
C2 C23 H23A . . 109.5 ?
C2 C23 H23B . . 109.5 ?
H23A C23 H23B . . 109.5 ?
C2 C23 H23C . . 109.5 ?
H23A C23 H23C . . 109.5 ?
H23B C23 H23C . . 109.5 ?
C31 C3 C32 . . 109.7(2) ?
C31 C3 P1 . . 112.9(2) ?
C32 C3 P1 . . 118.2(2) ?
C31 C3 H3 . . 104.9 ?
C32 C3 H3 . . 104.9 ?
P1 C3 H3 . . 104.9 ?
C3 C31 H31A . . 109.5 ?
C3 C31 H31B . . 109.5 ?
H31A C31 H31B . . 109.5 ?
C3 C31 H31C . . 109.5 ?
H31A C31 H31C . . 109.5 ?
H31B C31 H31C . . 109.5 ?
C3 C32 H32A . . 109.5 ?
C3 C32 H32B . . 109.5 ?
H32A C32 H32B . . 109.5 ?
C3 C32 H32C . . 109.5 ?
H32A C32 H32C . . 109.5 ?
H32B C32 H32C . . 109.5 ?
C41 C4 C43 . . 108.2(3) ?
C41 C4 C42 . . 109.0(3) ?
C43 C4 C42 . . 108.1(3) ?
C41 C4 P2 . . 107.4(2) ?
C43 C4 P2 . . 111.2(2) ?
C42 C4 P2 . . 112.8(3) ?
C4 C41 H41A . . 109.5 ?
C4 C41 H41B . . 109.5 ?
H41A C41 H41B . . 109.5 ?
C4 C41 H41C . . 109.5 ?
H41A C41 H41C . . 109.5 ?
H41B C41 H41C . . 109.5 ?
C4 C42 H42A . . 109.5 ?
C4 C42 H42B . . 109.5 ?
H42A C42 H42B . . 109.5 ?
C4 C42 H42C . . 109.5 ?
H42A C42 H42C . . 109.5 ?
H42B C42 H42C . . 109.5 ?
C4 C43 H43A . . 109.5 ?
C4 C43 H43B . . 109.5 ?
H43A C43 H43B . . 109.5 ?
C4 C43 H43C . . 109.5 ?
H43A C43 H43C . . 109.5 ?
H43B C43 H43C . . 109.5 ?
C52 C5 C51 . . 109.6(3) ?
C52 C5 P2 . . 114.2(2) ?
C51 C5 P2 . . 116.3(2) ?
C52 C5 H5 . . 105.2 ?
C51 C5 H5 . . 105.2 ?
P2 C5 H5 . . 105.2 ?
C5 C51 H51A . . 109.5 ?
C5 C51 H51B . . 109.5 ?
H51A C51 H51B . . 109.5 ?
C5 C51 H51C . . 109.5 ?
H51A C51 H51C . . 109.5 ?
H51B C51 H51C . . 109.5 ?
C5 C52 H52A . . 109.5 ?
C5 C52 H52B . . 109.5 ?
H52A C52 H52B . . 109.5 ?
C5 C52 H52C . . 109.5 ?
H52A C52 H52C . . 109.5 ?
H52B C52 H52C . . 109.5 ?
C61 C6 C62 . . 108.3(3) ?
C61 C6 C63 . . 109.1(3) ?
C62 C6 C63 . . 107.3(3) ?
C61 C6 P2 . . 113.4(3) ?
C62 C6 P2 . . 109.3(2) ?
C63 C6 P2 . . 109.3(2) ?
C6 C61 H61A . . 109.5 ?
C6 C61 H61B . . 109.5 ?
H61A C61 H61B . . 109.5 ?
C6 C61 H61C . . 109.5 ?
H61A C61 H61C . . 109.5 ?
H61B C61 H61C . . 109.5 ?
C6 C62 H62A . . 109.5 ?
C6 C62 H62B . . 109.5 ?
H62A C62 H62B . . 109.5 ?
C6 C62 H62C . . 109.5 ?
H62A C62 H62C . . 109.5 ?
H62B C62 H62C . . 109.5 ?
C6 C63 H63A . . 109.5 ?
C6 C63 H63B . . 109.5 ?
H63A C63 H63B . . 109.5 ?
C6 C63 H63C . . 109.5 ?
H63A C63 H63C . . 109.5 ?
H63B C63 H63C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Pd1 Cl1 . 2.3100(7) y
Pd1 Cl2 . 2.3169(7) y
Pd1 Se1 . 2.4411(4) y
Pd1 Se2 . 2.4573(4) y
Se1 P1 . 2.1870(8) y
Se2 P2 . 2.1936(8) y
P1 C3 . 1.856(3) ?
P1 C2 . 1.886(3) ?
P1 C1 . 1.887(3) ?
P2 C5 . 1.840(3) ?
P2 C6 . 1.869(3) ?
P2 C4 . 1.913(4) ?
C1 C11 . 1.534(4) ?
C1 C13 . 1.537(4) ?
C1 C12 . 1.544(4) ?
C11 H11A . 0.9800 ?
C11 H11B . 0.9800 ?
C11 H11C . 0.9800 ?
C12 H12A . 0.9800 ?
C12 H12B . 0.9800 ?
C12 H12C . 0.9800 ?
C13 H13A . 0.9800 ?
C13 H13B . 0.9800 ?
C13 H13C . 0.9800 ?
C2 C21 . 1.532(4) ?
C2 C22 . 1.540(4) ?
C2 C23 . 1.543(4) ?
C21 H21A . 0.9800 ?
C21 H21B . 0.9800 ?
C21 H21C . 0.9800 ?
C22 H22A . 0.9800 ?
C22 H22B . 0.9800 ?
C22 H22C . 0.9800 ?
C23 H23A . 0.9800 ?
C23 H23B . 0.9800 ?
C23 H23C . 0.9800 ?
C3 C31 . 1.534(4) ?
C3 C32 . 1.541(4) ?
C3 H3 . 1.0000 ?
C31 H31A . 0.9800 ?
C31 H31B . 0.9800 ?
C31 H31C . 0.9800 ?
C32 H32A . 0.9800 ?
C32 H32B . 0.9800 ?
C32 H32C . 0.9800 ?
C4 C41 . 1.517(5) ?
C4 C43 . 1.535(5) ?
C4 C42 . 1.541(5) ?
C41 H41A . 0.9800 ?
C41 H41B . 0.9800 ?
C41 H41C . 0.9800 ?
C42 H42A . 0.9800 ?
C42 H42B . 0.9800 ?
C42 H42C . 0.9800 ?
C43 H43A . 0.9800 ?
C43 H43B . 0.9800 ?
C43 H43C . 0.9800 ?
C5 C52 . 1.532(5) ?
C5 C51 . 1.547(5) ?
C5 H5 . 1.0000 ?
C51 H51A . 0.9800 ?
C51 H51B . 0.9800 ?
C51 H51C . 0.9800 ?
C52 H52A . 0.9800 ?
C52 H52B . 0.9800 ?
C52 H52C . 0.9800 ?
C6 C61 . 1.520(5) ?
C6 C62 . 1.524(5) ?
C6 C63 . 1.547(5) ?
C61 H61A . 0.9800 ?
C61 H61B . 0.9800 ?
C61 H61C . 0.9800 ?
C62 H62A . 0.9800 ?
C62 H62B . 0.9800 ?
C62 H62C . 0.9800 ?
C63 H63A . 0.9800 ?
C63 H63B . 0.9800 ?
C63 H63C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
C11 H11B Se1 . 0.98 3.08 3.633(3) 117.1 yes
C12 H12C Se1 . 0.98 2.72 3.282(3) 117.1 yes
C21 H21C Cl1 . 0.98 2.77 3.741(3) 169.9 yes
C21 H21C Se1 . 0.98 2.92 3.478(3) 116.8 yes
C3 H3 Cl2 . 1.00 2.77 3.608(3) 141.9 yes
C31 H31B Se1 . 0.98 2.99 3.606(3) 122.0 yes
C41 H41C Se2 . 0.98 3.08 3.632(4) 116.8 yes
C43 H43A Se2 . 0.98 2.67 3.300(4) 122.6 yes
C5 H5 Cl1 . 1.00 2.83 3.484(4) 123.5 yes
C51 H51C Cl1 3_666 0.98 2.76 3.642(3) 149.5 yes
C52 H52B Cl1 . 0.98 2.81 3.439(4) 122.5 yes
C52 H52B Se2 . 0.98 2.97 3.507(4) 115.6 yes
C62 H62B Se2 . 0.98 2.91 3.456(4) 116.2 yes
C62 H62C Cl1 . 0.98 2.82 3.552(4) 131.7 yes
C63 H63A Se1 4_575 0.98 3.05 3.948(4) 153.2 yes
C63 H63A Pd1 4_575 0.98 2.87 3.793(4) 157.5 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Cl1 Pd1 Se1 P1 . . . . -115.18(3) ?
Cl2 Pd1 Se1 P1 . . . . 70.19(3) ?
Cl1 Pd1 Se2 P2 . . . . 20.17(3) ?
Cl2 Pd1 Se2 P2 . . . . -165.29(3) ?
Pd1 Se1 P1 C3 . . . . -74.49(10) ?
Pd1 Se1 P1 C2 . . . . 43.37(10) ?
Pd1 Se1 P1 C1 . . . . 164.54(9) ?
Pd1 Se2 P2 C5 . . . . -53.52(13) ?
Pd1 Se2 P2 C6 . . . . 68.63(12) ?
Pd1 Se2 P2 C4 . . . . -171.93(11) ?
C3 P1 C1 C11 . . . . 169.5(2) ?
C2 P1 C1 C11 . . . . 47.7(2) ?
Se1 P1 C1 C11 . . . . -72.4(2) ?
C3 P1 C1 C13 . . . . 47.0(3) ?
C2 P1 C1 C13 . . . . -74.7(2) ?
Se1 P1 C1 C13 . . . . 165.09(19) ?
C3 P1 C1 C12 . . . . -72.8(2) ?
C2 P1 C1 C12 . . . . 165.5(2) ?
Se1 P1 C1 C12 . . . . 45.3(2) ?
C3 P1 C2 C21 . . . . 158.0(2) ?
C1 P1 C2 C21 . . . . -76.8(2) ?
Se1 P1 C2 C21 . . . . 38.8(2) ?
C3 P1 C2 C22 . . . . 39.5(2) ?
C1 P1 C2 C22 . . . . 164.73(19) ?
Se1 P1 C2 C22 . . . . -79.7(2) ?
C3 P1 C2 C23 . . . . -81.1(2) ?
C1 P1 C2 C23 . . . . 44.2(2) ?
Se1 P1 C2 C23 . . . . 159.75(18) ?
C2 P1 C3 C31 . . . . -175.8(2) ?
C1 P1 C3 C31 . . . . 59.3(3) ?
Se1 P1 C3 C31 . . . . -55.4(2) ?
C2 P1 C3 C32 . . . . 54.2(3) ?
C1 P1 C3 C32 . . . . -70.6(3) ?
Se1 P1 C3 C32 . . . . 174.7(2) ?
C5 P2 C4 C41 . . . . -45.7(3) ?
C6 P2 C4 C41 . . . . -167.4(2) ?
Se2 P2 C4 C41 . . . . 74.9(2) ?
C5 P2 C4 C43 . . . . -163.9(2) ?
C6 P2 C4 C43 . . . . 74.4(3) ?
Se2 P2 C4 C43 . . . . -43.3(3) ?
C5 P2 C4 C42 . . . . 74.4(3) ?
C6 P2 C4 C42 . . . . -47.3(3) ?
Se2 P2 C4 C42 . . . . -165.0(2) ?
C6 P2 C5 C52 . . . . -154.2(3) ?
C4 P2 C5 C52 . . . . 82.4(3) ?
Se2 P2 C5 C52 . . . . -31.8(3) ?
C6 P2 C5 C51 . . . . 76.6(3) ?
C4 P2 C5 C51 . . . . -46.9(3) ?
Se2 P2 C5 C51 . . . . -161.0(2) ?
C5 P2 C6 C61 . . . . -43.2(3) ?
C4 P2 C6 C61 . . . . 78.9(3) ?
Se2 P2 C6 C61 . . . . -167.7(2) ?
C5 P2 C6 C62 . . . . 77.6(3) ?
C4 P2 C6 C62 . . . . -160.2(2) ?
Se2 P2 C6 C62 . . . . -46.8(3) ?
C5 P2 C6 C63 . . . . -165.2(2) ?
C4 P2 C6 C63 . . . . -43.1(3) ?
Se2 P2 C6 C63 . . . . 70.4(3) ?