#------------------------------------------------------------------------------ #$Date: 2025-02-05 05:03:59 +0200 (Wed, 05 Feb 2025) $ #$Revision: 297594 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/33/2023373.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023373 loop_ _publ_author_name 'Upmann, Daniel' 'Jones, Peter G.' _publ_section_title ; Crystal structures of six complexes of phosphane chalcogenides R 1 R 2 R 3PE (R = tert-butyl or isopropyl, E = S or Se) with the metal halides MX 2 (M = Pd or Pt, X = Cl or Br), two halochalcogenylphosphonium derivatives ( t Bu2 iPrPEBr)2[Pd2Br6] and one hydrolysis product ; _journal_coeditor_code YZ2063 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989025000805 _journal_volume 81 _journal_year 2025 _chemical_formula_iupac '[Pd Cl2 (C11 H25 P1 Se1)2]' _chemical_formula_moiety 'C22 H50 Cl2 P2 Pd Se2' _chemical_formula_sum 'C22 H50 Cl2 P2 Pd Se2' _chemical_formula_weight 711.78 _chemical_name_systematic ; (Di-tert-butylisopropylphosphine selenide-\kSe)dichloridopalladium(II) ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL2019/3 _cell_angle_alpha 90 _cell_angle_beta 117.306(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 15.3744(4) _cell_length_b 13.2969(2) _cell_length_c 16.0503(3) _cell_measurement_reflns_used 15039 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 30.8273 _cell_measurement_theta_min 2.1330 _cell_volume 2915.57(13) _computing_cell_refinement ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2012) ; _computing_data_collection ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2012) ; _computing_data_reduction ; CrysAlisPro, Version 1.171.35.11 (Rigaku OD, 2012) ; _computing_molecular_graphics ; Bruker XP, Version 5.1 (Bruker, 1998) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL2019/3 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS-97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 16.1419 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Oxford Diffraction Xcalibur, Eos' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0912 _diffrn_reflns_av_unetI/netI 0.0340 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 134870 _diffrn_reflns_theta_full 28.000 _diffrn_reflns_theta_max 28.281 _diffrn_reflns_theta_min 2.137 _diffrn_source 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 3.435 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.71342 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2012) ; _exptl_crystal_colour 'dichroic red orange' _exptl_crystal_density_diffrn 1.622 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 1440 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.020 _refine_diff_density_max 1.353 _refine_diff_density_min -0.783 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 278 _refine_ls_number_reflns 7231 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.041 _refine_ls_R_factor_all 0.0477 _refine_ls_R_factor_gt 0.0321 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0234P)^2^+4.2293P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0629 _refine_ls_wR_factor_ref 0.0679 _reflns_number_gt 5841 _reflns_number_total 7231 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yz2063.cif _cod_data_source_block 2 _cod_original_cell_volume 2915.56(12) _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2023373 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.547 _shelx_estimated_absorpt_t_max 0.934 _shelx_hkl_file ; 0 0 2 37295.2 506.422 0 0 -2 37558.8 614.638 0 0 2 38720.5 651.102 0 0 -2 37235.1 569.764 0 0 -2 37313.2 491.838 0 0 -2 38035.5 642.145 0 0 2 39321.6 656.043 0 0 2 38860.1 655.377 0 0 2 39774.6 655.335 0 0 -2 37347.4 635.660 0 0 -2 37610.0 495.949 0 0 2 39137.2 574.823 0 0 -2 38277.3 567.800 0 0 -2 36848.8 472.634 0 0 -2 37955.6 485.126 0 0 2 38895.6 694.568 0 0 2 37163.0 554.059 0 0 -2 38562.7 656.747 0 0 -2 38927.0 694.518 0 0 2 37943.5 490.801 0 0 2 36604.7 606.077 0 0 -3 22.4153 51.9291 0 0 -3-7.56973 100.462 0 0 -3 14.9720 74.5621 0 0 3 76.9514 61.5440 0 0 3 3.56961 72.8972 0 0 3-20.2070 92.3393 0 0 -3 34.5686 53.0713 0 0 -3 19.4358 47.9904 0 0 3-52.9719 82.1302 0 0 3 73.4552 102.898 0 0 3 56.2460 43.9045 0 0 -3 36.5587 62.8852 0 0 3 107.086 84.9680 0 0 -3 46.5716 61.7577 0 0 3 10.3779 47.7134 0 0 -3-37.2065 90.0377 0 0 3 140.412 98.0027 0 0 -3-18.0897 53.0899 0 0 3-172.878 110.320 0 0 -3-1.01821 51.1283 0 0 3-58.7416 67.4159 0 0 3 32.1312 72.6693 0 0 -3-38.4722 76.5012 0 0 3-46.9867 62.2300 0 0 3-19.5189 45.4804 0 0 4-27.8938 86.1445 0 0 -4 12.4249 89.1744 0 0 4 91.1829 55.7868 0 0 -4 50.0963 64.1477 0 0 -4 10.0609 77.8342 0 0 -4 68.2026 64.6096 0 0 -4 57.2043 64.5177 0 0 4 220.754 98.3236 0 0 -4 12.6528 59.0120 0 0 4-51.1258 95.6927 0 0 4 27.4736 110.837 0 0 4 44.4953 87.8907 0 0 4 55.9447 60.6038 0 0 4 56.6259 72.6846 0 0 -4 94.1776 62.1977 0 0 4 18.4122 78.4417 0 0 -4 23.0054 100.657 0 0 4-3.55685 139.206 0 0 4 162.912 103.053 0 0 -4 100.078 95.2396 0 0 4 125.119 89.7525 0 0 -4 64.0456 109.299 0 0 -4 35.8608 53.9843 0 0 4 83.6803 73.0232 0 0 4 70.8867 112.630 0 0 4 32.0866 115.210 0 0 5 20.2379 106.528 0 0 -5-42.8881 60.8053 0 0 -5 108.371 87.2278 0 0 -5 69.6843 113.276 0 0 -5-71.6325 75.2648 0 0 -5-28.2714 67.3484 0 0 -5 32.7058 80.3546 0 0 5 68.9174 70.4723 0 0 -5 30.0862 119.933 0 0 5 56.5126 67.1705 0 0 5-24.7390 74.2599 0 0 5 45.9873 119.802 0 0 5 151.400 89.7196 0 0 5 37.5033 97.3449 0 0 -5-13.9580 69.9008 0 0 -5-25.0083 117.107 0 0 5-7.14398 141.498 0 0 -5-3.12727 72.4656 0 0 -5-23.4235 48.4898 0 0 -6 44512.0 1216.40 0 0 6 46761.7 1115.21 0 0 6 43944.3 868.905 0 0 -6 44142.8 1179.07 0 0 -6 43110.8 880.315 0 0 6 45603.7 1325.85 0 0 6 45896.8 1268.53 0 0 6 45577.6 945.764 0 0 -6 43233.5 936.087 0 0 -6 46295.3 1247.88 0 0 -6 43444.5 886.109 0 0 6 47218.7 966.604 0 0 6 45406.1 865.436 0 0 6 43153.0 872.928 0 0 -6 44437.7 633.559 0 0 -6 41997.5 915.482 0 0 -6 45914.9 1062.26 0 0 -6 44401.5 827.453 0 0 6 47007.0 1089.67 0 0 -7-26.3815 101.786 0 0 7-117.523 185.730 0 0 7 39.5388 78.5985 0 0 7 170.386 134.522 0 0 -7 22.2697 86.0050 0 0 -7-60.0557 81.3175 0 0 -7-6.68770 175.502 0 0 7-21.5227 82.4554 0 0 -7-104.896 155.953 0 0 7-48.3590 90.8537 0 0 -7 32.4304 71.7413 0 0 -7-32.6446 44.7521 0 0 7-97.9877 148.389 0 0 7 71.1031 74.8847 0 0 7-14.6203 94.9846 0 0 7-6.78499 81.4529 0 0 -7 102.085 152.210 0 0 -7-19.6002 71.8582 0 0 -8 64953.9 1308.70 0 0 -8 64762.8 1242.50 0 0 -8 65505.0 1307.60 0 0 8 64403.9 1301.97 0 0 8 65725.0 1246.40 0 0 -8 69441.3 1785.17 0 0 8 66339.0 1179.77 0 0 8 66576.6 1550.79 0 0 -8 66467.4 1738.39 0 0 -8 64585.8 1662.38 0 0 -8 63473.7 842.412 0 0 8 63508.6 1179.30 0 0 8 66266.4 1521.41 0 0 8 68275.9 1902.48 0 0 8 68767.0 1810.75 0 0 -8 63782.0 1232.63 0 0 9 37.3949 114.893 0 0 9 151.813 106.949 0 0 9 48.4734 134.350 0 0 -9 132.948 126.873 0 0 -9 103.389 61.1592 0 0 -9-80.2457 224.109 0 0 9 0.62316 71.0155 0 0 -9-109.101 218.229 0 0 -9 172.836 126.247 0 0 9 194.506 231.174 0 0 9-71.6046 214.121 0 0 9 56.1788 78.6329 0 0 9 127.440 147.209 0 0 -9-124.571 160.308 0 0 10 32131.1 906.040 0 0 -10 35612.4 1087.74 0 0 10 34482.5 925.532 0 0 10 35605.4 1023.96 0 0 -10 34067.0 1358.29 0 0 -10 36008.3 1085.30 0 0 10 32786.5 927.102 0 0 -10 37025.3 1477.25 0 0 10 35470.8 1558.68 0 0 -10 36519.0 1474.33 0 0 10 36401.0 1274.39 0 0 10 35055.9 1474.65 0 0 10 37075.8 1326.50 0 0 10 35314.5 1067.82 0 0 11 199.909 246.456 0 0 11-7.91996 155.230 0 0 11 61.3855 108.771 0 0 -11-70.8898 164.048 0 0 11-95.4403 114.987 0 0 11 198.106 176.735 0 0 11-209.553 126.177 0 0 -11 40.8963 47.0723 0 0 -11 214.213 254.030 0 0 -11-14.7744 111.121 0 0 -11 146.772 220.971 0 0 -11-25.8838 115.163 0 0 11 123.166 242.255 0 0 11 55.0346 103.128 0 0 11 73.9760 86.9803 0 0 12 118.992 198.510 0 0 12 34.2739 121.510 0 0 12-362.997 328.420 0 0 12-65.6730 141.794 0 0 12 202.755 137.776 0 0 -12-80.8339 194.450 0 0 12 47.9632 163.951 0 0 -12-131.983 181.413 0 0 -12-123.096 171.494 0 0 12-132.283 124.882 0 0 -12 112.205 233.049 0 0 12-460.019 305.365 0 0 -12-18.0071 128.400 0 0 13-131.940 118.300 0 0 13-247.433 301.184 0 0 -13 129.757 189.394 0 0 13 321.088 139.392 0 0 13 149.259 184.872 0 0 -13 215.602 243.863 0 0 13 367.110 338.621 0 0 13-129.052 145.170 0 0 -13 173.745 132.403 0 0 -13 215.646 171.259 0 0 -13 22.7438 217.314 0 0 14 4143.00 690.634 0 0 -14 5924.63 763.405 0 0 -14 5438.53 721.527 0 0 14 4232.99 661.816 0 0 14 6824.08 680.824 0 0 -14 4165.45 594.380 0 0 14 5274.43 632.269 0 0 15-283.734 284.649 0 0 -15 209.531 234.643 0 0 15-130.617 362.913 0 0 15 407.266 242.318 0 0 -15-41.3850 302.454 0 0 -15-115.696 212.502 0 0 15-32.1798 277.918 0 0 -16 3160.18 643.780 0 0 16 3793.35 749.155 0 0 -16 4779.17 758.667 0 0 16 3635.20 574.878 0 0 16 3348.12 658.305 0 0 17-50.5425 333.349 0 0 -17-64.9484 233.512 0 0 17-389.896 383.474 0 0 -17-293.486 303.882 0 0 18 1539.89 552.115 0 0 18 919.479 472.690 0 0 -18 711.264 376.480 0 0 -18 496.994 354.359 0 0 -19 131.154 269.228 0 0 -19 510.806 336.681 0 0 19 248.261 373.188 0 0 19-245.447 396.606 0 -1 2 168291. 1455.65 0 1 -2 166971. 1438.03 0 1 2 167901. 1399.63 0 1 2 169463. 1378.79 0 1 -2 163946. 1163.15 0 -1 -2 162073. 1188.43 0 -1 2 165940. 1128.19 0 1 2 172352. 1442.62 0 1 2 168130. 1337.01 0 -1 -2 170978. 1372.38 0 1 -2 173260. 1387.13 0 -1 2 169580. 1373.13 0 1 2 162455. 1276.15 0 1 -2 165781. 1101.04 0 1 -2 171194. 1295.74 0 -1 -2 164241. 1205.05 0 -1 -2 161919. 1524.08 0 -1 -2 169737. 1242.27 0 -1 -2 170672. 1438.27 0 -1 2 168908. 1337.27 0 1 -2 163873. 1622.80 0 -1 2 169981. 1637.42 0 -1 2 167147. 1300.08 0 1 2 173633. 1185.32 0 -1 2 169755. 1477.76 0 1 -2 170842. 1492.22 0 -1 2 171199. 1174.38 0 -1 2 170197. 1458.22 0 -1 -2 168783. 1244.04 0 1 2 167656. 1186.24 0 1 2 170210. 1248.29 0 1 2 171217. 1241.47 0 1 -2 168175. 1163.79 0 -1 -2 166538. 1386.90 0 -1 -2 167292. 1342.99 0 1 2 161374. 1277.08 0 1 -2 169801. 1452.97 0 1 -2 170401. 1222.53 0 -1 -2 172824. 1286.59 0 1 2 169378. 1229.53 0 -1 -2 169893. 1268.02 0 1 -2 169545. 1332.26 0 -1 2 169196. 1192.35 0 -1 2 171021. 1369.78 0 -1 2 169893. 1167.01 0 -1 -3 698.271 132.329 0 1 3 689.264 98.3871 0 1 3 536.885 124.896 0 1 3 614.237 104.721 0 -1 3 670.398 128.807 0 -1 -3 775.415 138.645 0 -1 -3 727.881 128.764 0 1 -3 554.309 126.412 0 -1 -3 749.542 132.883 0 -1 3 590.538 86.1402 0 -1 3 620.764 116.283 0 1 -3 682.414 151.066 0 1 -3 762.336 107.459 0 -1 3 704.683 87.1185 0 1 3 568.596 100.497 0 -1 3 548.757 91.7384 0 1 3 683.987 94.9594 0 1 -3 686.547 137.592 0 -1 3 619.455 125.328 0 1 3 760.345 90.7652 0 -1 3 588.384 74.6208 0 -1 3 783.451 103.913 0 -1 3 913.825 149.156 0 -1 -3 666.132 81.1524 0 1 3 620.066 145.654 0 1 -3 604.445 82.6667 0 1 -3 711.215 91.1671 0 -1 3 651.567 125.712 0 1 -3 716.330 105.905 0 1 -3 480.248 101.282 0 -1 -3 670.015 135.854 0 1 -3 551.176 154.259 0 -1 -3 646.749 102.523 0 -1 3 722.836 105.489 0 -1 3 704.583 159.794 0 -1 -3 557.278 97.1393 0 -1 3 575.683 120.312 0 1 3 686.727 124.491 0 -1 -3 796.878 134.266 0 1 3 647.958 103.385 0 -1 -3 619.909 119.280 0 1 3 710.013 113.241 0 1 3 584.931 134.218 0 1 -3 489.637 136.843 0 -1 -3 676.029 94.7990 0 1 -3 601.422 120.037 0 -1 -3 619.003 102.780 0 1 3 837.768 134.280 0 1 -3 601.255 100.861 0 -1 3 738.104 143.661 0 1 3 768.074 127.593 0 -1 3 702.645 133.304 0 1 4 152753. 1472.70 0 -1 -4 154456. 1328.61 0 1 4 153351. 1339.93 0 1 4 144341. 1944.88 0 -1 -4 156616. 1852.29 0 1 4 162137. 1824.46 0 1 -4 154477. 1450.52 0 -1 -4 152923. 1485.82 0 -1 -4 154000. 1776.52 0 -1 -4 149371. 1348.38 0 -1 -4 152185. 1652.41 0 1 4 159770. 1819.29 0 -1 4 150693. 1401.24 0 -1 4 154475. 1823.16 0 1 -4 155871. 1907.48 0 1 4 154130. 1374.50 0 -1 4 153386. 1165.15 0 -1 4 158039. 1883.66 0 -1 -4 150351. 1752.15 0 1 4 154696. 1352.78 0 -1 -4 147528. 1958.18 0 1 -4 148641. 1268.37 0 -1 -4 153456. 1483.27 0 -1 -4 154258. 1766.72 0 1 4 154634. 1923.62 0 -1 4 154715. 1525.35 0 1 -4 159162. 1838.94 0 -1 4 153932. 1841.82 0 1 -4 152500. 1291.03 0 1 4 155606. 1865.37 0 -1 4 153577. 1615.68 0 -1 4 152367. 1275.68 0 1 4 161571. 1824.79 0 1 -4 150181. 1492.85 0 -1 -4 154396. 1367.14 0 1 -4 156380. 1826.74 0 -1 4 151232. 1441.35 0 1 4 152393. 1728.29 0 1 -4 150134. 1792.33 0 -1 4 151313. 1414.38 0 1 -4 149977. 2009.02 0 1 -4 154501. 1902.32 0 1 -4 157779. 1797.47 0 1 -4 157162. 1614.81 0 1 4 151063. 1473.48 0 -1 4 151001. 1256.67 0 -1 4 148315. 1811.60 0 -1 4 155534. 1794.77 0 -1 4 160410. 1940.11 0 -1 4 158382. 2059.37 0 1 4 156300. 1686.28 0 1 -4 153187. 1314.34 0 -1 -4 150621. 1761.66 0 -1 4 159968. 1934.41 0 1 -5 2218.35 179.787 0 -1 -5 2466.69 213.690 0 1 5 2650.72 306.966 0 1 -5 2541.53 193.263 0 1 5 2347.26 164.246 0 1 5 2202.25 186.118 0 1 -5 2095.22 287.102 0 1 -5 2581.77 278.841 0 1 5 2269.33 214.342 0 1 -5 2311.83 213.424 0 -1 5 2313.25 183.375 0 1 5 2252.00 203.299 0 -1 5 2337.83 204.633 0 1 5 2465.81 247.136 0 -1 -5 2071.26 191.600 0 1 -5 2432.74 184.753 0 -1 5 2083.45 264.507 0 -1 5 2275.96 226.137 0 1 -5 2289.00 223.537 0 -1 5 2374.75 201.346 0 1 -5 2575.86 297.622 0 1 5 2385.41 271.527 0 -1 -5 2233.89 274.554 0 -1 5 3072.77 316.164 0 -1 -5 2390.28 262.682 0 -1 5 2443.50 202.731 0 -1 -5 2325.03 193.408 0 -1 5 2190.18 222.991 0 1 -5 2534.69 229.643 0 -1 -5 1998.57 222.320 0 1 -5 2544.85 269.060 0 1 5 2364.42 316.843 0 -1 5 2486.36 192.507 0 1 5 2427.10 217.090 0 1 -5 2354.75 284.247 0 -1 5 2186.99 152.709 0 -1 -5 2360.43 211.406 0 -1 -5 1752.20 241.429 0 1 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359.430 7 -11 7-150.698 300.960 7 -11 7-90.2016 369.753 7 11 7 486.416 315.049 7 -11 7 103.743 223.015 -7 11 -7 267.032 260.274 -7 11 -7 563.038 385.983 -7 11 -7 569.888 385.644 7 11 7 408.264 372.036 7 11 7 1100.85 535.010 7 -11 7 500.665 473.669 -7 11 -7 175.922 291.998 -7 -11 -7 127.251 273.130 7 11 7 19.0626 314.789 -7 -11 -8 585.419 409.585 -7 11 -8 229.429 287.351 -7 -11 -8 837.289 404.817 7 -11 8 553.502 411.069 7 11 8 476.702 321.195 7 -11 8 265.051 225.271 -7 11 -8 1350.50 477.958 -7 11 -8 149.304 348.106 7 11 8 542.402 482.558 7 -11 8-349.562 383.968 7 -11 8 456.953 350.533 -7 11 -8 40.8807 316.157 7 11 8 584.810 447.583 7 11 8 1146.97 490.719 7 11 8 306.277 418.353 -7 -11 -9 670.114 411.838 -7 11 -9-124.910 271.810 7 -11 9 666.034 398.156 7 -11 9 232.012 470.288 7 11 9 72.1501 331.094 -7 11 -9 280.757 314.523 -7 11 -9 441.527 314.181 -7 -11 -9 435.784 397.305 7 11 9 77.6919 357.039 7 -11 9-307.146 403.084 -7 11 -9 64.6531 309.188 7 11 9-397.656 362.109 7 11 9-244.570 426.291 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7 -6 554.266 241.136 -10 7 6 272.063 235.003 10 -7 -6 961.271 317.034 10 7 -6 286.416 255.967 10 -7 -6 539.362 285.909 10 -7 -6 571.128 301.506 -10 7 6 472.727 282.326 10 7 -6 918.190 325.705 10 7 -6 514.802 266.076 10 7 -6 1021.90 310.081 -10 -7 6 753.980 301.135 10 7 -6 524.735 254.181 -10 -7 6 286.188 245.977 -10 -7 5 1232.88 365.677 10 -7 -5 1281.25 403.891 -10 -7 5 1135.18 302.256 10 -7 -5 1458.22 349.515 -10 7 5 1304.82 390.766 10 -7 -5 510.398 280.423 -10 -7 5 1025.14 225.873 10 -7 -5 1330.07 285.682 10 7 -5 335.304 238.926 10 7 -5 1173.71 297.911 10 7 -5 1012.12 267.103 -10 7 5 1422.05 415.049 10 -7 -5 816.751 297.632 10 7 -5 1557.68 488.803 10 7 -5 1354.66 299.767 -10 7 5 1163.94 381.465 10 -7 -5 818.077 272.908 10 7 -5 486.165 247.477 10 -7 -5 719.404 327.415 10 -7 -5 632.846 277.996 10 -7 -5 926.376 381.285 10 7 -5 1631.68 383.097 10 7 -5 1122.95 341.531 10 7 -5 1479.95 358.625 -10 -7 5 897.816 293.602 -10 -7 4 1495.25 391.189 10 7 -4 1851.22 320.829 10 -7 -4 1713.79 369.429 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280.959 -10 7 3 279.194 263.626 10 7 -3 467.201 239.114 -10 -7 3 610.671 265.362 -10 -7 2 2340.72 469.521 10 7 -2 2177.34 334.274 10 -7 -2 2540.73 492.955 -10 -7 2 2501.44 407.719 10 -7 -2 2235.39 374.377 -10 7 2 2545.16 514.759 -10 -7 2 1931.25 409.415 10 -7 -2 2725.56 487.358 10 7 -2 2741.48 480.762 10 -7 -2 2428.71 411.136 10 7 -2 2625.15 417.592 10 -7 -2 1981.68 455.186 10 7 -2 2210.54 340.273 -10 7 2 2259.68 443.970 10 7 -2 2251.77 446.076 10 7 -2 3303.42 537.709 10 -7 -2 1834.69 323.323 10 -7 -2 1745.24 450.225 10 7 -2 2519.78 435.047 10 7 -2 1850.38 450.759 -10 7 2 1907.74 464.181 10 7 -2 1795.97 420.963 -10 -7 2 2324.93 402.362 -10 -7 1 1710.32 426.227 10 7 -1 2483.28 347.082 -10 -7 1 2617.98 428.904 10 -7 -1 2583.77 365.817 -10 7 1 2222.09 470.320 10 -7 -1 1966.17 388.247 10 7 -1 2107.94 387.151 10 -7 -1 1824.10 457.742 10 7 -1 2862.85 382.695 -10 7 1 2379.19 457.711 10 7 -1 1909.83 411.533 10 7 -1 1919.06 441.741 10 -7 -1 1817.16 326.739 10 -7 -1 3000.59 602.369 10 7 -1 1876.25 395.153 10 -7 -1 2566.10 522.905 10 7 -1 1923.78 443.457 10 7 -1 2101.89 445.799 -10 7 1 2788.62 554.635 -10 -7 1 1586.20 321.260 -10 7 0 8920.31 896.432 10 -7 0 8873.38 637.316 10 -7 0 9770.09 842.898 10 -7 0 8736.23 988.475 10 7 0 8440.53 765.889 10 7 0 9969.96 925.408 -10 7 0 10028.3 846.757 10 7 0 7850.31 618.229 10 -7 0 8112.35 822.490 -10 7 0 8755.11 837.661 10 -7 0 8599.09 623.438 -10 -7 0 10297.6 873.353 10 -7 0 8576.28 943.322 10 7 0 8650.42 767.113 -10 7 0 8905.24 903.672 10 -7 0 8265.16 865.904 10 7 0 8325.74 864.160 10 7 0 8295.51 895.928 -10 -7 0 8709.48 684.162 10 7 0 7045.95 814.644 -10 -7 0 9069.04 837.850 10 7 0 8541.02 624.196 -10 -7 -1 1098.02 322.161 -10 7 -1 1208.29 404.759 10 7 1 1645.53 302.584 -10 7 -1 1081.79 409.230 10 -7 1 1361.21 270.601 10 -7 1 1409.93 351.849 -10 -7 -1 1581.68 377.563 10 -7 1 889.759 335.832 10 -7 1 1123.53 483.831 10 7 1 1353.32 379.751 -10 7 -1 1730.51 425.644 10 -7 1 937.336 380.227 -10 7 -1 1460.25 377.435 10 7 1 977.101 391.091 10 7 1 836.982 358.755 10 -7 1 1445.22 436.941 10 -7 1 1021.39 226.578 10 7 1 1107.49 309.372 10 -7 1 1332.09 406.532 10 7 1 746.193 378.756 10 7 1 1204.53 367.845 -10 -7 -1 832.490 229.799 -10 -7 -1 722.890 249.831 -10 -7 -2 1967.86 414.194 -10 7 -2 2244.79 503.940 -10 7 -2 1833.64 439.495 10 -7 2 2255.79 412.698 -10 -7 -2 2014.86 432.803 10 -7 2 1306.99 424.576 10 -7 2 1869.29 373.123 10 -7 2 1363.03 455.370 10 7 2 1715.02 439.568 10 7 2 1219.35 402.289 -10 -7 -2 2049.97 358.744 -10 7 -2 1711.95 385.443 10 -7 2 2189.35 482.789 -10 7 -2 1955.26 405.718 10 7 2 2165.96 516.447 10 7 2 2071.24 495.953 10 -7 2 2036.14 527.266 -10 -7 -2 1977.08 353.721 10 7 2 1951.34 372.589 10 -7 2 1744.34 479.080 10 7 2 2691.33 591.994 -10 -7 -2 1895.92 445.764 -10 -7 -3-70.0167 201.026 -10 7 -3 159.193 223.685 -10 7 -3 294.720 268.386 10 -7 3 203.990 230.767 -10 -7 -3-223.263 239.349 10 -7 3-168.542 314.355 10 -7 3 100.150 194.218 10 -7 3 250.658 400.255 10 7 3 76.3740 316.428 -10 -7 -3 129.420 206.341 -10 7 -3 399.403 295.689 10 -7 3-267.865 330.010 -10 7 -3-13.4432 200.618 10 7 3 326.649 322.980 10 -7 3-12.6679 272.856 -10 -7 -3-184.353 205.779 10 7 3 371.075 203.780 10 -7 3 367.108 342.836 10 7 3-174.017 295.231 10 7 3 19.4935 290.908 -10 -7 -3 5.62656 188.780 10 -7 4-184.217 314.948 -10 7 -4-50.3130 261.888 10 -7 4 316.121 208.281 -10 -7 -4-265.649 237.158 10 -7 4 477.650 289.051 10 -7 4-144.554 221.722 10 -7 4-41.1307 360.502 10 7 4 247.332 310.232 -10 7 -4 386.485 207.660 10 -7 4-131.440 281.031 10 7 4-313.331 293.977 10 -7 4 344.540 309.036 10 7 4 396.878 219.191 -10 7 -4 225.290 284.203 10 7 4 137.332 359.497 10 7 4 119.451 293.239 -10 -7 -4 750.008 363.246 10 7 5 1935.45 507.361 -10 7 -5 1423.17 445.811 -10 7 -5 1806.03 487.507 -10 -7 -5 1558.74 392.500 10 -7 5 1611.24 454.102 10 -7 5 1088.17 347.257 10 -7 5 1044.77 517.949 10 7 5 1525.57 472.184 -10 7 -5 1740.11 529.008 -10 7 -5 1560.12 378.381 10 -7 5 1763.47 483.779 10 7 5 1300.98 446.268 10 -7 5 908.879 445.870 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289.601 -10 -8 19-459.041 349.982 -10 -8 19 526.791 458.981 10 -8 -19-56.2265 304.256 10 -8 -19 103.066 335.026 10 8 -19 139.731 286.337 10 8 -19 845.977 454.806 -10 8 19 131.554 253.367 10 8 -19 287.124 273.650 -10 -8 19 198.337 316.919 10 -8 -19-1174.56 498.341 -10 8 19-378.375 462.627 10 8 -19 780.395 395.876 10 -8 -19 632.133 428.128 -10 8 19-483.164 341.916 -10 -8 18-119.391 339.608 -10 -8 18 244.687 332.067 10 -8 -18 449.735 400.201 10 -8 -18 455.043 382.755 10 8 -18 53.1522 296.256 10 8 -18 123.866 333.094 -10 8 18 365.843 285.527 10 8 -18 85.0546 308.179 -10 -8 18-213.971 379.842 10 -8 -18 655.671 347.594 -10 8 18-350.356 367.026 10 8 -18 442.868 347.656 10 -8 -18 723.237 433.779 -10 8 18 86.3688 259.166 -10 -8 17-74.1901 291.545 -10 -8 17 131.149 254.634 10 -8 -17-70.4989 277.044 10 -8 -17 588.642 403.330 10 8 -17 505.855 367.100 10 8 -17 681.912 491.772 -10 8 17 99.7212 389.085 10 8 -17 676.920 324.404 -10 -8 17 129.905 263.719 10 -8 -17 917.108 410.719 10 8 -17 172.921 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370.983 -10 -12 -3 114.257 345.437 -10 -12 -3-275.058 244.749 -10 -12 -3 258.473 389.340 10 -12 3-176.656 257.722 10 -12 3-635.834 396.981 -10 12 -3 146.241 277.214 10 -12 3 514.531 335.501 -10 12 -3 204.734 386.719 -10 12 -3 349.240 418.534 -10 12 -3 521.705 385.779 10 12 3-310.172 414.660 10 -12 3-358.439 373.125 -10 12 -3 127.203 301.568 10 12 3-125.467 297.480 10 12 3-183.019 374.411 -10 -12 -4 180.167 309.295 -10 12 -4 48.0033 295.762 -10 -12 -4 50.5373 319.944 10 -12 4 48.6287 296.668 10 -12 4 174.136 324.259 -10 12 -4-339.563 342.474 -10 12 -4-428.910 417.563 10 12 4-175.633 483.151 10 -12 4-405.571 468.268 -10 12 -4 615.205 370.800 10 12 4 282.078 401.115 10 12 4 599.759 378.185 10 12 4 81.2680 344.877 -10 -12 -5 491.678 429.985 10 -12 5 627.974 371.757 10 -12 5 624.329 385.816 -10 12 -5 367.549 321.059 -10 12 -5 322.343 297.162 10 12 5 635.579 570.602 10 -12 5 602.202 431.110 -10 12 -5-13.5696 333.802 -10 12 -5 209.750 320.306 10 12 5-193.763 424.478 10 12 5 608.055 426.446 10 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4598.69 846.517 -11 -8 -8 4632.72 857.693 11 -8 8 3097.70 716.511 11 8 8 3877.44 870.480 11 8 8 3777.24 811.625 -11 8 -9 83.6703 283.305 11 8 9 287.927 437.604 11 -8 9 389.666 388.504 11 8 9 521.315 397.806 11 -8 10 1305.18 429.726 11 -9 -20-851.996 456.147 -11 9 20-780.952 419.010 -11 -9 19-123.438 275.818 11 -9 -19 167.469 325.062 11 9 -19-137.764 303.078 -11 9 19-50.4211 310.199 -11 9 19 322.103 341.638 -11 -9 18 597.065 425.252 -11 -9 18 1368.20 515.233 11 -9 -18 913.901 510.736 11 -9 -18 718.835 469.558 11 9 -18 460.329 368.691 11 9 -18 500.644 397.787 11 9 -18 393.804 405.020 -11 9 18 361.413 323.931 -11 -9 18 625.636 405.280 11 -9 -18 410.638 386.079 -11 9 18 953.076 460.241 11 -9 -18 731.129 437.063 -11 9 18 1881.79 581.972 -11 -9 17-6.45014 265.953 -11 -9 17 1879.14 545.861 11 -9 -17 100.346 330.375 11 -9 -17 942.492 469.660 11 9 -17 1560.72 501.964 11 9 -17 1105.67 538.307 11 9 -17 1529.46 648.688 -11 9 17 635.738 384.062 -11 -9 17 1148.42 491.702 11 -9 -17 881.801 452.906 11 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970.035 417.805 11 -9 -12 996.694 370.480 11 9 -12 853.470 331.028 -11 9 12 1006.73 452.811 11 -9 -12 320.117 348.908 11 9 -12 530.027 299.053 -11 9 12 391.179 225.341 -11 9 12 321.538 226.255 -11 -9 12 306.270 263.216 -11 -9 11 323.146 340.048 11 -9 -11 36.4167 265.381 -11 9 11 46.3802 206.192 11 -9 -11-821.030 370.490 11 -9 -11 87.1412 264.709 11 -9 -11 257.844 190.841 11 9 -11 137.435 239.790 11 9 -11 230.502 395.394 11 9 -11 300.586 231.872 -11 9 11 353.233 353.238 11 -9 -11-6.81374 268.907 11 9 -11 244.234 234.059 -11 9 11-20.3426 267.870 11 -9 -11 443.631 370.367 11 9 -11-340.366 321.745 11 9 -11 88.2996 173.285 11 9 -11 274.637 213.045 -11 -9 11 636.730 384.456 -11 -9 10 2087.60 555.227 11 9 -10 2479.53 522.277 11 -9 -10 1606.78 441.122 -11 9 10 1450.69 418.646 11 -9 -10 1010.44 362.411 11 -9 -10 2553.28 581.032 11 -9 -10 1244.76 301.489 11 9 -10 1959.27 481.458 11 9 -10 2387.51 612.337 11 9 -10 1739.90 441.025 -11 9 10 929.303 393.244 11 -9 -10 2977.23 584.225 11 9 -10 1120.18 370.953 11 -9 -10 2383.16 442.393 -11 9 10 2018.20 508.321 11 -9 -10 1367.77 490.796 11 9 -10 1944.41 391.281 11 9 -10 2015.87 378.310 -11 -9 10 1568.93 472.476 -11 -9 9 411.422 326.973 11 -9 -9 539.844 290.187 11 -9 -9 930.573 342.803 -11 9 9 805.840 326.799 11 -9 -9 1341.63 467.417 11 -9 -9 816.346 249.125 11 9 -9 659.473 345.907 -11 -9 9 910.725 257.213 11 9 -9 788.237 404.922 11 9 -9 588.812 286.154 -11 9 9 789.934 301.410 11 -9 -9 751.030 352.701 11 9 -9 807.586 309.287 11 -9 -9 341.036 210.090 11 -9 -9 1413.01 487.073 11 9 -9 1044.93 330.749 -11 9 9 878.140 367.662 11 9 -9 759.988 324.503 11 9 -9 376.317 241.675 -11 -9 9 892.006 358.025 -11 -9 8 2607.59 589.687 11 -9 -8 4285.73 662.901 11 -9 -8 4579.10 675.709 -11 9 8 4060.48 665.556 11 -9 -8 4079.53 712.699 11 -9 -8 4601.29 652.767 11 -9 -8 3636.49 446.761 11 9 -8 3653.80 613.446 -11 -9 8 4038.26 502.162 11 9 -8 3559.74 692.470 11 9 -8 3560.71 563.765 -11 9 8 4054.10 682.878 11 -9 -8 3808.21 606.427 11 9 -8 3484.12 587.576 11 -9 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537.024 11 -9 -4 3671.99 604.563 11 9 -4 2437.71 645.086 11 9 -4 2545.30 423.718 -11 9 4 2730.89 556.437 11 9 -4 3152.55 548.545 11 -9 -4 3503.05 530.643 11 -9 -4 3066.47 573.536 11 -9 -4 2940.20 557.178 11 9 -4 2650.07 504.224 11 9 -4 2654.12 556.956 -11 9 4 4016.56 642.773 11 9 -4 2777.02 555.289 -11 -9 4 2042.47 425.033 11 9 -4 3091.50 437.004 -11 -9 3-136.854 300.284 11 -9 -3 245.016 231.264 -11 9 3 95.1446 299.499 -11 -9 3-51.0083 267.648 11 -9 -3-94.9998 290.252 11 9 -3 198.987 253.644 11 -9 -3 432.083 278.045 11 9 -3 545.817 453.446 -11 9 3-84.9405 250.788 11 9 -3-35.2375 278.899 11 -9 -3 372.498 210.008 11 9 -3 1394.15 486.173 11 -9 -3-199.112 301.242 11 9 -3-168.692 285.200 11 9 -3 498.711 280.857 -11 9 3 93.0698 243.353 11 9 -3 317.193 327.662 -11 -9 3-130.058 274.589 11 9 -3-205.292 225.023 -11 -9 2-34.6104 239.065 -11 -9 2 54.9639 182.583 -11 9 2 284.922 273.742 11 -9 -2 194.808 206.031 11 -9 -2-14.2192 224.590 11 9 -2 748.257 418.230 11 -9 -2 186.088 278.826 -11 9 2 345.086 337.275 11 9 -2 284.781 311.002 11 9 -2 338.708 330.021 11 -9 -2-40.4190 184.625 11 -9 -2-108.982 245.386 11 9 -2 777.727 278.704 11 9 -2 471.047 288.333 11 9 -2 202.936 331.142 11 9 -2 1137.93 345.524 -11 9 2 437.721 320.566 -11 -9 2 6.74043 186.053 -11 -9 1 725.755 265.555 -11 -9 1 921.988 326.672 -11 -9 1 820.720 304.406 -11 9 1 801.632 370.031 11 -9 -1 320.491 153.643 11 -9 -1 875.411 355.029 11 -9 -1 582.294 338.308 11 9 -1 632.999 289.657 -11 9 1 733.914 376.662 -11 9 1 743.039 388.308 11 9 -1 369.929 333.024 11 -9 -1 951.557 267.224 11 -9 -1 1012.65 412.487 11 9 -1 223.401 230.907 11 9 -1 744.057 351.410 11 9 -1 613.688 357.298 11 9 -1 415.106 360.835 -11 9 1 650.087 314.955 -11 -9 0 603.586 381.386 -11 -9 0 553.006 237.003 -11 9 0 146.405 276.061 11 -9 0 829.975 383.992 11 -9 0 469.590 333.613 -11 9 0 393.810 317.843 -11 9 0 464.450 280.121 11 9 0 544.789 313.212 11 -9 0 886.658 430.968 -11 9 0 722.462 345.014 11 9 0 442.793 234.089 11 9 0 1103.91 434.649 11 9 0 1238.63 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439.845 -11 9 -6 1277.57 562.153 -11 9 -6 1549.24 502.411 11 9 6 1966.10 683.676 11 9 6 1271.41 524.948 -11 9 -7-25.6050 237.424 11 -9 7 603.385 375.538 11 -9 7-242.123 476.597 -11 -9 -7 865.717 503.152 11 9 7 96.9462 362.838 -11 9 -7 367.519 493.120 11 -9 7-465.089 305.782 11 9 7-793.715 471.023 -11 9 -7 2.34122 266.617 11 -9 7 511.719 545.271 -11 9 -7 83.3711 364.424 11 9 7-236.370 405.913 11 9 7 343.910 434.549 11 -9 8-151.865 415.686 11 9 8 104.418 378.630 11 -9 8 281.031 306.386 -11 9 -8 138.710 270.072 11 9 8 1378.06 582.130 11 9 8-44.8596 345.184 11 9 9 1283.96 535.116 -11 9 -9 1504.94 519.289 11 -9 9 492.092 298.012 11 10 -19-89.7143 349.156 -11 10 19-748.980 448.113 -11 -10 18 607.217 410.971 11 -10 -18-392.386 390.040 11 10 -18-171.975 288.916 11 10 -18 2.78870 359.029 11 10 -18 174.271 408.082 -11 10 18-563.535 381.423 -11 10 18 296.423 341.713 -11 -10 17 481.313 378.212 -11 -10 17 490.474 349.191 11 -10 -17 431.896 370.652 11 -10 -17-128.920 344.050 11 10 -17 457.011 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472.545 481.347 11 13 -7-35.0177 270.475 -11 13 7-93.1361 305.096 -11 -13 7 75.0028 281.208 11 -13 -7 639.660 293.419 11 13 -7-248.300 330.560 11 -13 -7-19.7080 296.692 -11 13 7 322.920 308.097 11 13 -7 36.8498 262.374 11 13 -7 102.923 267.989 -11 13 7 210.196 273.416 11 13 -7 61.9302 268.653 -11 -13 6-138.359 313.043 -11 -13 6 250.199 326.883 11 -13 -6 256.262 338.863 -11 13 6 327.632 294.595 -11 13 6 200.975 299.534 11 -13 -6-318.774 326.200 11 -13 -6 524.525 433.507 -11 -13 6 419.070 244.503 11 13 -6 899.409 502.089 11 13 -6-398.369 297.303 -11 13 6 270.399 359.626 -11 -13 6-64.6695 297.324 11 -13 -6 123.239 236.879 11 -13 -6 76.6596 286.033 11 13 -6 562.285 386.133 11 -13 -6 283.093 413.043 -11 13 6-304.768 321.480 11 13 -6 605.568 359.719 11 13 -6 330.238 308.759 11 13 -6 40.3118 298.802 -11 -13 5 671.178 355.729 -11 -13 5 756.073 401.773 11 -13 -5 824.854 432.831 -11 13 5 354.653 348.495 11 -13 -5 629.917 352.877 11 -13 -5 321.291 356.785 -11 13 5 1236.61 404.597 -11 -13 5 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311.476 -12 -11 14 492.085 427.820 -12 11 14-231.475 260.561 12 -11 -14 349.945 380.404 12 -11 -14 395.906 457.176 12 11 -14 296.882 268.980 12 11 -14-426.216 464.164 12 11 -14 4.36629 340.340 -12 11 14 125.519 437.414 -12 -11 14 24.7580 312.276 12 -11 -14 273.296 415.176 12 11 -14-4.52278 323.256 -12 11 14-46.9790 309.994 12 -11 -14-25.8632 280.594 12 11 -14 82.3838 349.014 -12 -11 13 276.360 329.543 -12 -11 13-36.2912 322.497 -12 11 13 347.204 265.573 12 -11 -13 4.36465 288.262 12 -11 -13 671.307 420.763 12 11 -13 386.316 260.415 12 11 -13 397.508 393.835 12 11 -13 497.204 354.543 -12 11 13 173.781 426.240 -12 -11 13 83.3940 313.164 12 -11 -13 470.531 363.847 12 11 -13 622.372 386.390 -12 11 13 280.115 278.458 12 -11 -13 1015.93 490.500 12 11 -13 201.837 306.758 -12 11 13 432.372 299.813 -12 -11 12 1257.22 504.800 -12 -11 12 656.324 408.827 12 -11 -12 761.773 320.885 -12 11 12 286.850 256.349 12 -11 -12 1197.92 463.990 12 -11 -12 22.0231 330.384 12 11 -12 512.029 313.082 12 11 -12 827.817 445.301 12 11 -12 802.140 400.770 -12 11 12 1085.99 475.444 -12 -11 12 484.254 340.473 12 -11 -12 331.000 363.406 12 11 -12 333.322 341.753 -12 11 12 146.145 298.935 12 -11 -12 471.337 314.577 12 11 -12 103.594 240.536 -12 11 12 694.098 363.174 -12 -11 11-167.508 306.834 -12 -11 11 568.064 317.549 12 -11 -11-190.517 309.334 -12 11 11 654.691 386.014 12 -11 -11 16.0087 316.187 12 -11 -11-260.059 430.392 12 11 -11-264.004 297.957 12 11 -11-296.782 348.448 12 11 -11 102.895 248.982 -12 11 11 289.666 343.416 -12 -11 11-652.319 465.659 12 -11 -11 131.013 257.648 12 11 -11 136.112 319.634 12 -11 -11 889.184 454.694 -12 11 11 289.206 322.329 12 11 -11 380.185 311.211 -12 11 11-193.553 245.571 -12 -11 10 617.492 315.214 -12 -11 10 130.595 374.415 12 -11 -10 549.427 369.925 -12 11 10 540.230 324.666 12 -11 -10 622.306 366.261 12 -11 -10 458.891 318.947 12 11 -10 817.519 348.023 12 11 -10 616.847 394.612 12 11 -10 767.449 432.904 -12 11 10 738.427 414.987 -12 11 10 311.254 242.392 12 -11 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1355.59 450.447 12 -11 -8 1346.16 429.385 12 -11 -8 898.150 437.294 -12 11 8 1505.25 471.585 12 11 -8 2516.39 542.114 12 11 -8 1270.24 406.782 12 11 -8 661.493 325.952 -12 -11 7-17.1985 239.232 -12 -11 7 111.193 318.571 12 -11 -7 550.723 365.877 -12 11 7 318.378 289.547 12 -11 -7-45.6986 247.308 12 -11 -7-81.9919 320.271 -12 -11 7 549.137 278.163 12 -11 -7 712.383 324.444 12 11 -7 610.058 348.334 12 11 -7 138.441 348.084 -12 11 7-71.1489 312.256 12 -11 -7 72.4573 254.530 12 11 -7 87.2398 290.711 12 -11 -7 321.245 301.043 12 -11 -7 484.009 379.857 -12 11 7 709.513 370.623 12 11 -7 236.351 265.430 12 11 -7 97.7454 275.065 12 11 -7 175.262 277.112 -12 -11 6 281.352 255.363 -12 -11 6 279.196 313.790 12 -11 -6-11.9538 344.557 -12 11 6 118.966 291.299 12 -11 -6 350.001 258.137 12 -11 -6 116.758 310.268 -12 -11 6-24.9864 163.637 12 -11 -6 311.207 311.026 12 11 -6 215.269 278.220 12 11 -6 389.126 367.929 -12 11 6-6.76480 295.185 12 -11 -6 628.782 305.894 12 11 -6 478.234 346.209 12 -11 -6 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355.138 13 9 4 557.261 460.473 -13 9 -5-162.184 295.605 13 -9 5 380.393 503.692 -13 9 -5 767.549 503.236 13 -9 5 136.299 317.756 13 9 5 341.017 503.884 -13 9 -5 79.6856 344.932 -13 -9 -5 957.976 462.746 13 9 5 87.5183 363.772 13 -9 6 512.822 344.321 -13 9 -6 467.622 365.236 13 9 6 148.326 336.658 13 10 -18 3715.31 747.721 13 -10 -17 404.758 444.411 13 10 -17 1879.91 553.751 13 10 -17 779.828 467.001 -13 10 17-111.907 454.020 13 10 -17 1351.79 421.288 -13 10 17 1509.96 516.907 -13 -10 16 480.876 459.151 -13 -10 16-194.684 431.748 13 -10 -16 76.6415 324.390 13 -10 -16 97.2288 393.821 -13 -10 16-103.748 301.853 13 10 -16 57.6975 314.651 13 10 -16 607.741 450.040 13 10 -16-154.210 310.349 -13 10 16-53.4018 373.316 -13 -10 16 351.625 282.815 13 10 -16-429.450 333.220 13 -10 -16-97.0183 332.271 -13 10 16 870.443 463.444 13 -10 -16-421.139 367.981 13 10 -16-786.298 422.835 -13 -10 15 2040.85 618.747 -13 10 15 2012.03 500.049 13 -10 -15 1768.79 569.061 13 -10 -15 1866.57 593.342 -13 -10 15 1482.15 493.604 13 10 -15 3058.10 663.354 13 10 -15 1963.94 599.131 13 10 -15 2162.43 577.865 -13 10 15 2488.83 651.206 -13 -10 15 1998.03 539.909 13 10 -15 1374.82 453.303 13 -10 -15 2188.92 642.586 -13 10 15 3088.22 700.541 13 -10 -15 2431.92 675.787 13 10 -15 1982.94 553.864 -13 -10 15 1633.18 526.065 -13 -10 14 1025.93 471.372 13 -10 -14-12.9884 276.913 -13 10 14 299.192 278.686 13 -10 -14 78.3815 295.041 13 -10 -14 111.877 291.248 13 10 -14 433.663 344.756 13 10 -14 440.109 357.449 13 10 -14-290.695 376.793 -13 10 14 298.066 433.208 -13 -10 14 512.635 373.135 13 10 -14 255.324 235.482 13 -10 -14 1035.59 480.210 -13 10 14 161.217 352.188 13 -10 -14-423.089 441.562 13 10 -14-171.364 324.163 -13 -10 14 336.898 299.542 -13 -10 13-147.906 374.690 13 -10 -13 113.834 248.562 -13 10 13-219.486 232.060 13 -10 -13-156.993 284.066 13 -10 -13 350.428 318.427 13 10 -13 664.420 359.399 13 10 -13 819.847 485.139 13 10 -13 306.260 296.203 -13 10 13-188.791 323.431 13 10 -13 96.8750 230.382 13 -10 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2066.13 565.446 13 10 -6 1993.49 516.958 13 -10 -6 2877.75 569.234 13 10 -6 1507.06 539.063 -13 10 6 2147.61 559.990 13 10 -6 1521.78 457.895 13 -10 -6 2628.94 519.273 13 -10 -6 2219.79 553.124 13 -10 -6 2309.67 605.053 13 10 -6 2541.47 559.726 13 10 -6 2564.68 544.891 -13 10 6 2752.41 613.086 13 10 -6 2774.94 597.644 -13 -10 6 2120.82 509.286 -13 -10 5 1314.27 473.135 13 -10 -5 1016.23 436.794 -13 -10 5 1522.30 381.229 -13 10 5 1560.82 530.161 13 -10 -5 2049.09 484.452 13 -10 -5 210.587 258.266 13 10 -5 1438.67 473.803 13 -10 -5 778.344 329.993 13 10 -5 1161.27 544.881 -13 10 5 1740.78 509.478 13 10 -5 1546.60 499.600 13 -10 -5 1999.96 469.364 13 -10 -5 1910.61 564.516 13 -10 -5 1488.53 439.757 13 -10 -5 1485.82 524.095 13 10 -5 1814.33 467.613 13 10 -5 1174.49 387.971 13 10 -5 1255.23 434.517 -13 10 5 1541.59 507.589 13 10 -5 789.132 372.663 -13 -10 5 2088.47 501.102 -13 -10 4 2394.77 575.178 -13 -10 4 2632.99 499.027 13 -10 -4 2053.62 593.233 -13 10 4 2303.04 579.456 13 -10 -4 1877.88 448.565 13 -10 -4 2465.11 612.730 13 10 -4 2166.17 544.949 13 -10 -4 1981.61 500.283 13 10 -4 3339.20 747.656 13 10 -4 2203.17 539.714 -13 10 4 2801.19 623.730 13 -10 -4 2010.79 469.079 13 -10 -4 2322.98 576.118 13 -10 -4 2015.69 538.156 13 -10 -4 3116.79 761.046 13 10 -4 1651.45 483.639 13 10 -4 3407.15 605.751 13 10 -4 2920.60 603.066 -13 10 4 2516.40 577.228 13 10 -4 2219.77 543.739 -13 -10 4 2662.08 562.481 -13 -10 3 2043.99 444.172 -13 -10 3 2016.47 532.341 -13 -10 3 1982.79 440.050 -13 10 3 1915.70 521.145 13 -10 -3 1098.19 432.232 13 10 -3 1922.67 523.002 13 -10 -3 1800.91 494.171 13 10 -3 2704.50 685.743 -13 10 3 2025.84 559.384 13 10 -3 2119.11 468.000 13 -10 -3 2675.78 663.059 13 -10 -3 1179.45 478.221 13 10 -3 2145.95 565.515 13 10 -3 2393.07 587.726 13 10 -3 1685.90 519.991 -13 10 3 2799.09 640.593 -13 -10 2 2532.23 581.778 -13 -10 2 2191.03 469.837 -13 10 2 2552.89 629.681 13 -10 -2 2652.28 565.038 -13 -10 2 1646.22 475.813 13 10 -2 2146.68 543.728 13 -10 -2 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4357.61 714.020 14 7 -3 3654.84 658.127 14 7 -3 3294.43 656.412 -14 -7 3 4237.62 600.973 -14 -7 3 3280.06 552.314 -14 7 3 4570.77 791.618 -14 -7 2 151.509 236.835 -14 7 2 60.2095 270.101 -14 -7 2 337.399 287.633 14 -7 -2 48.0713 281.711 -14 -7 2 476.210 313.720 14 -7 -2-241.420 286.554 14 7 -2 380.512 367.538 14 -7 -2 806.318 407.566 -14 7 2-89.6560 330.588 14 7 -2 304.214 316.351 14 -7 -2 715.602 430.068 14 -7 -2 592.601 403.882 14 7 -2 224.278 232.229 14 -7 -2 81.3997 291.176 14 7 -2 740.579 398.402 14 7 -2 305.857 345.952 -14 -7 2 110.340 173.321 -14 -7 2 1.53727 208.223 -14 7 2 124.754 331.919 -14 -7 1-9.80401 233.335 -14 7 1 789.477 440.206 -14 7 1 1383.80 492.856 14 -7 -1 758.101 343.024 -14 -7 1 664.552 354.441 14 -7 -1 1366.64 424.893 14 -7 -1 380.136 330.743 -14 7 1 321.042 248.902 14 7 -1 892.038 366.173 14 -7 -1 1575.09 509.275 14 -7 -1 204.729 335.738 14 7 -1 910.937 351.686 14 -7 -1 1739.72 536.299 14 7 -1 1113.73 447.657 -14 -7 1 402.710 221.954 14 7 -1 679.749 439.271 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526.330 -14 7 -3 1942.95 581.334 -14 -7 -3 1594.39 493.430 14 -7 3 2133.80 783.341 14 7 3 1575.10 528.359 14 -7 3 2122.95 566.911 14 7 3 1240.77 507.868 14 -7 3 1605.07 546.225 -14 -7 -3 1365.52 440.277 14 -7 3 1757.78 567.739 14 7 3 739.291 514.259 14 7 3 2283.02 626.496 -14 7 -4 1424.35 432.922 -14 7 -4 2006.20 590.274 -14 -7 -4 880.135 343.083 14 -7 4 1872.15 688.343 14 7 4 2679.49 677.332 14 -7 4 1239.33 499.713 14 7 4 1818.93 520.948 14 -7 4 909.943 505.263 -14 7 -4 2037.80 671.877 -14 -7 -4 1541.07 527.256 14 -7 4 638.638 465.602 14 7 4 984.785 612.953 14 7 4 943.706 480.953 -14 7 -5 1345.41 471.190 -14 7 -5 999.571 425.167 14 -7 5 316.663 520.556 14 7 5 918.894 571.873 -14 7 -5 852.267 422.704 14 -7 5 226.610 344.938 14 7 5 972.070 469.141 14 -7 5 402.436 421.610 -14 7 -5 798.526 507.833 -14 -7 -5 238.738 311.964 14 -7 5 923.255 511.913 14 7 5 619.152 490.941 14 7 5 346.168 397.868 14 7 6 249.651 445.940 14 7 6 71.0830 403.623 14 7 7 86.1941 435.575 -14 8 19-117.590 290.023 14 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655.680 14 -10 -10 3190.50 662.277 14 -10 -10 2592.43 547.755 14 -10 -10 3180.01 738.308 -14 10 10 4108.85 765.432 14 10 -10 3746.32 697.433 14 10 -10 2995.03 606.766 14 10 -10 3603.13 629.341 -14 -10 10 4359.44 736.527 -14 -10 9 698.017 427.023 14 -10 -9 900.979 479.704 -14 10 9 1087.08 485.589 14 -10 -9 930.105 424.562 14 -10 -9-138.386 335.486 14 -10 -9 428.614 297.707 14 10 -9 255.773 284.195 14 10 -9 1326.82 544.044 -14 10 9 747.120 425.398 14 10 -9 656.038 412.184 14 -10 -9 205.905 355.986 14 -10 -9 116.533 281.330 14 -10 -9-480.945 488.277 -14 10 9 46.3711 293.994 14 10 -9 619.791 353.531 14 10 -9 316.066 309.999 14 10 -9 527.687 335.806 -14 -10 9 383.445 279.107 -14 -10 8 2465.07 646.734 14 -10 -8 1571.29 503.390 -14 10 8 2465.36 631.226 14 -10 -8 1815.57 465.470 14 -10 -8 1769.48 542.975 14 -10 -8 2990.84 613.172 14 10 -8 2748.03 611.618 14 10 -8 1240.81 520.275 -14 10 8 1665.76 548.242 14 10 -8 2031.63 571.285 14 -10 -8 1770.09 479.684 14 -10 -8 2075.27 544.759 14 -10 -8 2414.10 634.041 14 10 -8 2091.77 528.048 -14 10 8 2420.04 610.713 14 10 -8 1694.78 470.182 14 10 -8 2129.50 526.155 -14 -10 8 1719.50 494.448 -14 -10 7 1040.55 428.729 14 -10 -7 110.425 340.022 -14 10 7 1123.26 544.403 14 -10 -7 789.711 359.867 14 -10 -7 1634.50 506.599 -14 -10 7 873.538 398.308 14 -10 -7 1108.02 475.876 14 10 -7 1187.89 442.565 14 10 -7 599.471 472.716 14 10 -7 674.262 399.176 -14 10 7 768.939 375.094 14 -10 -7 1427.40 477.394 14 -10 -7 625.518 385.019 14 -10 -7 163.742 348.252 14 10 -7 1723.16 497.449 14 10 -7 577.639 325.800 -14 10 7 515.498 367.603 14 10 -7 563.075 305.768 -14 -10 7 753.569 368.227 -14 -10 6 3296.74 708.842 -14 -10 6 2676.67 483.774 14 -10 -6 2682.81 689.110 -14 10 6 2630.78 635.899 14 -10 -6 3260.47 591.660 14 -10 -6 2930.61 670.971 -14 -10 6 3624.17 700.570 14 10 -6 4142.17 755.038 14 -10 -6 2539.10 568.648 14 10 -6 3663.44 766.908 -14 10 6 2582.42 636.136 14 -10 -6 3157.46 580.135 14 -10 -6 2340.78 574.261 14 -10 -6 3314.00 734.068 14 10 -6 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520.289 371.789 14 -11 -8-341.124 340.747 14 -11 -8-187.081 332.748 14 -11 -8 377.858 334.900 14 11 -8 18.8083 254.411 -14 11 8 729.772 400.922 14 11 -8-81.1731 230.688 14 11 -8 17.1834 260.535 -14 -11 8-198.294 318.671 -14 -11 7 1240.93 440.282 14 -11 -7 2077.15 590.195 -14 11 7 1748.47 570.426 14 -11 -7 1441.02 460.631 14 -11 -7 1221.83 538.513 14 -11 -7 2547.08 595.972 14 11 -7 963.739 396.389 14 11 -7 2593.10 752.720 -14 11 7 1785.23 591.656 14 11 -7 1779.24 521.228 14 -11 -7 1173.50 473.744 14 -11 -7 2083.19 585.261 14 -11 -7 1585.46 610.053 14 11 -7 1433.78 491.973 14 11 -7 2425.42 591.456 -14 11 7 2224.28 584.496 14 11 -7 2537.21 576.701 -14 -11 7 1755.87 504.343 -14 -11 6-138.885 319.745 -14 -11 6 1571.22 495.181 14 -11 -6 916.662 440.624 -14 -11 6 765.457 302.342 -14 11 6 875.320 467.066 14 -11 -6 1148.73 388.986 14 -11 -6 1213.58 496.483 14 -11 -6 928.134 475.811 14 11 -6 426.602 358.453 14 11 -6 545.656 519.573 14 11 -6 1292.15 446.184 -14 11 6 477.330 388.919 14 -11 -6 236.504 263.252 14 -11 -6 676.811 385.207 14 -11 -6 1831.05 625.880 14 11 -6 991.859 426.034 14 11 -6 1161.53 502.859 -14 11 6 1153.73 464.202 14 11 -6 418.514 313.263 -14 -11 5-30.0192 238.188 -14 -11 5 23.0290 319.733 -14 -11 5-312.206 239.756 14 -11 -5 224.329 359.240 -14 11 5 446.016 387.416 14 -11 -5 302.399 358.057 14 11 -5-370.094 412.711 14 -11 -5-135.685 358.707 14 11 -5 382.160 380.247 -14 11 5 177.420 328.036 14 -11 -5-98.3097 290.498 14 -11 -5-22.3523 263.040 14 -11 -5 8.94776 328.225 14 11 -5-174.089 247.167 14 11 -5 547.513 369.758 -14 11 5 254.089 371.526 14 11 -5 404.425 384.384 -14 -11 4 5922.49 935.109 -14 -11 4 6045.67 771.998 14 -11 -4 7183.52 1042.89 -14 11 4 7122.71 1036.82 14 -11 -4 6394.99 932.481 -14 -11 4 7520.69 1017.66 14 11 -4 6243.21 907.047 14 -11 -4 7459.35 996.620 14 11 -4 5725.89 978.673 -14 11 4 5460.23 880.958 14 -11 -4 6305.16 958.024 14 -11 -4 5598.79 912.433 14 -11 -4 6640.20 1071.38 14 11 -4 7645.94 932.790 14 11 -4 6155.44 923.585 14 11 -4 6083.89 890.903 -14 11 4 7058.45 994.235 14 11 -3 637.137 303.069 -14 -11 3 1040.70 450.839 -14 -11 3 759.005 378.687 -14 11 3 1372.11 555.381 14 -11 -3 657.921 361.156 -14 -11 3 1640.17 540.186 14 11 -3 287.152 353.311 14 -11 -3 615.034 431.821 14 11 -3 720.096 483.685 -14 11 3 418.802 282.238 14 -11 -3 821.755 404.645 14 -11 -3 1104.85 483.320 14 11 -3 1386.16 462.272 14 11 -3 335.647 405.168 14 11 -3 1493.83 525.065 -14 11 3 892.754 416.013 -14 11 2 2667.37 612.937 -14 -11 2 3622.84 721.467 -14 11 2 3075.09 732.002 14 -11 -2 3229.82 677.437 -14 -11 2 2963.29 663.932 14 11 -2 2490.92 640.730 14 -11 -2 3048.17 650.866 14 11 -2 2997.69 795.407 -14 11 2 2563.84 638.597 14 11 -2 3115.52 677.979 14 -11 -2 2396.52 672.458 14 -11 -2 3181.42 686.815 14 11 -2 2751.80 689.132 14 11 -2 2585.08 649.414 14 11 -2 2537.41 654.995 -14 -11 2 3301.60 611.295 -14 -11 1 1509.83 499.441 -14 11 1 1878.05 543.016 -14 11 1 2369.41 654.245 14 -11 -1 1340.71 455.726 -14 -11 1 2525.12 584.685 14 11 -1 2497.04 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361.045 14 -12 -12 851.517 463.431 14 12 -12 711.580 379.329 14 12 -12 17.4076 430.995 -14 -12 12 119.506 281.065 14 12 -12 573.325 374.170 14 -12 -12 589.572 421.484 14 -12 -12 226.102 356.475 -14 12 12-245.473 355.159 14 12 -12-237.651 282.813 -14 -12 11 2272.78 678.041 -14 -12 11 3170.68 772.481 -14 12 11 2902.36 694.687 14 -12 -11 2187.77 576.147 -14 12 11 2019.46 513.250 14 -12 -11 3896.05 854.741 14 12 -11 3543.22 655.900 14 12 -11 3169.29 805.253 -14 12 11 4617.10 931.517 14 12 -11 1984.45 593.030 14 -12 -11 2241.66 620.907 14 -12 -11 3038.79 772.933 -14 12 11 3808.01 753.017 14 12 -11 2887.34 659.554 -14 -12 10 2108.36 659.801 -14 -12 10 2900.81 719.244 14 -12 -10 2479.87 594.744 -14 12 10 2177.26 596.975 14 -12 -10 2323.12 616.410 14 -12 -10 2185.76 677.193 14 12 -10 1664.23 478.463 14 12 -10 1759.81 617.520 -14 12 10 1606.62 608.289 14 12 -10 2757.71 643.358 -14 12 10 2341.25 555.639 14 -12 -10 2628.51 639.373 14 -12 -10 2259.38 670.886 -14 12 10 2307.95 597.694 14 12 -10 2122.35 575.937 -14 -12 9 14.0547 279.247 -14 -12 9 606.015 411.715 14 -12 -9-263.176 356.615 -14 12 9-139.315 414.574 14 -12 -9 256.176 367.808 14 -12 -9-321.524 352.706 -14 12 9 332.725 294.598 14 12 -9 460.486 364.017 14 12 -9 74.5287 426.300 -14 12 9 374.819 425.043 14 12 -9 1152.65 470.447 14 -12 -9 171.218 285.746 14 -12 -9-58.8591 376.424 -14 12 9 196.846 391.858 14 12 -9 81.0400 295.984 14 12 -9-133.061 287.198 14 12 -9 145.066 298.508 -14 -12 8 2313.84 573.569 -14 -12 8 1982.43 634.908 -14 12 8 2221.33 554.429 14 -12 -8 2793.90 708.587 -14 12 8 2762.78 696.883 14 -12 -8 2167.36 548.832 14 -12 -8 1896.61 607.878 14 12 -8 1780.21 537.396 14 12 -8 2589.97 740.348 -14 12 8 2855.01 725.896 14 12 -8 2390.52 626.437 14 -12 -8 1556.76 479.429 14 -12 -8 2240.66 675.682 -14 12 8 3704.41 741.678 14 12 -8 2025.26 547.255 14 12 -8 2247.34 557.582 14 12 -8 2051.10 545.034 -14 -12 7 661.631 475.677 -14 -12 7 155.479 271.940 14 -12 -7 239.555 335.659 -14 12 7 1766.03 583.986 14 -12 -7 701.083 376.718 14 -12 -7 128.404 311.100 14 -12 -7 1254.64 480.021 14 12 -7 1210.32 453.544 14 12 -7 1161.72 635.325 -14 12 7 665.368 435.914 14 12 -7 1227.33 470.606 14 -12 -7 484.530 338.843 14 -12 -7 351.966 289.415 14 -12 -7 1117.21 555.248 -14 12 7 552.303 291.876 14 12 -7 1214.14 429.377 14 12 -7 1602.76 542.006 -14 12 7 603.059 349.260 14 12 -7 1411.19 453.082 -14 -12 6 6642.48 1004.58 -14 -12 6 5078.29 834.574 14 -12 -6 5437.44 888.378 -14 12 6 5454.02 844.588 -14 -12 6 6719.34 820.629 -14 12 6 6282.01 996.000 14 -12 -6 5744.57 848.044 14 -12 -6 6016.77 941.141 14 -12 -6 7335.00 1005.65 14 12 -6 6355.76 913.985 14 12 -6 5268.96 1008.76 -14 12 6 5890.86 1013.78 14 12 -6 4824.47 823.155 14 -12 -6 4912.65 750.684 14 -12 -6 6136.98 914.088 14 -12 -6 6830.99 1079.81 14 12 -6 5982.69 868.081 14 12 -6 6353.58 940.941 -14 12 6 5262.98 862.102 14 12 -6 6216.93 918.665 -14 -12 5 1672.45 577.906 -14 -12 5 864.114 438.543 14 -12 -5 2239.36 638.221 -14 -12 5 2298.47 501.906 -14 12 5 1937.85 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1928.71 543.739 15 9 -8 2113.05 642.961 -15 9 8 1956.21 604.356 15 -9 -8 1355.66 450.786 15 -9 -8 1199.99 472.488 15 -9 -8 1015.48 437.979 15 9 -8 2519.46 554.373 15 9 -8 3638.02 664.949 -15 9 8 2031.16 608.978 -15 -9 8 1773.35 476.832 15 9 -8 2510.24 526.405 -15 -9 7-1.67799 291.750 15 -9 -7 182.991 332.161 -15 9 7 296.332 343.082 15 -9 -7 455.817 276.480 15 -9 -7 603.872 391.136 -15 -9 7 101.264 288.692 15 9 -7 45.0094 322.859 15 -9 -7 193.917 300.718 15 9 -7 781.329 482.516 -15 9 7 1104.29 531.614 15 -9 -7 367.125 296.695 15 -9 -7 462.309 265.001 15 -9 -7 819.067 407.709 15 9 -7 758.389 340.377 15 9 -7 733.652 390.692 -15 9 7 826.860 385.808 -15 -9 7 267.917 239.157 -15 -9 6 2141.51 599.329 15 -9 -6 2868.87 700.312 -15 9 6 3665.56 728.625 15 -9 -6 3521.50 608.695 -15 -9 6 3154.72 570.662 15 -9 -6 3022.34 660.351 -15 -9 6 2662.94 643.664 15 9 -6 3336.53 748.778 15 -9 -6 2408.10 582.611 15 9 -6 2166.10 672.165 -15 9 6 3342.04 728.664 15 -9 -6 2772.53 546.181 15 -9 -6 2701.91 591.315 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21 -4 -12-455.069 414.484 21 -4 -12 998.374 453.595 -21 -4 11 303.415 390.683 21 -4 -11-249.365 372.223 21 4 -11-404.832 446.388 21 -4 -11 499.285 396.149 -21 -4 10 689.070 465.033 21 -4 -10 298.253 359.040 21 -4 -10 1053.39 604.581 21 4 -10 1353.33 471.471 -21 4 10 846.015 414.178 -21 -4 10 589.518 406.706 21 -4 -10 1157.03 460.639 -21 -4 10 312.066 340.423 21 4 -9 645.668 450.072 21 -4 -9-226.053 349.729 21 -4 -9 1222.65 530.255 21 4 -9 1268.71 536.619 -21 4 9-120.595 300.404 -21 -4 9 264.906 304.595 21 -4 -9-120.375 436.329 21 4 -9-560.907 393.312 -21 -4 9 240.990 355.979 21 4 -8 93.1587 350.554 21 -4 -8 183.261 323.006 21 -4 -8-660.724 483.868 21 4 -8 531.555 368.504 -21 4 8 652.536 384.922 21 4 -8 712.492 414.752 21 4 -7-105.257 322.885 21 4 -7 81.0389 305.965 21 4 -6 281.811 468.336 21 4 -6 1008.28 452.257 21 -5 -14 12.2060 337.145 -21 -5 13-1070.89 500.043 -21 -5 12 1062.91 488.045 21 -5 -12 1167.02 550.578 -21 -5 11 643.125 397.140 21 -5 -11 430.262 410.087 -21 -5 10 351.656 448.767 21 -5 -10 463.285 335.809 21 -5 -10 699.896 444.861 21 5 -9 907.076 525.491 21 -5 -9 101.932 318.447 21 -5 -9 734.898 497.727 -21 5 9 520.760 399.079 -21 -5 9-872.177 430.024 21 5 -9 185.675 335.825 -21 -5 9 386.368 297.768 21 5 -8 1299.00 539.854 21 -5 -8 1218.99 565.117 21 -5 -8-269.591 399.400 -21 5 8 1167.58 484.527 21 -5 -7 766.634 494.377 21 -6 -12-5.07065 292.408 -21 -6 11 695.671 446.025 -21 -6 10 116.301 348.761 22 0 -9 512.423 429.004 22 -1 -10 1098.46 535.535 22 -1 -9-997.944 464.807 22 -2 -9 296.588 342.983 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 57621 _shelx_res_file ; TITL Dana in P2(1)/c shelx.res created by SHELXL-2019/3 at 11:49:45 on 28-Jan-2025 CELL 0.71073 15.3744 13.2969 16.0503 90.000 117.306 90.000 ZERR 4.00 0.0004 0.0002 0.0003 0.000 0.003 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H P CL SE PD UNIT 88 200 8 8 8 4 MERG 2 SHEL 999 0.75 CONF 2.5 HTAB C11 Se1 HTAB C12 Se1 HTAB C21 Cl1 HTAB C21 Se1 HTAB C3 Cl2 HTAB C31 Se1 HTAB C41 Se2 HTAB C43 Se2 HTAB C5 Cl1 EQIV $1 -x+1, -y+1, -z+1 HTAB C51 Cl1_$1 HTAB C52 Cl1 HTAB C52 Se2 HTAB C62 Se2 HTAB C62 Cl1 EQIV $2 x, -y+3/2, z-1/2 HTAB C63 Se1_$2 HTAB C63 Pd1_$2 FMAP 2 PLAN 10 SIZE 0.020 0.100 0.200 ACTA 56.00 BOND $H L.S. 6 TEMP -173.00 WGHT 0.023400 4.229300 FVAR 0.92035 PD1 6 0.216307 0.753496 0.434743 11.00000 0.01474 0.01251 = 0.01476 0.00004 0.00538 0.00092 CL1 4 0.271191 0.592165 0.433004 11.00000 0.02292 0.01529 = 0.03197 0.00041 0.01028 0.00385 CL2 4 0.169156 0.914558 0.451749 11.00000 0.02087 0.01515 = 0.02674 -0.00215 0.01145 0.00094 SE1 5 0.083715 0.676802 0.456218 11.00000 0.01708 0.01778 = 0.01473 0.00452 0.00516 -0.00054 SE2 5 0.347015 0.849362 0.423225 11.00000 0.02171 0.01730 = 0.02555 -0.00411 0.01387 -0.00316 P1 3 -0.053824 0.711070 0.332089 11.00000 0.01485 0.01147 = 0.01288 0.00052 0.00561 -0.00031 P2 3 0.436308 0.771694 0.368856 11.00000 0.01796 0.02415 = 0.01875 0.00274 0.00841 0.00482 C1 1 -0.143295 0.619865 0.340799 11.00000 0.01928 0.01386 = 0.01956 -0.00021 0.00813 -0.00355 C11 1 -0.121944 0.513404 0.318242 11.00000 0.02429 0.01435 = 0.03054 0.00147 0.01182 -0.00328 AFIX 137 H11A 2 -0.160709 0.464688 0.332998 11.00000 -1.50000 H11B 2 -0.052156 0.498536 0.355833 11.00000 -1.50000 H11C 2 -0.139325 0.508954 0.251481 11.00000 -1.50000 AFIX 0 C12 1 -0.130067 0.618799 0.442164 11.00000 0.03124 0.02429 = 0.02787 0.00210 0.01903 -0.00563 AFIX 137 H12A 2 -0.176767 0.571550 0.446459 11.00000 -1.50000 H12B 2 -0.141840 0.686386 0.459183 11.00000 -1.50000 H12C 2 -0.063198 0.597785 0.485175 11.00000 -1.50000 AFIX 0 C13 1 -0.250295 0.647951 0.275364 11.00000 0.02012 0.02545 = 0.03332 0.00128 0.01325 -0.00299 AFIX 137 H13A 2 -0.260177 0.651640 0.210622 11.00000 -1.50000 H13B 2 -0.265127 0.713400 0.293923 11.00000 -1.50000 H13C 2 -0.293788 0.596718 0.279834 11.00000 -1.50000 AFIX 0 C2 1 -0.041650 0.694332 0.221200 11.00000 0.01890 0.01913 = 0.01427 0.00128 0.00707 0.00076 C21 1 0.021475 0.602474 0.228002 11.00000 0.02247 0.02651 = 0.01962 -0.00265 0.00988 0.00240 AFIX 137 H21A 2 0.031078 0.598683 0.171795 11.00000 -1.50000 H21B 2 -0.011447 0.541326 0.232944 11.00000 -1.50000 H21C 2 0.085160 0.608671 0.283618 11.00000 -1.50000 AFIX 0 C22 1 0.009228 0.787954 0.207374 11.00000 0.02397 0.02210 = 0.01689 0.00202 0.01064 -0.00095 AFIX 137 H22A 2 0.070588 0.800034 0.264343 11.00000 -1.50000 H22B 2 -0.033787 0.846468 0.194614 11.00000 -1.50000 H22C 2 0.023270 0.776957 0.154365 11.00000 -1.50000 AFIX 0 C23 1 -0.142569 0.680888 0.135097 11.00000 0.02114 0.02643 = 0.01689 0.00012 0.00679 0.00009 AFIX 137 H23A 2 -0.134537 0.679690 0.077960 11.00000 -1.50000 H23B 2 -0.185338 0.736972 0.131925 11.00000 -1.50000 H23C 2 -0.171914 0.617463 0.140730 11.00000 -1.50000 AFIX 0 C3 1 -0.086072 0.844832 0.336460 11.00000 0.01995 0.01272 = 0.02030 0.00069 0.01014 0.00070 AFIX 13 H3 2 -0.029117 0.883940 0.339530 11.00000 -1.20000 AFIX 0 C31 1 -0.091163 0.871588 0.427067 11.00000 0.03475 0.02013 = 0.02762 -0.00371 0.01713 0.00246 AFIX 137 H31A 2 -0.088046 0.944789 0.435029 11.00000 -1.50000 H31B 2 -0.035950 0.840529 0.480612 11.00000 -1.50000 H31C 2 -0.152747 0.846544 0.423459 11.00000 -1.50000 AFIX 0 C32 1 -0.175862 0.888350 0.251488 11.00000 0.02469 0.01864 = 0.02797 0.00338 0.01116 0.00334 AFIX 137 H32A 2 -0.235194 0.854274 0.244931 11.00000 -1.50000 H32B 2 -0.168594 0.877950 0.194552 11.00000 -1.50000 H32C 2 -0.180919 0.960508 0.260924 11.00000 -1.50000 AFIX 0 C4 1 0.537160 0.867529 0.389935 11.00000 0.02699 0.02989 = 0.03909 0.00863 0.01769 0.00238 C41 1 0.607310 0.866703 0.493988 11.00000 0.02608 0.04011 = 0.04819 0.00266 0.00703 -0.00673 AFIX 137 H41A 2 0.655858 0.920298 0.508305 11.00000 -1.50000 H41B 2 0.640662 0.801528 0.511255 11.00000 -1.50000 H41C 2 0.570742 0.877751 0.529645 11.00000 -1.50000 AFIX 0 C42 1 0.594407 0.843028 0.334871 11.00000 0.03780 0.04375 = 0.06207 0.01149 0.03293 0.00655 AFIX 137 H42A 2 0.645149 0.894025 0.348349 11.00000 -1.50000 H42B 2 0.549428 0.842777 0.267542 11.00000 -1.50000 H42C 2 0.625043 0.776703 0.353712 11.00000 -1.50000 AFIX 0 C43 1 0.495052 0.974103 0.362934 11.00000 0.03637 0.02849 = 0.04621 0.00635 0.02189 -0.00308 AFIX 137 H43A 2 0.453950 0.989210 0.393325 11.00000 -1.50000 H43B 2 0.455536 0.978337 0.294732 11.00000 -1.50000 H43C 2 0.548795 1.022783 0.383513 11.00000 -1.50000 AFIX 0 C5 1 0.490760 0.654210 0.431711 11.00000 0.02794 0.02559 = 0.03215 0.00622 0.01343 0.00497 AFIX 13 H5 2 0.438287 0.602317 0.402417 11.00000 -1.20000 AFIX 0 C51 1 0.579143 0.612741 0.421025 11.00000 0.03490 0.03381 = 0.05095 0.01596 0.01950 0.01944 AFIX 137 H51A 2 0.636018 0.656369 0.454863 11.00000 -1.50000 H51B 2 0.563010 0.611008 0.354459 11.00000 -1.50000 H51C 2 0.594383 0.544578 0.446984 11.00000 -1.50000 AFIX 0 C52 1 0.515214 0.655561 0.535593 11.00000 0.03606 0.04141 = 0.03054 0.01502 0.01154 0.00448 AFIX 137 H52A 2 0.535191 0.588088 0.562099 11.00000 -1.50000 H52B 2 0.457333 0.676426 0.541816 11.00000 -1.50000 H52C 2 0.568761 0.703035 0.569321 11.00000 -1.50000 AFIX 0 C6 1 0.360080 0.743570 0.241499 11.00000 0.03083 0.03400 = 0.02259 -0.00139 0.01162 0.00491 C61 1 0.408675 0.670851 0.202640 11.00000 0.04622 0.04919 = 0.03402 -0.00641 0.02007 0.01395 AFIX 137 H61A 2 0.419072 0.606082 0.234969 11.00000 -1.50000 H61B 2 0.471833 0.698348 0.212523 11.00000 -1.50000 H61C 2 0.366455 0.661231 0.135372 11.00000 -1.50000 AFIX 0 C62 1 0.262837 0.698255 0.226352 11.00000 0.03018 0.04343 = 0.02922 -0.01129 0.00875 -0.00939 AFIX 137 H62A 2 0.222619 0.683661 0.159586 11.00000 -1.50000 H62B 2 0.228373 0.746102 0.247212 11.00000 -1.50000 H62C 2 0.275005 0.635872 0.262518 11.00000 -1.50000 AFIX 0 C63 1 0.336825 0.842815 0.185060 11.00000 0.04392 0.04364 = 0.02173 0.00486 0.01312 0.00977 AFIX 137 H63A 2 0.289663 0.829621 0.119645 11.00000 -1.50000 H63B 2 0.397166 0.870319 0.187677 11.00000 -1.50000 H63C 2 0.308914 0.891380 0.212100 11.00000 -1.50000 AFIX 0 HKLF 4 REM Dana in P2(1)/c REM wR2 = 0.0679, GooF = S = 1.041, Restrained GooF = 1.041 for all data REM R1 = 0.0321 for 5841 Fo > 4sig(Fo) and 0.0477 for all 7231 data REM 278 parameters refined using 0 restraints END WGHT 0.0234 4.2290 REM Highest difference peak 1.353, deepest hole -0.783, 1-sigma level 0.106 Q1 1 0.3861 0.8125 0.4742 11.00000 0.05 1.35 Q2 1 0.4238 0.7158 0.3663 11.00000 0.05 0.74 Q3 1 0.3473 0.6582 0.4215 11.00000 0.05 0.59 Q4 1 0.4303 0.9241 0.2599 11.00000 0.05 0.58 Q5 1 0.2904 0.5964 0.4882 11.00000 0.05 0.57 Q6 1 0.2161 0.7614 0.3632 11.00000 0.05 0.53 Q7 1 0.3302 0.6839 0.2400 11.00000 0.05 0.52 Q8 1 0.0199 0.7244 0.4003 11.00000 0.05 0.52 Q9 1 0.2228 0.7530 0.5072 11.00000 0.05 0.49 Q10 1 0.0830 0.8272 0.4528 11.00000 0.05 0.49 ; _shelx_res_checksum 24924 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd Pd1 0.21631(2) 0.75350(2) 0.43474(2) 0.01454(6) Uani d 1 . . Cl Cl1 0.27119(6) 0.59216(5) 0.43300(6) 0.02429(16) Uani d 1 . . Cl Cl2 0.16916(5) 0.91456(5) 0.45175(5) 0.02071(15) Uani d 1 . . Se Se1 0.08372(2) 0.67680(2) 0.45622(2) 0.01735(7) Uani d 1 . . Se Se2 0.34701(2) 0.84936(2) 0.42322(2) 0.02034(7) Uani d 1 . . P P1 -0.05382(5) 0.71107(5) 0.33209(5) 0.01336(14) Uani d 1 . . P P2 0.43631(6) 0.77169(6) 0.36886(5) 0.02029(17) Uani d 1 . . C C1 -0.1433(2) 0.6199(2) 0.3408(2) 0.0179(6) Uani d 1 . . C C11 -0.1219(2) 0.5134(2) 0.3182(2) 0.0234(7) Uani d 1 . . H H11A -0.160709 0.464688 0.332998 0.035 Uiso calc 1 . . H H11B -0.052156 0.498536 0.355833 0.035 Uiso calc 1 . . H H11C -0.139325 0.508954 0.251481 0.035 Uiso calc 1 . . C C12 -0.1301(2) 0.6188(2) 0.4422(2) 0.0257(7) Uani d 1 . . H H12A -0.176767 0.571550 0.446459 0.039 Uiso calc 1 . . H H12B -0.141840 0.686386 0.459183 0.039 Uiso calc 1 . . H H12C -0.063198 0.597785 0.485175 0.039 Uiso calc 1 . . C C13 -0.2503(2) 0.6480(2) 0.2754(2) 0.0259(7) Uani d 1 . . H H13A -0.260177 0.651640 0.210622 0.039 Uiso calc 1 . . H H13B -0.265127 0.713400 0.293923 0.039 Uiso calc 1 . . H H13C -0.293788 0.596718 0.279834 0.039 Uiso calc 1 . . C C2 -0.0416(2) 0.6943(2) 0.2212(2) 0.0176(6) Uani d 1 . . C C21 0.0215(2) 0.6025(2) 0.2280(2) 0.0228(7) Uani d 1 . . H H21A 0.031078 0.598683 0.171795 0.034 Uiso calc 1 . . H H21B -0.011447 0.541326 0.232944 0.034 Uiso calc 1 . . H H21C 0.085160 0.608671 0.283618 0.034 Uiso calc 1 . . C C22 0.0092(2) 0.7880(2) 0.2074(2) 0.0205(6) Uani d 1 . . H H22A 0.070588 0.800034 0.264343 0.031 Uiso calc 1 . . H H22B -0.033787 0.846468 0.194614 0.031 Uiso calc 1 . . H H22C 0.023270 0.776957 0.154365 0.031 Uiso calc 1 . . C C23 -0.1426(2) 0.6809(2) 0.1351(2) 0.0222(6) Uani d 1 . . H H23A -0.134537 0.679690 0.077960 0.033 Uiso calc 1 . . H H23B -0.185338 0.736972 0.131925 0.033 Uiso calc 1 . . H H23C -0.171914 0.617463 0.140730 0.033 Uiso calc 1 . . C C3 -0.0861(2) 0.8448(2) 0.3365(2) 0.0173(6) Uani d 1 . . H H3 -0.029117 0.883940 0.339530 0.021 Uiso calc 1 . . C C31 -0.0912(3) 0.8716(2) 0.4271(2) 0.0264(7) Uani d 1 . . H H31A -0.088046 0.944789 0.435029 0.040 Uiso calc 1 . . H H31B -0.035950 0.840529 0.480612 0.040 Uiso calc 1 . . H H31C -0.152747 0.846544 0.423459 0.040 Uiso calc 1 . . C C32 -0.1759(2) 0.8883(2) 0.2515(2) 0.0241(7) Uani d 1 . . H H32A -0.235194 0.854274 0.244931 0.036 Uiso calc 1 . . H H32B -0.168594 0.877950 0.194552 0.036 Uiso calc 1 . . H H32C -0.180919 0.960508 0.260924 0.036 Uiso calc 1 . . C C4 0.5372(3) 0.8675(3) 0.3899(3) 0.0310(8) Uani d 1 . . C C41 0.6073(3) 0.8667(3) 0.4940(3) 0.0420(10) Uani d 1 . . H H41A 0.655858 0.920298 0.508305 0.063 Uiso calc 1 . . H H41B 0.640662 0.801528 0.511255 0.063 Uiso calc 1 . . H H41C 0.570742 0.877751 0.529645 0.063 Uiso calc 1 . . C C42 0.5944(3) 0.8430(3) 0.3349(3) 0.0440(10) Uani d 1 . . H H42A 0.645149 0.894025 0.348349 0.066 Uiso calc 1 . . H H42B 0.549428 0.842777 0.267542 0.066 Uiso calc 1 . . H H42C 0.625043 0.776703 0.353712 0.066 Uiso calc 1 . . C C43 0.4951(3) 0.9741(3) 0.3629(3) 0.0359(8) Uani d 1 . . H H43A 0.453950 0.989210 0.393325 0.054 Uiso calc 1 . . H H43B 0.455536 0.978337 0.294732 0.054 Uiso calc 1 . . H H43C 0.548795 1.022783 0.383513 0.054 Uiso calc 1 . . C C5 0.4908(3) 0.6542(3) 0.4317(2) 0.0287(7) Uani d 1 . . H H5 0.438287 0.602317 0.402417 0.034 Uiso calc 1 . . C C51 0.5791(3) 0.6127(3) 0.4210(3) 0.0400(9) Uani d 1 . . H H51A 0.636018 0.656369 0.454863 0.060 Uiso calc 1 . . H H51B 0.563010 0.611008 0.354459 0.060 Uiso calc 1 . . H H51C 0.594383 0.544578 0.446984 0.060 Uiso calc 1 . . C C52 0.5152(3) 0.6556(3) 0.5356(2) 0.0375(9) Uani d 1 . . H H52A 0.535191 0.588088 0.562099 0.056 Uiso calc 1 . . H H52B 0.457333 0.676426 0.541816 0.056 Uiso calc 1 . . H H52C 0.568761 0.703035 0.569321 0.056 Uiso calc 1 . . C C6 0.3601(3) 0.7436(3) 0.2415(2) 0.0294(7) Uani d 1 . . C C61 0.4087(3) 0.6709(3) 0.2026(3) 0.0425(10) Uani d 1 . . H H61A 0.419072 0.606082 0.234969 0.064 Uiso calc 1 . . H H61B 0.471833 0.698348 0.212523 0.064 Uiso calc 1 . . H H61C 0.366455 0.661231 0.135372 0.064 Uiso calc 1 . . C C62 0.2628(3) 0.6983(3) 0.2264(3) 0.0362(9) Uani d 1 . . H H62A 0.222619 0.683661 0.159586 0.054 Uiso calc 1 . . H H62B 0.228373 0.746102 0.247212 0.054 Uiso calc 1 . . H H62C 0.275005 0.635872 0.262518 0.054 Uiso calc 1 . . C C63 0.3368(3) 0.8428(3) 0.1851(2) 0.0372(9) Uani d 1 . . H H63A 0.289663 0.829621 0.119645 0.056 Uiso calc 1 . . H H63B 0.397166 0.870319 0.187677 0.056 Uiso calc 1 . . H H63C 0.308914 0.891380 0.212100 0.056 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pd1 0.01474(11) 0.01251(10) 0.01476(11) 0.00092(8) 0.00538(9) 0.00004(8) Cl1 0.0229(4) 0.0153(3) 0.0320(4) 0.0039(3) 0.0103(3) 0.0004(3) Cl2 0.0209(4) 0.0151(3) 0.0267(4) 0.0009(3) 0.0115(3) -0.0021(3) Se1 0.01708(15) 0.01778(14) 0.01473(14) -0.00054(11) 0.00516(12) 0.00452(11) Se2 0.02171(16) 0.01730(15) 0.02555(17) -0.00316(12) 0.01387(14) -0.00411(12) P1 0.0149(4) 0.0115(3) 0.0129(3) -0.0003(3) 0.0056(3) 0.0005(3) P2 0.0180(4) 0.0242(4) 0.0187(4) 0.0048(3) 0.0084(3) 0.0027(3) C1 0.0193(15) 0.0139(14) 0.0196(15) -0.0036(11) 0.0081(13) -0.0002(11) C11 0.0243(17) 0.0143(14) 0.0305(18) -0.0033(12) 0.0118(15) 0.0015(12) C12 0.0312(18) 0.0243(16) 0.0279(17) -0.0056(13) 0.0190(16) 0.0021(13) C13 0.0201(16) 0.0254(16) 0.0333(18) -0.0030(13) 0.0133(15) 0.0013(14) C2 0.0189(15) 0.0191(15) 0.0143(14) 0.0008(11) 0.0071(12) 0.0013(11) C21 0.0225(16) 0.0265(17) 0.0196(16) 0.0024(13) 0.0099(14) -0.0026(13) C22 0.0240(16) 0.0221(15) 0.0169(15) -0.0010(12) 0.0106(13) 0.0020(12) C23 0.0211(16) 0.0264(16) 0.0169(15) 0.0001(13) 0.0068(13) 0.0001(12) C3 0.0200(15) 0.0127(13) 0.0203(15) 0.0007(11) 0.0101(13) 0.0007(11) C31 0.0347(19) 0.0201(16) 0.0276(17) 0.0025(14) 0.0171(16) -0.0037(13) C32 0.0247(17) 0.0186(15) 0.0280(17) 0.0033(13) 0.0112(15) 0.0034(13) C4 0.0270(18) 0.0299(18) 0.039(2) 0.0024(14) 0.0177(17) 0.0086(15) C41 0.026(2) 0.040(2) 0.048(2) -0.0067(16) 0.0070(18) 0.0027(18) C42 0.038(2) 0.044(2) 0.062(3) 0.0066(18) 0.033(2) 0.011(2) C43 0.036(2) 0.0285(19) 0.046(2) -0.0031(15) 0.0219(19) 0.0064(16) C5 0.0279(18) 0.0256(17) 0.0322(19) 0.0050(14) 0.0134(16) 0.0062(14) C51 0.035(2) 0.034(2) 0.051(2) 0.0194(17) 0.0195(19) 0.0160(18) C52 0.036(2) 0.041(2) 0.031(2) 0.0045(17) 0.0115(17) 0.0150(16) C6 0.0308(18) 0.0340(19) 0.0226(17) 0.0049(15) 0.0116(15) -0.0014(14) C61 0.046(2) 0.049(2) 0.034(2) 0.0139(19) 0.0201(19) -0.0064(18) C62 0.030(2) 0.043(2) 0.0292(19) -0.0094(17) 0.0088(16) -0.0113(16) C63 0.044(2) 0.044(2) 0.0217(18) 0.0098(18) 0.0131(17) 0.0049(16) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag Cl1 Pd1 Cl2 . . 174.61(3) y Cl1 Pd1 Se1 . . 86.97(2) y Cl2 Pd1 Se1 . . 92.46(2) y Cl1 Pd1 Se2 . . 99.50(2) y Cl2 Pd1 Se2 . . 80.81(2) y Se1 Pd1 Se2 . . 172.772(14) y P1 Se1 Pd1 . . 107.78(2) y P2 Se2 Pd1 . . 117.93(3) y C3 P1 C2 . . 107.01(13) ? C3 P1 C1 . . 113.37(13) ? C2 P1 C1 . . 112.67(13) ? C3 P1 Se1 . . 109.18(10) y C2 P1 Se1 . . 111.22(9) y C1 P1 Se1 . . 103.40(10) y C5 P2 C6 . . 109.22(16) ? C5 P2 C4 . . 109.91(16) ? C6 P2 C4 . . 112.17(16) ? C5 P2 Se2 . . 113.08(11) ? C6 P2 Se2 . . 109.66(11) ? C4 P2 Se2 . . 102.73(11) ? C11 C1 C13 . . 109.9(2) ? C11 C1 C12 . . 107.5(2) ? C13 C1 C12 . . 107.7(3) ? C11 C1 P1 . . 109.5(2) ? C13 C1 P1 . . 112.4(2) ? C12 C1 P1 . . 109.6(2) ? C1 C11 H11A . . 109.5 ? C1 C11 H11B . . 109.5 ? H11A C11 H11B . . 109.5 ? C1 C11 H11C . . 109.5 ? H11A C11 H11C . . 109.5 ? H11B C11 H11C . . 109.5 ? C1 C12 H12A . . 109.5 ? C1 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C1 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? C1 C13 H13A . . 109.5 ? C1 C13 H13B . . 109.5 ? H13A C13 H13B . . 109.5 ? C1 C13 H13C . . 109.5 ? H13A C13 H13C . . 109.5 ? H13B C13 H13C . . 109.5 ? C21 C2 C22 . . 107.9(2) ? C21 C2 C23 . . 108.4(2) ? C22 C2 C23 . . 109.5(2) ? C21 C2 P1 . . 111.1(2) ? C22 C2 P1 . . 108.51(19) ? C23 C2 P1 . . 111.4(2) ? C2 C21 H21A . . 109.5 ? C2 C21 H21B . . 109.5 ? H21A C21 H21B . . 109.5 ? C2 C21 H21C . . 109.5 ? H21A C21 H21C . . 109.5 ? H21B C21 H21C . . 109.5 ? C2 C22 H22A . . 109.5 ? C2 C22 H22B . . 109.5 ? H22A C22 H22B . . 109.5 ? C2 C22 H22C . . 109.5 ? H22A C22 H22C . . 109.5 ? H22B C22 H22C . . 109.5 ? C2 C23 H23A . . 109.5 ? C2 C23 H23B . . 109.5 ? H23A C23 H23B . . 109.5 ? C2 C23 H23C . . 109.5 ? H23A C23 H23C . . 109.5 ? H23B C23 H23C . . 109.5 ? C31 C3 C32 . . 109.7(2) ? C31 C3 P1 . . 112.9(2) ? C32 C3 P1 . . 118.2(2) ? C31 C3 H3 . . 104.9 ? C32 C3 H3 . . 104.9 ? P1 C3 H3 . . 104.9 ? C3 C31 H31A . . 109.5 ? C3 C31 H31B . . 109.5 ? H31A C31 H31B . . 109.5 ? C3 C31 H31C . . 109.5 ? H31A C31 H31C . . 109.5 ? H31B C31 H31C . . 109.5 ? C3 C32 H32A . . 109.5 ? C3 C32 H32B . . 109.5 ? H32A C32 H32B . . 109.5 ? C3 C32 H32C . . 109.5 ? H32A C32 H32C . . 109.5 ? H32B C32 H32C . . 109.5 ? C41 C4 C43 . . 108.2(3) ? C41 C4 C42 . . 109.0(3) ? C43 C4 C42 . . 108.1(3) ? C41 C4 P2 . . 107.4(2) ? C43 C4 P2 . . 111.2(2) ? C42 C4 P2 . . 112.8(3) ? C4 C41 H41A . . 109.5 ? C4 C41 H41B . . 109.5 ? H41A C41 H41B . . 109.5 ? C4 C41 H41C . . 109.5 ? H41A C41 H41C . . 109.5 ? H41B C41 H41C . . 109.5 ? C4 C42 H42A . . 109.5 ? C4 C42 H42B . . 109.5 ? H42A C42 H42B . . 109.5 ? C4 C42 H42C . . 109.5 ? H42A C42 H42C . . 109.5 ? H42B C42 H42C . . 109.5 ? C4 C43 H43A . . 109.5 ? C4 C43 H43B . . 109.5 ? H43A C43 H43B . . 109.5 ? C4 C43 H43C . . 109.5 ? H43A C43 H43C . . 109.5 ? H43B C43 H43C . . 109.5 ? C52 C5 C51 . . 109.6(3) ? C52 C5 P2 . . 114.2(2) ? C51 C5 P2 . . 116.3(2) ? C52 C5 H5 . . 105.2 ? C51 C5 H5 . . 105.2 ? P2 C5 H5 . . 105.2 ? C5 C51 H51A . . 109.5 ? C5 C51 H51B . . 109.5 ? H51A C51 H51B . . 109.5 ? C5 C51 H51C . . 109.5 ? H51A C51 H51C . . 109.5 ? H51B C51 H51C . . 109.5 ? C5 C52 H52A . . 109.5 ? C5 C52 H52B . . 109.5 ? H52A C52 H52B . . 109.5 ? C5 C52 H52C . . 109.5 ? H52A C52 H52C . . 109.5 ? H52B C52 H52C . . 109.5 ? C61 C6 C62 . . 108.3(3) ? C61 C6 C63 . . 109.1(3) ? C62 C6 C63 . . 107.3(3) ? C61 C6 P2 . . 113.4(3) ? C62 C6 P2 . . 109.3(2) ? C63 C6 P2 . . 109.3(2) ? C6 C61 H61A . . 109.5 ? C6 C61 H61B . . 109.5 ? H61A C61 H61B . . 109.5 ? C6 C61 H61C . . 109.5 ? H61A C61 H61C . . 109.5 ? H61B C61 H61C . . 109.5 ? C6 C62 H62A . . 109.5 ? C6 C62 H62B . . 109.5 ? H62A C62 H62B . . 109.5 ? C6 C62 H62C . . 109.5 ? H62A C62 H62C . . 109.5 ? H62B C62 H62C . . 109.5 ? C6 C63 H63A . . 109.5 ? C6 C63 H63B . . 109.5 ? H63A C63 H63B . . 109.5 ? C6 C63 H63C . . 109.5 ? H63A C63 H63C . . 109.5 ? H63B C63 H63C . . 109.5 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Pd1 Cl1 . 2.3100(7) y Pd1 Cl2 . 2.3169(7) y Pd1 Se1 . 2.4411(4) y Pd1 Se2 . 2.4573(4) y Se1 P1 . 2.1870(8) y Se2 P2 . 2.1936(8) y P1 C3 . 1.856(3) ? P1 C2 . 1.886(3) ? P1 C1 . 1.887(3) ? P2 C5 . 1.840(3) ? P2 C6 . 1.869(3) ? P2 C4 . 1.913(4) ? C1 C11 . 1.534(4) ? C1 C13 . 1.537(4) ? C1 C12 . 1.544(4) ? C11 H11A . 0.9800 ? C11 H11B . 0.9800 ? C11 H11C . 0.9800 ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? C13 H13A . 0.9800 ? C13 H13B . 0.9800 ? C13 H13C . 0.9800 ? C2 C21 . 1.532(4) ? C2 C22 . 1.540(4) ? C2 C23 . 1.543(4) ? C21 H21A . 0.9800 ? C21 H21B . 0.9800 ? C21 H21C . 0.9800 ? C22 H22A . 0.9800 ? C22 H22B . 0.9800 ? C22 H22C . 0.9800 ? C23 H23A . 0.9800 ? C23 H23B . 0.9800 ? C23 H23C . 0.9800 ? C3 C31 . 1.534(4) ? C3 C32 . 1.541(4) ? C3 H3 . 1.0000 ? C31 H31A . 0.9800 ? C31 H31B . 0.9800 ? C31 H31C . 0.9800 ? C32 H32A . 0.9800 ? C32 H32B . 0.9800 ? C32 H32C . 0.9800 ? C4 C41 . 1.517(5) ? C4 C43 . 1.535(5) ? C4 C42 . 1.541(5) ? C41 H41A . 0.9800 ? C41 H41B . 0.9800 ? C41 H41C . 0.9800 ? C42 H42A . 0.9800 ? C42 H42B . 0.9800 ? C42 H42C . 0.9800 ? C43 H43A . 0.9800 ? C43 H43B . 0.9800 ? C43 H43C . 0.9800 ? C5 C52 . 1.532(5) ? C5 C51 . 1.547(5) ? C5 H5 . 1.0000 ? C51 H51A . 0.9800 ? C51 H51B . 0.9800 ? C51 H51C . 0.9800 ? C52 H52A . 0.9800 ? C52 H52B . 0.9800 ? C52 H52C . 0.9800 ? C6 C61 . 1.520(5) ? C6 C62 . 1.524(5) ? C6 C63 . 1.547(5) ? C61 H61A . 0.9800 ? C61 H61B . 0.9800 ? C61 H61C . 0.9800 ? C62 H62A . 0.9800 ? C62 H62B . 0.9800 ? C62 H62C . 0.9800 ? C63 H63A . 0.9800 ? C63 H63B . 0.9800 ? C63 H63C . 0.9800 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C11 H11B Se1 . 0.98 3.08 3.633(3) 117.1 yes C12 H12C Se1 . 0.98 2.72 3.282(3) 117.1 yes C21 H21C Cl1 . 0.98 2.77 3.741(3) 169.9 yes C21 H21C Se1 . 0.98 2.92 3.478(3) 116.8 yes C3 H3 Cl2 . 1.00 2.77 3.608(3) 141.9 yes C31 H31B Se1 . 0.98 2.99 3.606(3) 122.0 yes C41 H41C Se2 . 0.98 3.08 3.632(4) 116.8 yes C43 H43A Se2 . 0.98 2.67 3.300(4) 122.6 yes C5 H5 Cl1 . 1.00 2.83 3.484(4) 123.5 yes C51 H51C Cl1 3_666 0.98 2.76 3.642(3) 149.5 yes C52 H52B Cl1 . 0.98 2.81 3.439(4) 122.5 yes C52 H52B Se2 . 0.98 2.97 3.507(4) 115.6 yes C62 H62B Se2 . 0.98 2.91 3.456(4) 116.2 yes C62 H62C Cl1 . 0.98 2.82 3.552(4) 131.7 yes C63 H63A Se1 4_575 0.98 3.05 3.948(4) 153.2 yes C63 H63A Pd1 4_575 0.98 2.87 3.793(4) 157.5 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Cl1 Pd1 Se1 P1 . . . . -115.18(3) ? Cl2 Pd1 Se1 P1 . . . . 70.19(3) ? Cl1 Pd1 Se2 P2 . . . . 20.17(3) ? Cl2 Pd1 Se2 P2 . . . . -165.29(3) ? Pd1 Se1 P1 C3 . . . . -74.49(10) ? Pd1 Se1 P1 C2 . . . . 43.37(10) ? Pd1 Se1 P1 C1 . . . . 164.54(9) ? Pd1 Se2 P2 C5 . . . . -53.52(13) ? Pd1 Se2 P2 C6 . . . . 68.63(12) ? Pd1 Se2 P2 C4 . . . . -171.93(11) ? C3 P1 C1 C11 . . . . 169.5(2) ? C2 P1 C1 C11 . . . . 47.7(2) ? Se1 P1 C1 C11 . . . . -72.4(2) ? C3 P1 C1 C13 . . . . 47.0(3) ? C2 P1 C1 C13 . . . . -74.7(2) ? Se1 P1 C1 C13 . . . . 165.09(19) ? C3 P1 C1 C12 . . . . -72.8(2) ? C2 P1 C1 C12 . . . . 165.5(2) ? Se1 P1 C1 C12 . . . . 45.3(2) ? C3 P1 C2 C21 . . . . 158.0(2) ? C1 P1 C2 C21 . . . . -76.8(2) ? Se1 P1 C2 C21 . . . . 38.8(2) ? C3 P1 C2 C22 . . . . 39.5(2) ? C1 P1 C2 C22 . . . . 164.73(19) ? Se1 P1 C2 C22 . . . . -79.7(2) ? C3 P1 C2 C23 . . . . -81.1(2) ? C1 P1 C2 C23 . . . . 44.2(2) ? Se1 P1 C2 C23 . . . . 159.75(18) ? C2 P1 C3 C31 . . . . -175.8(2) ? C1 P1 C3 C31 . . . . 59.3(3) ? Se1 P1 C3 C31 . . . . -55.4(2) ? C2 P1 C3 C32 . . . . 54.2(3) ? C1 P1 C3 C32 . . . . -70.6(3) ? Se1 P1 C3 C32 . . . . 174.7(2) ? C5 P2 C4 C41 . . . . -45.7(3) ? C6 P2 C4 C41 . . . . -167.4(2) ? Se2 P2 C4 C41 . . . . 74.9(2) ? C5 P2 C4 C43 . . . . -163.9(2) ? C6 P2 C4 C43 . . . . 74.4(3) ? Se2 P2 C4 C43 . . . . -43.3(3) ? C5 P2 C4 C42 . . . . 74.4(3) ? C6 P2 C4 C42 . . . . -47.3(3) ? Se2 P2 C4 C42 . . . . -165.0(2) ? C6 P2 C5 C52 . . . . -154.2(3) ? C4 P2 C5 C52 . . . . 82.4(3) ? Se2 P2 C5 C52 . . . . -31.8(3) ? C6 P2 C5 C51 . . . . 76.6(3) ? C4 P2 C5 C51 . . . . -46.9(3) ? Se2 P2 C5 C51 . . . . -161.0(2) ? C5 P2 C6 C61 . . . . -43.2(3) ? C4 P2 C6 C61 . . . . 78.9(3) ? Se2 P2 C6 C61 . . . . -167.7(2) ? C5 P2 C6 C62 . . . . 77.6(3) ? C4 P2 C6 C62 . . . . -160.2(2) ? Se2 P2 C6 C62 . . . . -46.8(3) ? C5 P2 C6 C63 . . . . -165.2(2) ? C4 P2 C6 C63 . . . . -43.1(3) ? Se2 P2 C6 C63 . . . . 70.4(3) ?