#------------------------------------------------------------------------------ #$Date: 2020-08-07 05:21:29 +0300 (Fri, 07 Aug 2020) $ #$Revision: 255156 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/22/2022219.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022219 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.4027 _cell_length_b 17.5277 _cell_length_c 30.9259 _exptl_crystal_F_000 2366.00 _reflns_d_resolution_high 0.7956 _cod_data_source_file fm3065aris40cultsup4.hkl _cod_data_source_block aris40cult _shelx_title ' aris40CuLT in P212121 No19' _shelx_refln_list_code 4 _shelx_f_calc_maximum 292.06 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 57483.06 54054.08 212.92 o 4 0 0 28933.66 30446.15 236.89 o 6 0 0 20.61 49.80 12.04 o 8 0 0 25.28 33.02 7.41 o 10 0 0 655.44 680.70 24.44 o 12 0 0 113.06 144.03 13.67 o 1 1 0 1204.64 956.31 13.34 o 2 1 0 3089.63 2808.71 48.18 o 3 1 0 6536.48 6763.62 102.38 o 4 1 0 32691.07 32024.39 132.14 o 5 1 0 1811.57 1874.70 36.97 o 6 1 0 5798.96 6045.26 73.98 o 7 1 0 76.46 64.20 13.93 o 8 1 0 146.94 173.12 9.07 o 9 1 0 135.42 126.78 8.77 o 10 1 0 2164.15 2249.19 30.21 o 11 1 0 107.01 85.11 7.19 o 12 1 0 26.23 52.37 10.68 o 1 2 0 4453.39 4133.26 34.52 o 2 2 0 4354.69 4190.69 39.60 o 3 2 0 36168.27 35243.90 138.25 o 4 2 0 9405.19 8848.09 69.64 o 5 2 0 4932.45 5631.74 63.44 o 6 2 0 268.51 275.28 22.48 o 7 2 0 643.64 609.94 52.99 o 8 2 0 87.01 68.10 6.30 o 9 2 0 1.89 10.29 5.45 o 10 2 0 2153.26 2283.95 30.18 o 11 2 0 47.36 46.89 6.52 o 12 2 0 1935.40 1861.57 44.17 o 1 3 0 539.40 525.83 14.80 o 2 3 0 898.84 994.84 28.51 o 3 3 0 15432.06 14738.13 97.00 o 4 3 0 2582.04 2732.02 86.70 o 5 3 0 1146.94 1201.73 35.48 o 6 3 0 9774.03 9736.12 188.79 o 7 3 0 192.15 250.03 36.14 o 8 3 0 833.57 757.49 19.92 o 9 3 0 2219.79 2467.48 37.69 o 10 3 0 531.29 484.86 16.85 o 11 3 0 130.24 138.71 11.53 o 12 3 0 3.69 19.46 9.37 o 1 4 0 2523.77 2487.47 36.05 o 2 4 0 11234.69 10607.44 149.83 o 3 4 0 2748.35 2966.26 46.51 o 4 4 0 3256.80 3300.35 94.87 o 5 4 0 9374.58 8690.55 96.79 o 6 4 0 114.56 126.02 25.08 o 7 4 0 10066.96 9783.29 216.38 o 8 4 0 3203.56 3234.99 40.47 o 9 4 0 268.05 243.11 12.80 o 10 4 0 116.50 90.30 8.71 o 11 4 0 1201.53 1206.52 43.57 o 12 4 0 508.32 579.50 25.51 o 1 5 0 807.59 717.35 22.15 o 2 5 0 975.60 1090.19 28.41 o 3 5 0 24170.32 24302.95 142.33 o 4 5 0 19117.32 18091.97 1168.46 o 5 5 0 661.96 700.39 29.12 o 6 5 0 1532.78 1476.36 78.50 o 7 5 0 182.70 211.06 36.90 o 8 5 0 1127.66 1128.40 25.55 o 9 5 0 813.06 881.22 22.96 o 10 5 0 76.79 87.64 8.65 o 11 5 0 11.95 4.68 10.91 o 12 5 0 5.11 9.63 8.96 o 1 6 0 8469.73 8359.60 81.12 o 2 6 0 11270.34 11864.81 330.81 o 3 6 0 19097.12 18857.71 135.04 o 4 6 0 15211.19 15495.71 131.18 o 5 6 0 3449.84 3559.64 113.82 o 6 6 0 22.87 26.48 19.12 o 7 6 0 7.29 3.59 13.25 o 8 6 0 2055.04 2096.37 33.25 o 9 6 0 4.66 1.94 6.03 o 10 6 0 990.02 962.73 42.18 o 11 6 0 377.35 393.20 25.63 o 12 6 0 2.31 14.36 7.90 o 1 7 0 3291.49 3149.90 54.63 o 2 7 0 4620.38 4701.41 69.23 o 3 7 0 27014.90 27445.79 185.95 o 4 7 0 697.73 688.07 30.00 o 5 7 0 599.65 664.31 51.97 o 6 7 0 841.44 859.25 64.81 o 7 7 0 23.63 17.97 5.38 o 8 7 0 5696.80 5884.96 88.23 o 9 7 0 1580.14 1654.25 37.77 o 10 7 0 452.14 495.76 30.60 o 11 7 0 43.36 25.91 11.14 o 12 7 0 3.32 10.58 8.30 o 0 8 0 4795.76 5400.07 115.78 o 1 8 0 11803.51 11797.73 114.51 o 2 8 0 81.94 83.46 11.63 o 3 8 0 12232.93 12494.14 127.09 o 4 8 0 185.52 224.32 36.35 o 5 8 0 188.84 118.07 25.64 o 6 8 0 1010.81 1035.94 73.58 o 7 8 0 5.85 27.16 6.99 o 8 8 0 5550.86 5597.08 82.01 o 9 8 0 132.38 83.40 15.47 o 10 8 0 673.96 735.10 35.23 o 11 8 0 993.00 956.67 34.22 o 12 8 0 327.70 310.96 15.29 o 1 9 0 893.69 823.26 33.34 o 2 9 0 1915.02 1822.25 50.23 o 3 9 0 1047.68 1145.57 41.66 o 4 9 0 986.62 1011.25 40.65 o 5 9 0 129.93 115.05 26.33 o 6 9 0 1868.27 1743.52 46.13 o 7 9 0 1069.09 1019.31 37.63 o 8 9 0 4276.41 4333.64 60.79 o 9 9 0 119.08 136.05 18.03 o 10 9 0 1001.96 999.86 38.58 o 11 9 0 80.92 72.73 11.65 o 0 10 0 30.59 19.81 13.34 o 1 10 0 1728.47 1667.91 49.85 o 2 10 0 1950.80 2083.48 57.19 o 3 10 0 65.80 81.96 14.16 o 4 10 0 2022.16 2274.28 98.44 o 5 10 0 638.61 708.49 60.37 o 6 10 0 1180.93 1154.88 29.60 o 7 10 0 2.06 3.15 6.80 o 8 10 0 2311.53 2475.97 45.27 o 9 10 0 5.78 4.87 10.73 o 10 10 0 766.93 784.31 32.06 o 11 10 0 809.54 708.79 24.70 o 1 11 0 4119.10 3627.35 103.66 o 2 11 0 5856.52 5748.36 100.91 o 3 11 0 3450.58 3644.25 83.15 o 4 11 0 1247.45 1252.24 77.29 o 5 11 0 2691.01 2843.22 63.55 o 6 11 0 1137.44 1136.94 41.63 o 7 11 0 648.04 639.70 19.77 o 8 11 0 3115.62 3182.04 70.57 o 9 11 0 320.15 343.43 23.24 o 10 11 0 801.37 762.81 28.85 o 11 11 0 56.15 38.96 7.16 o 2 12 0 932.79 843.19 56.46 o 3 12 0 1557.99 1515.68 39.08 o 4 12 0 60.05 53.12 11.29 o 5 12 0 2512.81 2480.63 61.76 o 6 12 0 565.91 567.37 35.89 o 7 12 0 503.98 476.14 21.42 o 8 12 0 973.36 1073.80 39.00 o 9 12 0 62.29 39.88 10.13 o 10 12 0 609.00 609.63 22.47 o 1 13 0 375.82 340.61 27.39 o 2 13 0 118.18 156.22 20.25 o 3 13 0 6.91 34.23 10.55 o 4 13 0 8678.78 8325.52 112.50 o 5 13 0 519.72 448.84 32.90 o 6 13 0 411.56 407.56 31.37 o 7 13 0 816.95 790.49 35.86 o 0 14 0 5755.58 6271.74 114.79 o 1 14 0 205.24 217.34 16.93 o 2 14 0 0.34 5.91 12.36 o 3 14 0 944.09 958.84 47.67 o 4 14 0 184.63 184.61 24.74 o 5 14 0 735.98 785.56 43.48 o 6 14 0 1123.37 999.23 47.54 o 7 14 0 273.22 262.41 23.92 o 1 15 0 224.94 200.07 21.28 o 2 15 0 473.91 508.48 36.43 o 3 15 0 200.98 170.22 24.15 o 4 15 0 1688.32 1760.35 65.44 o 5 15 0 393.93 397.80 32.01 o 6 15 0 638.48 628.91 37.40 o 7 15 0 220.98 212.85 21.38 o 0 16 0 1762.78 1759.58 64.97 o 1 16 0 177.74 171.02 20.70 o 2 16 0 2611.52 2779.33 82.27 o 3 16 0 271.53 293.72 29.21 o 4 16 0 12.75 10.82 14.84 o 5 16 0 624.85 557.02 36.91 o 6 16 0 19.92 9.06 6.34 o 7 16 0 2.61 23.85 10.42 o 1 17 0 16.15 18.45 14.45 o 2 17 0 57.09 56.14 18.76 o 3 17 0 282.92 242.83 27.98 o 4 17 0 903.49 899.64 46.23 o 5 17 0 350.53 411.66 31.40 o 6 17 0 196.39 191.74 13.10 o 7 17 0 91.78 111.29 13.30 o 0 18 0 47.52 74.92 17.75 o 1 18 0 49.86 50.80 10.84 o 2 18 0 14.48 13.47 15.11 o 3 18 0 641.24 642.30 39.05 o 4 18 0 536.18 502.84 34.28 o 5 18 0 123.33 134.37 18.85 o 6 18 0 16.60 11.34 7.31 o 1 19 0 777.40 808.92 41.61 o 2 19 0 17.01 38.79 15.24 o 3 19 0 8.90 -1.55 12.53 o 4 19 0 961.97 942.21 41.77 o 5 19 0 24.70 25.28 9.34 o 6 19 0 37.62 36.69 9.00 o 0 20 0 45.70 32.08 11.64 o 1 20 0 179.47 140.50 18.31 o 2 20 0 25.46 9.40 12.45 o 3 20 0 131.20 135.61 17.72 o 4 20 0 174.96 154.78 10.82 o 5 20 0 0.83 3.55 4.03 o 1 21 0 555.35 586.95 24.82 o 2 21 0 1.90 10.86 5.89 o 3 21 0 0.88 -2.32 9.27 o 1 0 1 12.98 2.42 2.57 o 2 0 1 1266.47 1213.39 31.55 o 3 0 1 100.63 81.08 8.94 o 4 0 1 917.86 863.36 29.04 o 5 0 1 995.07 901.95 33.99 o 6 0 1 31.46 27.22 7.59 o 7 0 1 19.28 29.55 11.74 o 8 0 1 108.09 89.43 7.54 o 9 0 1 765.91 779.88 18.68 o 10 0 1 135.65 154.37 9.31 o 11 0 1 156.28 170.81 8.45 o 12 0 1 127.85 113.12 8.91 o -12 1 1 42.06 46.24 10.25 o -11 1 1 94.09 98.43 8.17 o -10 1 1 100.52 113.59 8.44 o -9 1 1 770.37 816.87 26.44 o -8 1 1 387.62 318.48 11.37 o -7 1 1 453.42 466.56 32.02 o -6 1 1 648.77 676.38 33.73 o -5 1 1 65.65 59.09 7.89 o -4 1 1 801.25 811.69 22.71 o -3 1 1 1550.42 1445.71 31.69 o -2 1 1 231.48 213.17 8.67 o -1 1 1 588.13 580.09 11.47 o 1 1 1 586.57 596.79 10.72 o 2 1 1 232.38 248.01 14.41 o 3 1 1 1556.45 1500.80 42.67 o 4 1 1 796.36 787.18 40.20 o 5 1 1 65.46 52.77 12.02 o 6 1 1 645.14 675.13 27.35 o 7 1 1 453.31 451.02 31.91 o 8 1 1 382.02 322.47 11.65 o 9 1 1 771.01 754.41 19.06 o 10 1 1 99.48 129.44 8.93 o 11 1 1 93.99 98.97 6.99 o 12 1 1 42.34 50.21 10.79 o -12 2 1 146.94 139.49 14.14 o -11 2 1 8.09 15.50 7.04 o -10 2 1 457.90 459.42 14.27 o -9 2 1 70.84 80.21 7.47 o -8 2 1 36.88 40.95 6.51 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4819.67 57.73 o 4 3 1 1322.47 1295.51 34.21 o 5 3 1 88.27 111.61 12.46 o 6 3 1 66.36 35.84 18.52 o 7 3 1 647.98 761.57 60.24 o 8 3 1 159.14 163.25 10.06 o 9 3 1 212.72 219.84 12.29 o 10 3 1 16.29 8.98 8.14 o 11 3 1 25.58 26.98 12.88 o 12 3 1 139.01 146.81 14.86 o -12 4 1 147.29 157.60 14.99 o -11 4 1 44.98 39.24 13.23 o -10 4 1 47.46 42.09 9.82 o -9 4 1 140.42 133.56 10.45 o -8 4 1 36.72 32.11 6.40 o -7 4 1 1181.46 1092.21 73.28 o -6 4 1 301.87 322.98 36.96 o -5 4 1 1624.15 1644.54 71.70 o -4 4 1 830.59 858.87 30.21 o -3 4 1 4022.49 4028.45 52.35 o -2 4 1 1464.62 1234.24 34.54 o -1 4 1 154.70 164.34 13.84 o 0 4 1 15718.55 14860.21 126.77 o 1 4 1 157.29 175.80 10.57 o 2 4 1 1462.85 1264.34 28.28 o 3 4 1 4035.89 3952.28 55.06 o 4 4 1 838.28 841.81 28.69 o 5 4 1 1620.64 1637.65 43.78 o 6 4 1 300.38 262.59 33.11 o 7 4 1 1180.22 1315.48 80.12 o 8 4 1 36.82 34.36 6.70 o 9 4 1 138.50 117.59 9.96 o 10 4 1 48.29 44.35 6.74 o 11 4 1 45.91 43.56 14.74 o 12 4 1 148.85 157.83 14.86 o -12 5 1 127.69 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1 590.04 534.59 22.19 o 0 6 1 8949.34 8810.74 87.08 o 1 6 1 588.90 572.38 21.75 o 2 6 1 1810.47 1756.64 83.50 o 3 6 1 802.73 838.62 29.96 o 4 6 1 78.74 78.32 11.82 o 5 6 1 474.62 439.70 25.19 o 6 6 1 63.66 48.37 20.27 o 7 6 1 87.28 97.13 9.71 o 8 6 1 586.92 561.75 18.11 o 9 6 1 20.39 24.50 6.67 o 10 6 1 20.31 6.72 6.60 o 11 6 1 222.31 210.51 20.49 o 12 6 1 16.45 22.45 9.09 o -12 7 1 345.77 354.52 18.56 o -11 7 1 49.64 56.21 12.65 o -10 7 1 438.35 445.75 29.09 o -9 7 1 235.16 215.29 22.60 o -8 7 1 2035.39 2028.36 42.67 o -7 7 1 316.53 312.07 16.13 o -6 7 1 126.58 170.89 31.39 o -5 7 1 456.02 486.95 44.95 o -4 7 1 776.93 779.10 31.69 o -3 7 1 1998.25 1975.45 47.30 o -2 7 1 28.14 31.42 8.65 o -1 7 1 1160.22 1149.46 28.32 o 0 7 1 154.94 149.97 14.28 o 1 7 1 1160.35 1152.24 33.22 o 2 7 1 28.89 57.57 9.83 o 3 7 1 1989.95 2043.00 59.52 o 4 7 1 776.34 730.16 31.51 o 5 7 1 460.13 440.92 43.26 o 6 7 1 126.70 94.14 24.86 o 7 7 1 315.41 323.58 13.48 o 8 7 1 2032.22 2033.05 75.60 o 9 7 1 234.73 202.95 14.75 o 10 7 1 435.97 439.05 33.74 o 11 7 1 49.15 37.30 11.78 o 12 7 1 341.77 371.80 18.18 o -12 8 1 99.85 100.02 9.88 o -11 8 1 246.96 236.74 18.63 o -10 8 1 458.24 461.49 28.53 o -9 8 1 254.10 262.58 23.65 o -8 8 1 1383.44 1332.23 49.86 o -7 8 1 86.25 76.96 12.23 o -6 8 1 491.93 455.65 49.39 o -5 8 1 79.89 66.48 21.93 o -4 8 1 238.67 214.21 34.05 o -3 8 1 5344.11 5434.10 83.14 o -2 8 1 429.72 441.98 23.80 o -1 8 1 527.13 547.63 25.85 o 0 8 1 1089.42 1181.68 29.53 o 1 8 1 527.35 621.15 36.89 o 2 8 1 426.33 458.85 24.53 o 3 8 1 5361.79 5537.58 85.70 o 4 8 1 236.66 184.35 17.86 o 5 8 1 76.11 79.95 23.59 o 6 8 1 490.80 525.69 52.88 o 7 8 1 86.79 98.28 10.56 o 8 8 1 1385.60 1401.84 35.78 o 9 8 1 248.80 250.97 15.98 o 10 8 1 461.99 505.40 29.83 o 11 8 1 249.49 253.22 19.39 o 12 8 1 98.35 100.38 10.35 o -11 9 1 197.88 175.24 15.24 o -10 9 1 5.49 -0.21 11.67 o -9 9 1 229.29 259.79 23.01 o -8 9 1 720.59 761.26 37.69 o -7 9 1 487.49 495.63 26.64 o -6 9 1 298.51 261.37 18.78 o -5 9 1 452.88 426.06 44.62 o -4 9 1 802.67 714.98 54.66 o -3 9 1 412.92 409.14 32.69 o -2 9 1 812.92 787.84 33.61 o -1 9 1 1711.26 1721.33 47.76 o 0 9 1 863.38 888.06 32.82 o 1 9 1 1714.85 1730.61 56.42 o 2 9 1 819.36 772.45 59.12 o 3 9 1 415.63 385.96 24.92 o 4 9 1 800.88 748.95 55.47 o 5 9 1 455.34 403.98 45.65 o 6 9 1 298.44 287.78 32.93 o 7 9 1 486.21 536.33 21.32 o 8 9 1 715.77 717.33 25.95 o 9 9 1 228.27 247.25 15.43 o 10 9 1 4.91 -5.20 11.47 o 11 9 1 197.54 183.58 15.65 o -11 10 1 501.49 457.46 20.25 o -10 10 1 465.87 501.96 26.44 o -9 10 1 52.87 69.74 13.29 o -8 10 1 1005.67 1047.56 42.57 o -7 10 1 0.14 4.53 9.12 o -6 10 1 125.83 93.33 11.82 o -5 10 1 240.93 280.72 39.66 o -4 10 1 313.48 334.46 40.08 o -3 10 1 1098.62 1148.88 44.27 o -2 10 1 434.92 460.53 28.27 o -1 10 1 544.37 480.75 27.79 o 0 10 1 356.50 306.18 27.34 o 1 10 1 545.46 486.61 27.35 o 2 10 1 434.23 479.37 44.43 o 3 10 1 1099.35 1143.40 44.46 o 4 10 1 314.09 345.69 26.52 o 5 10 1 240.42 239.03 37.06 o 6 10 1 126.06 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