#------------------------------------------------------------------------------ #$Date: 2020-08-06 10:03:21 +0300 (Thu, 06 Aug 2020) $ #$Revision: 254857 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/22/2022217.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022217 _cell_angle_alpha 84.538 _cell_angle_beta 86.265 _cell_angle_gamma 85.919 _cell_length_a 12.5006 _cell_length_b 12.7609 _cell_length_c 15.0775 _exptl_crystal_F_000 980.00 _reflns_d_resolution_high 0.8406 _cod_data_source_file lf3118Isup2.hkl _cod_data_source_block I _shelx_title ' 061018a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.60 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 0 0 2256.63 2126.23 28.24 o 6 0 0 53.51 73.21 6.12 o 7 0 0 24.61 71.41 6.90 o 8 0 0 57.98 55.46 5.70 o 9 0 0 17.89 17.93 7.88 o 10 0 0 969.72 956.82 45.80 o 11 0 0 24.68 26.11 7.92 o 12 0 0 210.12 227.50 21.72 o 13 0 0 48.82 69.55 17.78 o 14 0 0 32.76 40.25 14.26 o -14 1 0 80.43 90.78 17.64 o -13 1 0 321.49 322.36 27.70 o -12 1 0 74.97 105.11 15.91 o -11 1 0 13.87 27.49 8.28 o -10 1 0 27.07 43.53 9.51 o -9 1 0 301.01 284.03 15.56 o -8 1 0 1.53 1.87 2.90 o -7 1 0 425.77 437.90 16.04 o -6 1 0 2434.33 2502.85 34.74 o -5 1 0 2112.43 2117.95 27.70 o -4 1 0 6779.30 6753.03 61.35 o -3 1 0 59859.57 60253.57 323.08 o -2 1 0 6956.45 8492.06 87.45 o 2 1 0 99.60 96.80 3.85 o 3 1 0 9373.40 10234.76 74.80 o 4 1 0 59.71 71.08 2.96 o 5 1 0 4.95 6.32 2.01 o 6 1 0 421.55 348.26 9.47 o 7 1 0 2866.88 2734.71 31.50 o 8 1 0 94.27 125.74 10.80 o 9 1 0 104.22 83.09 7.85 o 10 1 0 418.50 386.08 35.09 o 11 1 0 96.94 123.71 14.66 o 12 1 0 0.81 6.54 9.28 o 13 1 0 396.32 420.29 29.88 o 14 1 0 300.76 299.78 33.57 o -14 2 0 0.19 -6.68 12.90 o -13 2 0 0.65 16.88 11.76 o -12 2 0 40.14 43.66 13.13 o -11 2 0 22.24 35.13 12.04 o -10 2 0 201.04 240.74 16.82 o -9 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21.46 o 9 8 0 14.83 21.64 6.27 o 10 8 0 112.58 126.60 14.43 o 11 8 0 45.34 63.71 14.12 o 12 8 0 14.75 30.20 17.41 o 13 8 0 79.04 86.18 22.39 o -11 9 0 14.66 -11.80 14.42 o -10 9 0 127.47 129.49 24.32 o -9 9 0 261.80 262.03 30.29 o -8 9 0 665.42 641.70 43.38 o -7 9 0 3.95 -0.08 26.25 o -6 9 0 0.22 -31.38 30.32 o -5 9 0 24.31 0.85 27.51 o -4 9 0 754.48 803.21 67.57 o -3 9 0 591.74 589.99 57.14 o -2 9 0 44.13 47.93 25.17 o -1 9 0 226.96 271.72 39.77 o 0 9 0 40.89 66.32 24.91 o 1 9 0 1976.48 2086.10 86.22 o 2 9 0 1534.51 1682.65 77.49 o 3 9 0 137.42 119.04 25.08 o 4 9 0 42.22 21.70 13.34 o 5 9 0 119.72 127.32 17.60 o 6 9 0 7.03 18.52 10.69 o 7 9 0 60.24 63.04 10.95 o 8 9 0 704.51 641.75 25.16 o 9 9 0 506.22 497.68 23.55 o 10 9 0 36.68 39.85 16.37 o 11 9 0 402.87 416.96 42.29 o 12 9 0 149.22 210.52 31.71 o -10 10 0 40.91 34.60 51.87 o -9 10 0 35.43 42.47 25.28 o -8 10 0 623.64 632.66 65.35 o -7 10 0 634.52 547.21 60.50 o -6 10 0 76.23 7.13 26.37 o -5 10 0 0.62 25.41 18.65 o -4 10 0 211.08 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