#------------------------------------------------------------------------------ #$Date: 2020-07-22 08:05:11 +0300 (Wed, 22 Jul 2020) $ #$Revision: 254469 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/21/2022196.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022196 _cell_angle_alpha 90.000 _cell_angle_beta 90.720 _cell_angle_gamma 90.000 _cell_length_a 10.8071 _cell_length_b 23.4412 _cell_length_c 23.6644 _exptl_crystal_F_000 6188.00 _reflns_d_resolution_high 0.8083 _cod_data_source_file jx30582sup3.hkl _cod_data_source_block 2 _shelx_title ' ip2-2538 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 2119.34 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4387.56 27005.53 3831.49 o 6 0 0 149233.66 173509.11 4123.02 o 8 0 0 1470844.88 1697831.25 27449.76 o 10 0 0 127515.54 140450.94 4645.91 o 12 0 0 140654.58 159395.53 5511.24 o 2 1 0 1574.95 3840.48 3213.80 o 3 1 0 467756.47 467987.81 9874.88 o 4 1 0 54029.34 61974.81 3748.20 o 5 1 0 33151.25 38011.63 2343.17 o 6 1 0 7033.84 9122.64 1914.90 o 7 1 0 215258.36 242069.92 3559.49 o 8 1 0 26521.47 36587.70 2181.02 o 9 1 0 2818.82 5040.33 1830.60 o 10 1 0 913.96 1284.51 2178.55 o 11 1 0 46182.11 56055.64 2305.05 o 12 1 0 1223.58 1686.30 2146.46 o 13 1 0 1128.18 1306.98 1884.31 o 1 2 0 246.56 1048.12 4960.85 o 2 2 0 248767.69 273981.84 9687.47 o 3 2 0 24601.72 18895.54 6124.37 o 4 2 0 817539.69 839559.00 19287.02 o 5 2 0 12995.70 14090.44 3183.65 o 6 2 0 17134.06 13844.94 2327.90 o 7 2 0 58841.84 67648.40 2422.45 o 8 2 0 153393.98 182695.47 4398.34 o 9 2 0 25.29 51.00 2265.11 o 10 2 0 2784.37 2568.62 2113.58 o 11 2 0 33594.32 40389.40 2362.87 o 12 2 0 10942.27 12521.08 1942.26 o 13 2 0 63.53 1187.28 1872.85 o 1 3 0 72353.11 53538.31 47690.02 o 2 3 0 10095.67 11993.77 5830.81 o 3 3 0 10826.03 11665.94 3385.74 o 4 3 0 26171.77 22129.11 2730.51 o 5 3 0 380205.50 415536.19 12614.30 o 6 3 0 2049.61 2711.66 3155.89 o 7 3 0 7703.41 7888.30 2317.47 o 8 3 0 18639.96 16975.03 2077.68 o 9 3 0 107216.55 123469.69 2877.98 o 10 3 0 3901.14 3674.73 1976.04 o 11 3 0 5208.62 8168.88 1947.77 o 12 3 0 5480.50 6956.17 2118.10 o 13 3 0 20333.83 18559.86 1979.95 o 0 4 0 20903.39 18833.53 3206.79 o 1 4 0 916.26 209.65 2173.55 o 2 4 0 128.88 5491.04 4797.24 o 3 4 0 3258.12 5869.05 3784.66 o 4 4 0 4724.74 5849.43 2855.05 o 5 4 0 8548.54 10774.92 2107.26 o 6 4 0 3490.70 3748.20 3271.57 o 7 4 0 1032.16 2892.13 3192.91 o 8 4 0 1598.79 2109.52 1887.50 o 9 4 0 9125.23 10872.79 1948.99 o 10 4 0 383.03 403.33 2152.40 o 11 4 0 428.91 729.37 1722.53 o 12 4 0 164.45 1261.19 1690.66 o 13 4 0 2922.56 2072.69 1837.90 o 1 5 0 601425.44 555359.88 6439.02 o 2 5 0 2031.26 3534.16 2370.16 o 3 5 0 219886.44 212604.38 16073.29 o 4 5 0 645.78 -350.14 2755.81 o 5 5 0 272226.41 262680.84 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