#------------------------------------------------------------------------------ #$Date: 2020-06-30 07:56:05 +0300 (Tue, 30 Jun 2020) $ #$Revision: 253553 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/21/2022177.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022177 _cell_angle_alpha 90.000 _cell_angle_beta 98.393 _cell_angle_gamma 90.000 _cell_length_a 11.2862 _cell_length_b 29.3083 _cell_length_c 19.6024 _exptl_crystal_F_000 3428.00 _reflns_d_resolution_high 0.8406 _cod_data_source_file yo3074Isup2.hkl _cod_data_source_block I _shelx_title ' fe in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 584.57 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 48363.27 40544.45 369.69 o 4 0 0 2778.13 2740.90 63.12 o 6 0 0 19032.13 19308.69 238.61 o 8 0 0 42.71 61.79 21.54 o 10 0 0 132.36 -13.10 96.20 o 12 0 0 997.01 1329.19 246.80 o 2 1 0 270.84 38.60 10.73 o 3 1 0 137264.14 142073.19 837.11 o 4 1 0 20932.03 23627.22 155.85 o 5 1 0 1045.43 1296.69 29.63 o 6 1 0 5751.92 5853.27 102.26 o 7 1 0 91.15 166.25 15.11 o 8 1 0 7436.91 7301.70 174.60 o 9 1 0 94.55 97.68 31.55 o 10 1 0 4297.05 3617.55 247.70 o 11 1 0 785.60 724.24 118.96 o 12 1 0 10.44 81.75 81.09 o 13 1 0 3174.14 3657.66 206.02 o 2 2 0 175.27 248.78 14.32 o 3 2 0 8240.97 9287.66 180.92 o 4 2 0 1277.08 1401.43 31.39 o 5 2 0 19661.99 19381.25 184.23 o 6 2 0 6.95 -8.24 9.24 o 7 2 0 582.22 394.72 22.58 o 8 2 0 3517.91 3302.43 78.53 o 9 2 0 44.33 9.78 33.45 o 10 2 0 2636.94 2694.07 148.98 o 11 2 0 732.30 758.03 128.35 o 12 2 0 1264.18 1622.43 192.13 o 13 2 0 948.05 1239.27 125.81 o 2 3 0 1852.81 2812.18 55.34 o 3 3 0 262.36 544.38 28.72 o 4 3 0 10421.34 9255.59 131.21 o 5 3 0 7.93 120.42 14.90 o 6 3 0 5162.82 5576.43 92.19 o 7 3 0 275.20 314.76 22.11 o 8 3 0 2471.13 2531.57 92.21 o 9 3 0 1045.42 1398.87 107.88 o 10 3 0 121.53 106.62 43.62 o 11 3 0 2107.92 2160.51 204.71 o 12 3 0 719.87 759.19 193.71 o 13 3 0 860.28 997.08 130.57 o 1 4 0 1493.40 1663.85 70.26 o 2 4 0 153.89 791.68 52.07 o 3 4 0 18160.50 18565.97 208.47 o 4 4 0 96.19 84.27 23.61 o 5 4 0 9639.04 10344.61 155.37 o 6 4 0 1579.30 1537.56 59.97 o 7 4 0 2701.23 2664.04 94.17 o 8 4 0 2841.74 2816.14 100.79 o 9 4 0 3365.06 3353.01 167.76 o 10 4 0 3005.12 2883.52 224.73 o 11 4 0 205.71 117.90 68.72 o 12 4 0 352.31 289.51 134.23 o 13 4 0 0.83 48.91 56.79 o 1 5 0 36.75 96.45 14.66 o 2 5 0 7111.81 6858.90 72.85 o 3 5 0 2613.29 3471.18 64.41 o 4 5 0 38371.24 35981.07 370.95 o 5 5 0 1924.70 2396.22 103.33 o 6 5 0 646.70 526.59 43.79 o 7 5 0 6014.55 5564.94 142.47 o 8 5 0 2798.80 2546.75 98.62 o 9 5 0 1.24 -78.15 52.10 o 10 5 0 759.23 705.46 119.74 o 11 5 0 10.95 76.15 68.30 o 12 5 0 187.43 140.18 55.79 o 13 5 0 212.35 67.34 65.97 o 0 6 0 13268.80 12145.21 169.21 o 1 6 0 35386.81 40113.45 296.79 o 2 6 0 24285.38 25601.48 190.80 o 3 6 0 47644.66 43721.44 349.54 o 4 6 0 140.38 147.05 15.64 o 5 6 0 57.57 48.73 22.38 o 6 6 0 11420.88 11073.66 220.89 o 7 6 0 16343.92 16603.88 427.27 o 8 6 0 1118.97 1188.04 80.15 o 9 6 0 2170.30 2257.05 116.34 o 10 6 0 34.10 135.14 59.42 o 11 6 0 487.40 748.94 101.37 o 12 6 0 11.54 -53.79 89.66 o 13 6 0 250.30 249.38 93.13 o 1 7 0 747.30 635.48 26.28 o 2 7 0 81752.52 86782.49 630.48 o 3 7 0 1289.07 1478.87 45.64 o 4 7 0 383.90 391.25 26.72 o 5 7 0 18388.47 19590.90 326.59 o 6 7 0 11941.89 12916.24 290.78 o 7 7 0 488.43 539.02 59.18 o 8 7 0 1597.28 1448.02 104.18 o 9 7 0 50.93 8.06 29.51 o 10 7 0 5247.51 5739.87 245.26 o 11 7 0 7485.55 8054.72 312.69 o 12 7 0 604.57 677.62 154.12 o 13 7 0 259.94 413.25 111.63 o 0 8 0 124039.02 129360.66 1294.33 o 1 8 0 899.86 1338.23 39.14 o 2 8 0 83642.79 84394.52 553.35 o 3 8 0 5847.41 6055.34 95.99 o 4 8 0 5367.19 5340.13 90.97 o 5 8 0 598.20 765.65 49.00 o 6 8 0 943.63 963.46 110.19 o 7 8 0 345.15 520.74 62.33 o 8 8 0 6080.23 6161.36 193.25 o 9 8 0 2690.38 2677.30 131.98 o 10 8 0 79.29 34.07 54.89 o 11 8 0 20.50 144.57 84.77 o 12 8 0 36.92 63.22 63.82 o 1 9 0 16099.41 19663.49 197.68 o 2 9 0 9274.31 8928.97 109.00 o 3 9 0 677.90 860.90 58.25 o 4 9 0 18033.52 19257.44 214.43 o 5 9 0 37170.95 37724.42 698.76 o 6 9 0 93.36 138.07 25.87 o 7 9 0 3342.92 3382.38 157.78 o 8 9 0 336.99 418.63 61.36 o 9 9 0 291.98 280.37 41.71 o 10 9 0 1192.70 1003.55 130.20 o 11 9 0 3263.63 3164.74 194.51 o 12 9 0 58.16 45.77 69.26 o 0 10 0 4086.86 3989.38 109.27 o 1 10 0 3519.02 4072.37 67.76 o 2 10 0 12048.81 12831.25 194.04 o 3 10 0 32122.62 32723.85 356.37 o 4 10 0 9628.65 8857.11 168.73 o 5 10 0 4955.90 4211.72 76.25 o 6 10 0 3041.75 2874.51 81.03 o 7 10 0 788.30 674.29 94.41 o 8 10 0 1578.44 1747.28 100.67 o 9 10 0 610.19 563.17 55.58 o 10 10 0 1576.55 1606.03 145.25 o 11 10 0 14.31 -101.30 67.53 o 12 10 0 482.15 470.97 105.01 o 1 11 0 15549.61 15015.30 160.11 o 2 11 0 16461.78 17571.84 211.82 o 3 11 0 2177.62 1660.08 61.60 o 4 11 0 191.52 164.39 23.17 o 5 11 0 2067.50 2013.09 46.62 o 6 11 0 2011.43 1978.16 82.82 o 7 11 0 4263.82 3956.96 155.63 o 8 11 0 914.53 837.35 67.03 o 9 11 0 1278.16 1319.13 83.63 o 10 11 0 882.89 807.01 100.07 o 11 11 0 286.45 183.00 59.06 o 12 11 0 82.92 130.84 145.81 o 0 12 0 37561.23 39342.93 642.25 o 1 12 0 5484.63 6289.70 105.33 o 2 12 0 12495.52 14356.75 194.84 o 3 12 0 817.50 729.89 42.07 o 4 12 0 39.58 40.00 21.37 o 5 12 0 857.06 773.01 38.03 o 6 12 0 2957.01 2880.91 76.60 o 7 12 0 5253.76 4865.82 126.95 o 8 12 0 720.97 784.70 67.58 o 9 12 0 501.66 392.80 47.79 o 10 12 0 63.70 -44.57 52.77 o 11 12 0 2906.29 3105.71 199.90 o 12 12 0 27.44 6.09 62.02 o 1 13 0 3128.08 2960.35 77.41 o 2 13 0 40087.89 44689.66 425.34 o 3 13 0 465.75 470.39 36.48 o 4 13 0 1077.01 1306.29 68.41 o 5 13 0 5306.05 5582.84 155.50 o 6 13 0 36.21 42.70 8.16 o 7 13 0 1090.31 1136.23 53.23 o 8 13 0 61.76 42.15 24.40 o 9 13 0 40.15 38.60 46.70 o 10 13 0 1008.24 947.55 108.16 o 11 13 0 883.56 953.08 116.36 o 12 13 0 107.81 168.88 134.48 o 0 14 0 0.81 109.08 36.14 o 1 14 0 709.41 777.44 44.63 o 2 14 0 4271.12 3799.57 117.97 o 3 14 0 784.94 583.21 47.09 o 4 14 0 12.52 100.73 31.62 o 5 14 0 10217.93 9609.05 197.84 o 6 14 0 531.10 470.99 36.98 o 7 14 0 6.84 -0.28 18.41 o 8 14 0 346.09 393.19 47.45 o 9 14 0 9.77 4.23 47.49 o 10 14 0 2554.68 2410.99 172.32 o 11 14 0 451.08 700.24 118.87 o 12 14 0 291.13 380.92 167.72 o 1 15 0 5610.34 4534.21 113.26 o 2 15 0 15871.06 16206.97 239.40 o 3 15 0 1427.19 1308.43 71.79 o 4 15 0 25144.32 24920.72 437.55 o 5 15 0 0.62 41.64 30.75 o 6 15 0 169.74 155.45 29.41 o 7 15 0 4357.18 4076.87 263.99 o 8 15 0 2608.55 2574.21 202.08 o 9 15 0 163.55 39.66 78.98 o 10 15 0 20.97 -107.57 93.93 o 11 15 0 1263.04 1262.64 135.88 o 0 16 0 4585.31 4078.70 197.99 o 1 16 0 11.28 9.51 19.81 o 2 16 0 4115.80 3408.61 111.69 o 3 16 0 421.41 335.05 61.11 o 4 16 0 365.10 733.06 77.53 o 5 16 0 4363.66 4682.92 227.87 o 6 16 0 12966.45 12868.91 282.55 o 7 16 0 1671.13 1601.71 158.66 o 8 16 0 173.28 153.81 73.00 o 9 16 0 3108.25 2951.77 226.98 o 10 16 0 56.83 -40.29 113.33 o 11 16 0 421.87 506.58 104.14 o 1 17 0 932.00 900.32 53.14 o 2 17 0 1246.70 1223.94 44.35 o 3 17 0 732.46 838.48 75.56 o 4 17 0 8990.02 9438.25 261.32 o 5 17 0 588.24 462.80 64.58 o 6 17 0 173.60 193.82 38.84 o 7 17 0 25.81 178.49 75.33 o 8 17 0 247.49 191.04 221.87 o 9 17 0 1849.06 1868.99 190.49 o 10 17 0 961.73 1032.53 214.06 o 11 17 0 1924.63 2230.92 226.50 o 0 18 0 18301.35 18102.72 357.69 o 1 18 0 66.55 -3.86 29.13 o 2 18 0 4883.03 5126.22 117.83 o 3 18 0 3.74 226.70 56.99 o 4 18 0 25271.04 25601.87 607.43 o 5 18 0 427.67 357.49 54.76 o 6 18 0 1728.41 1383.58 93.48 o 7 18 0 5410.50 5813.65 313.36 o 8 18 0 3515.42 3453.49 277.52 o 9 18 0 1.97 99.52 110.56 o 10 18 0 36.16 133.98 115.34 o 11 18 0 1259.11 1319.87 178.92 o 1 19 0 577.82 738.30 60.71 o 2 19 0 2054.91 1692.42 92.57 o 3 19 0 12268.76 13286.03 336.92 o 4 19 0 4711.19 5729.96 259.12 o 5 19 0 3584.13 3355.44 159.68 o 6 19 0 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90.53 66.18 o 7 22 0 1690.32 1415.63 165.28 o 8 22 0 512.16 347.29 99.38 o 9 22 0 73.03 -13.10 89.15 o 10 22 0 72.76 -51.37 119.37 o 1 23 0 2291.79 2165.18 94.52 o 2 23 0 1629.31 1590.81 81.01 o 3 23 0 7072.33 7572.61 316.53 o 4 23 0 508.17 443.72 88.57 o 5 23 0 1966.22 1847.49 131.06 o 6 23 0 1270.20 1340.04 168.18 o 7 23 0 111.81 127.30 79.91 o 8 23 0 443.95 374.42 103.81 o 9 23 0 17.25 -83.11 119.87 o 0 24 0 5127.45 5549.57 212.94 o 1 24 0 326.08 385.82 44.84 o 2 24 0 1910.34 1971.55 117.98 o 3 24 0 1157.41 1194.74 112.53 o 4 24 0 914.02 988.38 104.38 o 5 24 0 769.85 709.87 87.58 o 6 24 0 2.64 151.25 89.40 o 7 24 0 1256.19 1104.81 161.87 o 8 24 0 16.12 -132.47 124.41 o 9 24 0 0.56 -66.99 105.27 o 1 25 0 1625.56 1833.28 91.53 o 2 25 0 1983.05 2080.29 124.56 o 3 25 0 3.68 -22.11 38.96 o 4 25 0 2206.64 2502.87 164.17 o 5 25 0 43.09 22.06 43.73 o 6 25 0 46.12 277.51 164.20 o 7 25 0 837.09 876.90 144.55 o 8 25 0 192.20 117.36 107.79 o 9 25 0 541.14 831.06 209.53 o 0 26 0 1556.51 1823.15 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