#------------------------------------------------------------------------------ #$Date: 2020-06-28 07:50:55 +0300 (Sun, 28 Jun 2020) $ #$Revision: 253532 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/21/2022169.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022169 _cell_angle_alpha 90.000 _cell_angle_beta 103.645 _cell_angle_gamma 90.000 _cell_length_a 7.0226 _cell_length_b 7.9585 _cell_length_c 12.5188 _exptl_crystal_F_000 280.00 _reflns_d_resolution_high 0.7902 _cod_data_source_file ky31962csup4.hkl _cod_data_source_block 2c _shelx_title ' KM-417' _shelx_refln_list_code 4 _shelx_f_calc_maximum 79.18 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -10 0 280.22 281.24 7.82 o 1 -9 0 12.44 9.12 1.11 o 2 -9 0 75.89 77.24 2.39 o 3 -9 0 9.28 7.91 0.66 o 0 -8 0 598.48 576.65 13.08 o 1 -8 0 82.81 82.68 2.17 o 2 -8 0 71.71 68.82 2.78 o 3 -8 0 278.42 278.83 5.31 o 4 -8 0 2.86 2.35 0.41 o 5 -8 0 63.33 61.91 2.16 o 1 -7 0 20.55 17.39 0.90 o 2 -7 0 370.43 353.31 5.14 o 3 -7 0 33.90 37.58 1.50 o 4 -7 0 321.50 327.59 4.59 o 5 -7 0 118.06 127.38 2.68 o 6 -7 0 19.39 17.65 1.06 o 0 -6 0 444.10 447.18 5.52 o 1 -6 0 252.99 251.40 3.78 o 2 -6 0 18.15 16.97 0.80 o 3 -6 0 309.35 294.30 3.94 o 4 -6 0 117.42 110.43 2.24 o 5 -6 0 11.93 11.63 0.98 o 6 -6 0 141.04 143.67 2.75 o 1 -5 0 198.39 188.97 2.64 o 2 -5 0 146.17 153.94 2.29 o 3 -5 0 15.48 16.16 0.79 o 4 -5 0 322.44 328.56 3.79 o 5 -5 0 98.11 96.34 2.26 o 6 -5 0 12.66 10.78 1.14 o 7 -5 0 45.71 43.41 1.98 o 0 -4 0 1629.19 1607.70 15.19 o 1 -4 0 190.06 201.04 2.68 o 2 -4 0 37.34 38.70 1.10 o 3 -4 0 626.65 596.93 5.81 o 4 -4 0 71.44 72.80 1.48 o 5 -4 0 185.30 184.51 2.59 o 6 -4 0 238.13 233.43 4.43 o 7 -4 0 113.25 120.63 3.85 o 1 -3 0 1084.27 1042.35 27.51 o 2 -3 0 31.74 25.96 0.70 o 3 -3 0 257.46 277.25 3.20 o 4 -3 0 121.61 115.22 1.95 o 5 -3 0 240.27 239.15 2.84 o 6 -3 0 142.25 140.58 2.55 o 7 -3 0 110.95 114.24 2.84 o 8 -3 0 4.29 4.37 0.63 o 0 -2 0 2710.37 2525.85 38.63 o 1 -2 0 397.50 388.42 6.34 o 2 -2 0 363.43 362.17 5.78 o 3 -2 0 1164.84 1187.02 11.08 o 4 -2 0 105.43 114.68 2.30 o 5 -2 0 12.40 11.86 0.68 o 6 -2 0 266.48 247.34 3.40 o 7 -2 0 81.33 78.42 2.22 o 8 -2 0 50.54 49.82 1.19 o 1 -1 0 187.61 227.77 3.63 o 2 -1 0 652.62 638.36 12.28 o 3 -1 0 324.09 337.28 3.74 o 4 -1 0 826.01 865.57 10.71 o 5 -1 0 269.95 281.75 3.11 o 6 -1 0 37.51 34.82 1.11 o 7 -1 0 192.66 198.61 3.90 o 8 -1 0 12.07 12.48 0.81 o 1 0 0 796.92 767.94 7.58 o 2 0 0 3028.58 3131.27 30.16 o 3 0 0 23.80 17.77 1.00 o 4 0 0 3.42 1.82 0.26 o 5 0 0 145.73 128.06 2.16 o 6 0 0 608.99 605.55 6.63 o 7 0 0 1.74 1.12 0.30 o 8 0 0 82.68 78.64 3.00 o 1 1 0 200.03 240.44 4.06 o 2 1 0 597.12 567.79 6.23 o 3 1 0 330.92 352.97 4.70 o 4 1 0 774.71 808.43 10.68 o 5 1 0 259.56 268.18 6.02 o 6 1 0 42.53 40.15 1.41 o 7 1 0 175.65 182.45 4.21 o 8 1 0 10.85 11.74 0.94 o 0 2 0 2477.08 2485.97 38.27 o 1 2 0 384.96 368.64 3.80 o 2 2 0 368.19 379.95 4.66 o 3 2 0 1194.77 1229.42 11.22 o 4 2 0 112.07 129.60 2.51 o 5 2 0 6.06 4.87 0.44 o 6 2 0 281.99 267.91 3.38 o 7 2 0 75.41 74.40 3.71 o 8 2 0 59.51 64.63 1.73 o 1 3 0 1164.96 1249.73 14.46 o 2 3 0 49.63 43.09 0.86 o 3 3 0 267.27 300.34 3.04 o 4 3 0 125.34 120.63 1.99 o 5 3 0 203.54 214.09 3.41 o 6 3 0 137.79 139.30 2.27 o 7 3 0 137.04 143.83 2.85 o 8 3 0 9.15 7.99 0.93 o 0 4 0 1724.71 1838.50 24.74 o 1 4 0 175.94 186.60 2.14 o 2 4 0 39.81 39.16 0.98 o 3 4 0 630.54 624.97 5.29 o 4 4 0 65.88 65.72 1.37 o 5 4 0 185.61 195.31 2.74 o 6 4 0 229.73 238.22 3.77 o 7 4 0 118.92 117.92 3.29 o 1 5 0 211.98 213.96 2.45 o 2 5 0 137.24 144.91 1.92 o 3 5 0 14.28 15.13 0.54 o 4 5 0 319.43 336.06 4.13 o 5 5 0 122.59 126.68 2.31 o 6 5 0 13.47 11.18 0.76 o 7 5 0 47.54 44.57 1.91 o 0 6 0 423.32 449.12 6.08 o 1 6 0 282.89 287.66 2.68 o 2 6 0 28.22 29.26 0.92 o 3 6 0 345.82 340.89 4.35 o 4 6 0 104.02 104.96 2.28 o 5 6 0 13.99 13.25 0.84 o 6 6 0 136.15 143.14 3.09 o 1 7 0 8.39 7.41 0.52 o 2 7 0 411.80 412.64 4.95 o 3 7 0 35.47 40.03 1.46 o 4 7 0 346.12 356.03 5.07 o 5 7 0 115.32 118.91 2.25 o 6 7 0 18.79 16.33 0.95 o 0 8 0 614.47 611.92 8.36 o 1 8 0 74.75 78.65 2.01 o 2 8 0 74.97 74.56 2.27 o 4 8 0 3.91 3.08 0.42 o 5 8 0 71.32 63.02 2.91 o 1 9 0 19.89 16.76 0.91 o 2 9 0 66.40 67.13 2.67 o 3 9 0 9.68 9.88 0.92 o 0 10 0 236.39 232.29 6.70 o -1 -10 1 110.92 106.76 3.79 o 0 -10 1 46.99 46.49 2.31 o -3 -9 1 35.95 36.96 1.23 o -2 -9 1 13.54 12.43 0.83 o -1 -9 1 27.63 28.63 1.50 o 0 -9 1 44.94 45.69 1.69 o 1 -9 1 59.45 62.07 2.85 o 2 -9 1 21.67 19.39 1.22 o 3 -9 1 72.65 66.99 1.92 o -5 -8 1 37.98 36.80 1.69 o -4 -8 1 69.84 70.05 2.07 o -3 -8 1 108.67 104.15 2.40 o -2 -8 1 96.04 94.46 4.10 o -1 -8 1 192.14 189.63 3.43 o 0 -8 1 20.15 20.98 1.37 o 1 -8 1 403.92 406.92 6.16 o 2 -8 1 16.17 14.44 1.08 o 3 -8 1 12.04 11.87 0.93 o 4 -8 1 39.59 38.78 1.62 o 5 -8 1 55.82 50.44 1.77 o -6 -7 1 69.80 66.82 1.82 o -5 -7 1 32.52 28.66 1.36 o -4 -7 1 29.15 24.95 1.30 o -3 -7 1 269.70 275.13 6.69 o -2 -7 1 178.49 173.39 2.69 o -1 -7 1 258.42 260.56 4.09 o 0 -7 1 39.56 36.17 1.20 o 1 -7 1 70.30 68.65 1.94 o 2 -7 1 74.16 75.71 1.69 o 3 -7 1 20.29 19.24 1.06 o 4 -7 1 257.63 250.07 3.98 o 5 -7 1 81.35 82.38 4.16 o -6 -6 1 2.12 1.94 0.33 o -5 -6 1 137.01 140.24 3.29 o -4 -6 1 65.99 64.82 1.72 o -3 -6 1 178.37 173.98 3.26 o -2 -6 1 265.25 261.03 3.14 o -1 -6 1 343.40 330.47 4.09 o 0 -6 1 45.43 44.15 1.09 o 1 -6 1 486.24 479.32 4.90 o 2 -6 1 213.41 206.40 3.03 o 3 -6 1 127.80 124.02 2.39 o 4 -6 1 243.21 234.32 3.87 o 5 -6 1 96.42 94.82 2.33 o 6 -6 1 95.20 96.57 2.34 o -7 -5 1 61.07 63.78 2.62 o -6 -5 1 8.17 8.40 1.15 o -5 -5 1 151.69 146.97 2.56 o -4 -5 1 231.53 228.48 2.97 o -3 -5 1 35.88 33.13 1.07 o -2 -5 1 130.34 117.76 1.85 o -1 -5 1 481.41 462.82 4.52 o 0 -5 1 114.45 105.99 1.69 o 1 -5 1 133.01 137.56 1.87 o 2 -5 1 111.32 104.28 1.48 o 3 -5 1 56.63 52.02 1.40 o 4 -5 1 68.73 67.75 1.56 o 5 -5 1 88.23 83.45 2.51 o 6 -5 1 91.92 95.58 3.17 o 7 -5 1 5.73 6.14 0.69 o -7 -4 1 45.28 49.03 1.80 o -6 -4 1 56.07 54.30 1.67 o -5 -4 1 149.81 147.09 2.75 o -4 -4 1 10.38 11.37 0.50 o -3 -4 1 46.95 46.41 1.33 o -2 -4 1 420.58 413.82 6.47 o -1 -4 1 215.84 192.11 2.32 o 0 -4 1 79.16 89.10 1.20 o 1 -4 1 265.94 262.38 2.79 o 2 -4 1 816.49 837.37 6.30 o 3 -4 1 218.88 219.49 2.44 o 4 -4 1 555.58 554.02 5.86 o 5 -4 1 179.99 171.42 3.80 o 6 -4 1 24.92 28.34 1.57 o 7 -4 1 186.05 192.71 5.27 o -8 -3 1 38.67 37.25 3.89 o -7 -3 1 302.42 297.64 4.41 o -6 -3 1 13.73 15.77 0.93 o -5 -3 1 52.91 51.17 1.15 o -4 -3 1 73.77 79.67 1.42 o -3 -3 1 521.54 506.12 5.37 o -2 -3 1 67.31 62.48 1.22 o -1 -3 1 1531.85 1539.16 15.73 o 0 -3 1 172.36 185.22 2.22 o 1 -3 1 519.25 515.14 6.57 o 2 -3 1 823.66 823.71 10.15 o 3 -3 1 81.02 75.50 1.26 o 4 -3 1 104.95 111.31 1.70 o 5 -3 1 105.20 103.75 1.77 o 6 -3 1 35.82 41.45 1.39 o 7 -3 1 112.20 100.12 2.59 o 8 -3 1 167.57 146.17 4.86 o -8 -2 1 49.59 47.20 1.23 o -7 -2 1 159.17 160.06 3.11 o -6 -2 1 9.17 9.21 0.51 o -5 -2 1 289.80 276.12 4.07 o -4 -2 1 172.96 164.13 2.59 o -3 -2 1 175.84 184.84 2.53 o -2 -2 1 860.93 835.86 9.02 o -1 -2 1 1275.32 1244.02 11.94 o 0 -2 1 1142.00 1109.37 12.37 o 1 -2 1 4426.32 4400.85 76.90 o 2 -2 1 142.59 134.60 2.41 o 3 -2 1 445.77 473.25 4.07 o 4 -2 1 342.09 335.64 3.28 o 5 -2 1 344.44 338.81 5.29 o 6 -2 1 164.10 159.97 2.98 o 7 -2 1 132.47 134.48 3.38 o 8 -2 1 32.63 26.05 1.24 o -8 -1 1 14.39 14.01 1.05 o -7 -1 1 39.90 39.67 1.35 o -6 -1 1 31.22 28.90 1.00 o -5 -1 1 259.29 268.16 2.98 o -4 -1 1 495.71 527.28 6.05 o -3 -1 1 116.33 110.20 2.11 o -2 -1 1 45.25 42.09 1.44 o -1 -1 1 641.11 586.65 7.85 o 0 -1 1 1157.30 1046.02 25.90 o 1 -1 1 3654.73 3547.34 54.65 o 2 -1 1 992.11 1006.81 9.05 o 3 -1 1 1109.50 1092.87 8.95 o 4 -1 1 181.80 194.13 2.44 o 5 -1 1 333.23 332.85 3.82 o 6 -1 1 64.35 68.07 1.56 o 7 -1 1 20.80 17.82 1.09 o 8 -1 1 52.58 50.20 1.80 o -8 0 1 64.55 59.60 2.31 o -7 0 1 1.87 0.96 0.27 o -6 0 1 155.08 159.73 2.51 o -5 0 1 81.16 66.06 1.42 o -4 0 1 909.64 898.65 8.44 o -3 0 1 769.63 801.43 19.76 o -2 0 1 539.21 528.38 6.01 o -1 0 1 248.40 232.04 2.71 o 0 0 1 3.14 3.03 0.20 o 1 0 1 89.11 80.76 1.73 o 2 0 1 4639.63 4606.44 68.40 o 3 0 1 93.65 105.96 1.83 o 4 0 1 50.92 47.99 1.19 o 5 0 1 78.31 85.90 1.87 o 6 0 1 100.63 101.64 2.15 o 7 0 1 120.54 117.30 3.25 o 8 0 1 200.00 202.69 6.81 o -8 1 1 10.48 11.07 0.94 o -7 1 1 43.23 44.17 2.16 o -6 1 1 54.36 54.15 2.05 o -5 1 1 243.08 252.82 3.74 o -4 1 1 472.25 481.17 6.88 o -3 1 1 142.72 139.25 2.78 o -2 1 1 43.06 44.74 1.42 o -1 1 1 733.79 704.12 8.65 o 0 1 1 1276.78 1199.04 15.38 o 1 1 1 3626.52 3646.87 45.18 o 2 1 1 1115.24 1201.61 13.79 o 3 1 1 1044.72 1096.16 11.93 o 4 1 1 180.72 190.03 2.78 o 5 1 1 327.06 327.75 3.75 o 6 1 1 66.77 71.46 1.58 o 7 1 1 21.29 20.19 1.14 o 8 1 1 68.69 69.10 2.16 o -8 2 1 46.49 49.11 1.41 o -7 2 1 151.99 146.26 4.33 o -6 2 1 9.14 8.65 0.60 o -5 2 1 276.57 262.59 3.68 o -4 2 1 146.61 135.35 2.30 o -3 2 1 180.14 185.17 2.38 o -2 2 1 887.73 882.58 12.46 o -1 2 1 1209.24 1199.07 19.09 o 0 2 1 1111.77 1112.49 20.57 o 1 2 1 4355.33 4599.31 55.56 o 2 2 1 177.07 171.80 2.39 o 3 2 1 452.73 495.16 5.32 o 4 2 1 418.48 429.14 4.57 o 5 2 1 358.52 365.79 4.17 o 6 2 1 174.26 173.34 3.21 o 7 2 1 123.64 128.11 5.31 o 8 2 1 35.05 34.98 2.37 o -8 3 1 28.21 25.76 1.63 o -7 3 1 290.20 292.79 4.34 o -6 3 1 3.41 4.14 0.38 o -5 3 1 66.64 66.50 1.53 o -4 3 1 91.98 102.98 1.68 o -3 3 1 460.66 459.77 5.61 o -2 3 1 65.53 60.14 1.48 o -1 3 1 1497.35 1605.44 23.63 o 0 3 1 227.34 240.92 3.50 o 1 3 1 508.02 503.26 5.10 o 2 3 1 795.94 816.02 6.54 o 3 3 1 89.26 88.34 1.59 o 4 3 1 107.91 117.20 1.89 o 5 3 1 96.36 97.00 1.73 o 6 3 1 37.75 41.99 1.60 o 7 3 1 112.61 109.66 2.83 o 8 3 1 158.49 152.66 4.51 o -8 4 1 27.50 26.70 2.42 o -7 4 1 33.53 36.53 1.30 o -6 4 1 57.11 58.56 1.57 o -5 4 1 171.43 174.36 2.94 o -4 4 1 2.19 2.28 0.28 o -3 4 1 48.60 49.95 1.07 o -2 4 1 359.10 372.77 4.26 o -1 4 1 231.13 215.34 3.19 o 0 4 1 79.37 93.86 1.51 o 1 4 1 214.69 216.13 2.21 o 2 4 1 851.55 894.38 6.96 o 3 4 1 207.94 217.11 2.30 o 4 4 1 585.48 595.34 5.40 o 5 4 1 175.32 169.78 2.41 o 6 4 1 28.32 29.23 1.15 o 7 4 1 182.96 184.59 4.02 o -7 5 1 56.48 50.72 2.28 o -6 5 1 18.69 20.02 1.09 o -5 5 1 151.40 153.58 2.38 o -4 5 1 239.15 239.26 3.09 o -3 5 1 50.66 49.53 1.13 o -2 5 1 134.11 126.39 2.11 o -1 5 1 467.04 466.26 4.37 o 0 5 1 99.34 96.94 2.36 o 1 5 1 148.60 158.28 1.93 o 2 5 1 106.58 106.71 1.59 o 3 5 1 74.12 73.50 1.52 o 4 5 1 66.25 68.35 1.65 o 5 5 1 100.88 100.32 2.16 o 6 5 1 84.21 94.78 2.18 o 7 5 1 6.15 5.94 0.71 o -6 6 1 1.91 2.17 0.33 o -5 6 1 126.61 133.18 3.04 o -4 6 1 68.84 74.29 1.88 o -3 6 1 174.15 170.26 3.82 o -2 6 1 250.44 259.84 3.43 o -1 6 1 358.65 370.62 4.00 o 0 6 1 46.42 47.51 1.09 o 1 6 1 521.81 528.42 4.35 o 2 6 1 183.86 184.36 2.32 o 3 6 1 115.00 116.07 1.96 o 4 6 1 204.22 208.80 3.55 o 5 6 1 110.02 118.12 2.52 o 6 6 1 96.76 96.89 2.07 o -6 7 1 77.05 76.76 2.40 o -5 7 1 23.81 22.16 1.03 o -4 7 1 26.50 25.84 1.27 o -3 7 1 219.13 234.89 4.86 o -2 7 1 189.69 193.32 2.65 o -1 7 1 226.44 241.08 3.26 o 0 7 1 61.90 59.48 1.35 o 1 7 1 73.29 75.58 1.54 o 2 7 1 61.10 67.97 1.47 o 3 7 1 8.04 7.20 0.63 o 4 7 1 266.83 272.12 3.91 o 5 7 1 85.61 87.87 2.02 o -5 8 1 31.68 26.07 1.69 o -4 8 1 70.74 72.91 3.10 o -3 8 1 109.38 105.34 3.02 o -2 8 1 107.18 113.41 3.10 o -1 8 1 189.39 196.23 3.74 o 0 8 1 22.87 23.63 1.06 o 1 8 1 367.30 385.67 5.51 o 2 8 1 23.39 24.79 1.92 o 3 8 1 9.02 8.89 0.77 o 4 8 1 61.13 62.59 1.86 o -3 9 1 22.68 26.28 1.26 o -2 9 1 16.98 17.95 0.89 o -1 9 1 32.41 35.71 1.18 o 0 9 1 66.84 73.47 1.96 o 1 9 1 56.21 56.98 1.67 o 2 9 1 31.83 36.56 1.97 o 3 9 1 73.73 72.89 1.74 o 0 10 1 46.62 44.38 2.28 o -3 -9 2 25.69 21.07 0.81 o -2 -9 2 8.97 11.40 0.79 o -1 -9 2 79.78 78.65 2.88 o 0 -9 2 6.76 7.23 0.66 o 1 -9 2 117.55 123.73 4.23 o 2 -9 2 16.22 16.68 1.33 o 3 -9 2 25.18 27.54 1.92 o -5 -8 2 11.74 11.41 0.94 o -4 -8 2 28.80 26.48 1.02 o -3 -8 2 228.47 224.57 4.10 o -2 -8 2 30.92 26.93 1.88 o -1 -8 2 49.28 45.63 1.56 o 0 -8 2 145.45 149.20 3.73 o 1 -8 2 86.24 82.92 2.36 o 2 -8 2 92.72 94.80 2.40 o 3 -8 2 117.12 123.83 3.04 o 4 -8 2 54.01 50.60 2.26 o -6 -7 2 33.17 29.58 1.18 o -5 -7 2 6.96 7.50 0.72 o -4 -7 2 51.98 49.72 1.48 o -3 -7 2 255.15 237.84 5.09 o -2 -7 2 53.63 46.24 1.18 o -1 -7 2 69.88 61.17 1.79 o 0 -7 2 65.70 60.70 1.39 o 1 -7 2 59.44 59.44 2.22 o 2 -7 2 94.35 94.69 1.89 o 3 -7 2 146.28 144.80 3.11 o 4 -7 2 219.33 222.11 4.00 o 5 -7 2 117.69 118.29 3.89 o -6 -6 2 217.97 227.48 5.57 o -5 -6 2 32.99 34.54 1.29 o -4 -6 2 71.51 72.50 1.69 o -3 -6 2 160.97 150.35 2.64 o -2 -6 2 166.34 163.07 2.42 o -1 -6 2 85.50 84.65 1.80 o 0 -6 2 898.65 879.12 7.36 o 1 -6 2 90.56 89.87 1.62 o 2 -6 2 319.42 302.70 3.14 o 3 -6 2 206.99 209.78 2.75 o 4 -6 2 38.24 37.44 1.38 o 5 -6 2 22.07 23.62 1.30 o 6 -6 2 130.39 129.55 2.98 o -7 -5 2 46.92 45.80 2.23 o -6 -5 2 39.51 36.24 1.66 o -5 -5 2 208.06 211.04 3.15 o -4 -5 2 80.40 81.64 1.53 o -3 -5 2 35.56 35.49 1.36 o -2 -5 2 265.66 258.66 3.51 o -1 -5 2 102.03 86.62 1.55 o 0 -5 2 336.65 356.25 3.89 o 1 -5 2 32.03 24.21 0.78 o 2 -5 2 28.64 25.59 0.77 o 3 -5 2 0.70 1.16 0.22 o 4 -5 2 36.90 36.51 1.24 o 5 -5 2 107.33 99.09 3.54 o 6 -5 2 4.08 4.15 0.57 o 7 -5 2 115.66 113.00 4.33 o -7 -4 2 109.44 112.58 3.35 o -6 -4 2 615.36 604.22 6.58 o -5 -4 2 34.05 33.51 1.17 o -4 -4 2 268.58 264.80 3.44 o -3 -4 2 367.55 360.61 5.37 o -2 -4 2 49.87 45.53 1.18 o -1 -4 2 664.10 653.69 6.56 o 0 -4 2 1695.21 1698.43 10.91 o 1 -4 2 48.08 48.97 0.87 o 2 -4 2 194.60 193.24 3.35 o 3 -4 2 491.72 479.65 4.41 o 4 -4 2 312.51 307.87 4.28 o 5 -4 2 124.32 119.69 2.65 o 6 -4 2 53.06 53.87 2.46 o 7 -4 2 8.96 9.23 0.94 o -8 -3 2 93.06 81.34 3.25 o -7 -3 2 126.98 123.46 2.39 o -6 -3 2 188.92 182.18 3.24 o -5 -3 2 192.77 193.53 2.94 o -4 -3 2 309.52 311.74 3.06 o -3 -3 2 231.94 233.60 5.26 o -2 -3 2 277.31 272.04 2.92 o -1 -3 2 264.62 258.93 2.95 o 0 -3 2 742.11 740.42 6.60 o 1 -3 2 356.72 332.95 4.80 o 2 -3 2 159.89 177.23 2.66 o 3 -3 2 125.99 137.17 1.92 o 4 -3 2 454.33 486.77 5.19 o 5 -3 2 180.55 180.98 2.56 o 6 -3 2 27.45 27.12 1.12 o 7 -3 2 60.72 66.27 3.00 o -8 -2 2 37.45 34.12 1.16 o -7 -2 2 10.07 12.64 0.87 o -6 -2 2 389.73 376.87 5.21 o -5 -2 2 28.35 25.94 0.85 o -4 -2 2 178.89 162.66 2.46 o -3 -2 2 599.19 602.23 8.98 o -2 -2 2 494.61 481.43 6.73 o -1 -2 2 267.52 249.21 2.74 o 0 -2 2 4432.15 4253.08 62.67 o 1 -2 2 303.51 308.58 11.58 o 2 -2 2 25.77 26.13 0.82 o 3 -2 2 616.01 614.33 5.06 o 4 -2 2 2.58 4.09 0.29 o 5 -2 2 279.68 270.49 3.43 o 6 -2 2 61.09 58.94 3.10 o 7 -2 2 0.61 0.59 0.27 o 8 -2 2 80.70 71.40 3.32 o -8 -1 2 107.40 109.20 5.57 o -7 -1 2 41.56 42.78 1.43 o -6 -1 2 154.74 153.64 2.95 o -5 -1 2 96.37 100.14 1.92 o -4 -1 2 398.61 445.69 6.30 o -3 -1 2 25.65 18.47 0.87 o -2 -1 2 669.87 645.61 8.45 o -1 -1 2 346.40 339.91 5.76 o 0 -1 2 756.83 764.81 8.44 o 1 -1 2 242.29 240.91 4.27 o 2 -1 2 150.48 154.18 2.43 o 3 -1 2 293.23 306.12 3.37 o 4 -1 2 465.28 461.77 4.61 o 5 -1 2 7.11 8.71 0.58 o 6 -1 2 186.72 188.04 3.18 o 7 -1 2 28.39 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129.24 132.64 2.86 o -4 7 8 36.82 34.60 1.37 o -3 7 8 57.66 58.41 2.43 o -2 7 8 33.80 31.36 1.78 o -1 7 8 11.50 10.64 0.81 o 0 7 8 219.61 242.94 4.81 o 1 7 8 13.04 11.42 0.97 o 2 7 8 2.54 2.47 0.48 o 3 7 8 6.49 6.45 0.65 o -3 8 8 59.55 66.03 3.55 o -2 8 8 38.92 38.66 1.36 o -1 8 8 72.49 79.50 1.96 o 0 8 8 26.80 26.48 1.22 o 1 8 8 150.59 26.05 77.81 o -3 -8 9 13.55 14.64 1.33 o -2 -8 9 38.78 41.17 1.73 o -1 -8 9 48.90 44.60 2.25 o 0 -8 9 42.80 36.89 1.47 o -4 -7 9 79.17 83.21 2.33 o -3 -7 9 21.86 19.44 0.84 o -2 -7 9 50.52 51.20 1.64 o -1 -7 9 3.00 3.07 0.51 o 0 -7 9 162.25 156.62 3.24 o 1 -7 9 1.09 1.32 0.34 o 2 -7 9 117.24 121.15 3.41 o -6 -6 9 78.54 76.46 3.25 o -5 -6 9 16.33 14.58 0.71 o -4 -6 9 183.74 178.61 5.36 o -3 -6 9 96.73 101.38 3.31 o -2 -6 9 193.28 193.09 4.31 o -1 -6 9 255.23 252.99 4.58 o 0 -6 9 261.30 262.55 7.42 o 1 -6 9 31.63 28.30 1.18 o 2 -6 9 122.55 120.10 3.68 o 3 -6 9 24.32 25.00 2.56 o -6 -5 9 70.12 76.06 2.35 o -5 -5 9 177.90 178.39 3.14 o -4 -5 9 20.16 16.66 1.11 o -3 -5 9 55.94 52.94 1.86 o -2 -5 9 158.03 159.09 3.34 o -1 -5 9 206.86 208.83 3.78 o 0 -5 9 235.23 242.95 5.15 o 1 -5 9 223.73 231.89 6.02 o 2 -5 9 25.33 22.44 1.07 o 3 -5 9 50.42 49.91 1.61 o 4 -5 9 3.29 2.21 0.34 o -7 -4 9 67.57 72.19 3.63 o -6 -4 9 80.73 86.73 2.84 o -5 -4 9 130.91 129.61 3.29 o -4 -4 9 0.15 0.74 0.32 o -3 -4 9 288.12 280.09 4.30 o -2 -4 9 262.09 248.16 3.46 o -1 -4 9 399.22 401.89 4.82 o 0 -4 9 189.99 172.74 2.80 o 1 -4 9 35.97 36.72 1.28 o 2 -4 9 139.02 143.81 2.65 o 3 -4 9 8.17 9.69 0.65 o 4 -4 9 87.32 86.39 2.27 o -7 -3 9 133.53 136.82 4.05 o -6 -3 9 3.68 3.84 0.65 o -5 -3 9 208.21 194.03 5.09 o -4 -3 9 91.55 90.25 2.38 o -3 -3 9 180.03 171.18 2.59 o -2 -3 9 92.15 88.45 1.70 o -1 -3 9 167.08 159.65 2.39 o 0 -3 9 220.84 218.66 3.35 o 1 -3 9 7.35 5.61 0.64 o 2 -3 9 197.75 189.07 2.97 o 3 -3 9 41.55 46.67 1.41 o 4 -3 9 111.63 111.33 2.10 o 5 -3 9 10.20 10.92 1.04 o -8 -2 9 15.52 13.66 1.21 o -7 -2 9 18.21 21.40 1.11 o -6 -2 9 91.32 98.44 2.96 o -5 -2 9 595.80 555.76 9.02 o -4 -2 9 676.94 660.83 6.83 o -3 -2 9 139.24 129.66 2.20 o -2 -2 9 71.82 68.61 1.51 o -1 -2 9 316.70 312.36 3.89 o 0 -2 9 557.12 544.12 5.69 o 1 -2 9 47.26 46.47 1.66 o 2 -2 9 241.96 246.75 3.33 o 3 -2 9 49.27 52.78 1.65 o 4 -2 9 10.05 10.32 0.72 o 5 -2 9 178.24 182.21 3.14 o -8 -1 9 32.06 33.05 2.26 o -7 -1 9 22.86 20.75 1.69 o -6 -1 9 18.31 15.23 1.21 o -5 -1 9 292.25 285.92 5.19 o -4 -1 9 267.58 248.05 3.17 o -3 -1 9 391.90 373.71 4.27 o -2 -1 9 86.34 87.05 1.71 o -1 -1 9 4.31 4.10 0.34 o 0 -1 9 210.10 209.87 2.90 o 1 -1 9 222.72 223.72 4.93 o 2 -1 9 156.06 151.46 3.19 o 3 -1 9 111.55 113.85 2.47 o 4 -1 9 65.41 63.44 1.89 o 5 -1 9 85.20 84.54 3.78 o -8 0 9 213.51 211.11 25.74 o -7 0 9 66.62 70.12 2.67 o -6 0 9 42.58 47.55 2.10 o -5 0 9 67.32 75.85 2.05 o -4 0 9 22.07 26.59 0.99 o -3 0 9 66.33 60.50 1.49 o -2 0 9 234.65 247.02 3.16 o -1 0 9 168.88 159.64 2.49 o 0 0 9 27.23 24.36 0.97 o 1 0 9 121.68 125.86 4.05 o 2 0 9 274.25 271.77 3.98 o 3 0 9 120.16 116.05 2.42 o 4 0 9 3.56 2.79 0.42 o 5 0 9 202.49 205.63 3.99 o -8 1 9 46.31 44.63 2.49 o -7 1 9 30.96 29.78 1.38 o -6 1 9 18.19 14.96 1.33 o -5 1 9 296.12 290.16 4.77 o -4 1 9 283.25 272.90 4.27 o -3 1 9 396.44 388.38 5.40 o -2 1 9 100.28 101.61 2.15 o -1 1 9 4.68 4.74 0.43 o 0 1 9 204.97 206.17 3.16 o 1 1 9 185.64 187.63 4.02 o 2 1 9 187.68 183.21 3.33 o 3 1 9 119.99 124.47 2.83 o 4 1 9 94.84 90.04 2.22 o 5 1 9 71.93 68.22 1.78 o -7 2 9 18.94 20.81 1.10 o -6 2 9 100.67 112.10 4.35 o -5 2 9 618.83 611.95 7.39 o -4 2 9 674.39 669.57 7.37 o -3 2 9 177.56 172.99 3.59 o -2 2 9 69.24 68.89 1.77 o -1 2 9 350.47 347.67 5.56 o 0 2 9 537.35 542.71 5.83 o 1 2 9 43.75 41.43 1.27 o 2 2 9 217.84 213.43 3.17 o 3 2 9 55.51 63.64 2.11 o 4 2 9 10.52 11.32 0.64 o 5 2 9 170.87 155.61 6.64 o -7 3 9 135.13 125.99 3.81 o -6 3 9 3.59 3.17 0.77 o -5 3 9 209.65 197.85 4.00 o -4 3 9 79.43 80.74 2.15 o -3 3 9 179.92 181.60 3.94 o -2 3 9 69.57 66.13 2.06 o -1 3 9 170.94 166.73 3.17 o 0 3 9 203.44 208.49 2.98 o 1 3 9 18.87 16.09 0.81 o 2 3 9 202.13 196.58 3.36 o 3 3 9 40.32 42.81 1.38 o 4 3 9 109.79 107.20 2.39 o 5 3 9 14.77 15.30 0.92 o -6 4 9 88.66 94.12 2.94 o -5 4 9 128.15 142.63 6.48 o -4 4 9 0.70 0.46 0.33 o -3 4 9 311.98 309.65 6.18 o -2 4 9 253.97 241.69 6.36 o -1 4 9 406.51 420.58 5.75 o 0 4 9 166.29 155.51 2.89 o 1 4 9 40.64 42.69 1.33 o 2 4 9 158.22 168.35 3.78 o 3 4 9 5.14 6.86 0.61 o 4 4 9 84.35 83.93 2.00 o 5 4 9 6.43 5.97 0.83 o -6 5 9 71.86 74.07 3.85 o -5 5 9 168.55 166.74 3.69 o -4 5 9 33.93 28.99 1.55 o -3 5 9 53.43 56.08 2.00 o -2 5 9 206.12 211.65 4.91 o -1 5 9 183.84 188.98 3.70 o 0 5 9 251.48 260.20 4.93 o 1 5 9 205.33 220.01 4.15 o 2 5 9 28.90 27.91 1.27 o 3 5 9 53.04 52.56 1.50 o 4 5 9 10.63 9.37 0.57 o -5 6 9 16.40 16.14 1.02 o -4 6 9 204.02 206.71 4.14 o -3 6 9 83.14 83.54 3.08 o -2 6 9 184.35 195.07 5.13 o -1 6 9 243.92 252.88 4.71 o 0 6 9 250.41 255.62 6.24 o 1 6 9 31.06 29.25 1.82 o 2 6 9 123.74 130.76 3.43 o 3 6 9 37.60 38.96 1.52 o -4 7 9 84.34 93.04 3.14 o -3 7 9 21.87 20.88 1.13 o -2 7 9 56.04 60.01 8.21 o -1 7 9 2.81 2.22 0.37 o 0 7 9 167.19 170.75 3.50 o 1 7 9 1.45 2.09 0.53 o 2 7 9 105.37 102.98 3.02 o -2 8 9 40.47 37.15 1.61 o -1 8 9 60.11 56.76 2.44 o 0 8 9 30.64 18.77 1.51 o -4 -7 10 79.81 68.58 2.95 o -3 -7 10 102.73 103.40 3.12 o -2 -7 10 0.65 0.87 0.30 o -1 -7 10 62.07 63.39 1.78 o 0 -7 10 42.11 42.72 2.04 o 1 -7 10 29.38 28.86 2.01 o -4 -6 10 102.40 99.01 3.12 o -3 -6 10 27.22 26.32 1.51 o -2 -6 10 119.69 118.16 3.10 o -1 -6 10 141.82 148.47 3.46 o 0 -6 10 16.34 18.17 0.94 o 1 -6 10 268.64 266.38 4.21 o 2 -6 10 48.55 53.64 2.32 o -6 -5 10 97.29 92.28 3.84 o -5 -5 10 11.83 12.54 0.84 o -4 -5 10 12.56 14.70 0.81 o -3 -5 10 165.22 156.91 3.18 o -2 -5 10 123.81 111.54 3.59 o -1 -5 10 0.04 0.74 0.43 o 0 -5 10 138.32 145.45 3.66 o 1 -5 10 40.89 41.06 1.46 o 2 -5 10 45.95 49.23 1.61 o 3 -5 10 137.66 139.29 4.08 o -7 -4 10 76.23 79.26 3.28 o -6 -4 10 1.02 1.77 0.40 o -5 -4 10 139.43 143.30 3.35 o -4 -4 10 159.09 151.49 3.69 o -3 -4 10 10.79 10.35 0.90 o -2 -4 10 253.80 242.27 3.38 o -1 -4 10 0.56 0.72 0.22 o 0 -4 10 32.18 30.04 1.12 o 1 -4 10 171.18 170.01 3.22 o 2 -4 10 27.37 23.58 1.18 o 3 -4 10 42.62 38.65 1.55 o 4 -4 10 135.35 137.85 5.44 o -7 -3 10 4.07 4.13 0.80 o -6 -3 10 100.14 100.64 3.12 o -5 -3 10 6.45 7.99 0.81 o -4 -3 10 61.41 62.17 2.02 o -3 -3 10 65.83 67.46 3.23 o -2 -3 10 30.65 31.19 1.14 o -1 -3 10 7.79 6.69 0.50 o 0 -3 10 224.70 224.35 3.23 o 1 -3 10 46.98 43.19 1.68 o 2 -3 10 147.48 148.52 3.08 o 3 -3 10 38.29 38.71 1.37 o 4 -3 10 109.04 102.41 2.92 o -7 -2 10 59.95 71.04 2.29 o -6 -2 10 21.96 17.50 1.30 o -5 -2 10 30.30 32.80 2.53 o -4 -2 10 91.60 87.10 2.23 o -3 -2 10 250.29 235.22 3.37 o -2 -2 10 621.56 608.07 5.28 o -1 -2 10 277.98 281.95 3.98 o 0 -2 10 140.19 131.77 2.51 o 1 -2 10 334.88 329.61 5.66 o 2 -2 10 91.32 98.64 2.50 o 3 -2 10 71.27 70.53 1.96 o 4 -2 10 184.04 194.24 3.83 o 5 -2 10 18.05 16.66 1.05 o -7 -1 10 36.09 36.65 1.64 o -6 -1 10 112.10 110.15 3.07 o -5 -1 10 1.83 1.91 0.65 o -4 -1 10 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