#------------------------------------------------------------------------------ #$Date: 2020-06-06 01:23:54 +0300 (Sat, 06 Jun 2020) $ #$Revision: 252947 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/21/2022135.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022135 _cell_angle_alpha 90.000 _cell_angle_beta 100.603 _cell_angle_gamma 90.000 _cell_length_a 7.1803 _cell_length_b 7.2139 _cell_length_c 8.6574 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.7334 _cod_data_source_file wp30044sup4.hkl _cod_data_source_block 4 _shelx_title ' pyra4 in P2/n No13' _shelx_refln_list_code 4 _shelx_f_calc_maximum 104.86 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 9125.34 11064.52 46.20 o 6 0 0 2712.93 3363.11 42.89 o 8 0 0 727.32 852.91 65.42 o 1 1 0 804.04 856.55 24.81 o 2 1 0 4003.13 4689.98 78.86 o 3 1 0 1090.29 975.11 45.11 o 4 1 0 1872.31 2172.37 21.07 o 5 1 0 604.50 662.83 18.73 o 6 1 0 643.39 820.68 12.31 o 7 1 0 206.18 262.91 2.94 o 8 1 0 183.09 232.40 5.82 o 9 1 0 56.00 62.07 3.19 o 0 2 0 445.72 523.59 31.93 o 1 2 0 10996.61 12401.29 420.13 o 2 2 0 254.90 357.79 6.69 o 3 2 0 5233.06 5824.12 159.45 o 4 2 0 104.45 139.30 1.28 o 5 2 0 2053.72 2407.62 41.01 o 6 2 0 41.59 48.45 2.48 o 7 2 0 674.91 802.28 23.47 o 8 2 0 12.30 14.80 0.88 o 9 2 0 178.38 145.98 8.35 o 0 3 0 1941.15 1134.67 84.27 o 1 3 0 360.99 287.85 21.07 o 2 3 0 1792.93 1925.75 29.26 o 3 3 0 327.12 416.07 5.42 o 4 3 0 1076.51 1227.49 14.73 o 5 3 0 217.08 246.88 10.65 o 6 3 0 413.15 437.51 23.11 o 7 3 0 96.56 96.30 12.88 o 8 3 0 122.30 117.59 3.32 o 9 3 0 31.38 28.80 1.14 o 0 4 0 3560.58 3876.24 7.09 o 1 4 0 1715.83 2214.36 22.90 o 2 4 0 2776.22 2818.63 135.74 o 3 4 0 866.53 947.40 51.06 o 4 4 0 1449.41 1644.24 12.66 o 5 4 0 321.25 396.60 22.22 o 6 4 0 554.60 775.53 19.57 o 7 4 0 98.02 97.80 4.48 o 8 4 0 162.08 191.89 14.99 o 0 5 0 238.77 306.02 99.92 o 1 5 0 1842.90 2481.78 65.83 o 2 5 0 194.22 293.06 6.73 o 3 5 0 1295.95 1632.32 26.32 o 4 5 0 118.42 159.24 7.24 o 5 5 0 639.27 854.60 7.98 o 6 5 0 56.28 60.48 2.92 o 7 5 0 237.70 273.37 23.19 o 8 5 0 20.00 21.75 1.14 o 0 6 0 269.50 329.16 112.78 o 1 6 0 833.19 877.13 69.30 o 2 6 0 209.93 231.82 9.49 o 3 6 0 582.69 699.92 22.40 o 4 6 0 110.33 140.08 4.10 o 5 6 0 288.74 371.48 8.11 o 6 6 0 43.97 58.59 1.28 o 7 6 0 106.49 134.03 5.58 o 0 7 0 466.96 658.86 24.13 o 1 7 0 22.72 21.10 1.06 o 2 7 0 409.30 425.97 30.81 o 3 7 0 13.52 11.67 1.14 o 4 7 0 271.62 293.30 13.13 o 5 7 0 4.84 2.80 0.80 o 6 7 0 135.30 122.63 5.53 o 0 8 0 309.47 429.22 19.23 o 1 8 0 211.88 278.47 26.78 o 2 8 0 263.67 325.67 18.57 o 3 8 0 146.69 174.80 5.85 o 4 8 0 163.22 167.46 10.98 o 5 8 0 72.90 79.13 4.71 o 0 9 0 8.61 6.38 1.18 o 1 9 0 148.14 178.57 21.31 o 2 9 0 7.51 3.74 0.80 o 3 9 0 114.95 94.77 6.29 o -9 0 1 68.74 88.94 3.18 o -7 0 1 245.29 277.69 6.89 o -5 0 1 556.52 597.99 20.43 o -3 0 1 701.07 673.64 7.52 o -1 0 1 1086.61 804.96 6.94 o 1 0 1 1926.46 1118.87 822.94 o 3 0 1 1856.12 1628.32 29.13 o 5 0 1 1135.16 1131.89 37.56 o 7 0 1 437.56 455.83 31.40 o 9 0 1 122.44 112.44 2.51 o -9 1 1 56.66 47.85 1.36 o -8 1 1 370.42 399.49 6.04 o -7 1 1 204.76 208.35 10.26 o -6 1 1 1159.23 1205.80 38.95 o -5 1 1 558.13 572.09 19.39 o -4 1 1 2958.96 2996.49 67.23 o -3 1 1 1042.87 897.88 29.55 o -2 1 1 5716.37 5567.52 85.08 o -1 1 1 1312.97 1047.26 42.97 o 0 1 1 6429.65 6185.31 202.34 o 1 1 1 1281.49 1206.64 16.91 o 2 1 1 3930.47 3803.05 46.96 o 3 1 1 989.07 774.69 22.45 o 4 1 1 1778.32 1738.12 31.34 o 5 1 1 517.47 531.60 2.04 o 6 1 1 638.28 697.84 9.36 o 7 1 1 190.69 186.25 9.59 o 8 1 1 185.31 159.41 4.92 o 9 1 1 54.79 44.88 3.05 o -9 2 1 3.90 2.95 0.87 o -8 2 1 304.78 340.50 5.21 o -7 2 1 15.67 16.68 0.88 o -6 2 1 978.15 920.82 19.16 o -5 2 1 45.45 40.53 0.92 o -4 2 1 2422.59 2228.07 82.45 o -3 2 1 88.20 72.43 2.21 o -2 2 1 4765.13 4252.08 92.12 o -1 2 1 153.27 113.06 2.11 o 0 2 1 6317.10 5536.17 113.17 o 1 2 1 148.33 122.84 2.21 o 2 2 1 4378.80 4113.09 58.34 o 3 2 1 76.16 73.06 1.45 o 4 2 1 2150.79 2202.53 9.56 o 5 2 1 43.46 46.96 0.98 o 6 2 1 818.87 881.35 23.05 o 7 2 1 19.61 19.27 0.75 o 8 2 1 233.48 188.60 5.57 o 9 2 1 6.24 4.94 0.86 o -9 3 1 152.59 126.50 3.99 o -8 3 1 81.73 97.31 3.09 o -7 3 1 518.25 500.91 36.24 o -6 3 1 290.12 330.46 3.50 o -5 3 1 1379.09 1521.34 36.89 o -4 3 1 779.41 774.82 24.36 o -3 3 1 2736.75 2616.41 59.57 o -2 3 1 1483.58 1276.91 36.04 o -1 3 1 3744.81 3215.72 39.05 o 0 3 1 1826.94 1657.35 46.28 o 1 3 1 3458.37 3026.34 147.92 o 2 3 1 1228.46 1023.26 47.14 o 3 3 1 2217.41 1858.52 18.33 o 4 3 1 526.20 558.65 3.69 o 5 3 1 1018.65 1054.61 8.22 o 6 3 1 180.46 213.21 1.81 o 7 3 1 362.71 381.78 11.59 o 8 3 1 51.45 39.74 2.23 o -8 4 1 5.59 5.81 1.09 o -7 4 1 353.95 396.23 3.44 o -6 4 1 14.40 14.55 0.83 o -5 4 1 969.42 1011.97 22.51 o -4 4 1 21.09 19.95 0.76 o -3 4 1 2094.75 2065.31 78.10 o -2 4 1 24.78 16.12 0.80 o -1 4 1 3219.80 3000.33 125.62 o 0 4 1 49.53 40.13 3.25 o 1 4 1 3099.22 2710.45 253.02 o 2 4 1 76.96 50.37 4.12 o 3 4 1 1999.00 1948.96 74.21 o 4 4 1 74.63 69.00 0.93 o 5 4 1 936.90 998.81 29.22 o 6 4 1 45.45 53.66 1.00 o 7 4 1 325.50 331.56 20.70 o 8 4 1 17.88 18.31 2.18 o -8 5 1 118.63 111.76 7.30 o -7 5 1 21.68 23.14 1.06 o -6 5 1 365.97 404.87 8.12 o -5 5 1 68.47 80.94 2.25 o -4 5 1 836.08 887.52 23.00 o -3 5 1 158.97 165.75 3.30 o -2 5 1 1346.87 1327.56 29.26 o -1 5 1 277.84 311.13 7.67 o 0 5 1 1550.38 1223.56 59.17 o 1 5 1 311.97 261.92 24.53 o 2 5 1 1277.42 1075.67 74.92 o 3 5 1 203.51 196.97 3.88 o 4 5 1 739.84 766.55 6.64 o 5 5 1 94.74 100.84 1.18 o 6 5 1 318.88 329.89 14.97 o 7 5 1 35.82 36.06 2.11 o 8 5 1 109.09 91.51 4.09 o -7 6 1 65.76 67.55 2.09 o -6 6 1 265.91 276.36 3.37 o -5 6 1 153.72 184.31 6.32 o -4 6 1 624.72 641.21 16.84 o -3 6 1 277.63 298.94 6.93 o -2 6 1 1091.82 1150.31 26.39 o -1 6 1 374.90 411.63 5.43 o 0 6 1 1291.94 1226.71 30.10 o 1 6 1 351.86 394.49 2.78 o 2 6 1 1023.06 991.31 54.17 o 3 6 1 226.64 226.35 12.45 o 4 6 1 563.31 592.20 22.06 o 5 6 1 104.15 113.60 2.78 o 6 6 1 223.74 222.36 5.24 o 7 6 1 34.64 30.28 1.33 o -6 7 1 37.07 27.79 1.09 o -5 7 1 301.81 342.77 12.62 o -4 7 1 80.84 72.59 1.93 o -3 7 1 570.30 595.95 29.83 o -2 7 1 130.90 103.05 6.04 o -1 7 1 763.50 587.97 30.71 o 0 7 1 145.23 148.13 5.81 o 1 7 1 709.85 727.32 41.66 o 2 7 1 102.31 95.80 3.14 o 3 7 1 458.82 356.18 23.88 o 4 7 1 47.63 46.78 2.92 o 5 7 1 218.00 238.95 6.96 o 6 7 1 15.97 12.09 1.17 o -5 8 1 68.40 47.03 3.26 o -4 8 1 64.37 43.61 4.24 o -3 8 1 141.18 153.05 11.65 o -2 8 1 109.56 84.49 3.38 o -1 8 1 209.34 178.22 9.66 o 0 8 1 135.98 167.78 8.01 o 1 8 1 213.28 218.14 15.62 o 2 8 1 119.80 114.71 9.80 o 3 8 1 150.37 188.19 5.58 o 4 8 1 75.46 77.85 2.56 o 5 8 1 75.72 64.04 2.48 o -3 9 1 2.66 1.58 0.81 o -2 9 1 178.74 209.14 5.84 o -1 9 1 3.58 3.40 0.96 o 0 9 1 199.73 245.14 11.75 o 1 9 1 3.56 1.41 0.77 o 2 9 1 158.89 130.53 4.77 o 3 9 1 2.54 0.72 0.86 o -8 0 2 587.95 562.20 11.67 o -6 0 2 1812.63 1571.57 81.90 o -4 0 2 4496.88 4508.62 96.23 o -2 0 2 8057.88 8466.18 143.73 o 0 0 2 9007.88 8124.54 29.42 o 2 0 2 5837.18 5840.27 108.26 o 4 0 2 2585.27 2218.32 155.50 o 6 0 2 879.88 742.22 75.88 o 8 0 2 237.15 236.79 2.36 o -9 1 2 97.69 84.09 3.58 o -8 1 2 225.65 231.52 1.90 o -7 1 2 408.14 441.59 12.25 o -6 1 2 738.88 750.11 10.88 o -5 1 2 1362.95 1176.16 26.49 o -4 1 2 1956.18 1798.66 134.56 o -3 1 2 3786.41 3393.00 188.10 o -2 1 2 4123.28 4015.05 74.68 o -1 1 2 7631.92 7694.15 119.37 o 0 1 2 4968.02 4380.79 91.35 o 1 1 2 6905.06 6292.93 225.02 o 2 1 2 2662.06 2453.04 70.13 o 3 1 2 3289.29 2614.82 93.52 o 4 1 2 1023.84 923.14 44.87 o 5 1 2 1230.53 1191.13 23.57 o 6 1 2 341.60 304.28 13.23 o 7 1 2 382.08 364.81 3.08 o 8 1 2 92.90 88.68 3.20 o 9 1 2 100.66 73.59 7.07 o -9 2 2 170.83 152.61 6.68 o -8 2 2 6.91 8.46 1.12 o -7 2 2 603.60 654.96 20.84 o -6 2 2 24.87 27.12 0.89 o -5 2 2 1736.96 1489.63 86.27 o -4 2 2 75.92 69.79 1.68 o -3 2 2 3895.50 4002.03 69.05 o -2 2 2 154.56 149.25 3.11 o -1 2 2 6188.84 5568.10 70.14 o 0 2 2 208.98 155.57 13.82 o 1 2 2 6120.51 5657.90 180.15 o 2 2 2 142.12 124.01 1.29 o 3 2 2 3746.81 3030.81 48.81 o 4 2 2 44.75 45.02 0.91 o 5 2 2 1608.22 1691.25 10.34 o 6 2 2 9.62 12.73 0.69 o 7 2 2 533.84 591.86 15.19 o 8 2 2 1.53 2.56 0.71 o -9 3 2 34.51 27.97 1.90 o -8 3 2 198.22 168.34 9.60 o -7 3 2 120.70 121.06 2.01 o -6 3 2 680.94 759.33 11.22 o -5 3 2 331.02 338.52 3.90 o -4 3 2 1806.52 1625.27 13.48 o -3 3 2 672.33 633.93 17.47 o -2 3 2 3544.13 3108.85 113.27 o -1 3 2 1042.85 884.27 8.22 o 0 3 2 4286.98 2628.03 33.35 o 1 3 2 1074.24 935.72 14.23 o 2 3 2 2857.68 2127.59 158.61 o 3 3 2 642.94 592.62 9.75 o 4 3 2 1277.35 1352.03 22.15 o 5 3 2 268.95 287.78 3.48 o 6 3 2 434.03 477.90 9.35 o 7 3 2 87.05 97.16 3.98 o 8 3 2 118.62 110.32 4.47 o -8 4 2 173.91 142.22 12.22 o -7 4 2 57.34 66.05 2.24 o -6 4 2 511.30 524.74 15.83 o -5 4 2 153.43 175.62 3.36 o -4 4 2 1165.57 1122.89 26.58 o -3 4 2 297.25 315.30 5.26 o -2 4 2 1927.48 1765.52 44.87 o -1 4 2 377.86 364.17 4.42 o 0 4 2 2141.88 1794.13 213.51 o 1 4 2 318.42 248.88 4.50 o 2 4 2 1672.68 1770.30 13.12 o 3 4 2 165.70 166.85 4.36 o 4 4 2 954.86 979.37 55.64 o 5 4 2 56.99 53.31 1.38 o 6 4 2 398.36 366.51 11.32 o 7 4 2 14.65 14.77 0.95 o 8 4 2 128.17 112.96 8.91 o -8 5 2 16.83 14.65 1.00 o -7 5 2 248.04 207.82 3.99 o -6 5 2 40.59 47.92 1.38 o -5 5 2 647.02 627.01 8.32 o -4 5 2 66.15 65.84 1.64 o -3 5 2 1242.75 1309.34 28.59 o -2 5 2 66.11 71.65 1.53 o -1 5 2 1667.86 1465.28 59.16 o 0 5 2 52.60 38.39 2.27 o 1 5 2 1466.28 1526.16 86.42 o 2 5 2 36.14 37.41 1.12 o 3 5 2 842.29 920.67 17.03 o 4 5 2 16.53 21.58 0.82 o 5 5 2 343.23 363.86 8.39 o 6 5 2 5.00 6.22 0.77 o 7 5 2 106.02 101.53 4.99 o -7 6 2 102.52 108.76 1.77 o -6 6 2 66.75 64.13 5.31 o -5 6 2 244.45 280.22 2.99 o -4 6 2 168.98 188.21 3.06 o -3 6 2 444.50 505.69 2.03 o -2 6 2 311.94 385.54 3.28 o -1 6 2 595.05 701.68 23.38 o 0 6 2 405.55 290.01 12.95 o 1 6 2 589.95 642.55 12.87 o 2 6 2 365.58 391.84 14.34 o 3 6 2 446.08 366.94 15.45 o 4 6 2 229.44 244.16 9.33 o 5 6 2 247.91 221.54 9.42 o 6 6 2 105.64 108.61 2.95 o 7 6 2 101.46 73.18 3.24 o -6 7 2 168.54 138.73 10.34 o -5 7 2 0.11 -0.05 0.83 o -4 7 2 361.74 414.86 16.19 o -3 7 2 0.07 1.27 0.72 o -2 7 2 567.85 712.45 34.78 o -1 7 2 0.21 2.45 0.82 o 0 7 2 637.66 731.78 50.86 o 1 7 2 1.62 2.46 0.80 o 2 7 2 498.63 461.58 24.56 o 3 7 2 3.76 6.40 0.99 o 4 7 2 276.01 200.98 11.07 o 5 7 2 3.93 3.40 0.90 o 6 7 2 114.70 91.68 5.43 o -5 8 2 74.02 56.80 1.76 o -4 8 2 116.72 95.18 3.91 o -3 8 2 124.96 150.44 2.13 o -2 8 2 163.81 183.10 11.42 o -1 8 2 157.73 127.80 9.82 o 0 8 2 175.64 207.89 6.53 o 1 8 2 148.39 138.29 11.50 o 2 8 2 145.68 133.05 13.76 o 3 8 2 105.28 99.76 14.36 o 4 8 2 92.76 66.30 3.43 o 5 8 2 56.19 47.30 4.73 o -3 9 2 139.03 126.34 8.07 o -2 9 2 0.02 1.38 0.76 o -1 9 2 174.05 167.79 11.52 o 0 9 2 0.01 1.08 0.83 o 1 9 2 159.66 154.58 9.94 o 2 9 2 0.00 -0.07 0.86 o 3 9 2 107.35 84.35 3.70 o -9 0 3 190.99 173.49 2.75 o -7 0 3 678.64 641.03 8.55 o -5 0 3 1888.51 1811.84 167.23 o -3 0 3 3624.17 3616.14 367.93 o -1 0 3 4389.50 4254.78 19.72 o 1 0 3 4123.41 4069.50 55.91 o 3 0 3 2789.23 2654.96 40.21 o 5 0 3 1260.73 1096.10 86.05 o 7 0 3 436.57 450.42 5.52 o -9 1 3 77.20 68.74 2.21 o -8 1 3 179.85 195.48 11.87 o -7 1 3 286.65 339.90 8.29 o -6 1 3 493.30 524.21 21.91 o -5 1 3 846.65 784.99 12.25 o -4 1 3 989.45 1190.97 46.98 o -3 1 3 2081.41 1689.48 21.17 o -2 1 3 1680.13 1416.83 28.92 o -1 1 3 3874.65 3700.55 81.76 o 0 1 3 1945.59 1870.39 13.07 o 1 1 3 3533.46 3666.91 74.36 o 2 1 3 1249.20 1263.21 64.13 o 3 1 3 1773.28 1793.07 15.58 o 4 1 3 662.59 748.70 6.83 o 5 1 3 685.41 718.41 11.39 o 6 1 3 260.39 268.56 14.85 o 7 1 3 210.05 191.34 8.25 o 8 1 3 71.29 62.54 2.08 o -9 2 3 11.69 4.88 0.98 o -8 2 3 268.75 227.68 5.85 o -7 2 3 34.24 71.38 2.79 o -6 2 3 740.91 735.97 34.60 o -5 2 3 75.51 141.11 9.09 o -4 2 3 1433.86 1177.61 27.05 o -3 2 3 115.28 121.88 8.66 o -2 2 3 1655.40 1366.87 49.00 o -1 2 3 133.63 121.52 2.55 o 0 2 3 1409.98 1112.59 39.90 o 1 2 3 165.74 249.03 13.43 o 2 2 3 1239.84 1107.56 16.02 o 3 2 3 129.96 284.18 11.52 o 4 2 3 771.83 767.52 15.17 o 5 2 3 64.08 117.39 7.68 o 6 2 3 320.23 367.37 4.67 o 7 2 3 25.97 37.00 2.58 o 8 2 3 101.38 88.67 4.63 o -9 3 3 115.72 68.81 3.14 o -8 3 3 82.67 99.64 1.61 o -7 3 3 379.93 302.35 10.82 o -6 3 3 250.50 320.78 25.80 o -5 3 3 963.94 1104.05 21.24 o -4 3 3 590.03 599.79 21.54 o -3 3 3 1920.71 1929.10 20.46 o -2 3 3 1020.87 1099.46 26.30 o -1 3 3 2896.78 2437.91 49.12 o 0 3 3 1180.99 1351.48 17.66 o 1 3 3 2628.42 1815.44 144.62 o 2 3 3 841.19 1041.54 67.37 o 3 3 3 1575.66 1633.61 12.15 o 4 3 3 405.31 454.54 26.65 o 5 3 3 718.27 780.53 22.51 o 6 3 3 149.92 177.71 1.47 o 7 3 3 241.43 275.65 7.99 o 8 3 3 44.33 31.86 1.90 o -8 4 3 39.82 35.63 1.38 o -7 4 3 288.35 323.97 8.88 o -6 4 3 114.97 146.21 3.53 o -5 4 3 726.74 763.15 30.22 o -4 4 3 248.48 300.36 18.63 o -3 4 3 1335.55 1344.37 5.03 o -2 4 3 365.71 279.72 9.74 o -1 4 3 1698.86 1377.47 139.48 o 0 4 3 406.45 535.23 44.83 o 1 4 3 1511.39 1418.57 197.91 o 2 4 3 357.08 472.16 31.26 o 3 4 3 940.29 943.87 36.11 o 4 4 3 211.92 272.10 9.43 o 5 4 3 412.35 368.55 6.44 o 6 4 3 92.42 86.41 9.61 o 7 4 3 137.59 132.47 4.24 o -8 5 3 179.26 143.10 4.36 o -7 5 3 81.49 112.64 2.93 o -6 5 3 528.65 567.80 13.46 o -5 5 3 242.78 263.60 15.50 o -4 5 3 1212.07 1346.13 40.39 o -3 5 3 537.25 707.72 17.59 o -2 5 3 2080.39 2357.97 54.05 o -1 5 3 804.65 666.24 35.19 o 0 5 3 2444.96 2432.04 165.45 o 1 5 3 776.88 1111.17 20.03 o 2 5 3 1874.31 2330.52 63.18 o 3 5 3 482.37 599.40 30.28 o 4 5 3 1009.95 799.83 69.57 o 5 5 3 211.45 220.22 16.14 o 6 5 3 408.29 416.24 17.18 o 7 5 3 72.49 57.51 3.20 o -7 6 3 19.71 18.47 2.49 o -6 6 3 182.08 204.60 3.07 o -5 6 3 35.89 49.58 2.45 o -4 6 3 376.19 427.03 9.73 o -3 6 3 42.05 64.97 7.61 o -2 6 3 559.47 677.63 12.94 o -1 6 3 30.66 111.97 4.97 o 0 6 3 567.98 471.33 23.60 o 1 6 3 19.47 52.03 5.14 o 2 6 3 397.11 519.57 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64.63 70.39 2.31 o 4 1 9 69.46 64.81 2.49 o -7 2 9 5.39 4.24 1.43 o -6 2 9 201.68 173.20 20.75 o -5 2 9 10.65 10.64 1.98 o -4 2 9 348.21 274.80 33.54 o -3 2 9 15.41 16.61 1.23 o -2 2 9 429.24 441.77 32.01 o -1 2 9 17.13 22.79 1.10 o 0 2 9 374.14 356.14 13.32 o 1 2 9 14.59 15.17 1.02 o 2 2 9 230.70 204.07 6.11 o 3 2 9 9.15 6.92 0.89 o 4 2 9 103.05 80.59 3.79 o -6 3 9 45.81 32.31 5.56 o -5 3 9 148.53 121.09 6.53 o -4 3 9 78.77 74.64 6.71 o -3 3 9 215.32 203.91 14.95 o -2 3 9 98.58 74.41 1.96 o -1 3 9 235.86 261.17 8.83 o 0 3 9 88.02 90.09 3.92 o 1 3 9 192.62 180.11 4.39 o 2 3 9 56.25 76.60 2.10 o 3 3 9 118.16 99.04 1.91 o 4 3 9 26.80 23.62 1.89 o -6 4 9 7.57 4.65 1.38 o -5 4 9 161.37 88.25 7.68 o -4 4 9 13.24 9.25 1.80 o -3 4 9 242.33 260.05 3.58 o -2 4 9 17.85 17.92 1.60 o -1 4 9 259.61 238.30 15.53 o 0 4 9 19.06 16.11 1.51 o 1 4 9 197.51 241.21 7.92 o 2 4 9 15.44 11.76 1.25 o 3 4 9 108.44 81.22 1.66 o -5 5 9 13.94 4.34 1.87 o -4 5 9 106.94 93.99 11.97 o -3 5 9 23.71 18.08 1.57 o -2 5 9 138.63 135.74 8.62 o -1 5 9 29.21 19.48 1.51 o 0 5 9 135.69 134.87 12.48 o 1 5 9 25.78 17.44 2.80 o 2 5 9 99.91 87.28 10.13 o -3 6 9 31.85 21.95 1.86 o -2 6 9 115.47 93.07 8.79 o -1 6 9 29.86 14.61 1.61 o 0 6 9 100.07 90.96 5.60 o -6 0 10 169.25 169.44 3.59 o -4 0 10 285.93 355.34 4.00 o -2 0 10 347.87 334.63 31.80 o 0 0 10 298.14 331.41 18.98 o 2 0 10 177.88 153.52 8.06 o -6 1 10 58.37 44.06 7.79 o -5 1 10 117.37 130.59 29.43 o -4 1 10 89.68 133.35 9.67 o -3 1 10 175.34 192.32 22.68 o -2 1 10 99.02 122.16 4.54 o -1 1 10 186.82 199.48 8.24 o 0 1 10 77.86 103.00 4.59 o 1 1 10 142.86 181.59 13.28 o 2 1 10 45.36 52.13 3.04 o 3 1 10 82.43 94.99 4.56 o -6 2 10 1.97 22.75 3.47 o -5 2 10 191.93 147.86 46.76 o -4 2 10 3.87 51.41 13.53 o -3 2 10 300.96 306.16 24.48 o -2 2 10 5.03 61.01 5.56 o -1 2 10 339.07 300.29 14.92 o 0 2 10 4.25 54.54 2.28 o 1 2 10 270.00 356.67 18.75 o 2 2 10 2.22 27.12 3.25 o 3 2 10 152.84 127.32 8.28 o -5 3 10 23.80 20.19 2.18 o -4 3 10 110.79 85.49 7.99 o -3 3 10 33.42 48.77 3.94 o -2 3 10 130.34 113.39 6.60 o -1 3 10 35.13 49.88 5.01 o 0 3 10 109.57 112.39 11.74 o 1 3 10 27.71 43.07 1.43 o 2 3 10 67.99 59.85 7.85 o -4 4 10 125.71 89.59 6.60 o -3 4 10 14.37 30.25 1.67 o -2 4 10 158.88 116.00 3.02 o -1 4 10 13.35 42.24 2.58 o 0 4 10 146.00 141.18 10.41 o 1 4 10 8.17 30.52 1.97 o -3 5 10 58.59 34.99 1.91 o -2 5 10 0.79 5.30 1.34 o -1 5 10 54.33 25.46 1.80 o -5 0 11 110.27 116.47 3.34 o -3 0 11 157.09 176.62 44.36 o -1 0 11 169.57 186.29 9.94 o 1 0 11 136.68 120.11 2.58 o -5 1 11 54.08 44.34 4.52 o -4 1 11 49.76 56.15 12.21 o -3 1 11 77.91 66.26 7.64 o -2 1 11 55.21 56.90 1.88 o -1 1 11 80.58 86.73 3.79 o 0 1 11 44.72 36.88 1.58 o 1 1 11 59.86 54.22 3.91 o -4 2 11 66.28 45.92 5.67 o -3 2 11 4.91 5.67 1.41 o -2 2 11 75.98 73.27 5.13 o -1 2 11 5.23 9.49 1.33 o 0 2 11 67.00 53.26 2.15 o 1 2 11 4.51 5.14 1.13 o -3 3 11 83.63 71.91 5.46 o -2 3 11 28.49 21.18 1.82 o -1 3 11 83.42 69.27 6.66 o 0 3 11 23.34 24.61 2.31 o