#------------------------------------------------------------------------------ #$Date: 2019-02-13 05:30:19 +0200 (Wed, 13 Feb 2019) $ #$Revision: 213617 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/14/2021477.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021477 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.7332 _cell_length_b 8.2012 _cell_length_c 28.0902 _exptl_crystal_F_000 1616.00 _reflns_d_resolution_high 0.7501 _cod_data_source_file ku32353csup8.hkl _cod_data_source_block 3c _shelx_title ' SIR2004 run in space group P b c a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 445.79 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 416.71 389.06 45.81 o 6 0 0 1137.83 1491.38 99.94 o 8 0 0 4893.87 5565.75 227.25 o 10 0 0 3967.68 4187.40 220.11 o 12 0 0 8718.66 9741.26 368.83 o 14 0 0 764.60 590.72 104.11 o 16 0 0 2.22 47.59 43.43 o 18 0 0 0.28 41.05 51.16 o 20 0 0 44.75 116.60 64.84 o 22 0 0 78.23 158.83 79.12 o 4 1 0 25807.80 27176.01 174.46 o 6 1 0 21682.12 25164.47 391.80 o 8 1 0 2072.95 1962.78 178.72 o 10 1 0 7599.16 8106.84 215.30 o 12 1 0 0.16 -13.41 24.09 o 14 1 0 1877.57 1984.96 130.92 o 16 1 0 795.25 1240.85 229.63 o 18 1 0 70.65 81.95 41.96 o 20 1 0 42.21 7.06 26.30 o 22 1 0 67.11 59.47 45.51 o 0 2 0 690.99 583.51 27.48 o 2 2 0 2436.06 2420.43 46.78 o 4 2 0 8719.33 9833.58 89.29 o 6 2 0 3190.68 3721.33 74.29 o 8 2 0 737.89 816.56 38.93 o 10 2 0 86.63 128.10 50.86 o 12 2 0 2600.71 2856.08 143.80 o 14 2 0 2.85 -4.40 24.73 o 16 2 0 0.49 -9.54 27.07 o 18 2 0 176.96 161.87 49.52 o 20 2 0 223.89 314.21 68.95 o 2 3 0 92.64 115.37 9.51 o 4 3 0 1350.93 1436.04 26.85 o 6 3 0 25305.02 28322.94 339.55 o 8 3 0 1116.29 958.76 45.82 o 10 3 0 2312.72 2451.18 97.65 o 12 3 0 2840.88 2943.96 118.07 o 14 3 0 1225.06 1272.00 104.32 o 16 3 0 478.61 528.34 78.77 o 18 3 0 310.66 458.08 75.85 o 20 3 0 509.21 713.27 154.67 o 0 4 0 261.77 173.84 32.72 o 2 4 0 12431.90 13272.56 148.43 o 4 4 0 3910.62 3552.93 131.46 o 6 4 0 2440.78 2565.51 66.00 o 8 4 0 1931.33 1922.55 76.82 o 10 4 0 71.14 100.28 25.09 o 12 4 0 2397.77 2279.85 104.87 o 14 4 0 922.95 1064.67 78.32 o 16 4 0 6.84 85.07 61.27 o 18 4 0 3206.38 3707.33 327.19 o 20 4 0 46.75 51.76 69.60 o 2 5 0 11.30 25.10 7.74 o 4 5 0 469.76 482.45 44.23 o 6 5 0 5668.29 6894.22 170.51 o 8 5 0 13.98 9.43 10.82 o 10 5 0 825.57 920.45 91.01 o 12 5 0 213.50 212.04 50.27 o 14 5 0 811.43 717.66 89.55 o 16 5 0 611.25 916.12 164.19 o 18 5 0 62.57 58.89 41.64 o 0 6 0 561.04 519.33 38.43 o 2 6 0 1626.88 1796.61 66.37 o 4 6 0 93.90 210.52 53.69 o 6 6 0 2473.87 2545.08 114.03 o 8 6 0 326.08 357.34 47.73 o 10 6 0 822.15 818.27 73.73 o 12 6 0 584.53 661.09 71.26 o 14 6 0 29.17 0.32 24.31 o 16 6 0 0.19 -13.74 31.76 o 18 6 0 300.11 523.50 127.31 o 2 7 0 1223.71 1272.29 56.29 o 4 7 0 1170.48 1302.81 70.27 o 6 7 0 894.86 835.03 69.14 o 8 7 0 896.19 823.89 73.60 o 10 7 0 2597.90 2630.17 135.60 o 12 7 0 71.58 6.68 25.06 o 14 7 0 111.45 83.06 67.36 o 16 7 0 453.09 541.25 74.68 o 0 8 0 104.26 133.98 35.00 o 2 8 0 0.15 -2.61 19.44 o 4 8 0 2003.85 2014.34 101.51 o 6 8 0 879.19 997.07 85.68 o 8 8 0 179.54 152.54 36.09 o 10 8 0 168.62 192.46 42.09 o 12 8 0 100.69 62.76 33.44 o 14 8 0 873.23 910.93 94.40 o 2 9 0 3.79 53.71 37.52 o 4 9 0 13.80 17.41 22.33 o 6 9 0 91.66 52.47 21.84 o 8 9 0 17.56 8.45 34.50 o 10 9 0 11.42 39.24 28.21 o 12 9 0 82.33 -4.58 31.25 o 0 10 0 1680.53 2036.89 238.55 o 2 10 0 160.29 132.18 37.91 o 4 10 0 498.38 509.20 109.76 o 6 10 0 71.13 75.14 41.59 o 8 10 0 27.43 14.75 22.94 o 3 1 1 37078.46 43528.37 172.22 o 4 1 1 5406.19 4944.77 41.96 o 5 1 1 53.56 59.32 6.02 o 6 1 1 2230.78 2779.02 59.02 o 7 1 1 9.57 9.71 5.81 o 8 1 1 800.84 781.33 29.40 o 9 1 1 2421.46 2644.46 99.96 o 10 1 1 388.36 329.30 37.91 o 11 1 1 105.44 68.03 10.26 o 12 1 1 2153.22 2188.76 88.25 o 13 1 1 1142.31 1156.68 68.54 o 14 1 1 2000.05 1932.52 92.15 o 15 1 1 245.50 225.86 36.20 o 16 1 1 47.20 0.25 21.35 o 17 1 1 8.80 17.60 22.28 o 18 1 1 40.16 24.71 25.67 o 19 1 1 13.20 -15.52 23.40 o 20 1 1 134.71 132.27 33.54 o 21 1 1 38.80 36.21 47.48 o 22 1 1 30.52 28.28 53.32 o 0 2 1 198730.11 224317.62 1087.61 o 1 2 1 263.09 287.05 8.22 o 2 2 1 6101.47 6744.61 46.67 o 3 2 1 1738.71 1612.56 24.71 o 5 2 1 658.17 690.63 23.82 o 6 2 1 1588.79 1590.38 38.66 o 7 2 1 100.96 84.22 12.20 o 8 2 1 1993.39 1916.25 47.02 o 9 2 1 1062.19 1141.44 38.25 o 10 2 1 531.04 540.28 29.54 o 11 2 1 14.72 11.72 11.02 o 12 2 1 3990.80 4401.13 124.47 o 13 2 1 67.90 42.01 18.23 o 14 2 1 1484.10 1503.73 80.26 o 15 2 1 6.88 17.69 19.61 o 16 2 1 9.40 -15.50 20.17 o 17 2 1 77.25 66.43 26.28 o 18 2 1 1437.92 1497.17 93.51 o 19 2 1 0.02 -28.34 28.34 o 20 2 1 39.61 -23.31 29.37 o 21 2 1 18.09 -3.77 26.78 o 1 3 1 712.74 693.89 14.58 o 2 3 1 2127.54 2378.09 31.08 o 3 3 1 10946.03 11674.55 88.27 o 4 3 1 1618.59 1519.59 24.28 o 5 3 1 50.21 74.32 6.48 o 6 3 1 7656.59 9401.74 133.95 o 7 3 1 22.58 29.62 8.63 o 8 3 1 1086.19 1230.86 39.47 o 9 3 1 71.69 104.78 14.25 o 10 3 1 763.40 636.43 31.98 o 11 3 1 293.47 280.76 22.59 o 12 3 1 225.38 245.87 26.06 o 13 3 1 135.43 102.59 22.85 o 14 3 1 297.29 274.29 36.70 o 15 3 1 36.50 25.78 18.17 o 16 3 1 2610.02 2969.76 121.05 o 17 3 1 54.30 30.62 20.67 o 18 3 1 160.74 142.79 31.21 o 19 3 1 16.32 -2.51 20.78 o 20 3 1 234.97 181.94 61.31 o 21 3 1 1.37 11.43 48.19 o 0 4 1 7013.04 8378.90 85.99 o 1 4 1 175.77 158.02 7.94 o 2 4 1 29.52 23.90 5.36 o 3 4 1 24111.32 27611.90 236.98 o 4 4 1 272.03 337.99 18.45 o 5 4 1 243.28 205.57 10.26 o 6 4 1 45.37 38.28 5.56 o 7 4 1 1518.97 1535.54 32.38 o 8 4 1 907.96 814.27 33.15 o 9 4 1 312.43 333.53 23.04 o 10 4 1 408.30 484.87 31.92 o 11 4 1 437.75 399.85 30.94 o 12 4 1 0.15 0.72 11.93 o 13 4 1 28.36 34.82 16.58 o 14 4 1 14.89 -3.50 12.94 o 15 4 1 5.24 -23.63 23.63 o 16 4 1 28.58 42.33 29.30 o 17 4 1 1.01 22.30 33.02 o 18 4 1 215.19 268.20 66.27 o 19 4 1 158.72 293.60 71.51 o 20 4 1 21.58 36.61 38.53 o 1 5 1 453.01 448.49 15.49 o 2 5 1 1980.87 1856.57 32.47 o 3 5 1 632.77 646.36 22.27 o 4 5 1 686.18 690.28 26.64 o 5 5 1 0.83 -0.99 8.02 o 6 5 1 351.45 447.55 24.78 o 7 5 1 1071.12 1024.44 41.65 o 8 5 1 511.04 507.51 24.30 o 9 5 1 110.44 129.66 18.73 o 10 5 1 6346.99 6629.00 164.33 o 11 5 1 25.41 34.44 20.50 o 12 5 1 46.39 25.64 19.39 o 13 5 1 0.91 -6.61 23.40 o 14 5 1 637.14 602.95 58.70 o 15 5 1 40.60 24.88 21.89 o 16 5 1 1000.31 1094.38 121.11 o 17 5 1 1.26 32.37 41.07 o 18 5 1 416.15 659.82 103.69 o 19 5 1 15.78 4.30 35.57 o 0 6 1 70.65 25.80 8.59 o 1 6 1 48.78 34.11 6.12 o 2 6 1 838.82 905.28 27.79 o 3 6 1 330.19 334.13 21.93 o 4 6 1 7523.69 7510.18 126.50 o 5 6 1 502.12 471.06 33.56 o 6 6 1 985.56 1029.20 50.60 o 7 6 1 10.55 -4.35 13.62 o 8 6 1 939.56 952.20 51.77 o 9 6 1 257.16 214.60 25.88 o 10 6 1 0.22 9.54 18.58 o 11 6 1 202.64 213.29 29.24 o 12 6 1 1576.07 1587.80 74.86 o 13 6 1 0.44 25.93 18.36 o 14 6 1 371.24 423.14 46.36 o 15 6 1 108.24 127.03 30.97 o 16 6 1 647.71 612.79 64.92 o 17 6 1 18.69 31.34 34.31 o 18 6 1 311.23 281.23 91.31 o 1 7 1 0.21 -9.77 9.77 o 2 7 1 1785.42 1754.15 50.40 o 3 7 1 76.73 55.41 11.19 o 4 7 1 443.35 464.07 37.30 o 5 7 1 553.10 522.34 34.77 o 6 7 1 1570.92 1555.12 66.53 o 7 7 1 82.83 47.77 17.20 o 8 7 1 112.49 143.54 24.73 o 9 7 1 753.60 777.02 51.22 o 10 7 1 407.12 446.15 41.73 o 11 7 1 0.32 9.78 17.39 o 12 7 1 362.30 337.32 38.07 o 13 7 1 63.03 52.59 20.94 o 14 7 1 450.66 384.02 43.30 o 15 7 1 26.79 53.44 28.61 o 16 7 1 85.92 93.01 24.71 o 17 7 1 30.83 -2.75 26.95 o 0 8 1 463.96 499.52 47.42 o 1 8 1 16.55 -6.66 16.37 o 2 8 1 907.64 961.62 55.81 o 3 8 1 10.71 12.99 16.46 o 4 8 1 30.95 53.35 17.98 o 5 8 1 55.93 12.79 19.37 o 6 8 1 57.35 38.64 22.04 o 7 8 1 0.22 26.34 17.33 o 8 8 1 12.33 29.95 17.25 o 9 8 1 234.01 166.27 28.66 o 10 8 1 6.49 -12.23 15.64 o 11 8 1 1.48 -19.64 20.71 o 12 8 1 223.07 188.77 30.72 o 13 8 1 75.72 69.46 26.63 o 14 8 1 380.22 486.35 49.40 o 15 8 1 12.66 27.75 23.89 o 1 9 1 5.48 -18.02 26.88 o 2 9 1 1399.44 1512.99 83.23 o 3 9 1 59.80 52.62 20.24 o 4 9 1 276.80 315.56 36.49 o 5 9 1 42.71 13.45 16.49 o 6 9 1 24.67 30.57 17.46 o 7 9 1 269.38 261.39 34.93 o 8 9 1 1.68 -16.02 22.77 o 9 9 1 21.16 -19.00 19.00 o 10 9 1 90.45 79.43 26.51 o 11 9 1 5.51 -7.74 22.11 o 12 9 1 119.62 162.83 44.75 o 0 10 1 80.97 110.31 45.74 o 1 10 1 0.15 -20.91 23.49 o 2 10 1 10.60 28.89 29.50 o 3 10 1 66.31 58.60 25.47 o 4 10 1 574.71 522.09 63.48 o 5 10 1 9.45 34.23 32.35 o 6 10 1 110.36 118.94 55.86 o 7 10 1 0.39 -8.32 17.36 o 8 10 1 37.71 21.26 17.18 o 9 10 1 154.72 76.20 34.24 o 4 0 2 1723.53 2261.76 74.33 o 5 0 2 231.53 292.36 32.08 o 6 0 2 9245.26 8791.96 171.97 o 7 0 2 412.34 450.89 44.79 o 8 0 2 4803.40 4570.08 144.28 o 9 0 2 1769.02 2045.51 104.09 o 10 0 2 0.29 13.65 22.73 o 11 0 2 133.86 140.56 34.46 o 12 0 2 4098.80 4031.76 170.12 o 13 0 2 11.92 -25.00 33.61 o 14 0 2 2135.48 2239.43 142.60 o 15 0 2 981.69 1069.08 102.12 o 16 0 2 827.20 757.38 114.22 o 17 0 2 216.25 289.77 61.02 o 18 0 2 278.06 199.41 54.43 o 19 0 2 0.85 -35.96 35.96 o 20 0 2 137.33 155.11 72.87 o 21 0 2 45.00 62.31 79.42 o 22 0 2 132.68 164.68 58.46 o 3 1 2 50623.18 58464.43 313.80 o 4 1 2 688.12 642.35 15.41 o 5 1 2 2235.24 2295.26 34.34 o 6 1 2 217.12 232.65 12.33 o 7 1 2 631.85 459.51 29.27 o 8 1 2 244.35 159.88 12.59 o 9 1 2 5261.98 6147.96 148.42 o 10 1 2 2869.16 2859.58 75.97 o 11 1 2 15.36 2.18 9.08 o 12 1 2 0.41 -0.23 14.49 o 13 1 2 594.28 751.23 55.75 o 14 1 2 1287.40 1385.11 78.29 o 15 1 2 79.30 57.11 26.19 o 16 1 2 146.35 142.17 29.45 o 17 1 2 66.66 33.16 20.41 o 18 1 2 534.91 527.64 58.30 o 19 1 2 0.29 20.68 25.67 o 20 1 2 69.49 67.17 28.55 o 21 1 2 82.94 79.05 29.75 o 22 1 2 36.76 61.50 26.03 o 0 2 2 30768.54 31848.39 220.00 o 1 2 2 830.68 761.92 13.23 o 2 2 2 7322.15 7232.76 54.19 o 3 2 2 113065.45 125280.95 572.22 o 4 2 2 1625.58 1544.66 24.16 o 5 2 2 2437.48 2424.29 44.71 o 6 2 2 10240.73 11325.24 131.07 o 7 2 2 2091.74 2536.16 75.12 o 8 2 2 646.05 657.60 28.60 o 9 2 2 27.46 79.56 12.03 o 10 2 2 563.84 578.28 31.01 o 11 2 2 447.94 496.94 32.21 o 12 2 2 519.76 457.40 33.14 o 13 2 2 103.37 80.36 28.94 o 14 2 2 111.27 95.21 24.36 o 15 2 2 305.31 292.57 39.58 o 16 2 2 7.17 13.42 19.52 o 17 2 2 105.32 112.23 26.41 o 18 2 2 33.10 13.56 26.27 o 19 2 2 62.08 89.23 26.26 o 20 2 2 82.71 133.28 32.85 o 21 2 2 96.84 99.02 31.80 o 1 3 2 1487.81 1428.72 22.51 o 2 3 2 3917.24 3923.36 37.89 o 3 3 2 3584.74 3975.85 40.74 o 4 3 2 2031.52 2245.17 31.36 o 5 3 2 6.20 6.58 3.23 o 6 3 2 1659.22 1572.10 39.50 o 7 3 2 2255.35 2299.69 51.00 o 8 3 2 60.47 67.46 11.13 o 9 3 2 5.06 -2.80 9.26 o 10 3 2 223.19 207.32 18.88 o 11 3 2 11.75 -0.81 9.22 o 12 3 2 4.87 6.64 9.32 o 13 3 2 1037.00 1124.35 66.91 o 14 3 2 444.13 414.01 44.25 o 15 3 2 0.98 12.53 16.96 o 16 3 2 1042.13 1180.29 77.41 o 17 3 2 1.68 -7.22 19.87 o 18 3 2 24.35 4.39 18.74 o 19 3 2 88.18 78.51 30.37 o 20 3 2 256.08 375.19 81.33 o 21 3 2 35.17 21.75 32.32 o 0 4 2 54.09 63.44 7.88 o 1 4 2 420.47 411.79 13.84 o 2 4 2 658.80 758.48 20.45 o 3 4 2 1503.73 1569.34 34.16 o 4 4 2 3413.31 3650.48 48.81 o 5 4 2 3273.49 3523.66 59.89 o 6 4 2 274.42 276.80 14.25 o 7 4 2 34.93 37.66 5.62 o 8 4 2 781.68 686.04 26.53 o 9 4 2 1.33 10.65 14.33 o 10 4 2 396.19 333.86 24.40 o 11 4 2 161.23 120.26 16.18 o 12 4 2 2688.28 2790.35 81.86 o 13 4 2 103.15 89.57 21.99 o 14 4 2 691.13 804.79 58.47 o 15 4 2 19.91 1.16 22.05 o 16 4 2 464.16 527.84 86.59 o 17 4 2 23.19 61.69 37.48 o 18 4 2 1835.76 2235.41 179.10 o 19 4 2 1.90 -20.23 39.09 o 20 4 2 0.03 -76.74 76.74 o 1 5 2 98.59 99.37 6.81 o 2 5 2 8.46 19.27 7.37 o 3 5 2 91.08 82.21 10.89 o 4 5 2 2.98 9.01 5.99 o 5 5 2 1507.09 1544.30 42.49 o 6 5 2 1006.01 1020.41 36.94 o 7 5 2 80.17 81.44 12.48 o 8 5 2 134.12 155.69 16.38 o 9 5 2 659.46 692.22 36.53 o 10 5 2 31.61 64.14 18.08 o 11 5 2 425.03 382.87 43.40 o 12 5 2 9.14 -3.18 23.27 o 13 5 2 0.67 -20.43 20.43 o 14 5 2 104.38 145.29 33.90 o 15 5 2 384.19 361.91 56.52 o 16 5 2 266.25 225.73 66.27 o 17 5 2 0.42 10.26 36.02 o 18 5 2 205.95 204.27 85.07 o 19 5 2 22.46 24.67 82.69 o 0 6 2 7.30 21.20 10.99 o 1 6 2 0.01 -4.53 5.79 o 2 6 2 1660.90 1675.47 40.11 o 3 6 2 1306.50 1446.53 44.12 o 4 6 2 548.23 538.18 33.68 o 5 6 2 1035.07 1121.38 51.16 o 6 6 2 123.39 175.93 24.66 o 7 6 2 393.43 347.55 31.67 o 8 6 2 103.00 146.91 24.82 o 9 6 2 597.59 619.87 44.36 o 10 6 2 180.38 109.17 20.97 o 11 6 2 557.67 444.42 40.02 o 12 6 2 183.40 240.22 31.61 o 13 6 2 488.54 501.83 49.40 o 14 6 2 324.18 356.62 43.21 o 15 6 2 158.80 156.14 30.76 o 16 6 2 0.24 -10.07 20.71 o 17 6 2 0.09 30.50 24.61 o 18 6 2 439.60 532.38 116.00 o 1 7 2 123.07 107.67 14.26 o 2 7 2 1968.37 2111.07 53.30 o 3 7 2 602.64 633.21 31.60 o 4 7 2 122.97 121.11 20.11 o 5 7 2 7.15 1.99 14.50 o 6 7 2 262.55 273.66 27.08 o 7 7 2 215.32 197.77 26.80 o 8 7 2 87.83 62.97 18.57 o 9 7 2 158.07 164.43 25.92 o 10 7 2 771.38 770.60 52.03 o 11 7 2 39.06 -5.87 17.83 o 12 7 2 162.54 282.54 36.77 o 13 7 2 247.57 213.07 32.49 o 14 7 2 631.46 677.05 55.67 o 15 7 2 23.96 17.50 19.15 o 16 7 2 400.08 440.34 50.86 o 17 7 2 132.32 100.67 34.31 o 0 8 2 3167.34 3321.00 115.91 o 1 8 2 3.30 -10.99 16.05 o 2 8 2 21.82 38.84 17.88 o 3 8 2 0.92 -13.60 15.82 o 4 8 2 831.48 836.94 47.44 o 5 8 2 15.65 4.80 17.11 o 6 8 2 392.86 480.20 48.03 o 7 8 2 17.39 41.91 21.98 o 8 8 2 378.92 376.30 38.17 o 9 8 2 399.69 387.46 36.66 o 10 8 2 473.68 479.29 44.12 o 11 8 2 152.71 94.62 21.79 o 12 8 2 79.58 70.21 22.65 o 13 8 2 104.60 73.09 25.60 o 14 8 2 232.10 325.83 41.33 o 15 8 2 41.32 -2.62 23.65 o 1 9 2 26.83 30.35 21.22 o 2 9 2 31.42 55.54 24.59 o 3 9 2 199.45 209.61 33.04 o 4 9 2 14.48 10.51 24.48 o 5 9 2 50.91 22.28 17.12 o 6 9 2 74.52 46.26 17.57 o 7 9 2 202.74 213.31 43.04 o 8 9 2 116.69 109.46 29.25 o 9 9 2 244.74 228.92 37.63 o 10 9 2 10.07 -29.06 44.74 o 11 9 2 183.36 125.90 34.15 o 12 9 2 220.24 177.85 38.02 o 0 10 2 1038.21 1218.01 134.54 o 1 10 2 0.60 -29.68 29.68 o 2 10 2 2.59 -22.73 26.79 o 3 10 2 18.77 27.40 25.69 o 4 10 2 283.68 262.06 46.36 o 5 10 2 77.16 96.49 35.00 o 6 10 2 111.66 123.91 31.32 o 7 10 2 30.72 66.01 24.68 o 8 10 2 5.26 13.73 19.14 o 3 1 3 11252.24 12753.25 71.81 o 4 1 3 3314.61 3079.79 37.37 o 5 1 3 204.86 210.61 10.43 o 6 1 3 2205.83 2049.65 42.90 o 7 1 3 1471.17 1478.57 38.44 o 8 1 3 77.39 48.86 14.21 o 9 1 3 439.89 565.81 39.72 o 10 1 3 23.73 23.04 12.57 o 11 1 3 223.20 206.87 20.01 o 12 1 3 288.61 199.52 30.24 o 13 1 3 1323.78 1430.32 102.18 o 14 1 3 186.16 149.54 31.00 o 15 1 3 123.60 75.49 23.19 o 16 1 3 67.12 52.03 22.97 o 17 1 3 0.07 -9.49 19.33 o 18 1 3 12.46 1.31 26.10 o 19 1 3 0.34 35.00 26.04 o 20 1 3 246.42 273.92 45.93 o 21 1 3 44.02 59.46 25.86 o 22 1 3 52.20 34.72 24.29 o 0 2 3 28199.92 33186.86 185.38 o 1 2 3 3276.13 3752.72 31.10 o 2 2 3 39.23 50.55 7.80 o 4 2 3 3178.29 3004.80 36.28 o 5 2 3 656.99 588.80 19.63 o 6 2 3 4160.48 4594.18 66.01 o 7 2 3 1.04 2.50 7.73 o 8 2 3 578.74 497.49 25.50 o 9 2 3 5.85 14.30 8.18 o 10 2 3 105.83 89.88 14.17 o 11 2 3 119.01 88.71 15.53 o 12 2 3 1135.22 1083.12 48.85 o 13 2 3 48.67 19.18 17.89 o 14 2 3 2209.63 2397.95 102.07 o 15 2 3 1116.65 1197.01 75.27 o 16 2 3 797.46 815.88 68.26 o 17 2 3 16.26 51.36 25.32 o 18 2 3 756.86 817.67 72.06 o 19 2 3 0.05 21.77 25.08 o 20 2 3 28.42 1.99 26.95 o 21 2 3 33.86 34.40 27.97 o 1 3 3 340.21 319.29 11.00 o 2 3 3 215.85 278.84 10.92 o 3 3 3 543.51 562.16 18.06 o 4 3 3 39.90 65.62 7.60 o 6 3 3 3200.60 3671.74 60.28 o 7 3 3 825.87 932.70 33.04 o 8 3 3 254.72 233.92 18.61 o 9 3 3 449.92 512.63 27.96 o 10 3 3 1362.34 1268.92 45.30 o 11 3 3 397.94 423.26 32.56 o 12 3 3 162.91 219.94 23.28 o 13 3 3 21.48 60.51 23.32 o 14 3 3 38.63 32.08 18.15 o 15 3 3 456.91 432.45 54.27 o 16 3 3 898.77 1041.52 72.58 o 17 3 3 11.09 3.45 20.32 o 18 3 3 696.53 616.97 59.34 o 19 3 3 11.93 -4.05 27.39 o 20 3 3 87.73 88.12 34.98 o 21 3 3 0.51 10.69 34.88 o 0 4 3 7844.74 8970.59 101.01 o 1 4 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4963.23 4830.20 130.18 o 3 0 10 197.68 150.70 15.27 o 4 0 10 19709.59 21953.21 230.50 o 5 0 10 14166.19 15723.06 216.89 o 6 0 10 804.92 806.20 44.51 o 8 0 10 2194.46 2008.47 67.09 o 9 0 10 70.42 51.87 16.18 o 10 0 10 248.62 170.16 17.87 o 11 0 10 23.70 11.97 5.82 o 12 0 10 2326.64 2137.60 103.08 o 13 0 10 197.88 175.77 41.94 o 14 0 10 4150.68 4383.16 202.65 o 15 0 10 18.25 19.08 31.54 o 16 0 10 952.12 1025.33 106.95 o 17 0 10 0.00 4.10 41.30 o 18 0 10 9.66 71.08 67.52 o 19 0 10 131.11 153.55 49.20 o 20 0 10 140.61 32.75 45.51 o 21 0 10 3.66 4.41 27.86 o 1 1 10 519.25 599.32 24.79 o 2 1 10 1897.37 1775.54 39.61 o 3 1 10 47.02 33.78 8.65 o 4 1 10 2.62 5.95 3.96 o 5 1 10 2107.56 2199.28 36.60 o 6 1 10 7813.34 7890.77 88.61 o 7 1 10 908.59 884.72 32.02 o 8 1 10 36.82 1.27 7.61 o 9 1 10 647.51 679.30 28.33 o 10 1 10 2368.83 2216.28 53.11 o 11 1 10 492.02 433.35 25.50 o 12 1 10 71.38 92.47 18.95 o 13 1 10 109.59 62.32 16.05 o 14 1 10 23.43 1.29 20.15 o 15 1 10 9.31 -5.12 16.99 o 16 1 10 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