#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/29/2012926.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012926_Fobs loop_ _publ_author_name 'Geller, Jordan' 'Wharf, Ivor' 'B\'elanger-Gari\'epy, Francine' 'Lebuis, Anne-Marie' 'Butler, Ian S.' 'Gilson, Denis F. R.' _publ_section_title ; Chlorotris(2,4,6-trimethylphenyl)tin(IV) and its ethanol hemisolvate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m466 _journal_page_last m468 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.996 _cell_angle_beta 96.568 _cell_angle_gamma 90.539 _cell_length_a 8.2564 _cell_length_b 16.8363 _cell_length_c 19.5759 _exptl_crystal_F_000 1100.00 _reflns_d_resolution_high 0.8067 _[local]_cod_data_source_file fg1654IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' butl70 in P-1 ccd' _shelx_refln_list_code 4 _shelx_f_calc_maximum 278.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6882.43 7908.30 45.96 o 2 0 0 5390.35 5789.62 51.71 o 3 0 0 2480.47 2782.45 44.27 o 4 0 0 310.11 357.12 27.73 o 5 0 0 1065.45 1091.40 52.17 o 6 0 0 287.08 328.08 57.39 o 7 0 0 1375.93 1358.41 121.47 o 8 0 0 1392.60 1265.88 106.89 o 9 0 0 19.55 9.29 35.13 o 10 0 0 162.05 124.86 33.87 o -10 1 0 125.55 104.03 32.82 o -9 1 0 567.86 557.78 71.12 o -8 1 0 12.04 22.56 41.12 o -7 1 0 251.33 308.09 77.66 o -6 1 0 0.71 30.95 36.79 o -5 1 0 82.78 55.05 21.87 o -4 1 0 15604.78 16488.01 294.68 o -3 1 0 7594.69 8440.97 76.74 o -2 1 0 1446.75 1472.77 26.61 o -1 1 0 55911.12 58532.77 210.06 o 0 1 0 30.12 21.37 2.11 o 1 1 0 625.39 664.58 13.49 o 2 1 0 12040.61 12801.20 107.63 o 3 1 0 3236.07 3601.61 50.91 o 4 1 0 16006.69 18038.17 134.66 o 5 1 0 553.08 548.48 83.03 o 6 1 0 5821.19 5346.53 184.05 o 7 1 0 1327.62 1576.21 131.74 o 8 1 0 25.78 30.54 40.83 o 9 1 0 42.27 53.79 38.36 o 10 1 0 71.61 64.62 32.46 o -10 2 0 225.75 265.31 42.22 o -9 2 0 63.59 58.78 38.14 o -8 2 0 165.27 194.25 51.59 o -7 2 0 312.67 376.59 56.23 o -6 2 0 667.18 666.28 68.29 o -5 2 0 2738.94 2758.17 81.24 o -4 2 0 84.66 88.71 18.85 o -3 2 0 11174.63 11641.18 86.91 o -2 2 0 1011.96 1147.40 23.17 o -1 2 0 1960.32 2327.06 23.02 o 0 2 0 5712.55 6609.67 42.41 o 1 2 0 7260.38 7379.93 75.98 o 2 2 0 5390.60 5718.45 52.76 o 3 2 0 19423.97 20534.04 142.31 o 4 2 0 128.53 163.88 21.00 o 5 2 0 708.04 630.96 67.42 o 6 2 0 207.63 218.76 56.82 o 7 2 0 22.66 35.00 50.30 o 8 2 0 1082.80 1152.95 129.01 o 9 2 0 15.20 32.10 33.55 o 10 2 0 319.21 309.47 40.19 o -9 3 0 640.86 566.73 64.84 o -8 3 0 1.21 8.02 36.78 o -7 3 0 3789.18 3868.62 130.72 o -6 3 0 1899.90 1684.01 74.34 o -5 3 0 399.77 314.75 37.58 o -4 3 0 71.72 50.59 18.95 o -3 3 0 248.51 247.63 24.19 o -2 3 0 1666.95 1739.56 26.74 o -1 3 0 23102.10 25676.00 223.61 o 0 3 0 37.51 57.04 6.24 o 1 3 0 17965.54 19267.52 88.12 o 2 3 0 1719.98 1827.84 30.21 o 3 3 0 1787.73 1904.48 37.95 o 4 3 0 443.85 476.98 34.74 o 5 3 0 468.34 381.63 79.20 o 6 3 0 2219.36 1984.63 116.63 o 7 3 0 3889.62 3560.91 163.52 o 8 3 0 60.31 43.83 44.28 o 9 3 0 154.20 108.67 41.63 o 10 3 0 31.07 18.92 57.80 o -9 4 0 0.62 27.35 33.38 o -8 4 0 365.86 393.90 52.76 o -7 4 0 54.86 89.74 41.06 o -6 4 0 89.69 92.66 32.13 o -5 4 0 3236.69 3013.54 89.30 o -4 4 0 34.77 110.45 22.39 o -3 4 0 13657.29 15217.10 153.36 o -2 4 0 10621.10 11656.83 74.57 o -1 4 0 4360.31 4853.62 45.54 o 0 4 0 15369.10 16366.48 82.97 o 1 4 0 18406.00 20683.34 194.36 o 2 4 0 6057.90 6415.74 76.74 o 3 4 0 10967.69 11332.26 128.46 o 4 4 0 196.18 205.14 26.41 o 5 4 0 2232.10 2092.25 87.12 o 6 4 0 120.76 154.35 51.91 o 7 4 0 326.57 392.10 74.97 o 8 4 0 1.71 24.71 40.62 o 9 4 0 9.07 31.20 35.22 o -9 5 0 0.51 5.94 30.43 o -8 5 0 1.21 53.12 36.71 o -7 5 0 1060.29 1174.92 83.40 o -6 5 0 2685.32 2387.25 76.75 o -5 5 0 136.72 133.97 30.86 o -4 5 0 10271.39 10713.23 173.22 o -3 5 0 604.23 694.94 36.82 o -2 5 0 778.25 827.13 22.58 o -1 5 0 1641.49 1803.55 30.98 o 0 5 0 16.32 22.96 6.95 o 1 5 0 16991.07 18147.93 179.45 o 2 5 0 7711.63 8443.31 87.88 o 3 5 0 10207.04 10167.41 128.45 o 4 5 0 7417.31 7371.46 122.34 o 5 5 0 522.05 515.32 44.51 o 6 5 0 13.75 80.41 59.96 o 7 5 0 671.42 623.38 85.81 o 8 5 0 118.94 108.09 47.19 o 9 5 0 608.44 589.72 66.60 o -9 6 0 40.37 54.71 30.48 o -8 6 0 1172.64 1294.21 76.77 o -7 6 0 412.39 409.00 48.45 o -6 6 0 16.04 71.63 34.81 o -5 6 0 225.59 216.74 35.75 o -4 6 0 239.65 236.39 30.77 o -3 6 0 116.95 107.55 17.75 o -2 6 0 3750.41 3601.09 47.32 o -1 6 0 2320.82 2309.90 38.25 o 0 6 0 37631.61 41820.87 443.75 o 1 6 0 3485.98 3397.65 46.75 o 2 6 0 4410.42 4620.94 80.27 o 3 6 0 123.88 175.00 23.03 o 4 6 0 103.86 87.74 22.11 o 5 6 0 2654.60 2276.36 81.31 o 6 6 0 1479.19 1846.07 120.95 o 7 6 0 916.55 897.90 110.49 o 8 6 0 1416.83 1188.75 95.50 o 9 6 0 20.41 -18.90 32.22 o -9 7 0 333.03 383.00 46.29 o -8 7 0 0.14 16.28 33.64 o -7 7 0 306.86 341.11 45.62 o -6 7 0 15.58 -3.43 34.28 o -5 7 0 130.11 110.64 33.88 o -4 7 0 3329.21 3269.20 90.46 o -3 7 0 2241.95 2216.83 59.62 o -2 7 0 973.02 1098.05 33.16 o -1 7 0 4934.61 5248.12 62.99 o 0 7 0 0.05 12.37 7.71 o 1 7 0 374.33 390.67 23.13 o 2 7 0 1020.43 896.40 40.07 o 3 7 0 4461.78 4433.00 100.85 o 4 7 0 16047.02 15733.53 219.59 o 5 7 0 344.67 272.47 39.87 o 6 7 0 2045.41 2087.63 101.07 o 7 7 0 1104.47 1174.76 96.14 o 8 7 0 18.18 3.86 73.77 o 9 7 0 212.21 236.70 45.39 o -9 8 0 61.64 54.24 39.92 o -8 8 0 54.21 64.16 33.09 o -7 8 0 113.39 74.11 36.99 o -6 8 0 909.83 974.00 66.48 o -5 8 0 2350.93 2316.78 92.64 o -4 8 0 55.75 63.21 24.81 o -3 8 0 4621.63 4575.16 86.35 o -2 8 0 655.17 753.30 33.64 o -1 8 0 44.18 58.75 12.06 o 0 8 0 7094.15 8270.06 82.91 o 1 8 0 1732.08 1685.13 61.59 o 2 8 0 10545.51 10524.07 138.87 o 3 8 0 10602.04 10653.46 218.57 o 4 8 0 3.91 -4.91 20.10 o 5 8 0 24.83 36.75 30.72 o 6 8 0 130.42 127.83 44.91 o 7 8 0 4.91 30.02 34.72 o 8 8 0 674.14 729.07 76.77 o 9 8 0 5.40 18.17 33.19 o -9 9 0 200.14 227.73 40.16 o -8 9 0 7.60 17.59 33.94 o -7 9 0 1111.74 1101.98 73.25 o -6 9 0 864.47 937.87 82.80 o -5 9 0 0.48 30.14 40.91 o -4 9 0 10.60 5.96 26.61 o -3 9 0 214.52 179.30 26.10 o -2 9 0 5692.70 5673.20 94.93 o -1 9 0 11171.52 11719.72 109.20 o 0 9 0 0.16 14.47 12.34 o 1 9 0 2986.97 2805.32 70.14 o 2 9 0 22.20 65.07 19.38 o 3 9 0 441.95 422.90 40.11 o 4 9 0 897.40 786.36 57.00 o 5 9 0 34.13 78.03 35.43 o 6 9 0 1202.98 1287.38 82.09 o 7 9 0 1671.24 1652.93 80.65 o 8 9 0 25.18 6.44 35.25 o 9 9 0 68.34 104.74 44.07 o -8 10 0 171.48 157.42 39.43 o -7 10 0 61.19 96.99 37.89 o -6 10 0 468.68 359.75 57.96 o -5 10 0 890.56 937.48 93.01 o -4 10 0 23.11 68.64 42.51 o -3 10 0 4675.20 4706.32 109.02 o -2 10 0 2907.51 2861.21 78.88 o -1 10 0 171.05 169.93 20.60 o 0 10 0 2568.27 2668.95 70.94 o 1 10 0 2.16 42.76 19.10 o 2 10 0 1590.10 1577.78 86.56 o 3 10 0 5488.73 5159.31 128.78 o 4 10 0 238.60 206.87 39.96 o 5 10 0 1436.00 1423.79 74.85 o 6 10 0 285.11 380.54 52.39 o 7 10 0 4.87 17.91 32.81 o 8 10 0 48.02 43.88 37.18 o -8 11 0 36.41 40.76 31.80 o -7 11 0 420.14 426.59 53.54 o -6 11 0 1432.44 1340.02 86.51 o -5 11 0 128.44 86.58 44.80 o -4 11 0 2914.53 3030.00 139.74 o -3 11 0 943.20 882.83 83.75 o -2 11 0 394.41 421.50 80.15 o -1 11 0 1945.30 2020.45 78.88 o 0 11 0 13.28 29.12 24.10 o 1 11 0 9139.76 8815.06 166.75 o 2 11 0 2663.37 2522.59 97.79 o 3 11 0 2102.20 1761.43 93.04 o 4 11 0 755.97 866.20 77.99 o 5 11 0 6.97 9.31 31.30 o 6 11 0 148.77 186.51 44.11 o 7 11 0 339.94 272.53 42.36 o 8 11 0 0.73 69.47 45.12 o -8 12 0 355.43 414.62 42.59 o -7 12 0 178.54 184.58 43.50 o -6 12 0 21.21 26.81 35.46 o -5 12 0 43.94 1.31 39.87 o -4 12 0 31.33 25.68 46.81 o -3 12 0 952.86 932.48 83.65 o -2 12 0 3481.82 3570.21 203.10 o 0 12 0 6681.70 6375.20 182.42 o 1 12 0 441.10 353.50 48.24 o 2 12 0 20.52 13.75 32.80 o 3 12 0 1.36 18.02 36.70 o 4 12 0 110.02 97.29 38.47 o 5 12 0 2283.96 2184.09 98.26 o 6 12 0 245.97 302.90 47.95 o 7 12 0 166.76 244.16 41.86 o -8 13 0 1.50 -33.02 33.83 o -7 13 0 0.82 -0.76 30.61 o -6 13 0 3.13 4.86 37.36 o -5 13 0 160.97 155.87 47.50 o -4 13 0 1750.97 1694.95 109.65 o -3 13 0 1021.38 923.77 104.06 o 0 13 0 0.18 -28.10 64.51 o 1 13 0 44.85 4.92 44.25 o 2 13 0 28.31 50.52 47.22 o 3 13 0 69.64 87.01 41.64 o 4 13 0 1985.61 1759.44 91.35 o 5 13 0 37.18 68.59 36.42 o 6 13 0 266.33 309.73 46.94 o 7 13 0 82.21 112.23 37.80 o -7 14 0 21.18 3.58 31.70 o -6 14 0 726.13 773.93 73.50 o -5 14 0 717.39 819.58 80.18 o -4 14 0 3.86 15.85 43.44 o -3 14 0 413.87 533.93 103.93 o 1 14 0 348.87 389.10 67.17 o 2 14 0 758.42 666.51 74.72 o 3 14 0 1088.56 981.87 83.50 o 4 14 0 0.43 8.06 32.90 o 5 14 0 8.75 0.94 30.72 o 6 14 0 122.50 142.95 34.59 o 7 14 0 38.11 35.23 41.83 o -7 15 0 284.80 374.65 44.69 o -6 15 0 126.11 111.45 42.11 o -5 15 0 10.08 47.09 42.36 o -4 15 0 31.81 31.25 54.18 o -3 15 0 17.76 159.67 110.49 o 1 15 0 977.68 1004.97 88.75 o 2 15 0 42.63 25.98 43.03 o 3 15 0 57.37 38.84 41.00 o 4 15 0 484.49 482.42 61.23 o 5 15 0 5.22 6.80 32.49 o 6 15 0 404.73 410.39 45.82 o -6 16 0 63.39 56.63 38.82 o -5 16 0 367.80 450.26 62.45 o -4 16 0 13.35 54.93 82.39 o 1 16 0 8.58 18.48 61.99 o 2 16 0 655.86 596.12 66.64 o 3 16 0 1109.51 1170.20 91.63 o 4 16 0 81.24 119.22 41.85 o 5 16 0 641.76 737.04 60.71 o 6 16 0 40.31 20.41 25.55 o -5 17 0 3.46 -19.80 71.53 o 1 17 0 1947.32 1841.56 143.03 o 2 17 0 498.61 488.70 69.65 o 3 17 0 125.56 100.87 44.18 o 4 17 0 373.48 360.44 50.21 o 5 17 0 0.08 0.76 29.92 o 1 18 0 62.16 84.76 78.56 o 2 18 0 31.61 83.90 47.68 o 3 18 0 5.14 -1.11 35.45 o 4 18 0 10.70 36.73 31.76 o 2 19 0 169.87 273.96 73.77 o 3 19 0 54.76 50.86 45.42 o -4 -19 1 0.59 9.58 46.62 o -3 -19 1 10.09 53.08 43.79 o -2 -19 1 143.12 130.96 64.91 o -5 -18 1 171.85 244.61 65.15 o -4 -18 1 26.75 22.69 33.80 o -3 -18 1 632.24 645.12 61.72 o -2 -18 1 509.09 511.31 78.57 o -1 -18 1 19.33 63.83 62.30 o -5 -17 1 6.41 31.32 29.20 o -4 -17 1 531.56 581.75 59.34 o -3 -17 1 89.57 97.49 42.97 o -2 -17 1 4.23 15.97 44.97 o -1 -17 1 43.22 114.55 66.09 o 4 -17 1 243.34 312.95 111.13 o 5 -17 1 13.90 85.96 52.15 o -6 -16 1 65.26 77.73 31.97 o -5 -16 1 154.42 123.60 34.32 o -4 -16 1 18.15 -3.93 34.00 o -3 -16 1 268.61 242.42 51.68 o -2 -16 1 529.79 512.82 69.26 o -1 -16 1 547.91 501.45 93.38 o 4 -16 1 18.14 -5.50 53.18 o 5 -16 1 145.70 141.10 55.25 o 6 -16 1 77.56 113.96 40.05 o -6 -15 1 41.26 54.10 28.43 o -5 -15 1 16.89 25.04 30.96 o -4 -15 1 1068.37 1083.40 74.57 o -3 -15 1 183.34 192.31 45.03 o -2 -15 1 2457.15 2463.12 125.62 o -1 -15 1 751.58 803.58 109.20 o 0 -15 1 4.81 69.62 104.10 o 3 -15 1 354.83 330.61 80.99 o 4 -15 1 1019.19 1079.24 109.30 o 5 -15 1 210.67 154.50 52.04 o 6 -15 1 240.95 270.81 47.88 o 7 -15 1 64.95 115.67 40.16 o -7 -14 1 80.70 127.86 32.26 o -6 -14 1 337.46 376.35 43.48 o -5 -14 1 1177.30 1223.87 74.60 o -4 -14 1 9.92 36.12 35.76 o -3 -14 1 627.07 623.91 62.77 o -2 -14 1 14.97 47.33 43.44 o -1 -14 1 249.79 338.60 82.96 o 0 -14 1 1693.12 2000.98 229.92 o 3 -14 1 1847.00 1537.06 120.80 o 4 -14 1 52.79 17.09 48.74 o 5 -14 1 81.81 159.03 50.33 o 6 -14 1 0.31 13.07 35.63 o 7 -14 1 104.72 122.49 36.09 o -7 -13 1 427.02 497.29 51.24 o -6 -13 1 406.16 440.65 48.35 o -5 -13 1 0.91 1.33 31.25 o -4 -13 1 22.62 49.06 36.22 o -3 -13 1 324.67 365.68 61.03 o -2 -13 1 65.87 79.29 43.31 o -1 -13 1 2064.42 1903.00 115.20 o 0 -13 1 18.39 75.36 75.36 o 3 -13 1 16.37 78.63 62.08 o 4 -13 1 680.75 618.07 79.61 o 5 -13 1 23.62 16.25 36.72 o 6 -13 1 604.84 617.70 70.73 o 7 -13 1 649.91 660.81 60.01 o 8 -13 1 0.51 -30.69 31.72 o -8 -12 1 147.92 217.42 53.54 o -7 -12 1 14.86 3.62 32.80 o -6 -12 1 0.60 6.85 33.46 o -5 -12 1 352.70 371.47 52.77 o -4 -12 1 281.92 253.34 46.16 o -3 -12 1 1807.45 1705.40 91.01 o -2 -12 1 4712.79 4247.42 163.83 o -1 -12 1 42.27 67.81 32.77 o 0 -12 1 538.49 592.38 57.49 o 1 -12 1 17.46 38.50 36.10 o 2 -12 1 1519.13 1392.96 130.29 o 3 -12 1 3006.85 2932.81 124.38 o 4 -12 1 2.20 -0.03 45.07 o 5 -12 1 1460.41 1452.21 98.23 o 6 -12 1 424.74 416.90 59.26 o 7 -12 1 12.25 -24.02 29.54 o 8 -12 1 7.10 6.39 30.07 o -8 -11 1 21.90 2.21 40.83 o -7 -11 1 623.73 714.01 63.94 o -6 -11 1 1016.49 1111.44 87.73 o -5 -11 1 98.36 102.05 36.94 o -4 -11 1 1941.59 1888.27 95.56 o -3 -11 1 177.15 123.24 37.07 o -2 -11 1 543.53 458.87 50.61 o -1 -11 1 1061.04 861.10 80.43 o 0 -11 1 0.17 6.62 26.14 o 1 -11 1 7825.52 7918.55 151.47 o 2 -11 1 2844.83 2733.09 83.56 o 3 -11 1 774.99 814.95 60.00 o 4 -11 1 485.93 562.44 69.84 o 5 -11 1 38.65 41.78 39.20 o 6 -11 1 114.92 69.37 42.17 o 7 -11 1 215.66 222.79 46.18 o 8 -11 1 11.46 -2.19 30.08 o -8 -10 1 708.07 796.06 64.76 o -7 -10 1 426.17 404.18 58.91 o -6 -10 1 440.84 519.53 57.11 o -5 -10 1 511.20 496.59 57.96 o -4 -10 1 8.69 3.26 30.51 o -3 -10 1 481.01 461.46 51.21 o -2 -10 1 2531.78 2174.93 109.34 o -1 -10 1 1314.85 1293.03 63.10 o 0 -10 1 9296.71 9687.48 133.22 o 1 -10 1 1914.64 1992.43 64.14 o 2 -10 1 703.10 652.40 43.63 o 3 -10 1 5.58 11.39 20.22 o 4 -10 1 127.98 134.99 39.06 o 5 -10 1 1344.13 1401.90 88.92 o 6 -10 1 282.27 287.80 47.94 o 7 -10 1 241.69 349.56 50.83 o 8 -10 1 359.31 397.43 50.04 o -9 -9 1 455.27 417.06 63.23 o -8 -9 1 187.24 207.26 45.31 o -7 -9 1 47.69 90.92 35.99 o -6 -9 1 298.99 297.65 50.43 o -5 -9 1 24.43 30.76 35.39 o -4 -9 1 3018.02 2824.06 91.22 o -3 -9 1 2564.70 2384.68 76.83 o -2 -9 1 5605.72 5479.57 104.68 o -1 -9 1 6713.22 7265.47 125.24 o 0 -9 1 30.22 39.93 13.48 o 1 -9 1 186.11 182.52 18.71 o 2 -9 1 190.41 200.23 22.64 o 3 -9 1 1962.09 1854.74 67.16 o 4 -9 1 7483.67 7060.87 209.61 o 5 -9 1 225.93 209.34 44.65 o 6 -9 1 799.00 720.47 63.94 o 7 -9 1 143.42 144.81 47.75 o 8 -9 1 1.53 7.32 32.18 o 9 -9 1 15.44 -3.47 56.84 o -9 -8 1 2.50 25.04 35.59 o -8 -8 1 396.35 430.40 56.09 o -7 -8 1 533.20 572.84 68.09 o -6 -8 1 628.61 580.88 61.55 o -5 -8 1 1950.62 1830.33 79.43 o -4 -8 1 476.62 453.36 43.24 o -3 -8 1 1098.03 1065.19 57.34 o -2 -8 1 1515.13 1727.42 56.88 o -1 -8 1 1718.10 1976.06 47.05 o 0 -8 1 14454.45 15512.61 244.31 o 1 -8 1 3617.50 3943.26 58.21 o 2 -8 1 9989.85 10012.16 106.30 o 3 -8 1 1559.28 1437.09 50.71 o 4 -8 1 150.24 138.80 31.47 o 5 -8 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