#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012860.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012860_Fobs loop_ _publ_author_name 'Crozet, M. D.' 'Vanelle, P.' 'Giorgi, M.' 'Gellis, A.' _publ_section_title ; 2-[2-Methyl-5-nitro-4-(phenylsulfonylmethyl)imidazol-1-yl]ethanol and 2-methyl-5-nitro-4-phenylsulfonylmethyl-1,3-thiazole ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o496 _journal_page_last o498 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _[local]_cod_data_source_file dn1013IIsup3.hkl _[local]_cod_data_source_block II loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma 0 0 2 699.5 738.6 23.0 0 0 6 581.5 641.5 12.2 0 0 8 529.2 553.5 9.5 0 0 10 1095.1 1035.1 20.1 0 0 12 47.9 34.2 1.7 0 0 14 149.2 152.6 3.9 0 1 2 1628.1 1681.6 45.8 0 1 3 1027.6 1025.9 18.2 0 1 5 174.3 126.6 4.6 0 1 6 596.7 602.6 8.4 0 1 7 631.0 606.3 8.5 0 1 8 1085.7 1032.2 14.1 0 1 9 235.2 243.6 3.4 0 1 10 93.7 101.2 1.6 0 1 11 340.1 335.5 5.0 0 1 12 201.7 215.9 3.2 0 1 13 46.9 44.6 1.4 0 1 14 71.8 74.7 2.0 0 1 16 17.8 14.0 3.0 0 2 0 35.1 40.7 0.9 0 2 1 12.4 6.7 0.3 0 2 2 2186.6 2061.5 64.9 0 2 3 2150.0 2297.8 62.1 0 2 4 58.8 58.9 1.0 0 2 5 660.5 718.5 10.0 0 2 6 1077.5 1061.0 16.0 0 2 7 619.0 592.2 8.4 0 2 8 50.8 48.4 1.1 0 2 9 18.7 17.4 0.7 0 2 10 319.2 304.8 4.4 0 2 12 41.8 41.0 1.3 0 2 13 40.3 38.9 1.3 0 2 14 31.0 28.3 1.4 0 2 15 14.1 7.2 1.4 0 2 16 15.1 22.4 1.9 0 3 2 1006.9 1014.0 14.7 0 3 3 1755.6 1756.1 27.8 0 3 4 3.2 4.8 0.3 0 3 5 125.6 112.9 1.9 0 3 6 336.9 328.5 4.6 0 3 7 17.9 20.3 0.8 0 3 8 45.3 46.2 1.1 0 3 9 15.0 14.2 0.7 0 3 10 294.7 296.8 4.3 0 3 11 24.7 28.0 1.0 0 3 12 9.1 9.3 0.8 0 3 14 231.4 224.9 4.0 0 3 15 6.2 6.3 1.5 0 4 1 1042.8 1071.1 21.2 0 4 2 1336.4 1327.8 21.4 0 4 3 144.4 141.0 2.1 0 4 4 2296.6 2112.2 45.2 0 4 5 1079.6 1080.3 14.7 0 4 6 339.6 330.4 4.6 0 4 7 18.0 19.9 0.7 0 4 8 238.3 213.7 3.8 0 4 9 79.3 69.9 1.5 0 4 10 5.6 6.7 0.7 0 4 11 36.9 39.5 1.3 0 4 12 71.6 63.9 1.7 0 4 13 11.7 9.4 1.1 0 4 15 25.2 18.4 2.1 0 5 1 460.2 430.2 7.1 0 5 2 9.8 11.1 0.3 0 5 3 15.7 20.2 0.4 0 5 4 519.6 506.1 7.6 0 5 5 8.2 3.2 0.5 0 5 6 1.4 0.0 0.4 0 5 7 615.5 593.6 8.1 0 5 8 186.9 178.8 2.8 0 5 9 72.4 82.4 1.5 0 5 11 250.6 249.5 4.1 0 5 12 14.9 18.1 1.1 0 5 13 10.7 9.1 1.1 0 5 14 14.1 18.8 1.2 0 6 0 212.0 212.6 4.7 0 6 1 1588.0 1617.2 37.6 0 6 2 146.5 110.8 2.6 0 6 3 1654.8 1685.8 37.9 0 6 4 5.0 1.0 0.4 0 6 5 628.2 632.5 8.9 0 6 6 175.0 156.0 2.6 0 6 7 586.2 600.3 8.0 0 6 8 161.7 153.6 2.5 0 6 9 366.3 348.0 5.2 0 6 10 102.3 99.6 2.0 0 6 11 99.8 102.5 2.0 0 6 12 16.0 17.9 1.1 0 6 13 86.1 81.7 2.1 0 7 1 17.4 20.2 0.4 0 7 2 212.3 201.7 4.7 0 7 3 6.2 1.5 0.3 0 7 4 19.4 17.2 0.5 0 7 5 1.1 0.0 0.3 0 7 6 120.9 111.0 2.0 0 7 7 77.3 72.8 1.4 0 7 8 21.1 20.4 0.8 0 7 9 13.9 12.0 0.9 0 7 10 39.7 50.1 1.2 0 7 11 44.7 45.2 1.3 0 7 12 8.2 8.1 1.0 0 8 0 18.7 25.7 0.6 0 8 1 266.9 298.3 6.0 0 8 2 7.5 6.5 0.6 0 8 3 756.7 757.9 17.4 0 8 4 70.4 76.4 1.8 0 8 5 22.2 29.7 1.2 0 8 6 24.0 27.3 0.8 0 8 7 253.9 247.8 4.2 0 8 8 11.4 10.0 0.7 0 8 9 74.6 81.8 1.6 0 8 10 4.4 4.1 0.9 0 9 1 20.2 15.8 0.7 0 9 2 15.1 11.8 0.7 0 9 3 15.8 17.0 0.8 0 9 4 51.8 50.3 1.7 0 9 5 2.8 6.8 0.9 0 9 6 20.7 16.0 1.2 0 9 7 7.0 3.9 1.3 0 9 8 4.4 1.7 1.4 0 9 9 9.5 14.2 1.3 0 10 2 186.8 201.8 7.0 0 10 3 109.3 106.6 4.4 0 10 4 47.1 50.5 2.6 0 10 5 4.8 0.7 1.5 0 10 6 26.3 31.1 2.1 1 0 -15 6.1 10.5 1.7 1 0 -13 5.2 1.3 1.5 1 0 -11 839.4 792.3 16.0 1 0 -9 1429.7 1343.4 24.8 1 0 5 145.0 42.9 9.4 1 0 9 422.7 413.6 8.1 1 0 11 302.7 304.2 6.2 1 0 13 319.9 314.0 6.8 1 0 15 38.1 28.8 2.1 1 1 -16 31.9 50.0 2.3 1 1 -15 28.8 29.0 1.6 1 1 -14 122.3 112.3 2.5 1 1 -13 33.3 40.2 1.4 1 1 -12 19.1 18.4 1.0 1 1 -11 4.1 3.2 0.7 1 1 -10 37.8 40.4 1.0 1 1 -9 19.5 20.6 0.8 1 1 -8 1179.4 1087.0 17.2 1 1 -7 410.7 403.2 5.7 1 1 -6 347.5 313.4 5.6 1 1 -5 168.5 176.4 3.3 1 1 -3 142.8 129.2 2.4 1 1 -2 6.5 6.0 0.4 1 1 -1 899.2 2739.9 100.6 1 1 1 841.5 1339.0 47.8 1 1 3 2092.8 2060.8 37.1 1 1 4 1361.9 1241.6 20.6 1 1 5 2.1 0.3 0.5 1 1 7 27.9 27.2 1.0 1 1 8 868.4 851.3 10.8 1 1 9 482.6 480.8 6.3 1 1 10 263.5 243.7 3.8 1 1 11 28.0 30.2 1.0 1 1 12 478.7 479.5 6.9 1 1 13 67.3 62.9 1.8 1 1 14 30.5 30.7 1.5 1 1 15 24.1 34.7 1.5 1 1 16 92.4 105.7 6.2 1 2 -16 12.5 17.1 2.4 1 2 -14 70.8 81.6 1.8 1 2 -13 205.6 200.6 3.6 1 2 -12 10.8 4.0 0.9 1 2 -10 64.6 70.2 1.4 1 2 -9 423.0 419.6 5.5 1 2 -8 92.2 94.4 1.5 1 2 -7 36.5 36.6 0.9 1 2 -6 1543.9 1573.6 21.2 1 2 -5 81.5 89.7 1.4 1 2 -4 517.7 498.7 7.5 1 2 -3 41.7 58.2 0.8 1 2 -1 82.3 75.8 1.7 1 2 1 59.9 53.7 1.1 1 2 2 1931.0 1946.8 30.7 1 2 3 61.2 73.2 1.1 1 2 4 2265.6 2329.5 33.3 1 2 5 35.0 35.5 0.8 1 2 6 9.0 0.1 0.9 1 2 7 227.1 223.3 3.1 1 2 8 225.2 214.8 3.2 1 2 9 39.0 37.2 1.1 1 2 10 19.9 21.9 0.9 1 2 11 52.5 47.6 1.4 1 2 12 79.0 61.4 1.8 1 2 13 42.4 41.7 1.6 1 3 -15 17.5 17.9 1.5 1 3 -13 18.9 11.7 1.1 1 3 -12 4.4 0.4 0.8 1 3 -11 49.3 49.1 1.2 1 3 -10 56.8 57.6 1.3 1 3 -9 233.0 243.7 3.3 1 3 -8 103.0 95.4 1.8 1 3 -7 574.6 547.3 7.7 1 3 -6 1376.2 1376.4 18.4 1 3 -5 6.9 9.0 0.5 1 3 -4 11.8 13.6 0.6 1 3 -3 146.5 176.8 2.2 1 3 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1 5 -9 94.0 84.3 1.7 1 5 -8 37.7 41.8 0.9 1 5 -7 3.1 2.4 0.5 1 5 -6 63.4 63.5 1.2 1 5 -5 28.9 37.4 0.7 1 5 -4 880.4 880.3 12.9 1 5 -3 4.1 4.1 0.2 1 5 -2 11.5 15.7 0.7 1 5 -1 92.1 65.9 2.0 1 5 0 311.3 250.1 4.7 1 5 1 12.8 9.3 0.3 1 5 2 1122.8 1006.6 16.7 1 5 3 10.2 5.0 0.4 1 5 4 6.0 0.2 0.5 1 5 5 24.2 24.1 0.6 1 5 6 979.1 977.9 13.0 1 5 7 238.1 247.5 3.3 1 5 8 10.3 8.4 0.8 1 5 9 53.8 58.5 1.3 1 5 10 3.7 4.1 0.7 1 5 11 175.2 177.8 3.1 1 5 12 53.5 61.3 1.6 1 5 13 19.7 19.0 1.4 1 5 14 100.1 109.7 2.6 1 6 -13 105.3 116.0 2.5 1 6 -12 159.5 167.1 3.0 1 6 -11 28.5 31.1 1.2 1 6 -10 191.6 197.0 3.2 1 6 -9 70.7 66.6 1.5 1 6 -8 224.2 230.0 3.6 1 6 -7 22.5 16.9 0.7 1 6 -6 291.5 287.2 4.1 1 6 -5 237.9 241.5 3.5 1 6 -4 562.4 566.7 10.3 1 6 -3 22.0 18.4 1.0 1 6 -2 94.5 104.3 2.2 1 6 -1 619.3 590.8 12.9 1 6 0 1616.6 1544.7 32.4 1 6 1 115.8 107.8 1.9 1 6 2 88.8 100.3 1.4 1 6 3 5.1 2.3 0.4 1 6 4 814.8 806.2 11.7 1 6 5 262.1 276.0 3.9 1 6 6 30.6 25.0 0.8 1 6 7 98.5 98.6 1.8 1 6 8 52.0 51.0 1.2 1 6 9 49.3 49.5 1.3 1 6 10 2.8 0.2 0.7 1 6 12 28.1 28.6 1.4 1 7 -12 16.3 19.1 1.2 1 7 -11 32.7 35.1 1.3 1 7 -9 1.9 0.1 0.6 1 7 -8 3.3 2.8 0.5 1 7 -7 607.1 606.9 9.6 1 7 -6 61.2 62.9 1.2 1 7 -5 543.8 549.6 11.3 1 7 -4 142.4 148.6 3.1 1 7 -3 584.8 592.4 11.1 1 7 -2 25.5 23.1 1.0 1 7 -1 1354.8 1362.1 30.0 1 7 0 93.6 88.8 2.2 1 7 1 129.6 137.1 2.2 1 7 2 53.1 46.1 1.1 1 7 3 656.0 679.2 9.6 1 7 4 5.2 3.4 0.4 1 7 5 617.6 630.2 9.8 1 7 6 135.2 134.0 2.4 1 7 7 161.4 161.5 2.6 1 7 8 4.3 2.0 0.6 1 7 9 611.8 603.4 8.5 1 7 10 37.7 41.2 1.3 1 7 11 35.9 41.4 1.4 1 7 12 3.8 3.3 1.0 1 8 -10 61.3 54.0 2.0 1 8 -9 91.0 95.2 2.4 1 8 -8 89.2 98.4 2.0 1 8 -7 6.9 8.1 0.3 1 8 -6 47.2 41.6 1.6 1 8 -5 36.6 46.6 1.4 1 8 -4 5.4 7.4 0.8 1 8 -3 1.8 0.4 0.6 1 8 -2 18.0 15.6 0.8 1 8 -1 53.1 43.7 1.4 1 8 0 201.5 175.1 4.8 1 8 1 5.6 6.8 0.4 1 8 2 7.5 11.8 0.3 1 8 3 41.2 44.1 0.8 1 8 4 93.1 94.8 1.8 1 8 5 26.9 27.3 0.7 1 8 6 269.3 283.8 4.6 1 8 7 49.5 47.2 1.1 1 8 8 4.7 4.4 0.6 1 8 10 164.0 182.7 4.1 1 8 11 37.1 41.4 1.9 1 9 -9 5.1 1.8 1.4 1 9 -7 219.3 226.4 5.3 1 9 -6 33.8 34.5 1.4 1 9 -5 8.8 5.3 1.0 1 9 -3 68.5 71.5 2.0 1 9 -2 281.0 296.5 7.0 1 9 -1 176.9 153.5 4.6 1 9 0 100.4 102.6 2.8 1 9 1 31.3 33.7 0.9 1 9 2 97.1 117.2 2.4 1 9 3 139.2 136.3 3.3 1 9 4 146.0 135.6 3.4 1 9 5 115.8 121.3 2.1 1 9 6 2.6 3.7 0.6 1 9 7 5.6 5.5 0.6 1 9 8 26.0 29.7 1.0 1 9 9 119.3 122.5 3.6 1 10 -6 7.7 8.6 1.9 1 10 -5 266.4 249.7 9.6 1 10 -4 74.7 73.9 3.7 1 10 -3 9.5 9.1 1.3 1 10 -1 200.6 191.4 8.3 1 10 3 3.8 4.9 0.7 1 10 4 16.3 14.5 1.3 1 10 5 124.5 144.0 5.5 2 0 -16 12.8 12.2 1.9 2 0 -14 135.4 143.8 3.5 2 0 -12 14.9 8.5 1.5 2 0 -10 144.9 140.3 3.2 2 0 -8 19.6 18.6 1.5 2 0 -6 1640.3 1576.3 34.8 2 0 0 280.2 342.4 6.4 2 0 6 1496.2 1384.3 28.1 2 0 8 3129.8 3019.2 110.8 2 0 10 103.4 104.6 2.4 2 0 12 297.9 278.9 6.6 2 1 -16 7.7 16.7 1.7 2 1 -15 47.7 60.4 1.8 2 1 -14 88.6 90.9 2.2 2 1 -12 76.2 84.8 1.7 2 1 -11 547.3 505.7 7.8 2 1 -10 141.5 143.9 2.3 2 1 -9 119.7 124.7 1.9 2 1 -8 19.2 19.7 0.8 2 1 -7 786.4 791.4 10.9 2 1 -6 67.1 79.3 1.2 2 1 -5 491.7 519.2 7.9 2 1 -4 327.7 367.1 5.4 2 1 -3 1.1 2.5 0.2 2 1 -2 138.1 157.6 5.5 2 1 0 112.1 130.9 1.7 2 1 1 1349.1 1367.3 20.2 2 1 2 189.7 178.0 2.7 2 1 3 64.6 86.5 1.3 2 1 4 2009.4 2086.1 29.8 2 1 5 143.8 153.0 2.2 2 1 6 624.5 606.3 8.5 2 1 7 52.8 49.9 1.2 2 1 8 775.6 738.4 10.3 2 1 9 1980.1 1911.5 28.8 2 1 10 358.4 359.4 5.2 2 1 11 19.5 17.5 1.1 2 1 13 478.8 469.8 7.2 2 1 14 71.8 76.0 2.0 2 1 15 40.7 53.7 1.7 2 2 -15 23.8 24.3 1.3 2 2 -12 2.6 0.6 0.7 2 2 -11 39.4 48.8 1.2 2 2 -10 179.1 179.3 2.7 2 2 -9 119.7 100.4 2.1 2 2 -8 7.1 6.6 0.5 2 2 -7 399.0 397.8 5.8 2 2 -6 843.7 823.6 12.2 2 2 -5 1588.7 1616.1 24.0 2 2 -4 221.2 229.1 3.6 2 2 -3 119.9 126.8 2.1 2 2 -2 181.2 185.1 2.8 2 2 0 1158.0 1292.2 19.7 2 2 1 2490.5 2632.4 58.4 2 2 2 382.1 378.0 5.5 2 2 3 12.9 5.9 0.4 2 2 4 116.3 114.4 1.9 2 2 5 412.0 431.2 6.1 2 2 6 177.8 171.9 2.6 2 2 7 417.4 425.9 5.6 2 2 8 181.5 179.1 3.0 2 2 9 69.5 65.7 1.5 2 2 11 49.5 59.2 1.4 2 2 12 162.5 157.1 2.9 2 2 13 33.2 30.8 1.4 2 2 15 117.1 121.5 2.7 2 3 -15 15.1 13.6 1.3 2 3 -14 8.5 8.1 1.1 2 3 -13 139.7 152.0 2.8 2 3 -12 536.6 522.0 7.8 2 3 -11 120.7 117.4 2.2 2 3 -10 171.8 147.3 2.9 2 3 -9 366.5 369.0 5.1 2 3 -8 741.4 693.9 9.7 2 3 -7 680.7 658.2 9.2 2 3 -5 64.1 60.2 1.4 2 3 -4 90.8 69.0 1.7 2 3 -3 2568.6 2470.2 112.3 2 3 -2 4689.4 5033.8 221.5 2 3 -1 221.4 232.4 3.4 2 3 0 200.3 193.8 3.0 2 3 2 1223.1 1209.1 20.6 2 3 3 2559.8 2616.7 56.8 2 3 4 1908.5 1958.8 29.8 2 3 5 1032.3 1000.7 15.2 2 3 6 487.0 458.9 7.3 2 3 7 1148.2 1168.1 14.7 2 3 8 460.7 479.1 6.1 2 3 9 9.6 8.6 0.8 2 3 10 467.7 476.6 6.3 2 3 11 85.7 85.1 2.0 2 3 12 3.6 4.6 1.0 2 3 14 147.8 155.4 2.9 2 4 -15 37.3 38.1 2.3 2 4 -13 19.6 18.5 1.2 2 4 -12 78.0 66.5 1.9 2 4 -11 91.4 93.6 1.8 2 4 -10 12.5 10.2 0.8 2 4 -9 36.5 30.1 1.0 2 4 -8 128.6 121.7 2.1 2 4 -7 63.2 53.0 1.3 2 4 -6 298.3 288.8 4.1 2 4 -5 656.4 622.0 9.2 2 4 -4 378.2 379.8 5.8 2 4 -3 482.3 534.8 7.3 2 4 -2 2677.1 2544.7 110.5 2 4 -1 871.3 762.7 18.7 2 4 0 343.5 379.7 5.8 2 4 1 6.4 1.8 0.3 2 4 2 2772.7 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61.1 71.4 1.8 10 3 6 12.8 13.1 1.1 10 3 7 9.4 7.3 1.2 10 3 8 90.5 95.0 2.4 10 4 -8 33.6 34.6 1.5 10 4 -6 4.2 5.9 0.8 10 4 -5 24.1 26.0 1.0 10 4 -4 4.7 2.0 0.8 10 4 -3 148.6 145.3 2.6 10 4 -2 184.6 213.6 3.2 10 4 -1 2.7 0.1 0.7 10 4 0 118.9 112.9 2.2 10 4 1 63.0 65.7 1.7 10 4 2 179.6 188.1 3.3 10 4 3 101.3 98.6 2.2 10 4 4 7.0 5.7 1.1 10 4 5 13.2 10.6 1.2 10 4 6 6.3 4.7 1.1 10 4 7 63.2 71.2 2.0 10 4 8 15.6 21.7 1.3 10 5 -9 37.0 67.4 2.2 10 5 -8 143.2 161.6 2.9 10 5 -7 92.1 91.6 2.2 10 5 -6 89.7 87.3 1.9 10 5 -5 95.8 89.7 1.9 10 5 -4 239.5 245.1 3.8 10 5 -3 14.8 16.1 0.9 10 5 -2 85.7 70.7 1.9 10 5 -1 14.5 12.8 1.0 10 5 0 244.0 238.5 4.2 10 5 1 123.0 118.1 2.4 10 5 2 31.8 24.9 1.2 10 5 3 168.7 181.7 3.0 10 5 4 130.4 142.7 2.8 10 5 5 10.4 14.0 1.2 10 5 6 3.9 3.4 1.0 10 5 7 6.2 13.4 1.1 10 6 -7 6.0 6.6 1.2 10 6 -6 125.0 136.5 3.0 10 6 -5 70.6 78.7 1.9 10 6 -4 71.5 76.0 1.8 10 6 -3 3.8 3.2 0.8 10 6 -2 2.8 2.7 0.8 10 6 -1 41.1 44.1 1.2 10 6 0 47.5 35.7 1.4 10 6 1 2.7 0.3 0.9 10 6 2 55.0 52.1 1.6 10 6 3 6.1 3.5 1.0 10 6 4 29.6 30.1 1.4 10 6 5 13.9 13.2 1.3 10 7 -4 208.5 216.0 5.4 10 7 -3 27.7 37.1 1.3 10 7 -2 51.5 57.5 2.2 10 7 -1 107.0 102.5 3.0 10 7 0 277.9 276.3 5.7 10 7 1 4.0 2.9 1.1 10 7 2 209.5 222.8 4.4 10 7 3 93.7 97.5 2.9 10 7 4 78.2 78.3 6.3 11 0 -9 24.9 38.3 2.0 11 0 -5 823.4 789.7 15.7 11 0 -3 36.1 43.9 1.9 11 0 -1 1015.6 971.6 18.5 11 0 1 594.1 600.0 11.9 11 0 3 100.5 104.9 3.0 11 0 5 927.5 930.0 20.4 11 0 7 37.8 52.0 2.6 11 1 -10 17.2 23.4 1.5 11 1 -9 67.0 83.3 2.1 11 1 -8 191.1 196.8 4.0 11 1 -7 97.0 99.2 2.6 11 1 -6 18.3 21.0 1.2 11 1 -5 19.7 17.7 1.2 11 1 -4 663.7 661.9 9.0 11 1 -3 3.9 0.4 0.8 11 1 -2 56.3 53.2 1.6 11 1 -1 34.9 34.6 1.4 11 1 0 74.2 80.6 1.8 11 1 1 119.7 125.7 2.3 11 1 3 38.1 41.5 1.4 11 1 4 177.0 172.9 3.3 11 1 5 6.8 8.9 1.0 11 1 6 29.6 32.6 1.5 11 1 8 45.7 53.6 1.8 11 2 -10 31.6 36.6 2.0 11 2 -9 10.2 12.4 1.1 11 2 -8 119.2 111.9 2.9 11 2 -7 52.6 64.1 1.8 11 2 -6 166.3 150.7 3.1 11 2 -5 204.4 199.8 3.4 11 2 -4 89.7 84.5 2.1 11 2 -3 14.5 16.4 1.0 11 2 -2 74.4 89.1 1.8 11 2 -1 283.1 299.5 4.5 11 2 0 3.0 0.6 0.9 11 2 1 69.0 72.4 1.7 11 2 2 337.8 333.3 5.5 11 2 3 78.5 87.2 2.0 11 2 4 12.2 9.8 1.2 11 2 5 189.7 193.6 3.5 11 2 7 18.5 25.9 1.7 11 3 -9 192.2 190.9 3.9 11 3 -7 62.9 65.2 1.8 11 3 -6 111.0 118.7 2.2 11 3 -5 187.3 171.9 3.2 11 3 -4 8.8 12.6 0.8 11 3 -3 11.8 11.3 1.0 11 3 -2 18.7 23.7 1.0 11 3 -1 4.2 4.4 0.9 11 3 0 16.3 15.1 1.0 11 3 1 309.2 301.1 4.9 11 3 2 12.5 12.9 1.0 11 3 3 90.4 98.6 2.2 11 3 4 88.5 92.1 2.3 11 3 5 31.2 30.6 1.6 11 3 6 17.8 19.4 1.3 11 3 8 8.5 12.0 2.4 11 4 -7 23.7 34.6 1.2 11 4 -6 277.5 272.8 4.9 11 4 -5 58.9 55.7 1.8 11 4 -4 17.7 16.9 1.0 11 4 -3 16.5 17.6 1.0 11 4 -2 75.0 74.3 1.7 11 4 -1 66.2 63.8 1.7 11 4 0 206.4 207.2 3.6 11 4 1 7.2 8.4 1.1 11 4 2 5.2 3.8 1.0 11 4 3 23.8 19.9 1.4 11 4 4 169.7 179.3 3.4 11 4 5 43.2 50.7 1.8 11 4 6 17.6 24.3 1.3 11 4 7 5.6 4.5 1.7 11 5 -7 90.9 117.1 3.0 11 5 -6 96.5 95.4 2.2 11 5 -5 222.8 225.0 4.0 11 5 -4 91.3 91.5 2.2 11 5 -3 94.6 93.6 2.2 11 5 -2 212.8 204.3 3.9 11 5 -1 87.8 91.7 2.0 11 5 0 26.9 21.8 1.2 11 5 1 38.6 34.0 1.5 11 5 2 18.8 20.3 1.2 11 5 3 4.4 7.8 1.0 11 5 4 80.8 89.3 2.2 11 5 5 13.7 13.7 1.2 11 6 -5 50.3 49.6 2.1 11 6 -4 63.9 74.8 2.2 11 6 -3 156.9 153.3 3.6 11 6 -2 140.8 140.1 3.0 11 6 -1 51.5 51.4 1.6 11 6 0 71.2 86.8 1.8 11 6 1 20.5 24.6 1.2 11 6 2 202.8 209.0 3.9 11 6 3 31.0 33.9 1.4 12 0 -8 239.1 215.9 7.5 12 0 -6 6.7 2.3 1.6 12 0 -4 32.5 21.5 1.9 12 0 -2 93.6 89.1 3.4 12 0 0 8.6 6.1 1.5 12 0 2 441.5 414.8 10.0 12 0 4 8.6 9.7 1.7 12 0 6 34.1 37.7 2.5 12 1 -9 5.2 15.9 0.9 12 1 -8 4.0 8.3 1.0 12 1 -7 61.6 63.8 2.0 12 1 -6 31.7 37.3 1.4 12 1 -5 8.1 10.8 1.0 12 1 -4 72.7 77.5 2.0 12 1 -3 3.5 6.2 0.9 12 1 -1 45.5 43.1 1.5 12 1 0 88.3 96.5 2.1 12 1 1 146.4 146.5 3.0 12 1 2 57.2 52.9 1.7 12 1 3 15.4 15.5 1.4 12 1 4 6.2 3.1 1.1 12 1 5 51.1 59.0 1.9 12 1 6 26.2 30.7 1.5 12 1 7 67.9 86.2 4.3 12 2 -8 299.3 300.4 7.0 12 2 -7 32.7 38.4 1.6 12 2 -6 64.8 63.0 1.9 12 2 -5 14.2 6.6 1.3 12 2 -4 285.7 272.0 4.9 12 2 -3 324.0 313.5 5.7 12 2 -2 209.2 190.1 3.8 12 2 -1 23.1 16.8 1.4 12 2 0 56.1 53.8 1.8 12 2 1 60.3 54.1 2.0 12 2 2 158.4 154.5 3.2 12 2 3 25.8 18.9 1.5 12 2 4 11.7 11.0 1.1 12 2 5 47.9 56.5 2.1 12 2 6 8.6 6.1 1.5 12 3 -6 52.3 59.8 1.9 12 3 -5 12.3 19.0 1.1 12 3 -4 174.0 183.0 3.2 12 3 -2 168.7 168.1 3.1 12 3 -1 7.8 11.8 1.2 12 3 0 141.6 139.5 3.0 12 3 1 7.0 9.9 1.1 12 3 2 10.7 11.8 1.2 12 3 4 33.0 38.6 1.6 12 3 5 20.1 19.0 1.9 12 3 6 11.8 13.2 1.8 12 4 -6 125.7 129.5 3.7 12 4 -5 63.3 66.7 2.0 12 4 -4 43.2 47.1 1.5 12 4 -3 518.2 496.4 8.5 12 4 -2 38.8 39.1 1.7 12 4 -1 26.4 27.6 1.4 12 4 0 67.6 69.6 1.8 12 4 1 271.8 258.5 4.9 12 4 2 7.6 3.9 1.1 12 4 3 78.0 91.6 2.4 12 4 4 6.2 3.3 1.4 12 5 -2 8.2 5.6 1.2 12 5 -1 36.8 35.0 1.5 12 5 0 5.0 2.0 1.1 12 5 1 78.0 79.1 2.1 13 0 -5 350.9 335.2 9.4 13 0 -3 18.6 17.2 2.0 13 0 -1 189.6 170.5 5.2 13 0 1 24.3 27.9 1.9 13 0 3 17.1 18.4 2.3 13 1 -6 166.8 201.0 4.0 13 1 -5 7.3 4.4 1.3 13 1 -3 6.1 4.6 1.1 13 1 -2 278.4 272.3 5.3 13 1 0 6.7 4.4 1.1 13 1 1 4.3 4.0 1.1 13 1 2 15.6 17.3 1.3 13 1 3 17.2 18.5 1.3 13 1 4 79.6 91.5 2.9 13 2 -6 205.8 215.3 5.6 13 2 -5 85.5 81.9 2.5 13 2 -3 10.3 12.9 1.2 13 2 -2 37.5 46.6 1.6 13 2 -1 76.9 70.2 2.1 13 2 0 90.1 98.2 2.5 13 2 1 51.9 47.7 2.0 13 2 2 6.9 2.8 1.2 13 2 4 25.9 32.8 2.2 13 3 -4 62.2 58.9 2.7 13 3 -3 60.8 69.9 2.2 13 3 -2 88.6 92.6 2.6 13 3 -1 72.2 67.8 2.3 13 3 0 101.9 102.5 2.8 13 3 1 8.5 7.3 1.5 13 3 2 50.5 62.9 2.6 13 3 3 203.8 216.3 6.7