#------------------------------------------------------------------------------
#$Date: 2016-04-02 21:34:15 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180790 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/21/2012187.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2012187_Fobs
loop_
_publ_author_name
'Dean, Philip A. W.'
'Dance, Ian G.'
'Craig, Donald C.'
'Scudder, Marcia L.'
_publ_section_title
;
 Bis(tetraphenylphosphonium)
 tris(oxalato-<i>O</i>,<i>O</i>')germanate(IV)
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1030
_journal_page_last               1031
_journal_volume                  57
_journal_year                    2001
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cod_data_source_file            da1190Isup2.hkl
_cod_data_source_block           I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_meas
_refln_F_calc
_refln_F_sigma
2 0 0 129.782 134.682 1.856
4 0 0 32.890 -33.462 0.786
6 0 0 73.167 81.784 1.298
8 0 0 139.028 141.357 2.046
10 0 0 83.535 -78.865 1.309
12 0 0 59.662 64.298 1.856
14 0 0 7.077 6.699 0.583
16 0 0 25.034 24.073 2.341
18 0 0 89.150 90.628 1.411
20 0 0 14.474 -13.607 0.674
22 0 0 8.821 8.537 0.769
24 0 0 32.967 34.253 1.052
26 0 0 25.069 24.600 1.451
-26 0 2 45.100 -46.900 1.024
-24 0 2 7.579 9.462 1.041
-22 0 2 20.553 -19.603 0.744
-20 0 2 14.023 -13.548 0.813
-18 0 2 67.517 -71.923 1.513
-16 0 2 32.103 31.627 0.791
-14 0 2 75.910 -79.137 1.691
-12 0 2 3.686 -6.248 3.126
-10 0 2 47.903 46.426 1.072
-8 0 2 103.844 -113.671 2.196
-6 0 2 147.352 -152.307 3.011
-4 0 2 74.382 75.561 1.575
-2 0 2 274.717 -273.709 5.752
0 0 2 408.704 -414.863 8.391
2 0 2 34.065 34.407 0.773
4 0 2 255.804 -260.059 5.543
6 0 2 286.963 -292.564 5.784
8 0 2 119.212 -121.354 2.513
10 0 2 143.279 -150.611 3.005
12 0 2 206.324 -206.010 4.253
14 0 2 4.486 -7.576 4.487
16 0 2 51.197 -51.718 1.139
18 0 2 32.460 -33.174 0.838
20 0 2 42.023 44.823 1.014
22 0 2 7.729 -6.904 0.972
24 0 2 54.592 -55.489 1.228
26 0 2 17.529 -18.122 0.612
-26 0 4 12.686 10.898 0.830
-24 0 4 17.890 -15.998 0.882
-22 0 4 69.466 71.343 1.553
-20 0 4 111.753 112.294 2.506
-18 0 4 4.197 7.993 6.469
-16 0 4 2.263 -1.937 3.542
-14 0 4 99.964 99.882 2.227
-12 0 4 27.932 -30.114 0.718
-10 0 4 31.762 -29.372 0.744
-8 0 4 43.930 -35.183 0.980
-6 0 4 14.198 12.653 0.481
-4 0 4 76.609 75.941 1.671
-2 0 4 175.054 179.665 3.580
0 0 4 125.093 -119.656 2.611
2 0 4 286.521 290.246 5.789
4 0 4 77.790 81.248 1.726
6 0 4 115.212 122.156 2.496
8 0 4 157.294 159.788 3.324
10 0 4 255.069 254.010 5.243
12 0 4 88.462 88.565 1.974
14 0 4 0.000 2.824 13.918
16 0 4 79.144 78.277 1.758
18 0 4 58.032 56.899 1.334
20 0 4 4.719 6.688 2.165
22 0 4 24.630 26.161 0.855
24 0 4 25.512 23.720 0.791
-26 0 6 17.596 -17.568 0.801
-24 0 6 13.275 -14.134 0.976
-22 0 6 59.418 -59.946 1.349
-20 0 6 117.245 -118.966 2.610
-18 0 6 38.012 38.603 0.977
-16 0 6 97.244 -100.606 2.162
-14 0 6 23.394 -22.372 0.719
-12 0 6 31.489 26.453 0.791
-10 0 6 58.476 -59.897 1.307
-8 0 6 119.193 -112.836 2.596
-6 0 6 4.664 -6.807 3.299
-4 0 6 45.803 -47.903 1.029
-2 0 6 238.852 227.093 4.871
0 0 6 112.607 107.483 2.443
2 0 6 203.540 -200.896 4.190
4 0 6 232.500 -230.667 4.770
6 0 6 71.165 -73.598 1.585
8 0 6 139.561 -142.544 3.059
10 0 6 129.401 -130.679 2.840
12 0 6 46.394 -49.709 1.091
14 0 6 32.761 -33.016 0.919
16 0 6 18.117 -16.823 0.881
18 0 6 40.849 -42.572 1.062
20 0 6 41.470 -41.012 1.039
22 0 6 47.615 -49.158 1.113
-26 0 8 5.000 3.287 1.279
-24 0 8 6.774 7.292 1.205
-22 0 8 69.415 70.235 1.547
-20 0 8 42.629 41.638 1.081
-18 0 8 20.161 -21.093 0.822
-16 0 8 108.801 113.479 2.428
-14 0 8 73.086 71.534 1.630
-12 0 8 65.812 66.619 1.478
-10 0 8 80.692 81.388 1.810
-8 0 8 100.119 96.049 2.247
-6 0 8 25.098 -20.054 0.676
-4 0 8 42.672 44.918 0.964
-2 0 8 69.630 -65.821 1.562
0 0 8 0.821 -7.312 6.602
2 0 8 86.146 93.039 1.956
4 0 8 69.239 73.470 1.569
6 0 8 37.769 36.777 0.910
8 0 8 75.948 75.691 1.681
10 0 8 74.556 74.917 1.653
12 0 8 14.187 13.375 0.941
14 0 8 47.606 47.396 1.163
16 0 8 56.647 56.067 1.305
18 0 8 40.782 42.364 1.047
20 0 8 27.658 28.058 0.844
-26 0 10 4.780 -2.208 1.506
-24 0 10 5.126 -4.534 1.660
-22 0 10 25.305 -24.304 0.877
-20 0 10 12.333 14.693 1.005
-18 0 10 46.541 -44.509 1.144
-16 0 10 72.248 -72.899 1.620
-14 0 10 50.320 -50.878 1.175
-12 0 10 112.898 -111.969 2.494
-10 0 10 144.442 -144.680 3.224
-8 0 10 66.002 -64.350 1.485
-6 0 10 0.000 -3.902 14.029
-4 0 10 94.187 -88.025 2.085
-2 0 10 14.285 -14.309 0.790
0 0 10 13.732 -11.601 0.777
2 0 10 60.215 -63.297 1.350
4 0 10 6.968 8.657 1.385
6 0 10 3.041 4.037 9.248
8 0 10 4.965 -7.803 2.085
10 0 10 59.181 -62.095 1.357
12 0 10 30.534 -28.247 0.963
14 0 10 81.362 -80.456 1.790
16 0 10 43.556 -44.891 1.089
18 0 10 2.471 1.228 6.177
-24 0 12 12.839 11.886 0.826
-22 0 12 0.000 -2.784 14.207
-20 0 12 19.198 21.027 0.869
-18 0 12 46.586 46.947 1.148
-16 0 12 35.660 36.686 1.006
-14 0 12 29.861 28.466 0.931
-12 0 12 128.327 127.063 2.863
-10 0 12 26.290 25.831 0.882
-8 0 12 17.252 -17.448 0.866
-6 0 12 90.201 85.963 2.024
-4 0 12 115.152 111.703 2.557
-2 0 12 22.811 22.787 0.835
0 0 12 37.683 36.877 0.990
2 0 12 91.958 97.117 2.072
4 0 12 17.961 -15.866 0.891
6 0 12 17.271 -20.342 0.906
8 0 12 23.795 18.872 0.902
10 0 12 36.228 35.897 1.015
12 0 12 35.780 36.227 0.993
14 0 12 55.402 54.258 1.271
16 0 12 6.670 -4.727 1.149
-22 0 14 12.437 13.141 0.773
-20 0 14 33.042 -33.364 0.906
-18 0 14 50.310 -49.007 1.194
-16 0 14 6.214 -10.258 4.112
-14 0 14 7.021 8.336 1.604
-12 0 14 49.778 -50.038 1.202
-10 0 14 14.648 -12.637 0.962
-8 0 14 33.869 -31.855 0.990
-6 0 14 81.147 -78.283 1.835
-4 0 14 63.889 -63.910 1.444
-2 0 14 42.514 -41.637 1.097
0 0 14 67.078 -67.939 1.513
2 0 14 47.045 -50.580 1.171
4 0 14 19.861 20.548 0.938
6 0 14 36.034 -34.453 1.016
8 0 14 28.074 -25.369 0.910
10 0 14 0.000 4.497 14.887
12 0 14 34.278 -34.411 0.933
-20 0 16 32.436 31.401 0.863
-18 0 16 26.427 24.605 0.825
-16 0 16 28.037 -29.779 0.873
-14 0 16 5.822 2.806 3.853
-12 0 16 42.517 40.717 1.087
-10 0 16 59.814 59.368 1.372
-8 0 16 52.042 49.223 1.242
-6 0 16 46.828 49.176 1.163
-4 0 16 26.945 29.388 0.976
-2 0 16 28.889 27.749 0.963
0 0 16 46.658 46.728 1.155
2 0 16 20.178 -20.398 0.849
4 0 16 23.392 19.690 0.853
6 0 16 55.663 54.386 1.271
8 0 16 19.430 19.239 0.752
1 1 0 81.148 83.652 1.763
3 1 0 113.624 118.972 1.639
5 1 0 182.454 -187.279 2.812
7 1 0 21.033 -18.808 0.819
9 1 0 29.313 29.677 0.468
11 1 0 16.460 -15.817 0.432
13 1 0 5.630 6.166 0.787
15 1 0 13.454 13.173 0.863
17 1 0 31.391 31.580 0.570
19 1 0 32.292 31.638 0.597
21 1 0 27.684 27.206 0.565
23 1 0 0.000 5.412 4.183
25 1 0 16.529 17.594 0.496
-27 1 1 16.402 -15.990 0.594
-25 1 1 10.499 12.197 0.829
-23 1 1 27.532 -26.915 0.786
-21 1 1 49.054 -48.838 1.125
-19 1 1 0.000 1.313 11.690
-17 1 1 32.552 -34.033 0.809
-15 1 1 37.770 -39.587 0.864
-13 1 1 19.506 18.120 0.565
-11 1 1 75.779 -76.602 1.701
-9 1 1 28.543 -34.556 0.642
-7 1 1 53.054 -55.326 1.181
-5 1 1 229.225 -239.307 4.621
-3 1 1 294.224 -302.785 6.133
-1 1 1 14.826 -14.620 0.338
1 1 1 201.041 -205.338 4.274
3 1 1 194.106 -201.235 3.915
5 1 1 198.954 -204.871 4.026
7 1 1 63.981 -67.721 1.422
9 1 1 140.822 -149.074 2.933
11 1 1 110.297 -109.314 2.394
13 1 1 48.266 -48.889 1.079
15 1 1 43.480 -46.995 0.980
17 1 1 0.000 -4.408 11.750
19 1 1 17.936 -17.428 0.731
21 1 1 28.666 -27.429 0.795
23 1 1 18.363 -17.290 0.735
25 1 1 11.719 12.546 0.731
-27 1 2 15.594 -14.760 0.594
-25 1 2 3.765 -6.881 1.692
-23 1 2 5.853 -5.673 1.174
-21 1 2 31.269 -31.909 0.850
-19 1 2 54.761 -56.518 1.237
-17 1 2 4.642 6.715 1.485
-15 1 2 59.241 -63.623 1.327
-13 1 2 21.946 -24.704 0.590
-11 1 2 17.274 15.876 0.504
-9 1 2 17.866 -18.284 0.469
-7 1 2 125.899 -125.390 2.607
-5 1 2 91.201 -92.784 1.913
-3 1 2 86.920 -88.439 1.808
-1 1 2 28.153 -27.334 0.624
1 1 2 66.337 -68.309 1.412
3 1 2 87.675 89.353 1.840
5 1 2 142.156 142.278 2.917
7 1 2 67.902 66.603 1.508
9 1 2 98.049 -99.261 2.140
11 1 2 28.332 28.445 0.679
13 1 2 2.148 -2.599 5.980
15 1 2 10.918 -12.040 0.733
17 1 2 24.413 -23.474 0.733
19 1 2 18.518 18.427 0.756
21 1 2 20.534 -19.567 0.740
23 1 2 20.177 -19.704 0.709
25 1 2 17.616 -16.263 0.651
-27 1 3 5.621 5.643 0.866
-25 1 3 14.002 14.609 0.709
-23 1 3 36.020 37.279 0.914
-21 1 3 50.417 51.233 1.144
-19 1 3 9.182 -9.267 0.800
-17 1 3 124.114 126.751 2.704
-15 1 3 0.000 -1.954 11.703
-13 1 3 76.687 -74.293 1.720
-11 1 3 33.033 36.735 0.744
-9 1 3 31.423 32.486 0.700
-7 1 3 115.056 -112.062 2.405
-5 1 3 8.269 7.773 0.430
-3 1 3 313.471 309.240 6.621
-1 1 3 119.766 117.351 2.458
1 1 3 424.101 409.005 8.779
3 1 3 26.276 29.610 0.598
5 1 3 163.451 161.777 3.346
7 1 3 195.337 198.251 3.990
9 1 3 160.523 164.645 3.338
11 1 3 6.526 8.425 0.833
13 1 3 79.743 79.470 1.762
15 1 3 53.907 55.659 1.193
17 1 3 0.000 -0.611 11.837
19 1 3 20.955 19.530 0.741
21 1 3 45.740 46.668 1.066
23 1 3 17.200 16.723 0.700
25 1 3 0.000 1.133 12.147
-27 1 4 0.000 -5.211 13.934
-25 1 4 11.931 -12.744 0.940
-23 1 4 21.549 20.432 0.854
-21 1 4 40.353 39.805 1.056
-19 1 4 42.390 42.051 1.041
-17 1 4 39.344 38.981 0.972
-15 1 4 60.075 60.775 1.348
-13 1 4 60.569 60.388 1.374
-11 1 4 15.032 15.859 0.571
-9 1 4 38.448 37.924 0.857
-7 1 4 12.363 -10.218 0.483
-5 1 4 62.342 60.373 1.393
-3 1 4 83.895 -76.897 1.842
-1 1 4 231.478 228.594 4.693
1 1 4 8.691 -6.890 0.563
3 1 4 21.260 23.255 0.537
5 1 4 20.273 -17.829 0.543
7 1 4 78.204 77.697 1.757
9 1 4 78.858 80.030 1.774
11 1 4 2.498 4.514 7.597
13 1 4 29.358 -28.247 0.829
15 1 4 5.286 3.871 1.616
17 1 4 23.909 -24.850 0.897
19 1 4 13.336 -10.385 0.859
21 1 4 18.388 17.236 0.830
23 1 4 17.770 18.977 0.824
-27 1 5 10.976 -11.611 0.750
-25 1 5 23.186 -22.893 0.805
-23 1 5 21.145 -20.586 0.856
-21 1 5 37.225 -34.946 0.994
-19 1 5 22.318 -21.590 0.844
-17 1 5 103.336 -104.083 2.285
-15 1 5 44.415 42.578 1.021
-13 1 5 39.171 -39.553 0.915
-11 1 5 117.241 -116.054 2.599
-9 1 5 43.585 -39.328 0.973
-7 1 5 84.791 76.138 1.880
-5 1 5 152.829 -149.150 3.181
-3 1 5 49.015 44.557 1.103
-1 1 5 59.601 58.884 1.339
1 1 5 199.738 -201.487 4.091
3 1 5 26.450 22.106 0.635
5 1 5 100.674 -98.536 2.249
7 1 5 213.281 -211.449 4.409
9 1 5 138.447 -141.034 3.029
11 1 5 21.900 -22.864 0.703
13 1 5 137.409 -135.659 3.032
15 1 5 50.792 -51.171 1.194
17 1 5 10.811 9.146 1.133
19 1 5 22.259 -20.806 0.882
21 1 5 25.409 -24.240 0.850
23 1 5 13.992 -14.858 0.842
-27 1 6 7.221 5.122 0.932
-25 1 6 4.599 -5.758 5.143
-23 1 6 33.702 -34.176 0.955
-21 1 6 7.925 -6.233 1.290
-19 1 6 31.880 -32.383 0.914
-17 1 6 46.113 -45.614 1.092
-15 1 6 20.558 20.572 0.723
-13 1 6 49.573 -50.673 1.120
-11 1 6 72.493 -72.222 1.622
-9 1 6 24.583 -25.652 0.663
-7 1 6 70.996 -67.638 1.592
-5 1 6 43.688 -42.780 0.961
-3 1 6 16.949 -16.204 0.515
-1 1 6 22.240 18.857 0.580
1 1 6 60.586 -63.220 1.349
3 1 6 41.855 -43.442 0.941
5 1 6 71.498 -69.057 1.602
7 1 6 63.840 -63.114 1.414
9 1 6 19.456 -19.004 0.706
11 1 6 59.221 -59.203 1.327
13 1 6 9.677 -10.894 1.210
15 1 6 8.071 -7.110 1.212
17 1 6 25.597 26.547 0.923
19 1 6 4.280 -2.060 4.786
21 1 6 5.365 -7.906 4.243
23 1 6 3.040 -1.378 2.286
-27 1 7 0.000 -0.472 13.892
-25 1 7 30.639 31.025 0.864
-23 1 7 21.416 21.141 0.862
-21 1 7 22.712 21.490 0.854
-19 1 7 56.665 56.022 1.287
-17 1 7 49.202 49.762 1.143
-15 1 7 14.563 14.996 0.839
-13 1 7 143.462 141.520 3.161
-11 1 7 90.391 89.299 2.002
-9 1 7 22.059 -20.612 0.648
-7 1 7 8.392 14.535 0.721
-5 1 7 69.025 66.963 1.544
-3 1 7 66.397 -64.163 1.492
-1 1 7 99.647 95.822 2.188
1 1 7 62.982 68.151 1.404
3 1 7 62.356 -56.564 1.390
5 1 7 58.630 60.835 1.318
7 1 7 131.070 130.751 2.849
9 1 7 23.471 21.818 0.770
11 1 7 23.130 22.656 0.801
13 1 7 113.723 115.214 2.547
15 1 7 45.973 45.436 1.140
17 1 7 39.013 37.459 1.026
19 1 7 50.149 51.845 1.185
21 1 7 6.397 5.277 1.332
-27 1 8 4.044 2.389 3.198
-25 1 8 13.814 14.275 0.810
-23 1 8 6.484 5.634 3.838
-21 1 8 3.595 0.465 2.322
-19 1 8 29.598 30.841 0.917
-17 1 8 4.893 -5.779 2.026
-15 1 8 10.168 -9.532 0.990
-13 1 8 71.413 70.934 1.609
-11 1 8 97.474 92.262 2.157
-9 1 8 25.758 -23.759 0.709
-7 1 8 81.474 78.465 1.834
-5 1 8 20.254 19.740 0.637
-3 1 8 13.028 11.204 0.628
-1 1 8 9.768 9.665 0.713
1 1 8 124.831 123.004 2.757
3 1 8 51.680 51.516 1.175
5 1 8 59.327 61.483 1.325
7 1 8 0.000 2.194 14.170
9 1 8 4.108 5.520 7.263
11 1 8 19.988 18.619 0.826
13 1 8 20.106 20.909 0.886
15 1 8 0.000 5.826 14.270
17 1 8 17.735 16.858 0.885
19 1 8 20.333 19.652 0.794
21 1 8 4.435 1.823 1.571
-25 1 9 36.907 -37.021 0.937
-23 1 9 7.407 9.167 1.277
-21 1 9 16.707 -17.471 0.876
-19 1 9 78.373 -78.611 1.733
-17 1 9 4.388 -3.555 4.106
-15 1 9 29.014 -30.054 0.865
-13 1 9 114.556 -113.301 2.556
-11 1 9 57.640 -57.876 1.285
-9 1 9 67.824 -63.136 1.517
-7 1 9 112.886 -108.585 2.512
-5 1 9 17.063 16.476 0.667
-3 1 9 35.777 33.054 0.854
-1 1 9 9.606 -10.398 0.733
1 1 9 67.594 -67.175 1.511
3 1 9 55.982 -51.783 1.257
5 1 9 95.283 -95.166 2.116
7 1 9 6.504 4.589 3.505
9 1 9 0.000 -0.953 14.307
11 1 9 94.157 -95.323 2.112
13 1 9 56.179 -56.128 1.302
15 1 9 17.215 15.441 0.934
17 1 9 40.604 -37.864 1.036
19 1 9 43.144 -45.178 1.048
-25 1 10 9.806 -9.492 0.864
-23 1 10 12.732 12.254 0.851
-21 1 10 20.385 -21.711 0.932
-19 1 10 9.201 -8.351 1.227
-17 1 10 0.000 2.793 14.185
-15 1 10 18.155 -20.562 0.857
-13 1 10 50.775 -49.815 1.173
-11 1 10 25.358 -27.208 0.816
-9 1 10 43.289 -43.000 1.011
-7 1 10 55.869 -54.168 1.252
-5 1 10 14.058 -14.744 0.772
-3 1 10 27.588 26.795 0.775
-1 1 10 35.159 -36.002 0.875
1 1 10 22.175 -23.247 0.736
3 1 10 58.756 -59.032 1.330
5 1 10 5.130 2.187 1.732
7 1 10 0.000 -5.784 14.435
9 1 10 22.603 -18.934 0.865
11 1 10 32.246 -31.919 0.968
13 1 10 34.940 -34.984 0.995
15 1 10 0.000 -5.819 14.579
17 1 10 21.143 -22.282 0.822
19 1 10 4.138 -4.793 1.760
-25 1 11 30.496 29.324 0.830
-23 1 11 12.840 -10.237 0.766
-21 1 11 30.522 29.184 0.914
-19 1 11 37.863 36.547 1.020
-17 1 11 18.589 16.871 0.927
-15 1 11 91.751 89.831 2.045
-13 1 11 42.002 39.357 1.039
-11 1 11 18.684 -17.991 0.830
-9 1 11 79.719 75.460 1.801
-7 1 11 109.983 107.334 2.481
-5 1 11 7.409 -5.585 1.307
-3 1 11 58.262 56.110 1.288
-1 1 11 78.769 79.033 1.743
1 1 11 32.733 32.524 0.891
3 1 11 16.869 17.675 0.888
5 1 11 44.963 47.957 1.105
7 1 11 3.231 -5.806 10.593
9 1 11 16.834 14.349 0.908
11 1 11 42.091 40.605 1.096
13 1 11 1.230 1.145 7.558
15 1 11 23.503 23.860 0.851
17 1 11 59.367 60.312 1.336
-25 1 12 5.545 -7.218 1.197
-23 1 12 0.000 -4.349 14.093
-21 1 12 10.136 11.882 1.006
-19 1 12 5.329 9.094 5.104
-17 1 12 22.415 22.636 0.890
-15 1 12 35.177 35.866 0.995
-13 1 12 21.147 21.404 0.856
-11 1 12 12.831 14.245 1.088
-9 1 12 55.411 53.062 1.262
-7 1 12 6.133 -6.534 5.201
-5 1 12 16.097 14.947 0.846
-3 1 12 11.945 9.591 0.988
-1 1 12 13.573 11.816 0.910
1 1 12 25.027 24.574 0.852
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