#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/83/2008302.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008302_Fobs loop_ _publ_author_name 'Low, J. N.' 'L\'opez, M. D.' 'Quijano, M. L.' 'S\'anchez, A.' 'Nogueras, M.' _publ_section_title ; (3R,4S,4aR,10aS)-5,10-Diacetyl-3,4,4a,5,6,7,10,10a-octahydro-8-methoxy-6-oxo-2H-pyrano[3,2-g]pteridin-3,4-diyl diacetate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 452 _journal_page_last 454 _journal_volume 55 _journal_year 1999 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.9410 _cell_length_b 17.4810 _cell_length_c 14.5110 _exptl_crystal_F_000 920.00 _reflns_d_resolution_high 0.8382 _[local]_cod_data_source_file sk1253sup2.hkl _[local]_cod_data_source_block sp49 #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 172.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14473.68 13929.18 193.40 o 4 0 0 2860.14 2561.87 127.14 o 6 0 0 84.33 112.53 29.10 o 8 0 0 146.70 177.25 62.12 o 1 1 0 10911.91 10510.42 372.55 o 2 1 0 13140.66 14665.14 603.85 o 3 1 0 1418.96 1259.97 53.92 o 4 1 0 210.66 211.65 29.21 o 5 1 0 597.04 653.88 42.96 o 6 1 0 103.98 107.56 27.24 o 7 1 0 534.01 492.25 49.08 o 8 1 0 187.32 176.95 45.52 o 0 2 0 3257.16 2761.61 176.46 o 1 2 0 8789.40 8618.21 864.52 o 2 2 0 15943.52 16031.98 226.95 o 3 2 0 1.11 129.55 60.05 o 4 2 0 1324.72 1609.60 158.19 o 5 2 0 480.33 478.59 45.92 o 6 2 0 41.79 55.55 22.24 o 7 2 0 284.11 303.73 52.16 o 8 2 0 48.44 31.77 26.88 o 1 3 0 1905.00 1737.70 523.89 o 2 3 0 92.79 102.41 15.65 o 3 3 0 656.54 645.50 40.55 o 4 3 0 2620.47 3259.57 524.25 o 5 3 0 0.51 14.61 22.73 o 6 3 0 627.55 615.23 58.71 o 7 3 0 1016.44 1021.85 82.52 o 8 3 0 88.09 77.23 29.95 o 0 4 0 1465.34 1596.36 46.28 o 1 4 0 29689.41 27213.66 1628.13 o 2 4 0 2023.57 1694.08 169.07 o 3 4 0 271.87 346.70 31.80 o 4 4 0 108.40 100.63 21.14 o 5 4 0 1269.00 1315.60 73.73 o 7 4 0 348.45 363.23 54.83 o 8 4 0 0.00 14.70 40.38 o 1 5 0 1043.05 975.14 36.71 o 2 5 0 4774.63 3057.75 93.70 o 3 5 0 4966.26 4708.77 1305.27 o 4 5 0 544.48 458.53 41.07 o 5 5 0 0.80 16.98 29.61 o 6 5 0 42.47 34.34 21.51 o 7 5 0 271.02 330.25 51.14 o 8 5 0 36.65 39.28 26.74 o 0 6 0 3806.14 3893.32 180.59 o 1 6 0 1655.91 1777.53 45.48 o 2 6 0 21.36 16.94 7.76 o 3 6 0 31.56 16.98 16.77 o 4 6 0 328.36 326.07 36.96 o 5 6 0 110.14 123.93 29.04 o 6 6 0 66.92 77.25 28.06 o 7 6 0 58.01 36.50 23.04 o 8 6 0 0.15 10.97 29.82 o 1 7 0 2256.93 2495.37 134.55 o 2 7 0 1428.77 1369.40 46.61 o 3 7 0 266.23 276.50 30.36 o 4 7 0 68.85 65.90 20.49 o 5 7 0 24.36 44.68 20.88 o 6 7 0 3.95 22.78 37.89 o 7 7 0 224.76 236.44 45.65 o 8 7 0 8.46 15.32 29.61 o 0 8 0 66.55 55.68 10.30 o 1 8 0 286.40 297.52 21.83 o 2 8 0 130.02 137.24 17.05 o 3 8 0 57.02 60.48 14.17 o 4 8 0 13.48 15.13 17.11 o 5 8 0 202.58 218.91 36.53 o 6 8 0 206.29 202.81 41.36 o 7 8 0 211.59 175.24 40.60 o 8 8 0 34.91 29.82 39.96 o 1 9 0 71.96 70.96 12.94 o 2 9 0 1410.09 1507.03 52.71 o 3 9 0 508.05 494.81 34.30 o 4 9 0 45.10 37.61 15.72 o 5 9 0 275.74 256.85 38.96 o 6 9 0 0.02 4.97 31.27 o 7 9 0 131.88 159.71 39.66 o 8 9 0 2.92 18.84 33.34 o 0 10 0 59.74 54.95 13.19 o 1 10 0 879.49 813.64 38.67 o 2 10 0 10.89 2.30 13.81 o 3 10 0 4.72 20.09 22.16 o 4 10 0 236.92 243.31 28.83 o 5 10 0 37.71 25.45 18.54 o 6 10 0 1.44 17.47 24.18 o 7 10 0 14.31 16.75 26.23 o 1 11 0 94.85 76.12 15.30 o 2 11 0 134.64 124.42 19.99 o 3 11 0 19.47 22.77 15.78 o 4 11 0 0.09 11.71 18.38 o 5 11 0 26.63 19.24 14.88 o 6 11 0 262.90 247.15 37.68 o 7 11 0 5.31 4.68 19.60 o 0 12 0 3.40 2.69 19.46 o 1 12 0 44.00 31.73 11.26 o 2 12 0 67.16 79.65 16.49 o 3 12 0 1020.81 995.47 53.73 o 4 12 0 24.96 15.20 15.07 o 5 12 0 940.64 855.43 58.16 o 6 12 0 6.04 17.44 25.27 o 7 12 0 39.94 43.88 29.83 o 1 13 0 83.06 79.15 14.28 o 2 13 0 11.25 11.89 14.17 o 3 13 0 199.62 197.42 26.91 o 4 13 0 0.04 10.56 33.13 o 5 13 0 8.14 9.11 26.50 o 6 13 0 23.99 24.58 25.37 o 7 13 0 104.65 107.88 50.73 o 0 14 0 263.96 274.27 34.21 o 1 14 0 160.08 139.76 18.92 o 2 14 0 138.69 108.74 19.33 o 3 14 0 177.47 170.08 26.59 o 4 14 0 21.36 27.39 17.20 o 5 14 0 483.61 499.65 48.98 o 6 14 0 231.73 229.65 39.31 o 1 15 0 1.85 3.52 20.09 o 2 15 0 82.52 73.78 16.96 o 3 15 0 0.30 9.73 26.50 o 4 15 0 138.73 120.70 24.89 o 5 15 0 314.62 311.59 39.37 o 0 16 0 131.59 167.93 42.45 o 1 16 0 0.86 10.20 15.81 o 2 16 0 9.23 10.92 18.96 o 3 16 0 55.45 61.68 20.63 o 4 16 0 508.05 498.53 46.10 o 5 16 0 2.40 5.18 23.40 o 1 17 0 53.76 56.76 15.20 o 2 17 0 1.85 1.04 26.50 o 4 17 0 0.56 15.94 25.06 o 5 17 0 8.59 12.01 40.79 o 1 18 0 44.33 31.13 18.91 o 2 18 0 7.32 2.07 18.80 o 3 18 0 11.93 17.39 24.02 o 4 18 0 21.46 7.25 38.52 o 1 0 1 3001.25 3130.21 158.74 o 2 0 1 742.77 648.73 47.85 o 3 0 1 1131.21 1216.18 95.09 o 4 0 1 11.23 14.33 13.02 o 5 0 1 59.17 42.82 16.54 o 6 0 1 353.17 315.53 42.92 o 7 0 1 95.70 97.79 38.25 o 8 0 1 2.16 2.90 38.52 o -8 1 1 76.94 57.12 29.65 o -7 1 1 77.70 94.05 38.11 o -6 1 1 341.19 331.27 36.26 o -5 1 1 346.66 447.05 46.27 o -4 1 1 799.69 810.43 53.42 o -3 1 1 722.31 743.14 42.81 o -2 1 1 5688.52 6404.32 293.34 o -1 1 1 1974.80 2006.93 49.08 o 0 1 1 17891.04 4124.06 1836.83 o 1 1 1 1973.63 2091.01 113.74 o 2 1 1 5686.90 6643.13 168.78 o 3 1 1 722.07 866.79 55.41 o 4 1 1 799.78 834.87 23.47 o 5 1 1 346.74 378.50 41.01 o 6 1 1 342.22 320.86 44.89 o 7 1 1 77.62 103.69 34.41 o 8 1 1 76.76 56.39 24.93 o -8 2 1 105.20 97.92 32.28 o -7 2 1 16.61 23.19 22.49 o -6 2 1 238.81 245.11 36.82 o -5 2 1 165.97 178.89 24.46 o -4 2 1 2168.54 2020.83 79.28 o -3 2 1 163.77 140.31 11.78 o -2 2 1 3443.32 3703.29 109.75 o -1 2 1 2965.34 3239.53 128.59 o 0 2 1 1.03 2.74 0.98 o 1 2 1 2962.73 3019.94 114.93 o 2 2 1 3448.39 3571.96 106.64 o 3 2 1 163.72 127.66 19.90 o 4 2 1 2167.85 2040.66 80.23 o 5 2 1 165.55 179.69 29.64 o 6 2 1 239.25 277.02 45.11 o 7 2 1 16.55 20.59 30.12 o 8 2 1 105.29 105.84 37.14 o -8 3 1 1.88 15.94 39.14 o -7 3 1 11.61 36.65 40.17 o -6 3 1 218.19 238.63 38.92 o -5 3 1 287.76 331.05 40.61 o -4 3 1 559.52 636.41 31.70 o -3 3 1 2954.88 3750.45 131.49 o -2 3 1 1173.74 1040.58 40.26 o -1 3 1 2516.08 2279.34 43.62 o 0 3 1 89.18 86.83 4.62 o 1 3 1 2517.95 1856.39 370.01 o 2 3 1 1173.37 1043.36 44.05 o 3 3 1 2951.63 2309.04 76.65 o 4 3 1 559.37 559.80 44.73 o 5 3 1 287.23 280.94 37.21 o 6 3 1 218.02 219.82 35.92 o 7 3 1 11.69 38.52 43.48 o 8 3 1 1.88 41.00 46.38 o -8 4 1 302.57 326.37 56.63 o -7 4 1 136.95 127.98 37.80 o -6 4 1 616.07 643.39 60.32 o -5 4 1 86.40 69.14 21.26 o -4 4 1 751.66 694.73 47.88 o -3 4 1 134.48 170.14 22.88 o -2 4 1 260.65 262.60 22.32 o -1 4 1 1395.69 1277.63 215.56 o 0 4 1 1024.76 1006.79 44.33 o 1 4 1 1394.94 1183.30 116.53 o 2 4 1 260.93 244.26 23.49 o 3 4 1 134.08 148.61 23.11 o 4 4 1 751.68 680.44 48.31 o 5 4 1 86.75 74.96 22.70 o 6 4 1 615.00 603.07 59.45 o 7 4 1 137.04 138.62 40.07 o 8 4 1 302.52 302.37 53.86 o -8 5 1 72.37 77.53 29.64 o -7 5 1 235.45 207.48 44.15 o -6 5 1 364.12 375.84 48.37 o -5 5 1 60.41 71.44 22.24 o -4 5 1 203.31 192.39 27.65 o -3 5 1 1614.59 1604.71 63.87 o -2 5 1 1790.76 1590.04 53.32 o -1 5 1 5672.60 5944.65 203.06 o 0 5 1 57.92 58.68 6.39 o 1 5 1 5677.23 6135.19 80.10 o 2 5 1 1790.43 1525.83 46.46 o 3 5 1 1614.58 1599.68 66.40 o 4 5 1 202.28 217.51 30.04 o 5 5 1 60.52 66.57 19.27 o 6 5 1 364.38 400.42 51.76 o 7 5 1 235.71 207.80 44.95 o 8 5 1 72.67 70.38 31.68 o -8 6 1 55.96 48.44 26.20 o -7 6 1 16.19 15.23 21.86 o -6 6 1 54.10 38.07 29.06 o -5 6 1 498.02 511.82 48.35 o -4 6 1 6.17 15.94 23.81 o -3 6 1 909.50 945.04 49.42 o -2 6 1 104.88 100.59 15.23 o -1 6 1 380.06 374.36 19.25 o 0 6 1 43.55 50.94 6.32 o 1 6 1 380.64 377.56 23.25 o 2 6 1 104.60 91.78 13.55 o 3 6 1 910.06 902.67 52.15 o 4 6 1 6.25 10.97 24.02 o 5 6 1 498.17 520.96 51.97 o 6 6 1 54.12 49.85 22.64 o 7 6 1 16.29 33.96 41.21 o 8 6 1 55.72 52.18 30.64 o -8 7 1 43.12 39.01 29.69 o -7 7 1 224.15 217.80 44.44 o -6 7 1 518.50 482.70 55.24 o -5 7 1 386.47 450.16 46.63 o -4 7 1 248.82 225.09 31.32 o -3 7 1 420.02 411.95 34.47 o -2 7 1 1461.93 1409.78 61.02 o -1 7 1 197.90 200.46 16.00 o 0 7 1 3482.89 3055.81 199.18 o 1 7 1 198.13 203.47 18.77 o 2 7 1 1460.97 1366.15 48.65 o 3 7 1 420.85 412.01 30.68 o 4 7 1 248.76 222.21 31.82 o 5 7 1 385.85 376.35 46.19 o 6 7 1 517.82 534.97 58.27 o 7 7 1 224.61 237.37 47.80 o 8 7 1 43.20 46.28 30.75 o -8 8 1 20.52 11.77 21.65 o -7 8 1 123.06 129.93 37.34 o -6 8 1 26.91 33.86 18.68 o -5 8 1 140.95 116.04 26.94 o -4 8 1 127.07 164.43 27.30 o -3 8 1 68.72 75.15 14.23 o -2 8 1 1272.02 1237.28 43.56 o -1 8 1 46.49 46.80 9.54 o 0 8 1 1791.92 1709.19 32.58 o 1 8 1 46.45 40.33 10.72 o 2 8 1 1273.27 1221.70 48.20 o 3 8 1 69.07 91.68 17.45 o 4 8 1 126.67 133.98 21.83 o 5 8 1 140.97 134.02 32.41 o 6 8 1 27.03 30.07 25.05 o 7 8 1 123.13 109.60 37.74 o 8 8 1 20.42 47.34 28.95 o -8 9 1 0.47 0.62 24.85 o -7 9 1 97.46 78.25 27.97 o -6 9 1 77.62 81.19 31.31 o -5 9 1 119.23 121.80 28.75 o -4 9 1 248.80 271.14 35.36 o -3 9 1 243.05 213.91 23.33 o -2 9 1 3079.53 3156.40 248.08 o -1 9 1 193.83 202.88 18.17 o 0 9 1 46.37 50.18 7.36 o 1 9 1 193.53 190.10 19.82 o 2 9 1 3080.12 3214.67 319.02 o 3 9 1 242.87 204.98 24.21 o 4 9 1 248.91 253.98 29.64 o 5 9 1 119.40 122.62 24.70 o 6 9 1 77.60 68.63 23.90 o 7 9 1 97.44 72.48 28.80 o -8 10 1 65.73 82.83 64.81 o -7 10 1 149.44 168.58 38.76 o -6 10 1 37.19 19.17 25.68 o -5 10 1 5.31 18.22 29.82 o -4 10 1 293.59 287.66 29.98 o -3 10 1 87.17 94.93 17.08 o -2 10 1 1205.62 1210.12 47.23 o -1 10 1 1096.55 1078.96 40.42 o 0 10 1 208.50 255.44 17.36 o 1 10 1 1097.73 1072.17 45.90 o 2 10 1 1205.30 1194.12 50.83 o 3 10 1 87.27 95.99 19.63 o 4 10 1 293.16 286.03 32.69 o 5 10 1 5.22 8.90 32.72 o 6 10 1 37.45 46.47 30.46 o 7 10 1 149.14 192.41 37.89 o -7 11 1 44.18 43.50 26.99 o -6 11 1 365.53 381.37 45.14 o -5 11 1 39.98 32.64 17.20 o -4 11 1 61.17 52.07 16.48 o -3 11 1 139.81 147.23 21.79 o -2 11 1 12.06 14.52 10.00 o -1 11 1 166.40 179.42 19.96 o 0 11 1 19.98 23.52 7.47 o 1 11 1 166.50 181.87 22.92 o 2 11 1 11.96 26.96 21.95 o 3 11 1 139.46 145.34 23.10 o 4 11 1 61.10 75.39 22.26 o 5 11 1 39.90 29.79 18.58 o 6 11 1 365.35 377.74 46.60 o 7 11 1 44.19 36.23 23.49 o -7 12 1 0.64 9.05 24.47 o -6 12 1 140.18 135.08 30.09 o -5 12 1 124.88 158.81 29.14 o -4 12 1 71.57 81.76 20.74 o -3 12 1 345.92 348.71 32.08 o -2 12 1 225.30 209.63 23.10 o -1 12 1 1244.00 1274.82 50.14 o 0 12 1 143.71 153.88 15.54 o 1 12 1 1243.27 1292.05 55.40 o 2 12 1 225.49 214.63 26.46 o 3 12 1 346.90 358.75 34.02 o 4 12 1 71.51 63.61 18.52 o 5 12 1 124.64 152.03 32.40 o 6 12 1 140.21 152.79 32.80 o 7 12 1 0.63 14.49 35.41 o -7 13 1 48.98 51.64 25.75 o -6 13 1 47.61 35.31 21.03 o -5 13 1 726.76 691.08 53.70 o -4 13 1 75.19 67.71 18.44 o -3 13 1 149.85 144.44 23.11 o -2 13 1 11.56 14.00 10.73 o -1 13 1 775.75 798.80 41.92 o 0 13 1 99.20 98.44 14.99 o 1 13 1 774.43 763.93 38.32 o 2 13 1 11.58 16.62 14.09 o 3 13 1 149.95 149.04 25.74 o 4 13 1 75.32 75.95 20.36 o 5 13 1 726.99 679.69 55.67 o 6 13 1 47.64 54.33 24.41 o -7 14 1 105.95 130.04 56.94 o -6 14 1 59.61 52.36 24.15 o -5 14 1 51.31 55.76 24.52 o -4 14 1 91.32 70.69 18.37 o -3 14 1 174.36 163.91 24.09 o -2 14 1 160.12 157.79 22.07 o -1 14 1 350.74 347.26 26.74 o 0 14 1 19.62 16.29 11.48 o 1 14 1 350.89 375.58 29.53 o 2 14 1 159.97 159.88 24.97 o 3 14 1 174.28 188.41 28.41 o 4 14 1 91.10 79.14 21.79 o 5 14 1 51.29 50.54 28.89 o 6 14 1 59.50 43.41 21.86 o -6 15 1 5.88 8.70 34.37 o -5 15 1 10.36 5.18 28.78 o -4 15 1 165.93 135.08 26.72 o -3 15 1 24.60 17.63 15.32 o -2 15 1 23.87 25.30 10.52 o -1 15 1 197.18 180.33 20.21 o 0 15 1 784.23 811.73 49.90 o 1 15 1 196.69 209.10 23.90 o 2 15 1 23.72 29.85 14.50 o 3 15 1 24.57 35.62 20.99 o 4 15 1 165.75 151.30 28.69 o 5 15 1 10.38 16.99 18.20 o 6 15 1 5.90 9.49 18.20 o -5 16 1 122.25 119.98 36.07 o -4 16 1 23.27 20.37 17.25 o -3 16 1 0.75 10.97 24.23 o -2 16 1 80.90 83.81 21.08 o -1 16 1 14.48 9.09 10.91 o 0 16 1 401.31 437.86 45.37 o 1 16 1 14.36 15.65 13.34 o 2 16 1 81.09 65.90 20.22 o 4 16 1 23.28 10.27 19.11 o 5 16 1 122.24 101.26 52.80 o 6 16 1 64.61 54.67 52.39 o -4 17 1 3.02 4.83 17.50 o -3 17 1 7.60 11.18 25.68 o -2 17 1 124.95 139.43 24.41 o -1 17 1 58.52 45.94 15.91 o 0 17 1 307.13 333.17 45.96 o 1 17 1 58.56 51.74 13.68 o 2 17 1 124.98 118.82 22.16 o 3 17 1 7.64 17.54 18.06 o 4 17 1 3.00 10.15 24.85 o 5 17 1 9.31 4.56 24.85 o -2 18 1 38.72 37.89 30.44 o -1 18 1 170.70 145.78 44.31 o 0 18 1 202.33 192.37 49.49 o 1 18 1 171.23 164.41 47.63 o 2 18 1 38.80 34.09 24.88 o 3 18 1 3.32 8.08 24.02 o 4 18 1 12.88 7.66 24.02 o 1 19 1 91.77 118.86 46.80 o 2 19 1 60.25 77.46 28.73 o 3 19 1 28.88 54.05 47.83 o 0 0 2 96.64 123.06 16.09 o 1 0 2 1.58 38.21 18.95 o 2 0 2 238.27 243.50 12.52 o 3 0 2 339.75 354.64 15.22 o 4 0 2 2468.08 3097.60 287.01 o 5 0 2 91.87 101.87 23.13 o 7 0 2 15.34 44.59 26.71 o 8 0 2 11.94 5.75 22.62 o -7 1 2 122.04 138.46 40.33 o -6 1 2 3.87 14.29 23.81 o -5 1 2 777.78 798.51 28.52 o -4 1 2 638.66 638.27 46.49 o -3 1 2 141.10 151.33 13.56 o -2 1 2 2191.80 2268.55 82.56 o -1 1 2 12.80 16.34 5.07 o 0 1 2 7540.09 7412.22 412.35 o 1 1 2 12.80 14.72 5.08 o 2 1 2 2189.34 2072.47 362.79 o 3 1 2 140.19 144.01 10.56 o 4 1 2 638.78 700.47 26.26 o 5 1 2 777.22 744.49 56.56 o 6 1 2 3.89 20.40 23.57 o 7 1 2 121.70 141.96 39.02 o 8 1 2 1.87 14.06 25.08 o -8 2 2 148.24 133.59 37.48 o -7 2 2 342.08 389.33 58.34 o -6 2 2 53.83 53.52 25.06 o -5 2 2 807.01 801.27 57.87 o -4 2 2 1424.83 1405.11 67.39 o -3 2 2 82.31 89.75 16.81 o -2 2 2 457.85 420.09 20.14 o -1 2 2 407.06 389.97 15.01 o 0 2 2 10190.60 7272.77 690.67 o 1 2 2 407.59 405.11 12.21 o 2 2 2 457.12 432.81 21.73 o 3 2 2 82.60 92.13 11.37 o 4 2 2 1425.56 1637.66 144.07 o 5 2 2 806.22 809.87 59.59 o 6 2 2 54.05 61.06 25.70 o 7 2 2 341.83 366.78 53.14 o 8 2 2 147.83 133.52 39.20 o -8 3 2 80.73 78.55 29.86 o -7 3 2 240.13 249.68 46.96 o -6 3 2 401.48 384.49 46.64 o -5 3 2 365.79 364.77 40.48 o -4 3 2 498.60 510.26 40.99 o -3 3 2 1106.91 1071.09 50.15 o -2 3 2 7.89 9.53 8.74 o -1 3 2 222.46 231.01 12.62 o 0 3 2 2633.02 2484.36 160.61 o 1 3 2 223.58 233.41 11.18 o 2 3 2 7.92 9.81 10.27 o 3 3 2 1105.62 1065.20 54.17 o 4 3 2 498.94 510.25 43.27 o 5 3 2 365.31 368.56 18.32 o 6 3 2 400.74 389.78 48.61 o 7 3 2 240.05 268.06 49.67 o 8 3 2 80.64 87.07 33.97 o -8 4 2 53.28 58.53 29.10 o -7 4 2 364.65 355.89 53.57 o -6 4 2 32.40 39.99 19.45 o -5 4 2 282.30 231.39 33.26 o -4 4 2 988.22 1053.13 57.25 o -3 4 2 173.54 167.36 22.10 o -2 4 2 2258.03 2821.03 224.46 o -1 4 2 11862.25 12063.21 1866.43 o 0 4 2 4122.29 4329.20 211.62 o 1 4 2 11862.38 11321.87 1355.91 o 2 4 2 2257.45 1809.28 60.25 o 3 4 2 173.12 162.87 22.97 o 4 4 2 986.83 1002.33 60.25 o 5 4 2 281.87 278.55 38.41 o 6 4 2 32.56 55.47 29.04 o 7 4 2 364.92 319.63 53.08 o 8 4 2 53.55 48.82 29.15 o -8 5 2 11.53 3.54 25.09 o -7 5 2 76.02 63.87 28.87 o -6 5 2 297.43 288.38 44.99 o -5 5 2 530.42 534.13 48.94 o -4 5 2 272.66 235.83 29.54 o -3 5 2 357.83 366.14 30.28 o -2 5 2 617.24 620.85 31.69 o -1 5 2 178.48 167.72 13.82 o 0 5 2 6932.14 7406.94 374.43 o 1 5 2 178.40 163.09 15.90 o 2 5 2 616.85 610.85 31.83 o 3 5 2 356.39 369.97 35.65 o 4 5 2 272.78 241.74 32.99 o 5 5 2 529.94 510.93 49.72 o 6 5 2 297.12 333.13 47.21 o 7 5 2 76.07 69.54 31.25 o 8 5 2 11.50 27.95 44.11 o -8 6 2 40.29 25.71 23.85 o -7 6 2 479.92 509.92 64.53 o -6 6 2 28.70 23.81 35.62 o -5 6 2 694.49 666.96 54.85 o -4 6 2 692.27 679.01 47.64 o -3 6 2 311.51 280.68 27.60 o -2 6 2 2176.51 1917.05 78.07 o -1 6 2 157.43 140.22 11.22 o 0 6 2 1138.78 1248.74 97.79 o 1 6 2 157.77 152.56 16.75 o 2 6 2 2174.89 1851.44 62.28 o 3 6 2 311.36 272.00 26.51 o 4 6 2 692.02 680.43 52.04 o 5 6 2 693.44 651.62 56.88 o 6 6 2 28.68 33.56 24.03 o 7 6 2 480.76 494.74 63.25 o 8 6 2 40.30 20.97 29.54 o -8 7 2 12.40 7.25 21.38 o -7 7 2 124.69 102.12 33.80 o -6 7 2 199.62 158.44 36.07 o -5 7 2 260.74 295.29 38.20 o -4 7 2 116.82 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