#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/64/2006412.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2006412_Fobs loop_ _publ_author_name 'Van Meervelt, L.' 'Kong Thoo Lin, P.' _publ_section_title ; 5,8-Bis(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-1,4-dioxa-5,8-diazocane ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1131 _journal_page_last 1133 _journal_volume 53 _journal_year 1997 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 74.490 _cell_angle_beta 80.000 _cell_angle_gamma 83.130 _cell_length_a 9.0790 _cell_length_b 10.1880 _cell_length_c 14.9200 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.9998 _[local]_cod_data_source_file mu1298sup2.hkl _[local]_cod_data_source_block kong3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' KONG3 P-1 re-ref. -11-' _shelx_refln_list_code 4 _shelx_f_calc_maximum 158.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 79.72 87.73 4.14 o 2 0 0 472.40 548.19 17.64 o 3 0 0 1636.58 1625.29 37.40 o 4 0 0 4517.51 5005.95 82.87 o 5 0 0 65.86 82.10 4.15 o 6 0 0 19.38 15.54 1.70 o 7 0 0 126.22 129.54 5.50 o 8 0 0 41.81 28.02 2.63 o -8 1 0 256.35 267.05 8.16 o -7 1 0 34.40 27.87 2.46 o -6 1 0 7.92 8.06 1.78 o -5 1 0 442.76 546.19 22.89 o -4 1 0 338.69 360.27 15.94 o -3 1 0 689.73 727.33 26.26 o -2 1 0 22.71 24.55 1.18 o -1 1 0 1455.00 1576.44 24.93 o 0 1 0 16.91 9.00 1.07 o 1 1 0 131.61 134.32 10.58 o 2 1 0 185.23 172.48 8.35 o 3 1 0 185.55 159.78 7.92 o 4 1 0 42.68 42.07 1.63 o 5 1 0 509.68 505.32 22.17 o 6 1 0 153.66 148.54 7.80 o 7 1 0 70.46 67.55 3.05 o 8 1 0 0.26 0.83 2.01 o -8 2 0 74.85 66.30 3.43 o -7 2 0 0.75 4.76 2.09 o -6 2 0 540.28 515.67 23.89 o -5 2 0 867.44 859.03 37.08 o -4 2 0 158.25 143.86 7.15 o -3 2 0 300.62 355.18 15.57 o -2 2 0 4210.45 4137.17 61.82 o -1 2 0 773.81 777.03 16.41 o 0 2 0 524.11 478.32 12.24 o 1 2 0 36.68 26.67 1.80 o 2 2 0 696.59 670.20 25.35 o 3 2 0 37.49 128.30 6.14 o 4 2 0 314.04 357.43 17.89 o 5 2 0 603.58 598.90 26.81 o 6 2 0 194.09 175.52 9.47 o 7 2 0 234.45 266.86 14.02 o 8 2 0 125.26 126.61 5.66 o -8 3 0 42.55 43.90 2.84 o -7 3 0 803.96 717.79 34.34 o -6 3 0 457.69 440.18 18.13 o -5 3 0 194.46 198.59 8.85 o -4 3 0 5.56 7.51 1.34 o -3 3 0 440.52 553.68 26.78 o -2 3 0 144.38 148.64 6.68 o -1 3 0 1425.23 1477.68 58.01 o 0 3 0 3911.39 3475.72 20.84 o 1 3 0 5.33 10.73 0.73 o 2 3 0 1487.10 1208.15 40.25 o 3 3 0 2.58 2.71 0.95 o 4 3 0 312.69 254.63 13.13 o 5 3 0 486.69 496.71 22.29 o 6 3 0 378.29 423.51 18.65 o 7 3 0 45.18 46.27 2.92 o 8 3 0 27.71 27.14 2.66 o -7 4 0 169.29 155.26 8.29 o -6 4 0 109.83 105.39 5.50 o -5 4 0 13.32 9.06 1.86 o -4 4 0 551.58 574.30 26.77 o -3 4 0 1.53 2.76 1.21 o -2 4 0 112.04 96.13 5.65 o -1 4 0 230.14 219.17 17.19 o 0 4 0 1740.02 1680.75 34.35 o 1 4 0 0.98 1.53 0.62 o 2 4 0 0.39 4.47 1.04 o 3 4 0 101.42 83.64 4.13 o 4 4 0 32.54 28.41 1.84 o 5 4 0 1016.37 1086.35 55.78 o 6 4 0 734.11 708.00 37.79 o 7 4 0 55.45 60.91 3.54 o 8 4 0 147.49 179.26 10.10 o -7 5 0 33.87 41.32 2.94 o -6 5 0 156.31 143.96 5.06 o -5 5 0 748.45 873.38 42.68 o -4 5 0 22.85 17.72 2.02 o -3 5 0 281.83 324.46 17.13 o -2 5 0 595.19 537.16 26.28 o -1 5 0 10.79 8.61 0.87 o 0 5 0 380.63 358.41 13.84 o 1 5 0 604.58 564.56 23.14 o 2 5 0 2232.28 2073.89 69.61 o 3 5 0 133.15 107.33 7.18 o 4 5 0 170.24 103.52 7.57 o 5 5 0 806.14 766.72 43.49 o 6 5 0 491.48 499.98 25.37 o 7 5 0 15.45 16.19 2.32 o -6 6 0 199.99 211.89 11.93 o -5 6 0 196.31 179.64 7.85 o -4 6 0 42.34 51.33 3.00 o -3 6 0 180.40 172.28 7.31 o -2 6 0 332.53 398.05 19.88 o -1 6 0 176.74 172.41 10.17 o 0 6 0 54.21 52.85 2.10 o 1 6 0 87.74 85.16 4.16 o 2 6 0 87.14 77.94 3.07 o 3 6 0 244.44 261.46 14.21 o 4 6 0 118.59 93.07 7.26 o 5 6 0 0.40 0.49 1.86 o 6 6 0 236.05 243.85 12.64 o 7 6 0 95.24 112.44 6.45 o -5 7 0 82.22 72.50 4.28 o -4 7 0 153.15 149.93 6.11 o -3 7 0 1667.01 1874.81 83.33 o -2 7 0 114.32 122.14 5.61 o -1 7 0 5.35 2.94 1.07 o 0 7 0 19.99 33.01 1.68 o 1 7 0 163.32 163.05 22.29 o 2 7 0 94.06 93.87 5.63 o 3 7 0 358.16 315.92 18.00 o 4 7 0 0.42 -1.47 2.07 o 5 7 0 281.49 278.82 14.86 o 6 7 0 208.22 212.41 12.03 o -4 8 0 300.15 332.91 16.57 o -3 8 0 66.85 80.85 4.47 o -2 8 0 127.00 160.27 8.29 o -1 8 0 339.54 375.08 14.26 o 0 8 0 16.13 22.42 1.62 o 1 8 0 441.40 410.69 39.11 o 2 8 0 282.57 263.59 16.64 o 3 8 0 153.51 145.48 11.56 o 4 8 0 36.29 38.17 2.79 o 5 8 0 2.48 5.35 1.70 o -2 9 0 106.66 127.80 7.21 o -1 9 0 20.28 21.48 2.68 o 0 9 0 62.54 66.35 2.60 o 1 9 0 18.63 19.36 1.68 o 2 9 0 8.84 7.47 2.11 o 3 9 0 87.37 98.21 4.31 o 4 9 0 5.90 8.29 1.96 o -3 -9 1 52.50 57.46 3.30 o -2 -9 1 6.15 7.03 1.89 o -1 -9 1 251.72 222.71 28.68 o 0 -9 1 234.88 210.93 22.11 o 1 -9 1 287.83 232.37 25.54 o 2 -9 1 6.60 9.04 1.93 o -5 -8 1 22.96 27.17 2.35 o -4 -8 1 21.78 42.54 3.13 o -3 -8 1 8.22 6.56 2.04 o -2 -8 1 760.99 830.82 40.29 o -1 -8 1 24.56 34.44 3.93 o 0 -8 1 35.04 45.73 2.02 o 1 -8 1 844.51 907.79 35.14 o 2 -8 1 23.28 18.42 2.48 o 3 -8 1 79.73 57.14 4.46 o 4 -8 1 63.61 80.25 4.60 o -6 -7 1 165.05 169.77 6.74 o -5 -7 1 246.25 251.48 13.05 o -4 -7 1 13.08 16.17 2.22 o -3 -7 1 111.04 109.85 4.50 o -2 -7 1 127.79 139.22 6.61 o -1 -7 1 9.91 11.28 1.33 o 0 -7 1 13.36 16.12 1.36 o 1 -7 1 6.77 8.52 1.23 o 2 -7 1 86.79 78.26 3.74 o 3 -7 1 784.82 925.54 43.97 o 4 -7 1 37.23 38.01 2.79 o 5 -7 1 1.84 2.59 1.89 o -7 -6 1 27.39 26.68 2.63 o -6 -6 1 0.04 12.86 2.58 o -5 -6 1 476.98 506.61 27.10 o -4 -6 1 121.87 102.10 7.36 o -3 -6 1 27.68 26.60 3.07 o -2 -6 1 168.99 142.01 8.82 o -1 -6 1 114.42 96.20 4.50 o 0 -6 1 947.58 884.02 32.69 o 1 -6 1 209.03 217.26 8.08 o 2 -6 1 27.44 28.25 2.63 o 3 -6 1 149.36 193.24 8.19 o 4 -6 1 2.64 1.81 1.96 o 5 -6 1 629.84 617.36 32.47 o 6 -6 1 272.72 258.31 9.37 o -7 -5 1 255.91 271.26 12.78 o -6 -5 1 269.48 277.08 13.75 o -5 -5 1 855.31 825.30 47.06 o -4 -5 1 0.48 1.09 1.26 o -3 -5 1 318.99 281.90 16.36 o -2 -5 1 77.34 69.14 4.67 o -1 -5 1 20.28 24.33 2.88 o 0 -5 1 939.88 1044.40 32.13 o 1 -5 1 2.08 2.43 0.78 o 2 -5 1 322.30 341.02 14.99 o 3 -5 1 630.13 807.20 36.19 o 4 -5 1 1157.46 1118.80 56.68 o 5 -5 1 1578.65 1613.03 67.76 o 6 -5 1 56.22 49.32 3.20 o 7 -5 1 164.63 160.16 7.31 o -8 -4 1 2.33 8.55 2.22 o -7 -4 1 205.08 244.00 12.88 o -6 -4 1 747.64 849.42 41.52 o -5 -4 1 137.01 157.70 7.10 o -4 -4 1 35.50 52.99 3.20 o -3 -4 1 3.49 2.89 1.13 o -2 -4 1 445.37 453.48 25.02 o -1 -4 1 26.87 24.55 1.20 o 0 -4 1 2214.36 2195.00 82.17 o 1 -4 1 16.46 40.51 2.02 o 2 -4 1 413.07 477.01 28.17 o 3 -4 1 26.66 34.52 2.63 o 4 -4 1 3.64 2.38 1.44 o 5 -4 1 90.47 97.80 5.04 o 6 -4 1 1122.71 1114.04 54.77 o 7 -4 1 61.50 61.25 3.57 o -8 -3 1 19.45 26.18 2.63 o -7 -3 1 41.40 49.92 3.77 o -6 -3 1 166.63 175.18 9.79 o -5 -3 1 216.98 218.64 11.17 o -4 -3 1 15.61 25.44 1.65 o -3 -3 1 251.06 214.09 12.18 o -2 -3 1 1192.79 1060.10 38.83 o -1 -3 1 2784.64 2353.57 177.58 o 0 -3 1 751.69 724.13 19.36 o 1 -3 1 1479.20 1637.64 51.32 o 2 -3 1 115.10 147.87 7.44 o 3 -3 1 2542.52 2714.48 65.05 o 4 -3 1 207.29 217.34 9.37 o 5 -3 1 347.16 436.36 18.06 o 6 -3 1 1235.36 1234.85 59.94 o 7 -3 1 474.23 466.27 21.43 o 8 -3 1 51.18 46.53 2.99 o -8 -2 1 29.72 31.64 2.77 o -7 -2 1 191.74 177.05 8.64 o -6 -2 1 34.43 35.23 2.42 o -5 -2 1 85.69 71.87 3.90 o -4 -2 1 20.96 34.63 2.56 o -3 -2 1 762.71 693.15 29.40 o -2 -2 1 61.00 67.72 3.38 o -1 -2 1 2.03 7.49 0.61 o 0 -2 1 2457.69 2324.78 99.49 o 1 -2 1 677.38 667.84 15.85 o 2 -2 1 3021.45 3446.34 56.81 o 3 -2 1 68.89 61.63 2.46 o 4 -2 1 1112.97 966.67 42.08 o 5 -2 1 1636.93 1448.41 58.01 o 6 -2 1 130.98 122.18 4.70 o 7 -2 1 13.40 9.69 2.14 o 8 -2 1 170.26 146.13 7.13 o -8 -1 1 13.39 10.56 2.37 o -7 -1 1 97.45 86.39 5.32 o -6 -1 1 6.50 6.90 1.75 o -5 -1 1 37.30 31.56 2.25 o -4 -1 1 79.99 93.95 3.80 o -3 -1 1 1656.99 1539.16 39.96 o -2 -1 1 55.52 72.13 3.56 o -1 -1 1 45.92 33.81 5.58 o 0 -1 1 18842.32 21156.73 1517.56 o 1 -1 1 5267.92 6517.32 325.82 o 2 -1 1 55.61 76.13 3.02 o 3 -1 1 338.95 405.86 16.88 o 4 -1 1 0.79 3.57 1.03 o 5 -1 1 526.69 494.57 22.93 o 6 -1 1 253.21 200.17 7.72 o 7 -1 1 1.04 2.32 1.75 o 8 -1 1 0.54 0.82 1.81 o -8 0 1 88.79 98.06 5.29 o -7 0 1 164.07 162.21 8.59 o -6 0 1 682.34 702.13 30.14 o -5 0 1 347.05 464.33 20.89 o -4 0 1 1031.05 908.41 38.33 o -3 0 1 522.44 523.41 22.73 o -2 0 1 1281.04 1245.04 28.29 o -1 0 1 25143.62 23945.94 528.88 o 0 0 1 210.88 227.68 4.70 o 1 0 1 1.85 2.83 0.79 o 2 0 1 871.28 914.05 22.22 o 3 0 1 70.16 84.02 3.33 o 4 0 1 6.10 2.89 0.96 o 5 0 1 29.81 23.71 1.60 o 6 0 1 28.42 13.12 1.75 o 7 0 1 22.04 10.75 1.96 o 8 0 1 2.76 2.22 2.17 o -8 1 1 183.23 199.78 9.63 o -7 1 1 113.46 109.38 5.73 o -6 1 1 152.46 204.67 9.09 o -5 1 1 317.52 314.77 15.70 o -4 1 1 100.78 133.30 7.04 o -3 1 1 405.72 416.38 19.68 o -2 1 1 572.65 587.80 20.39 o -1 1 1 6983.63 7136.15 192.96 o 0 1 1 365.58 351.48 10.05 o 1 1 1 384.87 261.42 7.69 o 2 1 1 4038.29 4398.30 50.70 o 3 1 1 543.85 697.55 24.53 o 4 1 1 321.29 304.48 14.18 o 5 1 1 361.82 328.92 14.06 o 6 1 1 1.98 4.06 1.48 o 8 1 1 158.84 192.52 6.37 o -8 2 1 24.93 27.48 2.59 o -7 2 1 79.79 75.08 4.10 o -6 2 1 58.10 62.90 2.87 o -5 2 1 211.84 181.87 8.62 o -4 2 1 658.30 719.82 33.19 o -3 2 1 51.59 70.18 3.53 o -2 2 1 1833.61 1860.41 42.04 o -1 2 1 5.73 1.72 0.54 o 0 2 1 553.36 483.54 31.56 o 1 2 1 2338.53 2083.06 124.14 o 2 2 1 1115.90 881.64 29.05 o 3 2 1 972.92 961.42 33.65 o 4 2 1 63.34 90.99 4.52 o 5 2 1 60.52 97.89 5.26 o 6 2 1 82.72 105.70 4.21 o 7 2 1 139.41 174.82 6.87 o 8 2 1 1.69 2.09 1.88 o -8 3 1 0.27 1.39 1.78 o -7 3 1 583.14 649.88 24.57 o -6 3 1 42.31 48.01 3.44 o -5 3 1 326.45 248.46 13.08 o -4 3 1 17.31 27.42 1.70 o -3 3 1 2238.64 2206.59 60.23 o -2 3 1 1.21 5.65 1.01 o -1 3 1 15.01 13.47 0.75 o 0 3 1 2355.72 2102.97 88.00 o 1 3 1 77.51 71.62 3.00 o 2 3 1 45.84 50.74 3.70 o 3 3 1 298.02 298.13 17.07 o 4 3 1 230.08 196.87 9.52 o 5 3 1 465.35 440.15 21.65 o 6 3 1 767.23 715.26 34.67 o 7 3 1 69.52 84.22 4.37 o 8 3 1 4.47 4.86 2.04 o -7 4 1 123.04 126.61 5.66 o -6 4 1 38.37 34.34 2.90 o -5 4 1 685.73 601.48 34.89 o -4 4 1 2.98 3.38 1.24 o -3 4 1 89.44 127.23 6.35 o -2 4 1 997.85 1008.27 41.25 o -1 4 1 34.18 16.84 1.43 o 0 4 1 168.29 134.39 8.52 o 1 4 1 348.11 276.06 14.30 o 2 4 1 130.45 109.40 6.29 o 3 4 1 18.69 11.37 1.34 o 4 4 1 77.22 47.50 2.46 o 5 4 1 111.61 102.54 5.91 o 6 4 1 1.37 0.75 1.48 o 7 4 1 5.90 11.50 1.94 o 8 4 1 66.17 72.45 4.75 o -7 5 1 62.75 56.76 3.12 o -6 5 1 468.16 539.57 26.45 o -5 5 1 519.78 502.76 27.02 o -4 5 1 465.24 480.72 23.46 o -3 5 1 1224.06 1490.75 60.27 o -2 5 1 1085.99 1365.68 52.21 o -1 5 1 490.89 423.65 17.97 o 0 5 1 383.41 289.99 23.32 o 1 5 1 19.10 24.82 1.11 o 2 5 1 146.15 134.94 8.86 o 3 5 1 451.75 484.28 27.69 o 4 5 1 663.38 593.19 39.59 o 5 5 1 3.95 4.59 1.63 o 6 5 1 500.70 590.43 28.95 o 7 5 1 232.37 260.54 13.88 o 8 5 1 25.50 30.96 2.79 o -6 6 1 498.94 516.37 26.81 o -5 6 1 51.20 42.04 2.92 o -4 6 1 599.46 604.91 34.30 o -3 6 1 1965.89 2184.49 78.29 o -2 6 1 68.50 80.84 3.72 o -1 6 1 102.74 106.23 8.57 o 0 6 1 42.64 39.13 2.24 o 1 6 1 7.80 8.71 0.99 o 2 6 1 477.09 406.27 28.07 o 3 6 1 180.21 148.51 10.38 o 4 6 1 290.62 278.25 15.89 o 5 6 1 119.28 121.03 6.76 o 6 6 1 81.88 99.61 5.70 o 7 6 1 32.81 36.29 2.59 o -5 7 1 26.25 24.05 2.43 o -4 7 1 37.03 37.05 2.69 o -3 7 1 594.64 629.65 31.27 o -2 7 1 62.07 70.28 3.18 o -1 7 1 372.22 338.64 13.75 o 0 7 1 10.05 12.74 2.42 o 1 7 1 93.90 84.98 3.14 o 2 7 1 539.74 491.96 30.39 o 3 7 1 133.35 139.61 9.61 o 4 7 1 1.58 41.17 2.95 o 5 7 1 2.68 2.76 1.88 o 6 7 1 84.56 95.59 5.27 o -4 8 1 87.03 77.89 3.82 o -3 8 1 39.87 34.76 2.92 o -2 8 1 18.03 25.31 2.53 o -1 8 1 17.47 26.76 1.72 o 0 8 1 491.03 410.45 55.07 o 1 8 1 22.43 27.68 1.68 o 2 8 1 190.91 198.66 11.15 o 3 8 1 108.86 108.61 6.15 o 4 8 1 197.30 217.35 12.24 o 5 8 1 0.07 0.47 1.57 o -2 9 1 64.93 61.94 3.53 o -1 9 1 9.97 9.84 1.62 o 0 9 1 52.16 53.59 2.70 o 1 9 1 20.33 17.41 1.64 o 2 9 1 11.76 12.57 2.12 o 3 9 1 95.65 98.93 5.81 o 4 9 1 92.50 92.38 6.30 o -2 -9 2 275.70 263.62 16.46 o -1 -9 2 198.15 184.20 7.83 o 0 -9 2 74.72 79.51 4.27 o 1 -9 2 35.70 40.33 2.11 o -4 -8 2 17.41 13.12 2.07 o -3 -8 2 171.40 176.37 10.46 o -2 -8 2 147.22 178.45 10.87 o -1 -8 2 0.01 0.47 1.24 o 0 -8 2 1447.67 1466.65 67.78 o 1 -8 2 81.29 77.58 4.11 o 2 -8 2 253.68 242.96 9.19 o 3 -8 2 317.30 331.90 17.18 o 4 -8 2 19.01 16.71 2.14 o -6 -7 2 27.61 25.65 2.71 o -5 -7 2 229.15 228.01 13.11 o -4 -7 2 6.83 7.88 2.22 o -3 -7 2 270.24 278.78 15.10 o -2 -7 2 0.01 -0.72 1.65 o -1 -7 2 2.65 1.97 1.44 o 0 -7 2 494.23 503.22 19.47 o 1 -7 2 41.89 40.53 1.94 o 2 -7 2 10.41 6.94 1.84 o 3 -7 2 29.42 36.49 2.58 o 4 -7 2 15.27 15.60 2.11 o 5 -7 2 0.77 -0.80 2.19 o -6 -6 2 28.40 30.32 2.81 o -5 -6 2 111.02 110.93 6.14 o -4 -6 2 56.35 55.83 3.18 o -3 -6 2 22.56 19.11 2.69 o -2 -6 2 549.52 565.33 31.40 o -1 -6 2 27.41 30.91 1.58 o 0 -6 2 57.18 68.94 5.32 o 1 -6 2 2.19 3.26 1.12 o 2 -6 2 1002.66 1211.12 54.19 o 3 -6 2 278.71 287.95 14.22 o 4 -6 2 780.55 753.27 38.36 o 5 -6 2 2438.17 2558.91 100.26 o 6 -6 2 167.66 153.58 8.46 o -7 -5 2 4.05 3.70 1.84 o -6 -5 2 561.32 603.51 30.36 o -5 -5 2 57.00 51.20 3.07 o -4 -5 2 1.06 1.57 3.95 o -3 -5 2 170.25 179.14 9.63 o -2 -5 2 26.74 34.06 2.06 o -1 -5 2 10.72 11.07 1.10 o 0 -5 2 384.23 454.55 17.62 o 1 -5 2 72.64 82.09 3.47 o 2 -5 2 166.79 184.85 7.40 o 3 -5 2 154.55 176.99 8.49 o 4 -5 2 465.83 530.77 25.17 o 5 -5 2 16.20 12.21 2.68 o 6 -5 2 0.75 0.62 2.06 o 7 -5 2 169.85 168.53 7.08 o -7 -4 2 4.29 3.36 2.09 o -6 -4 2 61.24 75.69 4.21 o -5 -4 2 1.53 5.74 1.68 o -4 -4 2 28.17 32.59 2.48 o -3 -4 2 61.06 53.73 3.23 o -2 -4 2 0.83 4.08 1.21 o -1 -4 2 599.85 623.97 24.31 o 0 -4 2 543.99 596.31 36.57 o 1 -4 2 169.59 224.50 18.04 o 2 -4 2 71.38 79.94 4.42 o 3 -4 2 615.28 728.08 35.49 o 4 -4 2 26.53 24.66 2.55 o 5 -4 2 221.48 170.02 7.53 o 6 -4 2 38.14 29.59 2.71 o 7 -4 2 2.98 7.13 2.04 o -8 -3 2 104.04 117.39 6.74 o -7 -3 2 374.94 431.48 20.04 o -6 -3 2 394.44 404.43 18.08 o -5 -3 2 549.13 533.96 29.66 o -4 -3 2 0.86 7.33 1.24 o -3 -3 2 156.62 136.67 7.10 o -2 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