#------------------------------------------------------------------------------ #$Date: 2025-01-22 03:24:03 +0200 (Wed, 22 Jan 2025) $ #$Revision: 297402 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/37/1573730.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573730 _journal_paper_doi 10.1039/D4NJ04028G _chemical_formula_moiety 'C16 H13 N3 O3, C H4 O' _chemical_formula_sum 'C17 H17 N3 O4' _chemical_formula_weight 327.33 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2019/3 _audit_update_record ; 2025-01-17 deposited with the CCDC. 2025-01-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 97.446(8) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.7501(10) _cell_length_b 8.9510(7) _cell_length_c 21.2255(13) _cell_measurement_reflns_used 4699 _cell_measurement_temperature 294.98(11) _cell_measurement_theta_max 38.0110 _cell_measurement_theta_min 2.9830 _cell_volume 1648.4(3) _computing_cell_refinement 'CrysAlisPro 1.171.41.92a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.41.92a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.41.92a (Rigaku OD, 2020)' _computing_molecular_graphics 'WINGX v2020.1 (Farrugia, 2022)' _computing_publication_material 'WINGX v2020.1 (Farrugia, 2022)' _computing_structure_refinement 'SHELXL-2019/2 (Sheldrick, 2019)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 294.98(11) _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0872 _diffrn_reflns_av_unetI/netI 0.0760 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 14101 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 24.992 _diffrn_reflns_theta_max 24.992 _diffrn_reflns_theta_min 2.988 _diffrn_source 'micro-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 0.096 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.35328 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.92a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.319 _exptl_crystal_description needle _exptl_crystal_F_000 688 _exptl_crystal_size_max 0.48 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.253 _refine_diff_density_min -0.265 _refine_diff_density_rms 0.053 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.024 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 231 _refine_ls_number_reflns 2904 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.024 _refine_ls_R_factor_all 0.0959 _refine_ls_R_factor_gt 0.0652 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0929P)^2^+0.3568P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1633 _refine_ls_wR_factor_ref 0.1817 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1993 _reflns_number_total 2904 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4nj04028g2.cif _cod_data_source_block SB8 _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1573730 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL shelxt_a.res in P2(1)/n shelx.res created by SHELXL-2019/3 at 10:31:01 on 09-Jan-2025 CELL 0.71073 8.7501 8.9510 21.2255 90.000 97.446 90.000 ZERR 4.00 0.0010 0.0007 0.0013 0.000 0.008 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N O UNIT 68 68 12 16 MERG 2 OMIT -4.00 50.00 FMAP 2 PLAN 20 ACTA BOND LIST 4 L.S. 10 TEMP 22.00 WGHT 0.092900 0.356800 FVAR 0.77565 O3 4 0.519090 0.694860 0.856953 11.00000 0.08184 0.07130 = 0.02995 -0.00974 0.00188 -0.02803 O1 4 0.360410 0.307691 0.571494 11.00000 0.07538 0.05228 = 0.04629 0.01076 -0.00670 0.01001 N2 3 0.333224 0.544509 0.532284 11.00000 0.03990 0.04560 = 0.02451 -0.00165 -0.00224 0.00340 O2 4 0.356527 0.558746 0.756131 11.00000 0.07639 0.09377 = 0.03805 -0.01895 0.01154 -0.03800 O4 4 0.204935 0.558455 0.858051 11.00000 0.06085 0.07176 = 0.06004 -0.01527 0.00388 -0.00277 N1 3 0.161860 0.606648 0.442137 11.00000 0.04426 0.04476 = 0.03325 0.00063 0.00134 0.00543 N3 3 0.454153 0.600977 0.577512 11.00000 0.04591 0.05417 = 0.03194 -0.00305 -0.00213 0.00140 C1 1 0.268118 0.644341 0.487431 11.00000 0.04038 0.04411 = 0.02991 -0.00051 0.00466 0.00513 C8 1 0.114192 0.457976 0.437492 11.00000 0.03614 0.04983 = 0.03386 -0.00525 0.00547 0.00449 C10 1 0.430186 0.580943 0.634966 11.00000 0.03833 0.05093 = 0.03318 -0.00493 0.00081 0.00386 AFIX 43 H10 2 0.343639 0.527367 0.642901 11.00000 -1.20000 AFIX 0 C13 1 0.574903 0.702831 0.800148 11.00000 0.05067 0.04823 = 0.03401 -0.00351 -0.00332 -0.00239 C11 1 0.533529 0.639015 0.688243 11.00000 0.03692 0.05296 = 0.03382 -0.00560 -0.00350 0.00704 C2 1 0.295752 0.392944 0.531398 11.00000 0.05192 0.04035 = 0.03446 0.00149 0.00895 0.00806 C3 1 0.177792 0.350738 0.480210 11.00000 0.03951 0.04459 = 0.03114 -0.00342 0.00529 0.00367 C12 1 0.487650 0.632805 0.748732 11.00000 0.04617 0.04838 = 0.03721 -0.00298 -0.00114 -0.00244 C7 1 0.002031 0.416209 0.387926 11.00000 0.04021 0.06330 = 0.04647 -0.00776 -0.00090 0.00528 AFIX 43 H7 2 -0.042290 0.487436 0.359304 11.00000 -1.20000 AFIX 0 C16 1 0.670032 0.714098 0.680020 11.00000 0.04251 0.07617 = 0.03956 -0.01073 0.00592 0.00231 AFIX 43 H16 2 0.702505 0.718182 0.640034 11.00000 -1.20000 AFIX 0 C9 1 0.321535 0.802578 0.492990 11.00000 0.05871 0.04626 = 0.05093 0.00244 0.00133 0.00149 AFIX 137 H9A 2 0.265411 0.860928 0.459763 11.00000 -1.50000 H9B 2 0.429620 0.806854 0.489258 11.00000 -1.50000 H9C 2 0.303959 0.841809 0.533528 11.00000 -1.50000 AFIX 0 C14 1 0.707482 0.776989 0.790621 11.00000 0.04684 0.06547 = 0.04609 -0.01450 -0.00700 -0.00439 AFIX 43 H14 2 0.765662 0.824713 0.824537 11.00000 -1.20000 AFIX 0 C4 1 0.130192 0.201584 0.473028 11.00000 0.06082 0.04588 = 0.05204 -0.00303 0.01040 -0.00074 AFIX 43 H4 2 0.172999 0.129771 0.501705 11.00000 -1.20000 AFIX 0 C15 1 0.755485 0.781275 0.730555 11.00000 0.04073 0.08399 = 0.05222 -0.01379 0.00422 -0.01050 AFIX 43 H15 2 0.846414 0.830268 0.724858 11.00000 -1.20000 AFIX 0 C5 1 0.020611 0.161172 0.423809 11.00000 0.05816 0.05449 = 0.07073 -0.01497 0.01212 -0.00948 AFIX 43 H5 2 -0.010785 0.062128 0.418888 11.00000 -1.20000 AFIX 0 C6 1 -0.042834 0.268973 0.381543 11.00000 0.04203 0.07741 = 0.06017 -0.02431 0.00224 -0.00522 AFIX 43 H6 2 -0.117154 0.241455 0.348210 11.00000 -1.20000 AFIX 0 C17 1 0.054585 0.534481 0.829844 11.00000 0.06631 0.12277 = 0.12502 -0.04919 -0.00318 -0.01419 AFIX 137 H17A 2 -0.010966 0.519435 0.862222 11.00000 -1.50000 H17B 2 0.051310 0.447597 0.803185 11.00000 -1.50000 H17C 2 0.019547 0.619848 0.804637 11.00000 -1.50000 AFIX 0 H2O 2 0.567217 0.750594 0.886296 11.00000 0.07574 H1O 2 0.333811 0.575943 0.796172 11.00000 0.08767 H3O 2 0.194351 0.651344 0.880512 11.00000 0.12290 HKLF 4 REM shelxt_a.res in P2(1)/n REM wR2 = 0.1817, GooF = S = 1.024, Restrained GooF = 1.024 for all data REM R1 = 0.0652 for 1993 Fo > 4sig(Fo) and 0.0959 for all 2904 data REM 231 parameters refined using 0 restraints END WGHT 0.0929 0.3568 REM Highest difference peak 0.253, deepest hole -0.265, 1-sigma level 0.053 Q1 1 0.1570 0.6450 0.8292 11.00000 0.05 0.25 Q2 1 0.1319 0.4690 0.3961 11.00000 0.05 0.19 Q3 1 0.1102 0.6755 0.4273 11.00000 0.05 0.19 Q4 1 0.4240 0.6572 0.6177 11.00000 0.05 0.19 Q5 1 0.3382 0.2782 0.6085 11.00000 0.05 0.19 Q6 1 0.2989 0.6017 0.6308 11.00000 0.05 0.19 Q7 1 0.1789 0.3422 0.5138 11.00000 0.05 0.17 Q8 1 0.6890 0.6807 0.8095 11.00000 0.05 0.17 Q9 1 -0.0661 0.2512 0.4138 11.00000 0.05 0.16 Q10 1 0.1591 0.5476 0.3824 11.00000 0.05 0.16 Q11 1 0.3472 0.8972 0.4211 11.00000 0.05 0.15 Q12 1 0.1411 0.1828 0.4277 11.00000 0.05 0.15 Q13 1 0.0477 0.6909 0.8444 11.00000 0.05 0.15 Q14 1 -0.0106 0.5419 0.3203 11.00000 0.05 0.15 Q15 1 0.2222 0.5360 0.5739 11.00000 0.05 0.15 Q16 1 0.0250 0.0088 0.4179 11.00000 0.05 0.15 Q17 1 0.4086 0.3662 0.7072 11.00000 0.05 0.15 Q18 1 0.3788 0.4700 0.7241 11.00000 0.05 0.14 Q19 1 -0.1655 0.6279 0.3213 11.00000 0.05 0.14 Q20 1 0.1308 0.6425 0.4836 11.00000 0.05 0.14 ; _shelx_res_checksum 25606 _shelx_hkl_file ; 0 0 -3-0.18112 1.90656 2 0 0 -3 1.00890 2.86214 8 0 0 -4 593.035 55.8822 2 0 0 -4 696.390 56.3027 8 0 0 -5 1.88635 4.26195 2 0 0 -5-0.64095 5.92832 8 0 0 -6 57.1984 8.91230 2 0 0 -6 92.3857 9.96159 8 0 0 -7 5.20137 5.19029 2 0 0 -7 2.04902 5.36881 8 0 0 -8 106.130 13.2232 2 0 0 -8 125.399 13.5668 8 0 0 -9 5.59128 5.45787 2 0 0 -9-2.90595 6.28117 8 0 0 -10 585.836 60.5504 2 0 0 -10 757.706 60.7941 8 0 0 -11 20.6701 7.04944 2 0 0 -11-3.29436 7.15562 8 0 0 -12 15.4630 6.52330 2 0 0 -12 5.83935 6.47411 8 0 0 -13 14.6431 6.34917 2 0 0 14 170.194 14.7458 3 0 0 -14 105.105 16.7392 2 0 0 -15 16.6459 7.53387 2 0 0 15-0.32637 1.84916 3 0 0 16 449.780 33.6389 3 0 0 16 409.094 34.9450 7 0 0 17-1.84445 2.63231 3 0 0 -17-20.7400 13.5155 2 0 0 -18 359.037 56.7382 2 0 0 18 837.901 56.1111 3 0 0 19-0.80236 2.74540 3 0 0 -19-13.1717 12.0902 2 0 0 20 39.8256 5.74044 3 0 0 -20 5.44478 10.6614 2 0 0 21 2.60330 3.37209 3 0 0 -21-4.64536 10.9160 2 0 0 -22 53.5424 15.7415 2 0 0 22 149.097 13.3973 3 0 0 23-0.49638 4.03733 3 0 0 -23-8.88036 11.9937 2 0 0 -24 22.9428 11.9720 2 0 0 24 75.7206 9.23155 3 0 0 25 2.58025 4.80992 3 0 0 -25 7.08333 10.2265 2 0 0 26 27.2864 7.66494 3 0 0 -26 2.05653 9.94064 2 0 0 27 1.34733 4.88115 3 0 0 -27-1.01135 10.6460 2 0 0 -28 25.6298 13.8864 2 0 0 28 94.9029 10.7295 3 0 0 29 7.71485 4.77751 3 0 0 -29 5.20335 11.4878 2 0 0 -30 4.22196 10.5651 2 0 0 30 0.52348 3.94199 3 0 0 30 6.48278 3.96424 10 0 0 -31 14.9088 11.6477 2 0 0 31 1.03721 4.37914 3 0 0 31 4.31945 3.80430 10 0 0 -32 11.8046 11.1481 2 0 0 32 4.85461 4.12076 10 0 0 32-1.04213 3.70906 3 0 0 33-1.55175 7.76557 9 0 0 33 2.10975 3.92703 10 0 0 33 1.54492 4.00257 3 0 0 34 3.95653 7.93633 9 0 0 34 6.29504 4.39204 3 0 0 -34 11.8375 10.9367 2 0 0 35 0.77897 7.94406 9 0 0 35 0.53114 4.47424 3 0 1 -2 63.2293 6.46429 7 0 1 2 63.0996 5.86217 6 0 -1 -2 49.0754 6.12498 2 0 -1 2 72.7816 5.96986 2 0 -1 3 3183.23 236.066 2 0 -1 -3 2300.15 236.126 2 0 -1 -4 95.7077 12.0752 2 0 -1 4 140.519 11.7020 2 0 1 -5 218.014 23.8312 8 0 -1 -5 211.501 23.3484 2 0 1 -6 124.771 14.8318 8 0 -1 -6 105.547 13.9660 2 0 1 -7 490.776 49.8862 8 0 -1 -7 398.941 49.1129 2 0 1 -8 69.5742 10.8478 8 0 1 8 59.6560 10.8517 8 0 -1 -8 66.2544 9.76478 2 0 -1 8 88.4096 8.73731 2 0 1 -9 172.337 19.6880 8 0 -1 -9 154.584 18.8268 2 0 -1 -10 12.3177 6.51752 2 0 1 -10 4.15442 7.35475 8 0 1 10 2.98947 7.35458 8 0 -1 -11 7.99352 6.27760 2 0 1 -11 1.25057 8.06659 8 0 -1 11 1.60651 6.74936 7 0 -1 -12 276.495 35.1820 2 0 -1 12 492.820 35.7161 7 0 -1 13 361.602 30.0071 7 0 -1 13 314.020 28.1507 3 0 -1 -14 45.2126 9.59154 2 0 -1 14 57.5244 6.35956 3 0 -1 14 46.7395 7.91323 7 0 -1 15 26.8144 4.14459 3 0 -1 -15 19.0180 8.76314 2 0 -1 -16 189.571 31.6499 2 0 -1 16 420.594 30.5041 3 0 -1 17 5.34131 2.68932 3 0 1 18 181.971 18.0055 7 0 -1 18 178.067 16.1118 3 0 -1 -19 2.64448 10.8729 2 0 1 19 15.2382 7.82981 7 0 -1 -20 38.2328 12.3958 2 0 -1 20 92.6214 9.47040 3 0 -1 -21 59.6270 16.1995 2 0 -1 21 175.055 14.5227 3 0 -1 -22 37.3820 13.1761 2 0 -1 22 110.424 10.7701 3 0 -1 -23 0.94979 10.0570 2 0 -1 23 7.37987 3.64046 3 0 -1 -24-4.82588 10.4332 2 0 -1 24 7.78923 4.47841 3 0 -1 -25 9.83163 10.6765 2 0 -1 25 28.7784 6.70904 3 0 -1 -26 14.9608 11.6112 2 0 -1 26 45.6826 9.57243 3 0 -1 -27 8.09975 11.3493 2 0 -1 27 14.7048 6.14416 3 0 -1 -28 15.3919 11.4462 2 0 1 28 10.7912 3.51494 10 0 -1 28 14.2042 5.44436 3 0 1 29 1.89710 3.22139 10 0 -1 -29 6.24796 10.5709 2 0 -1 29 1.09365 4.48103 3 0 1 30 18.7923 4.32261 10 0 -1 30 22.8575 5.25427 3 0 1 31 15.3215 4.18277 10 0 -1 31 15.5169 4.96008 10 0 -1 31 17.5638 5.13353 3 0 -1 32 4.63368 7.35972 9 0 -1 32 6.90656 4.34245 10 0 -1 -32 2.14466 10.0420 2 0 -1 32 6.04948 4.21810 3 0 -1 33-1.58323 8.04021 9 0 -1 33 1.58736 4.20538 10 0 -1 -33 5.37602 10.2813 2 0 -1 33 7.14915 4.56792 3 0 1 34-1.53384 7.71534 9 0 -1 34-0.79663 7.57874 9 0 -1 34 1.20715 4.40793 10 0 -1 34 6.24208 4.38995 3 0 -1 -34 12.6330 10.2256 2 0 -1 35 9.47980 5.09888 3 0 1 35 4.60045 7.86319 9 0 -1 35-5.57182 8.12460 9 0 2 0 1855.02 158.364 9 0 -2 0 1848.62 159.509 5 0 -2 1 6692.29 569.947 9 0 -2 1 6915.54 570.277 7 0 -2 -1 6253.15 570.554 5 0 2 -2 65.1556 6.36739 2 0 -2 -2 63.2982 6.51132 2 0 2 -2 58.2425 7.55482 7 0 -2 -2 60.6849 6.65010 5 0 -2 -2 61.8921 7.64247 6 0 -2 -3 385.062 30.2922 5 0 2 -3 348.988 31.1810 7 0 -2 -3 279.238 30.4658 2 0 2 -3 313.154 30.5579 2 0 -2 -3 394.849 30.6569 6 0 -2 -4 405.879 35.3230 5 0 -2 -4 406.663 35.4820 6 0 2 -4 337.023 35.9653 2 0 -2 -4 326.893 35.8693 2 0 2 5 2737.58 192.967 8 0 2 -5 1677.86 192.222 2 0 -2 -5 1575.05 192.175 2 0 2 5 2889.21 192.211 2 0 -2 -5 2403.36 191.748 6 0 2 6 320.164 28.5560 8 0 -2 -6 226.050 27.5567 2 0 2 -6 249.252 27.7831 2 0 -2 -6 295.326 26.6576 6 0 2 -7 258.544 28.7996 2 0 -2 -7 283.066 28.9204 2 0 2 7 377.079 30.6564 8 0 -2 7 343.664 28.6631 7 0 2 8 28.5427 8.07754 8 0 2 -8 43.4799 7.24907 2 0 -2 -8 31.4477 6.48396 2 0 -2 8 24.2380 6.32635 7 0 -2 -9 423.807 48.9539 2 0 2 -9 463.760 49.2597 2 0 2 9 666.812 51.7863 8 0 -2 9 700.189 49.3440 7 0 -2 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34.3759 6.52270 3 0 -5 20 25.8687 5.10441 3 0 5 -20 7.73579 10.6333 2 0 -5 -20 11.6160 8.58269 2 0 5 21 49.0726 6.76446 3 0 -5 21 47.1850 6.14768 3 0 5 -21 7.91716 11.1929 2 0 -5 -21 7.92479 9.74588 2 0 5 22 20.9038 4.24628 3 0 -5 22 15.5118 3.82078 3 0 5 -22 12.1365 10.6470 2 0 -5 -22 7.28297 8.29693 2 0 -5 -23 14.9155 9.53250 2 0 5 -23 13.2540 11.4962 2 0 -5 23 11.6727 3.63147 3 0 5 23 8.30929 3.38355 3 0 -5 23 10.3560 5.44494 9 0 5 -24 7.62379 11.3322 2 0 -5 -24 10.1702 9.08133 2 0 5 24 4.38002 3.21254 3 0 -5 24 5.64146 3.32966 3 0 -5 24-4.01077 5.39697 9 0 -5 -25 1.76832 8.71977 2 0 5 -25 14.6757 12.2471 2 0 5 25 4.22002 3.36965 3 0 -5 25 2.84133 3.08126 3 0 -5 25-3.00615 5.62798 9 0 5 -26 1.79642 11.8865 2 0 -5 -26 12.5808 10.7480 2 0 -5 26 4.72219 3.26477 3 0 5 26 3.08055 3.41644 3 0 -5 26 5.57919 5.64719 9 0 -5 -27 10.9448 10.8674 2 0 -5 27 1.85105 3.01874 3 0 5 27 1.57058 3.29291 3 0 -5 27 1.27162 5.78380 9 0 5 -28 17.5193 13.1111 2 0 -5 -28-5.53535 9.36506 2 0 5 28 1.19585 3.21939 3 0 -5 28 2.66534 3.16575 3 0 -5 28-1.98493 6.25800 9 0 -5 -29 8.37995 10.9016 2 0 5 29 4.49197 3.69418 3 0 -5 29-0.78781 3.25405 3 0 -5 29-0.67868 6.31476 9 0 -5 -30 21.5715 11.1863 2 0 5 -30 25.3053 12.8153 2 0 5 30 9.26243 4.16712 3 0 -5 30 2.02536 3.50282 3 0 -5 30 5.57448 6.61254 9 0 5 -31 20.8732 13.0650 2 0 -5 -31 10.4527 10.1805 2 0 5 31 6.03970 3.95444 3 0 -5 31 1.25274 3.60020 3 0 -5 31-3.56084 7.02684 9 0 -5 -32 19.2363 10.3826 2 0 5 -32 11.5272 12.4164 2 0 5 32 9.60200 6.74180 9 0 -5 32 6.52428 7.64968 9 0 -5 -33 8.72790 10.1011 2 0 5 -33 19.3657 13.6555 2 0 5 33 3.88327 6.56095 9 0 -5 33 2.20535 7.53470 9 0 -5 33 16.3458 6.05305 10 0 -6 0 49.8849 18.6280 5 0 6 0 40.5586 8.35626 7 0 6 0 36.7062 7.32339 5 0 6 -1 98.4603 12.4561 5 0 6 1 102.267 11.5524 5 0 6 1 108.634 12.4591 7 0 6 -1 79.8810 12.3910 7 0 6 2 69.9729 9.45638 5 0 6 -2 61.9691 11.1354 7 0 6 2 76.9995 10.0447 7 0 6 3 165.317 17.4482 5 0 6 -3 164.075 20.6802 5 0 6 -3 199.101 18.5355 8 0 6 3 182.095 18.2528 7 0 -6 -4 128.964 11.8057 10 0 -6 -4 126.871 12.0468 4 0 6 4 139.288 14.3687 7 0 6 4 133.403 13.8352 5 0 6 4 125.313 15.7733 6 0 6 -4 151.106 20.6079 5 0 6 4 151.732 11.7909 9 0 -6 4 142.530 12.3297 9 0 6 -4 147.350 15.4297 8 0 -6 -4 152.249 12.4974 2 0 -6 -4 123.091 11.7536 1 0 6 -4 134.440 11.8262 1 0 6 5 106.293 8.87352 9 0 -6 5 101.248 9.42335 9 0 -6 -5 95.4601 8.98553 1 0 6 -5 100.046 9.06695 1 0 6 -5 111.280 18.7951 5 0 6 5 91.2229 11.1106 7 0 6 5 100.576 12.0803 6 0 6 -5 111.691 13.1156 8 0 -6 -5 102.181 10.4090 2 0 6 -5 102.027 10.5163 2 0 -6 -5 99.0532 8.84235 10 0 -6 6 102.587 8.88841 9 0 6 -6 76.4156 12.4161 8 0 6 6 98.2358 10.4503 7 0 6 6 105.441 11.5258 6 0 6 -6 102.558 8.43065 1 0 -6 -6 87.2627 8.30428 1 0 6 -6 99.4408 20.4052 5 0 -6 -6 88.7547 7.99295 10 0 6 -6 92.1157 10.8184 2 0 -6 -6 92.4529 10.2236 2 0 6 -7 163.404 21.3843 8 0 6 7 232.673 20.0682 8 0 6 7 196.883 20.1837 6 0 6 7 225.770 19.3652 7 0 6 -7 219.932 29.1452 5 0 6 7 200.642 17.6043 3 0 -6 -7 185.684 17.7286 1 0 -6 -7 187.065 19.1789 2 0 6 -7 204.625 19.5079 2 0 -6 7 207.532 18.2585 9 0 6 -7 218.753 17.8452 1 0 6 -8 23.5991 7.35776 2 0 -6 -8 21.7219 6.40090 2 0 6 -8 32.0443 20.6988 5 0 6 8 13.3183 1.72921 3 0 -6 8 14.8648 1.70506 3 0 -6 8 13.3748 2.75136 9 0 6 8 6.41129 6.26015 8 0 -6 -8 11.1540 2.14426 1 0 6 -8 12.6794 2.43336 1 0 6 8 22.5352 4.46700 7 0 6 8 9.24413 5.78435 6 0 -6 9 243.667 22.2320 9 0 -6 9 252.308 21.5674 3 0 6 9 279.413 21.6973 3 0 -6 -9 219.848 21.6727 1 0 6 -9 257.169 21.8078 1 0 6 9 232.578 24.5445 8 0 -6 -9 189.983 23.2112 2 0 6 -9 233.266 23.7961 2 0 6 9 256.202 22.7738 7 0 6 -10 48.6273 9.96802 2 0 -6 -10 42.6054 9.11354 2 0 -6 10 58.1875 5.27687 3 0 6 10 50.2004 10.0202 8 0 6 10 57.3255 6.74359 7 0 6 -10 52.6393 5.50163 1 0 -6 -10 47.1784 5.45095 1 0 -6 10 62.0653 6.27931 9 0 -6 11 2.33195 2.59476 9 0 6 11 8.60105 3.65829 7 0 6 -11 7.70537 8.24039 2 0 -6 -11 6.97709 6.82801 2 0 6 11 12.6073 7.95765 8 0 -6 11 4.95311 1.39439 3 0 -6 -11 1.56381 1.96796 1 0 6 12 154.665 11.9021 3 0 -6 12 135.786 11.5788 3 0 6 -12 84.1965 14.7570 2 0 -6 12 108.570 12.1191 9 0 6 12 119.633 12.2698 7 0 -6 -12 78.2204 13.9415 2 0 6 12 118.020 15.8763 8 0 -6 -13 33.7759 8.81135 2 0 6 -13 34.4807 9.89012 2 0 6 13 56.0646 6.36839 7 0 -6 13 42.8376 6.35009 9 0 -6 13 56.1594 5.59228 3 0 6 13 56.6138 5.77534 3 0 6 -14 34.9133 9.88518 2 0 -6 -14 24.1374 8.05973 2 0 6 14 39.6506 5.23912 7 0 -6 14 32.1055 5.39400 9 0 -6 14 34.0185 4.32882 3 0 6 14 45.0082 4.78613 3 0 -6 -15 6.72510 7.16353 2 0 6 -15 2.78685 8.98079 2 0 -6 15 6.58019 3.58566 9 0 6 15 4.65840 3.26564 7 0 6 15 9.18453 2.58670 3 0 -6 15 6.39496 2.12081 3 0 -6 -16 4.17437 7.46031 2 0 6 -16 10.0929 9.31040 2 0 -6 16-2.82495 3.83043 9 0 6 16 1.52561 3.19834 7 0 6 16 0.50090 2.22392 3 0 -6 16 2.11631 2.12951 3 0 6 -17 15.1344 9.85538 2 0 -6 -17 1.26533 7.14704 2 0 -6 17 5.74616 2.31386 3 0 6 17 4.07208 2.41804 3 0 -6 17 0.37778 3.62703 9 0 6 17 2.60984 3.30155 7 0 -6 18 2.82158 3.89191 9 0 6 18 7.60611 3.69084 7 0 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12.4167 2 0 -6 25 1.14601 5.39398 9 0 -6 26-0.65588 2.99216 3 0 6 26 5.14125 3.10797 3 0 6 -26 21.8066 12.4333 2 0 -6 -26 14.2806 9.69699 2 0 -6 26 1.78316 5.68739 9 0 6 27 11.7704 3.57765 3 0 -6 27 8.21764 3.55482 3 0 -6 -27 11.0668 10.0988 2 0 -6 27-1.85823 5.71209 9 0 6 28 6.27436 3.56583 3 0 -6 28 6.03049 3.43170 3 0 -6 -28 13.8812 9.81013 2 0 -6 28 7.66025 6.32523 9 0 6 29 10.7143 4.08161 3 0 6 -29 22.0650 12.4569 2 0 -6 -29 20.3514 11.0670 2 0 -6 29 1.96619 6.18827 9 0 6 30 2.40605 5.99285 9 0 -6 30 2.03051 6.49677 9 0 -6 -30 25.1646 11.2234 2 0 6 -30 26.8851 12.9985 2 0 -6 31-2.07082 6.88442 9 0 -6 -31 18.1836 10.7260 2 0 6 -31 10.8800 12.4884 2 0 -6 32-0.70990 7.10316 9 0 -6 -32-0.91860 11.8427 2 0 6 -32 9.16195 14.3388 2 0 7 0-3.62229 8.81182 7 0 7 0-4.07287 6.67905 5 0 7 1 7.95603 7.48931 7 0 7 -1 3.05378 8.41394 7 0 7 -1 10.3950 5.61413 8 0 7 1 7.46075 6.34528 5 0 7 -1 13.0094 7.24268 5 0 7 -2 63.0653 10.3943 5 0 7 2 44.2179 11.2426 6 0 7 -2 51.2719 11.3738 7 0 7 2 54.7670 10.4372 7 0 7 -2 52.7162 8.59359 8 0 7 2 35.3917 7.85682 5 0 7 3 24.3195 10.0462 6 0 7 3 22.4629 5.89370 5 0 7 -3 49.8244 10.9312 5 0 7 3 22.8107 8.38661 7 0 7 -3 23.8776 7.47091 8 0 -7 -4 149.389 13.0024 10 0 7 -4 117.006 19.3751 5 0 7 4 140.061 17.8332 6 0 7 4 149.300 15.3526 5 0 7 4 173.509 17.5008 7 0 7 -4 129.922 16.5927 8 0 7 5 391.918 34.1271 6 0 -7 -5 350.924 30.5678 10 0 7 5 379.436 33.9707 7 0 7 -5 323.397 34.1901 8 0 7 -5 374.621 37.1873 5 0 7 -6 255.512 29.3306 8 0 7 6 305.087 26.6525 8 0 7 6 322.045 28.9830 6 0 7 6 319.377 29.0103 7 0 7 -6 300.557 33.5556 5 0 7 -6 311.627 26.1160 2 0 -7 -6 295.473 26.2591 2 0 -7 -6 268.802 25.3312 10 0 7 6 313.971 25.3229 9 0 -7 6 295.514 26.1140 9 0 -7 -6 283.142 25.5090 1 0 7 -6 304.180 25.5863 1 0 -7 -7 84.2887 8.79164 1 0 7 -7 95.2619 8.95279 1 0 7 7 102.241 12.3199 7 0 7 7 98.9318 12.5474 6 0 -7 7 105.636 9.48514 9 0 7 7 103.282 8.49893 9 0 7 -7 85.5274 10.8347 2 0 -7 -7 85.7339 10.4824 2 0 7 7 82.7179 10.6374 8 0 7 8 76.3258 9.75288 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39.8442 7 -1 3 5 453.725 39.8383 6 1 -3 -5 456.261 38.5357 10 -1 3 5 436.355 39.4966 7 -1 3 4 807.781 69.0925 6 1 3 -4 759.631 68.6673 7 1 -3 -4 756.913 68.9269 5 1 -3 -4 757.527 67.9043 1 1 3 -4 795.029 67.9358 1 1 -3 -4 762.422 67.8434 3 1 3 -4 787.883 67.8389 3 -1 -3 4 759.463 68.0312 9 1 -3 -4 871.093 67.8009 10 1 -3 -3 492.536 49.5690 5 1 3 -3 449.420 50.0161 5 -1 3 3 569.088 48.2314 1 -1 -3 3 559.452 48.2467 1 -1 3 3 576.006 49.8080 6 1 -3 -3 565.755 48.5024 7 1 3 -3 529.274 48.9470 7 1 3 -3 500.536 48.3628 1 1 -3 -3 484.269 48.3372 1 1 3 -3 505.100 48.4078 9 -1 -3 3 500.327 48.4451 9 1 -3 -3 630.537 48.2752 3 1 -3 -2 706.760 62.0295 5 1 3 -2 698.981 61.4669 5 -1 3 2 720.378 60.1270 1 -1 3 2 766.386 61.8055 6 1 -3 -2 735.592 60.6158 7 1 -3 -2 644.132 60.2548 1 -1 -3 2 715.569 60.1497 1 1 3 -2 645.311 60.2755 1 1 3 -2 724.121 60.3128 9 1 -3 -2 706.748 60.0415 3 1 3 -2 703.755 60.0360 3 1 3 -1 172.095 16.4922 2 -1 -3 1 203.190 19.4213 5 1 -3 -1 186.455 19.8800 5 1 3 -1 187.969 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20.8553 2.41720 9 1 5 -2 20.9590 3.04941 4 -1 5 1 80.7142 9.80875 5 1 5 -1 66.7197 8.48421 5 1 -5 -1 83.9239 15.2280 5 1 5 -1 68.0648 6.57171 9 -1 5 1 81.0302 11.8254 6 -1 -5 1 88.2225 15.9516 5 1 5 0 68.0297 8.82353 5 -1 5 0 101.245 11.7970 5 -1 -5 0 84.2005 14.5162 5 1 5 0 79.2367 7.54369 9 1 -5 0 78.2306 16.7083 5 -1 5 0 92.5702 14.1619 6 1 -5 0 92.7160 8.55157 7 1 5 0 95.8908 8.96025 7 1 5 0 96.1457 12.6827 6 -1 -5 0 80.2661 7.50609 10 1 5 1 62.5463 7.80090 5 -1 5 -1 66.3008 12.2040 5 -1 -5 -1 62.3226 12.4402 5 -1 5 -1 82.0659 8.47712 8 1 5 1 70.0925 6.45405 9 1 -5 1 66.9598 6.27124 9 -1 -5 -1 67.4095 6.33844 10 1 -5 1 71.5780 7.67574 7 1 5 1 82.6285 11.2952 6 1 5 1 83.9406 7.93153 7 -1 -5 -2 80.3701 7.35452 10 1 -5 2 88.3125 7.43190 9 -1 5 -2 76.6821 9.65439 8 1 -5 2 89.3690 8.99141 7 1 5 2 82.5739 10.8026 6 1 5 2 72.7893 8.50581 5 -1 5 -2 77.0792 14.8701 5 -1 -5 -2 88.9892 12.1948 5 -1 5 -2 82.9166 7.62064 1 -1 -5 -2 83.6640 7.59587 1 1 5 2 66.6295 7.82173 2 1 -5 2 81.7698 7.62705 2 1 -5 3 54.5466 4.93329 9 -1 5 -3 47.5963 7.68532 8 1 -5 3 45.7597 5.25345 2 1 5 3 58.3658 8.43260 6 -1 -5 -3 71.1333 8.76650 5 -1 5 -3 39.6529 13.6942 5 1 5 3 34.9398 5.43596 2 -1 -5 -3 51.1924 5.74885 4 -1 5 -3 55.4138 6.04325 4 -1 -5 -3 49.3240 4.66862 10 -1 -5 -3 53.6974 6.10068 2 -1 5 -3 54.8833 6.11431 2 -1 5 -4 30.4595 5.89313 2 -1 -5 -4 29.3175 5.72406 2 1 5 4 16.7375 6.13615 6 -1 -5 -4 42.5490 6.86741 5 -1 5 -4 34.3784 14.8366 5 1 -5 4 23.1066 3.59595 2 1 5 4 17.9772 3.82705 2 -1 5 -4 24.7830 6.60194 8 -1 -5 -4 25.8250 2.55225 10 1 5 5 47.3587 6.41385 6 -1 5 -5 51.6495 8.08762 2 -1 -5 -5 49.7259 7.41644 2 -1 -5 -5 45.6354 7.10971 5 -1 5 -5 52.5581 18.5442 5 -1 -5 -5 43.1784 3.91987 10 -1 5 -5 50.6694 8.38927 8 1 5 5 33.4883 5.25461 2 1 -5 5 32.1495 4.99837 2 1 5 6 98.8898 11.1355 6 -1 -5 -6 106.538 11.4900 5 -1 -5 -6 103.661 12.0088 2 -1 5 -6 99.0300 12.3804 2 -1 5 -6 92.3973 12.8604 8 1 -5 6 108.686 10.6161 2 1 5 6 106.085 10.8373 2 1 5 7 31.4520 5.74673 6 -1 5 -7 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1 1 6 -5-12.5098 5.55177 2 1 -6 -5-8.66210 5.24030 2 -1 6 5-4.67949 4.81010 5 -1 6 4 23.8796 6.49964 5 1 6 -4 25.1068 10.4695 5 1 6 -4 27.8338 3.95090 1 1 -6 -4 23.6531 4.39142 2 1 6 -4 27.6079 4.76449 2 1 -6 -4 21.1651 3.28170 4 1 -6 -4 29.8439 3.45169 1 -1 6 3-4.69139 5.98666 5 1 6 -3 25.0989 7.29694 5 -1 6 2 484.548 40.8540 5 1 6 -2 447.218 40.1974 5 1 6 -2 408.743 40.5678 7 1 6 -1-1.86851 4.03761 7 -1 6 1 6.42704 7.24391 5 1 6 -1-2.29920 5.17183 5 -1 6 0 76.9260 13.6840 6 1 6 0 74.3327 11.6280 6 -1 6 0 59.8037 9.20478 5 1 6 0 17.5657 5.54980 5 1 6 0 25.9113 5.49290 7 -1 -6 0 34.6434 16.4536 5 1 6 0 25.4830 2.96556 9 -1 -6 0 24.5936 2.86081 10 -1 -6 -1 82.5653 16.0965 5 1 6 1 57.8567 7.95758 5 -1 6 -1 75.0607 12.6883 5 1 6 1 99.2243 12.3424 6 1 6 1 66.6745 8.02753 7 1 6 1 65.8520 6.05641 9 -1 -6 -1 59.6067 5.98440 10 -1 6 -2 22.6215 5.59828 8 1 6 2 26.1964 4.67355 7 1 6 2 20.8808 4.86555 5 1 6 2 21.0977 7.94068 6 -1 6 -2 0.61672 12.6317 5 -1 -6 -2 12.8727 13.1956 5 -1 -6 -2 20.8335 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1.67563 9 -1 -6 -5 3.06729 0.83554 10 1 -6 6 19.0263 2.76665 9 1 6 6 12.4510 5.45506 6 -1 -6 -6 25.9312 6.75318 2 -1 6 -6 21.1750 7.58731 2 -1 6 -6 20.1852 19.3836 5 1 -6 6 16.8024 2.09630 3 -1 6 -6 6.53135 6.58300 8 1 6 6 15.6132 2.18769 3 -1 -6 -6 17.9752 1.82418 10 1 -6 7 39.5753 4.60191 9 -1 6 -7 45.3222 9.21687 2 -1 -6 -7 41.6164 8.06768 2 1 6 7 32.4080 6.73935 6 1 -6 7 44.5752 4.14592 3 1 6 7 34.9671 4.10669 3 -1 6 -7 31.1984 8.39651 8 1 6 8 1.27687 1.44257 3 1 -6 8 2.37897 1.36768 3 -1 6 -8-1.18692 8.52544 2 -1 -6 -8 5.24631 6.98637 2 -1 -6 -9 80.4432 11.8645 2 -1 6 -9 80.9579 12.6651 2 1 -6 9 89.4839 8.37081 3 1 6 9 86.4815 8.47123 3 -1 -6 -10 219.184 26.9164 2 -1 6 -10 222.347 27.3353 2 1 -6 10 316.449 25.2372 3 1 6 10 349.905 30.4163 8 1 -6 11 14.0042 2.52391 3 -1 -6 -11-0.83246 7.97432 2 -1 6 -11 4.50582 10.0866 2 -1 -6 -12 451.999 49.0924 2 -1 6 -12 433.960 49.3968 2 1 6 12 600.640 48.0612 3 1 -6 12 598.548 47.9231 3 -1 -6 -13 164.688 19.9562 2 -1 6 -13 167.076 20.6047 2 1 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22 64.9754 8.91783 3 1 6 22 43.6502 7.38394 3 -1 6 -22 60.5079 13.1063 2 1 6 23 37.7280 8.19368 3 1 -6 23 36.0974 6.61366 3 -1 -6 -23 36.7830 10.7823 2 -1 6 -23 53.6132 13.4590 2 1 -6 24 7.39364 3.99416 3 1 6 24 11.7487 5.20743 3 -1 -6 -24 29.3647 10.4311 2 -1 6 -24 41.6645 13.3737 2 1 -6 25 4.04034 3.54449 3 1 6 25 3.32187 4.36022 3 1 -6 25-0.61622 5.61777 9 -1 6 -25 25.9913 13.0916 2 -1 -6 -25 32.5269 10.7943 2 1 6 26 7.46693 3.84159 3 1 -6 26 5.02247 3.77446 3 1 -6 26 7.70567 6.35586 9 -1 6 -26-3.32984 13.4474 2 -1 -6 -26 15.9281 10.3712 2 1 6 27 1.25483 3.54923 3 1 -6 27 2.30813 3.43626 3 1 -6 27 0.65743 6.41739 9 -1 -6 -27 0.85685 12.0364 2 -1 6 -27-7.70426 14.5201 2 1 -6 28 5.83167 3.50109 3 1 6 28 6.22529 3.84392 3 1 -6 28 9.54477 6.70347 9 -1 -6 -28-5.24731 11.7678 2 -1 6 -28-12.2269 15.1178 2 1 6 29 11.2791 4.16757 3 1 -6 29 14.4888 4.16059 3 1 -6 29 13.8355 7.24881 9 -1 -6 -29-9.80044 12.3967 2 -1 6 -29-0.88937 14.7813 2 1 6 30 7.54391 4.19804 3 1 -6 30 5.56244 3.90465 3 1 -6 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8.44372 6.94964 2 -1 7 13 21.7177 2.56068 9 1 -7 -13 12.6676 7.09846 2 1 7 -13 20.1210 8.91006 2 -1 -7 13 22.6292 4.16958 9 1 -7 -12 49.5937 10.7324 2 1 7 -12 56.9647 11.8647 2 -1 -7 12 99.7681 9.47930 9 -1 7 12 92.3878 7.91894 9 1 7 -12 96.9007 24.3557 5 -1 7 11 137.969 11.7830 9 -1 -7 11 153.968 13.3679 9 1 -7 -11 132.966 12.7286 1 1 7 -11 112.481 15.0959 2 1 -7 -11 94.8203 14.4748 2 1 7 -11 165.254 25.8242 5 -1 -7 10 153.924 12.7629 9 1 7 -10 158.735 24.3665 5 1 -7 -10 122.588 12.0507 1 1 7 -10 143.354 12.3134 1 1 -7 -10 93.5393 13.7750 2 1 7 -10 102.968 14.3835 2 1 7 -9 165.549 23.5055 5 1 -7 -9 107.547 14.6778 2 1 7 -9 131.093 15.2535 2 1 -7 -9 145.751 13.2299 1 1 7 -9 163.856 13.4387 1 -1 -7 9 140.028 13.6764 9 1 7 -8 41.3031 7.65891 2 1 -7 -8 32.4490 6.72269 2 1 7 -8 44.9814 16.7459 5 1 7 -8 45.7497 5.15724 1 1 -7 -8 42.4050 4.76324 1 -1 -7 8 40.5188 5.08397 9 1 -7 -7 49.4085 7.39489 2 1 7 -7 61.0772 7.82345 2 1 -7 -7 53.2780 5.84769 1 1 7 -7 64.6680 6.23055 1 1 7 -7 49.2679 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116.489 25.3065 5 1 -7 7 111.936 11.6706 9 -1 7 -7 122.333 11.1831 1 -1 -7 -7 105.533 11.0866 1 1 7 7 138.031 13.0652 7 1 7 7 89.4808 13.6830 6 -1 -7 -7 109.180 12.5779 4 1 7 7 173.664 11.5109 3 1 -7 7 144.836 11.1271 3 -1 -7 -8 20.5529 7.20787 2 -1 7 -8 19.0252 7.71273 2 -1 7 -8 37.1896 21.9285 5 1 -7 8 19.2388 3.30220 9 1 7 8 31.6252 5.37550 7 1 7 8 13.3670 6.17004 6 1 -7 8 29.8974 2.84385 3 1 7 8 23.6972 2.82151 3 -1 7 -8 17.5639 2.76116 1 -1 -7 -8 15.4730 2.49086 1 -1 -7 -9 15.5872 7.25319 2 -1 7 -9 15.9049 8.53751 2 1 7 9 14.6862 2.32002 3 1 -7 9 14.4383 3.00797 9 -1 -7 -9 8.64906 2.13492 1 -1 7 -9 13.1103 2.41571 1 1 7 9 18.7727 4.68084 7 -1 7 -9 26.1800 22.0193 5 1 -7 9 26.9125 3.08140 3 1 7 10 19.5017 4.56030 7 -1 -7 -10 18.7822 7.08140 2 -1 7 -10 16.6332 8.36843 2 1 7 10 1.40601 8.60175 8 1 -7 10 12.2262 3.26037 9 1 -7 10 24.3825 2.89333 3 -1 7 -10 21.5717 24.8347 5 -1 -7 -10 13.1275 2.42394 1 -1 -7 -11 80.1665 8.97142 1 1 7 11 128.809 10.7556 7 -1 7 -11 107.653 29.8155 5 1 -7 11 149.088 9.91930 3 -1 7 -11 65.3753 12.9112 2 -1 -7 -11 61.0910 12.1243 2 1 -7 11 87.4749 9.79214 9 1 7 12 21.9723 3.21117 3 1 -7 12 24.5330 3.48672 3 1 -7 12 17.9649 3.96198 9 -1 7 -12 11.9484 9.60543 2 -1 -7 -12 7.15546 7.85580 2 1 7 13 69.9101 6.85253 3 1 -7 13 76.7404 7.16930 3 -1 -7 -13 40.0579 10.2034 2 -1 7 -13 35.9640 11.6327 2 1 -7 13 52.3654 7.24278 9 1 7 14 123.996 11.0546 3 1 -7 14 157.323 11.5068 3 1 7 14 96.1782 17.9651 8 -1 -7 -14 64.1474 13.4562 2 -1 7 -14 59.9623 14.5025 2 1 -7 14 89.0950 11.1107 9 1 7 15 40.8697 4.85691 3 1 -7 15 37.5573 4.91430 3 1 -7 15 26.0238 5.28494 9 -1 7 -15 12.9150 10.7338 2 -1 -7 -15 10.9539 9.15044 2 1 7 15 16.8758 13.1118 8 1 7 16 2.13914 10.8073 8 1 7 16 4.47409 3.69921 7 1 -7 16-2.60173 3.81440 9 -1 7 -16-9.27669 11.1580 2 -1 -7 -16-3.31361 8.94923 2 1 -7 16 4.14086 3.64296 3 1 7 16 6.35117 3.05944 3 1 7 17 6.61623 11.8156 8 1 7 17 7.66927 3.81330 7 1 -7 17 8.14962 4.13469 3 1 7 17 4.11425 2.95284 3 -1 -7 -17-9.87227 9.41544 2 1 -7 17 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16.3804 14.0391 2 1 -7 25 30.2899 4.89616 3 1 7 25 31.2548 5.21202 3 1 -7 25 22.8525 6.91937 9 -1 7 -26 0.80188 14.0330 2 -1 -7 -26 3.22144 11.6174 2 1 -7 26 1.62202 2.94081 3 1 7 26 3.14365 3.48597 3 1 -7 26 7.23743 6.29713 9 -1 7 -27-4.06961 13.7099 2 -1 -7 -27-10.7331 11.5079 2 1 7 27 10.9677 3.78635 3 1 -7 27 16.6351 4.12911 3 1 -7 27-3.72702 6.11079 9 -1 7 -28 3.32573 14.1540 2 -1 -7 -28-6.68514 11.5680 2 1 7 28 6.14439 3.70126 3 1 -7 28 3.77501 3.19169 3 1 -7 28 1.92740 6.31115 9 -1 7 -29 2.52070 14.3119 2 -1 -7 -29 1.68815 11.5156 2 1 -7 29 8.44585 3.71858 3 1 7 29 6.67969 3.86472 3 1 -7 29 5.25634 6.84994 9 -1 7 -30-10.2298 14.3469 2 -1 -7 -30-5.14260 12.1399 2 1 7 30 9.09467 4.14455 3 1 -7 30 7.36015 7.15548 9 -1 7 -31-2.57278 14.2015 2 -1 -7 -31-4.33406 11.5646 2 1 8 -31-8.02197 15.1869 2 1 8 -30 3.17651 13.8106 2 -1 -8 30 3.91310 6.37326 9 -1 -8 29 3.79882 6.31534 9 -1 -8 29 8.52372 5.89421 10 1 -8 -28 19.6660 9.38450 2 1 8 -28 30.1417 13.4050 2 -1 -8 28 7.36534 6.76501 9 1 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153.068 14.1922 6 2 2 2 168.769 14.0255 10 -2 -2 -2 142.581 13.9872 10 2 -2 3 386.942 36.6505 2 -2 -2 -3 459.916 37.2074 2 2 2 3 408.683 36.8440 2 -2 2 -3 459.829 37.2267 2 -2 -2 -3 413.434 35.7855 6 -2 -2 -3 386.164 35.3517 10 2 2 3 414.673 35.3440 10 -2 -2 -4 691.453 59.8687 2 -2 2 -4 683.771 59.8793 2 2 -2 4 684.270 59.6603 2 2 2 4 699.710 59.8110 2 -2 -2 -4 680.526 58.6058 6 2 2 4 663.089 58.1868 10 2 -2 5 216.841 19.5628 2 -2 -2 -5 179.490 18.9986 2 -2 2 -5 204.885 19.5122 2 2 2 5 235.348 19.8178 2 2 -2 5 225.465 20.7755 8 -2 -2 -5 181.436 17.1780 6 2 2 5 184.604 16.7920 10 2 -2 6 325.696 29.7057 2 -2 -2 -6 290.156 29.0223 2 2 2 6 308.166 29.6655 2 -2 2 -6 316.003 29.2264 2 2 -2 6 334.012 31.1531 8 -2 -2 -6 289.886 27.2860 6 2 2 6 320.882 26.9843 10 2 2 7 579.456 48.0324 10 -2 2 -7 519.309 50.1724 2 -2 -2 -7 520.164 50.0203 2 2 -2 7 526.112 50.9610 2 2 2 7 548.209 51.1431 2 2 -2 7 540.614 52.2637 8 2 2 8 275.601 27.8390 2 -2 2 -8 287.880 27.0491 2 -2 -2 -8 263.768 26.4480 2 2 -2 8 237.353 27.7379 2 2 -2 8 318.222 29.9256 8 -2 -2 -9 27.2849 7.49588 2 -2 2 -9 29.9366 8.06723 2 2 -2 9 44.7066 10.5289 2 2 -2 10 125.699 18.6760 8 2 -2 10 134.334 17.9627 2 -2 2 -10 133.697 15.4275 2 -2 -2 -10 131.231 15.4410 2 -2 2 -11 58.4764 10.9501 2 -2 -2 -11 60.8756 10.2878 2 2 -2 11 34.3355 12.0226 8 2 2 12 192.232 22.0914 8 2 -2 12 153.944 21.7506 8 -2 -2 -12 140.368 18.0249 2 -2 2 -12 160.066 17.8948 2 -2 2 -13 20.8711 9.65313 2 -2 -2 -13 11.8281 8.71480 2 2 -2 13-1.42881 10.3856 8 2 2 13 6.50176 10.6052 8 -2 2 -14 22.4720 10.3345 2 -2 -2 -14 25.9803 9.06042 2 2 -2 14 31.4329 12.9541 8 2 2 14 19.5107 13.0720 8 -2 -2 -15 58.7364 11.7846 2 -2 2 -15 62.5469 12.5949 2 2 2 15 57.4702 16.6141 8 2 -2 15 42.0320 15.6441 8 -2 2 -16 31.1101 10.8493 2 -2 -2 -16 19.4109 9.68091 2 2 -2 16 22.8053 13.8587 8 2 2 16 14.7935 15.3767 8 2 2 17 425.752 41.5829 8 2 -2 17 516.589 42.0087 8 -2 -2 -17 247.613 29.9528 2 -2 2 -17 271.695 30.3129 2 2 2 18 143.946 25.9288 8 -2 2 -18 122.461 16.7983 2 -2 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4.68828 2.10002 10 2 -3 -22 10.9229 8.54629 2 -2 -3 22 0.44476 3.77521 9 -2 3 22 4.33954 3.84307 9 -2 3 22 1.93327 2.18393 3 -2 -3 22 1.62586 2.31894 3 -2 3 22 0.85876 1.74222 10 2 3 -21-1.27419 8.33635 2 2 -3 -21 1.27771 7.24047 2 -2 3 21-1.01260 3.45109 9 -2 -3 21 7.53733 3.90248 9 -2 -3 21 5.33032 2.41300 3 -2 3 21 2.07011 2.05589 3 -2 -3 20 96.0325 9.35457 3 -2 3 20 113.206 9.58042 3 2 -3 -20 32.9551 12.8425 2 2 3 -20 35.2672 13.5756 2 -2 -3 20 97.9109 10.5295 9 -2 -3 19 32.6880 4.33453 3 -2 3 19 37.1430 4.46782 3 -2 -3 19 37.2313 5.72399 9 2 -3 -19 20.8534 8.89039 2 2 3 -19 33.4692 10.8920 2 2 3 -18 8.88996 8.43976 2 2 -3 -18 3.28486 7.50669 2 -2 3 18 6.39934 1.80742 10 -2 -3 18 6.89275 3.62147 9 -2 -3 18 6.97266 2.33328 3 -2 3 18 10.5138 2.24892 3 -2 3 17 96.0885 8.01583 3 -2 -3 17 80.8212 7.80619 3 -2 3 17 72.8320 7.34322 10 -2 -3 17 78.7288 8.74854 9 2 -3 -17 43.1692 10.9465 2 2 3 -17 37.8502 11.7221 2 -2 3 16 151.640 12.8918 3 -2 -3 16 155.119 12.9028 3 -2 3 16 134.779 12.4089 10 -2 -3 16 150.950 13.7422 9 2 -3 -16 58.1202 15.0737 2 2 3 -16 88.9980 16.0666 2 -2 3 15 342.561 29.8150 10 -2 3 15 374.253 30.2187 3 -2 -3 15 367.239 30.1912 3 2 -3 -15 201.014 32.3392 2 2 3 -15 205.482 32.4418 2 -2 -3 15 391.911 31.0753 9 2 3 -14-2.83992 5.64396 2 2 -3 -14-2.86065 5.68514 2 2 -3 -14-0.53707 5.89687 8 -2 3 14 2.54521 1.24720 3 -2 -3 14 1.52775 2.11725 9 -2 3 14 0.40250 1.12622 10 2 3 -13 22.3268 5.88334 2 2 -3 -13 15.9875 5.37976 2 -2 3 13 28.2593 2.96274 10 -2 -3 13 29.3583 3.95481 9 2 -3 -13 18.7134 6.69828 8 2 -3 -12 51.7593 8.68558 2 2 3 -12 50.6901 8.54279 2 2 -3 -12 55.4855 9.88660 8 -2 -3 12 83.4243 7.64673 9 -2 3 12 81.3938 7.21870 9 2 3 -12 61.1964 10.2633 7 -2 3 12 74.6059 6.72042 10 -2 3 11 149.493 13.5139 10 2 -3 -11 125.046 16.0442 8 2 3 -11 136.031 16.0932 7 -2 -3 11 157.493 14.2414 9 -2 3 11 167.095 13.8408 9 2 -3 -11 136.881 15.2962 2 2 -3 -11 156.872 14.0923 1 -2 3 10 1.09278 0.79391 10 -2 3 10 1.29799 1.26888 9 2 3 -10-2.92774 4.94923 7 -2 -3 10 0.90077 1.66003 9 2 -3 -10 2.58626 5.27462 8 2 -3 -10 3.24743 1.94445 1 2 -3 -9 50.1815 4.99162 1 2 3 -9 52.1687 5.12391 1 -2 -3 9 49.1897 4.97677 9 -2 3 9 49.7307 4.37864 9 2 3 -9 40.6123 6.28298 7 2 -3 -9 34.9207 4.46102 3 2 3 -9 39.5082 4.52716 3 2 -3 -9 34.4560 7.07627 8 -2 3 9 42.8998 4.20519 10 2 -3 -8 29.9593 3.67581 1 2 3 -8 32.3818 3.92151 1 -2 3 8 30.3624 3.05887 9 -2 -3 8 32.0117 3.67030 9 -2 3 8 28.4447 2.99864 10 2 -3 -8 29.9287 2.84728 10 2 -3 -8 29.9731 3.25023 3 2 3 -8 28.4451 3.21869 3 2 -3 -8 19.9241 5.93343 8 2 3 -8 26.8828 4.80746 7 2 3 -7 9.73868 3.36326 7 2 3 -7 2.91512 2.66234 1 -2 3 7 8.34212 1.69651 1 -2 -3 7 7.24599 1.70510 1 2 -3 -7 2.38713 2.31818 1 2 3 -7 5.63204 1.33146 3 2 -3 -7 7.63899 1.38896 3 -2 -3 7 7.19186 1.89456 9 -2 3 7 4.77525 1.18805 9 2 -3 -7 3.35200 4.17003 8 2 -3 -7 5.82334 1.01794 10 2 3 -6 558.502 50.3156 9 -2 -3 6 537.531 50.3807 9 2 -3 -6 558.440 50.8163 8 2 -3 -6 534.373 49.9810 7 2 3 -6 593.458 50.8990 7 -2 3 6 547.154 51.0795 5 -2 -3 6 568.758 50.1825 1 -2 3 6 591.284 50.1913 1 2 3 -6 687.948 50.1852 3 2 -3 -6 785.434 50.3814 3 2 -3 -6 550.951 49.9897 10 2 3 -6 540.636 50.3606 1 2 -3 -6 542.199 50.3376 1 2 -3 -5 1.23304 0.70290 3 2 3 -5 0.20103 0.59797 3 -2 3 5-1.59343 3.48387 6 2 -3 -5 0.84162 2.26236 7 -2 -3 5 0.98157 1.44962 1 -2 3 5 0.68841 1.46833 1 -2 3 5-2.02729 4.05979 5 2 3 -5 1.54495 2.58636 1 2 -3 -5 3.77443 2.26173 1 2 3 -5 0.51496 1.50053 9 2 -3 -5 0.51986 0.81121 10 -2 -3 5 1.48010 1.03606 10 2 3 -4 4.31342 1.57492 9 -2 3 4 1.37988 3.80358 6 2 -3 -4 4.28099 3.23996 7 -2 3 4 13.1423 1.86836 1 -2 -3 4 6.10268 1.68090 1 -2 3 4 0.53433 4.23670 5 2 -3 -4 7.01881 2.35264 1 2 3 -4 6.59054 2.63724 1 2 3 -4 6.28052 6.27621 5 2 -3 -4 7.84968 1.33620 10 -2 -3 4 6.01198 1.36507 10 -2 3 3 205.183 17.3048 6 -2 -3 3 168.730 15.3870 10 -2 3 3 197.726 17.2092 5 2 3 -3 171.100 15.9470 5 2 -3 -3 174.395 15.0040 9 2 3 -3 182.670 15.4901 9 -2 3 3 176.259 15.5084 1 2 -3 -3 158.821 15.6825 1 -2 -3 3 179.570 15.5183 1 2 3 -3 159.886 15.7616 1 -2 3 2 634.677 53.2630 6 2 3 -2 581.559 51.5902 5 -2 3 2 618.960 53.3729 5 -2 -3 2 584.113 51.6510 10 -2 -3 2 628.508 51.8453 1 2 3 -2 581.070 52.0002 1 2 -3 -2 563.171 51.9329 1 -2 3 2 610.329 51.8062 1 2 3 -2 633.589 51.7617 9 -2 3 1 81.4378 9.66428 6 2 3 -1 64.0621 6.01523 5 -2 -3 1 72.6966 8.47581 5 -2 3 1 72.5855 10.7266 5 2 3 -1 62.9836 7.27152 4 2 -3 -1 60.5067 7.11688 4 -2 -3 1 74.1002 6.61632 1 -2 3 1 65.3790 6.66712 1 -2 -3 1 62.9812 6.02949 10 2 -3 -1 51.7889 7.03309 2 2 3 -1 60.6143 7.35484 2 -2 -3 0 1489.49 122.382 5 -2 3 0 1602.56 125.260 5 -2 -3 0 1369.27 122.058 10 2 3 0 1511.34 121.933 10 2 -3 0 1331.87 122.556 4 2 3 0 1369.46 122.627 4 -2 -3 0 1476.21 122.483 1 -2 3 0 1482.91 122.453 1 -2 3 0 1430.95 124.067 6 2 3 0 1361.70 122.503 2 2 -3 0 1287.30 122.422 2 -2 -3 -1 1303.85 107.290 5 -2 3 -1 1265.05 110.540 5 2 3 1 1281.50 106.956 10 -2 -3 -1 1176.45 107.069 10 -2 3 -1 1290.23 107.643 4 -2 -3 -1 1251.01 107.618 4 -2 3 -1 1318.26 107.733 1 -2 -3 -1 1297.82 107.734 1 2 3 1 1133.68 107.797 6 2 -3 1 1197.50 107.670 2 2 3 1 1229.68 107.752 2 -2 3 -2 3307.03 287.484 5 -2 -3 -2 3490.71 283.839 5 2 3 2 3353.06 283.492 10 -2 -3 -2 3146.67 283.603 10 -2 -3 -2 3418.36 284.323 4 -2 3 -2 3409.77 284.305 4 2 3 2 3213.95 284.125 6 -2 3 -2 3399.95 284.371 2 -2 -3 -2 3373.33 284.420 2 2 -3 2 3244.65 284.330 2 2 3 2 3223.98 284.397 2 2 -3 2 3311.77 285.346 8 -2 -3 -3 226.246 19.6846 5 2 3 3 228.947 19.2359 10 -2 -3 -3 198.849 19.2919 10 -2 3 -3 245.651 21.0266 4 -2 -3 -3 220.164 20.7793 4 2 3 3 210.089 19.8957 6 -2 3 -3 241.367 21.2486 2 -2 -3 -3 223.738 21.0906 2 2 -3 3 239.578 20.9136 2 2 3 3 237.781 21.0931 2 2 -3 3 209.190 21.7770 8 -2 -3 -4 35.2101 6.11824 6 2 -3 4 15.5339 6.82718 8 2 3 4 24.8181 2.43762 10 -2 -3 -4 17.6957 2.41587 10 2 3 4 19.8581 3.38255 6 -2 -3 -4 28.9043 6.69893 2 2 -3 4 35.5210 6.80176 2 2 3 4 31.2699 7.56034 2 -2 3 -4 27.7092 7.70004 2 2 -3 5 24.6454 7.57771 2 2 3 5 25.7534 8.29972 2 2 3 5 20.9141 2.40427 10 -2 -3 -5 26.7184 5.15001 6 2 -3 5 19.1874 7.55335 8 -2 -3 -5 20.2786 7.25849 2 -2 3 -5 27.9055 7.98409 2 -2 -3 -6 161.180 16.0614 6 2 -3 6 169.413 19.8722 8 2 3 6 172.258 14.7497 10 -2 -3 -6 166.495 17.6643 2 -2 3 -6 152.655 17.8412 2 2 -3 6 153.518 18.2655 2 2 3 6 166.705 18.7311 2 -2 -3 -7 239.332 21.5235 6 2 -3 7 189.130 23.9532 2 -2 3 -7 230.781 23.5474 2 -2 -3 -7 211.502 23.1220 2 2 3 7 203.831 24.3656 2 2 -3 7 237.188 25.9187 8 2 3 7 244.385 20.4718 10 -2 3 -8 4.90897 8.63442 2 -2 -3 -8 4.91924 7.77730 2 2 3 8 18.2458 7.47695 2 -2 -3 -8 12.5344 3.84654 6 2 -3 8 11.3346 8.51269 8 2 3 8 13.4180 1.78324 10 -2 -3 -9 6.11116 3.30822 6 2 3 9 10.7981 1.57274 10 -2 3 -9 2.18835 9.28411 2 -2 -3 -9 3.06512 8.56830 2 2 -3 9 4.05780 8.35186 8 2 -3 10 33.4845 10.3426 2 -2 -3 -10 4.21868 3.57350 6 -2 3 -10 30.8229 9.83256 2 -2 -3 -10 35.9355 8.65768 2 2 -3 10 9.81637 9.03271 8 -2 -3 -11 10.0470 3.77385 6 -2 3 -11 27.2679 9.87811 2 -2 -3 -11 33.6634 9.35560 2 2 -3 11 12.8901 9.99126 8 2 3 11 11.4937 1.80846 10 2 -3 12 184.124 23.1258 8 -2 -3 -12 170.388 19.3091 2 -2 3 -12 173.807 20.0965 2 2 3 13 73.9900 15.3112 8 2 -3 13 82.4957 16.3181 8 -2 3 -13 78.3060 12.8154 2 -2 -3 -13 78.7094 12.6449 2 2 -3 14 6.92926 11.5071 8 2 3 14-2.82367 11.8024 8 -2 3 -14 19.1906 10.1804 2 -2 -3 -14 33.0878 9.59887 2 2 3 15-6.52547 13.7826 8 2 -3 15 1.46707 11.1604 8 -2 3 -15 18.8667 10.3775 2 -2 -3 -15 22.7292 8.77802 2 2 3 16 3.58427 14.9814 8 -2 -3 -16 17.3395 9.04297 2 -2 3 -16 29.6056 10.0519 2 2 3 17 74.0266 19.3080 8 -2 3 -17 59.8397 12.3610 2 -2 -3 -17 64.3969 11.9783 2 2 3 18 148.275 26.5067 8 -2 3 -18 122.021 17.5160 2 -2 -3 -18 134.318 16.7690 2 -2 3 -19 22.3885 11.6497 2 -2 -3 -19 36.0332 10.1914 2 2 3 19 26.9403 19.3329 8 -2 3 -20 38.3434 11.3502 2 -2 -3 -20 32.2573 10.7824 2 2 3 20 21.1372 18.3845 8 -2 -3 -21 18.7145 9.90394 2 -2 3 -21 24.2279 11.4012 2 2 3 21 15.0132 16.8703 8 -2 3 -22 46.6579 13.2680 2 -2 -3 -22 63.4273 12.5426 2 2 3 22 72.1640 9.65071 3 2 -3 22 71.7841 9.82011 3 -2 3 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2.91813 9 2 -4 -20 10.3467 7.77027 2 2 4 -20 14.8793 10.3420 2 -2 4 19 8.18135 3.17361 9 -2 -4 19 6.34713 3.80552 9 -2 4 19 2.62879 1.37437 10 2 -4 -19 8.12642 8.41761 2 -2 4 18 101.000 9.45671 10 -2 4 18 123.000 10.7237 9 -2 -4 18 126.333 11.6220 9 2 4 -18 58.5329 14.8369 2 2 -4 -18 65.4220 13.8482 2 -2 -4 17 3.92834 3.18317 9 -2 4 17 1.73228 1.15511 10 -2 4 17 1.32364 2.50460 9 2 -4 -17 9.33652 7.30580 2 2 4 -17 1.03090 7.93966 2 -2 4 16 53.4611 5.38809 10 -2 -4 16 69.3912 7.36087 9 -2 4 16 74.1959 6.63493 9 2 -4 -16 35.1914 9.99995 2 2 4 -16 36.6737 10.6943 2 -2 -4 15 0.56445 2.95779 9 -2 4 15 0.21471 0.96762 10 2 -4 -15-0.88099 5.95449 2 2 4 -15-0.87370 7.30891 2 -2 -4 14 4.99961 2.69987 9 -2 4 14 3.48830 1.04421 10 2 -4 -14 1.57420 5.71001 2 2 4 -14-1.55931 6.48351 2 -2 4 13 151.244 13.5840 10 -2 -4 13 167.431 14.8630 9 -2 4 13 190.085 14.2889 9 2 -4 -13 93.0818 16.2954 2 2 4 -13 109.871 16.7461 2 -2 -4 12 81.7319 7.45602 9 -2 4 12 78.1221 6.66360 9 2 4 -12 46.0777 10.1407 7 2 -4 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29.0455 7 -2 4 6 321.692 29.4639 5 -2 -4 6 318.005 27.9195 1 -2 4 6 338.627 27.9377 1 2 -4 -6 328.034 27.9244 3 2 4 -6 372.752 27.9855 3 2 -4 -6 307.342 27.8254 10 2 4 -6 297.852 28.2531 1 2 -4 -6 278.524 28.1470 1 2 4 -5 4.79532 1.84345 9 2 -4 -5 5.12471 1.30050 10 2 -4 -5 9.90960 1.44938 3 2 4 -5 9.11252 1.28606 3 -2 4 5 7.55165 4.53752 6 2 4 -5 7.39650 3.57816 7 2 -4 -5 6.50389 2.17210 7 -2 -4 5 7.46511 1.54965 1 -2 4 5 5.27834 1.56419 1 2 4 -5 12.0708 8.04309 5 -2 4 5-2.52332 5.15347 5 -2 -4 5 5.99920 1.41330 10 2 4 -5 9.92074 2.92821 1 2 -4 -5 7.75836 2.41626 1 -2 4 4 222.445 19.1487 6 2 -4 -4 184.724 17.1388 7 -2 4 4 181.602 18.4626 5 2 4 -4 180.174 18.4409 5 -2 -4 4 187.566 16.6669 1 -2 4 4 188.909 16.6424 1 2 4 -4 193.914 16.4279 3 2 -4 -4 194.596 16.4384 3 2 4 -4 200.369 16.8694 9 -2 -4 4 194.588 16.8161 10 2 -4 -4 165.049 16.9392 1 2 4 -4 168.299 17.0544 1 2 4 -3 558.135 49.8749 5 -2 4 3 550.127 51.0310 5 -2 4 3 579.501 49.2674 1 -2 -4 3 594.291 49.3105 1 2 4 -3 536.756 49.6131 1 2 -4 -3 513.287 49.5175 1 -2 -4 3 574.352 49.3953 10 2 4 -3 609.020 49.4554 9 2 -4 -3 556.540 50.0216 7 -2 4 3 694.640 51.9683 6 2 4 -2 1397.28 110.510 9 2 -4 -2 1245.91 111.426 7 2 4 -2 1294.48 110.638 5 2 4 -2 1179.76 110.605 2 -2 4 2 1482.51 112.765 6 2 4 -2 1212.59 110.759 4 2 -4 -2 1188.64 110.682 4 2 4 -2 1242.98 110.708 1 2 -4 -2 1226.56 110.659 1 -2 4 2 1347.50 110.389 1 -2 -4 2 1324.47 110.432 1 -2 -4 2 1335.74 110.447 10 2 -4 -1 411.316 38.0910 7 -2 4 1 534.677 39.7758 6 2 4 -1 436.333 36.7784 5 -2 -4 1 470.865 38.9134 5 2 4 -1 403.596 37.0481 2 2 -4 -1 380.787 36.8956 2 2 -4 -1 392.429 36.9868 4 2 4 -1 394.651 37.1051 4 -2 4 1 431.383 36.6769 1 -2 -4 1 439.539 36.7053 1 -2 -4 1 435.470 36.6037 10 -2 -4 0 71.8260 6.89927 10 -2 -4 0 75.7235 10.5094 5 2 -4 0 89.1943 8.48526 8 -2 -4 0 74.4888 7.52254 1 -2 4 0 68.3505 7.53468 1 2 -4 0 69.1231 8.36583 2 2 4 0 78.7643 8.83426 2 -2 4 0 88.6667 13.1528 6 2 4 0 86.5356 10.9089 6 2 -4 0 67.4973 9.70656 7 2 4 1 3175.50 264.215 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10.4893 2 2 4 4 91.0287 7.41266 10 -2 -4 -4 71.9537 7.49564 10 2 -4 4 81.9997 11.1446 8 -2 -4 -5 161.711 14.7357 5 2 4 5 160.673 13.6594 10 -2 -4 -5 149.512 13.8178 10 2 -4 5 165.820 17.5641 8 -2 4 -5 167.908 16.9754 2 -2 -4 -5 165.117 16.5351 2 2 -4 5 134.188 16.4628 2 2 4 5 149.526 17.0514 2 2 4 5 147.310 14.7350 6 -2 -4 -5 168.875 16.8894 6 -2 -4 -6 551.930 48.2148 5 2 -4 6 621.834 51.7447 8 2 4 6 567.460 47.2753 10 -2 4 -6 553.248 49.5848 2 2 -4 6 471.036 49.8826 2 -2 -4 -6 527.749 49.3797 2 2 4 6 424.787 49.8700 2 -2 -4 -6 565.748 49.1647 6 -2 -4 -7 1.16560 5.05113 6 2 -4 7 35.0274 8.05656 2 -2 4 -7 2.92952 8.86043 2 -2 -4 -7-5.93404 7.36126 2 2 4 7 4.42712 0.96375 10 2 -4 7 14.9350 8.10913 8 2 4 7 39.6873 8.93603 2 2 4 8 32.2647 7.53868 2 2 -4 8 50.0573 9.83852 2 -2 4 -8 27.4824 10.1154 2 -2 -4 -8 30.8962 8.96863 2 2 4 8 29.0167 2.91763 10 2 -4 8 35.2988 9.28276 8 -2 -4 -8 21.0279 6.57551 6 2 -4 9 26.0806 9.48610 2 -2 4 -9 19.2670 10.4696 2 -2 -4 -9 25.1358 9.30869 2 -2 -4 -9 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2 -2 4 -21 34.8503 11.6786 2 -2 -4 -21 27.0411 9.48217 2 2 -4 21 7.59500 4.44281 3 2 4 21 33.3317 18.5152 8 2 4 21 10.0713 4.60735 3 2 4 22 8.41727 18.2055 8 2 4 22-4.03321 4.98802 3 2 -4 22-5.03501 4.71614 3 -2 4 -22 23.0724 11.4221 2 -2 -4 -22 15.2185 9.14288 2 2 4 23 36.5646 19.9733 8 -2 -4 -23 54.2212 12.0584 2 -2 4 -23 60.9200 12.8476 2 2 4 23 38.4947 7.29016 3 2 -4 23 35.0990 7.06319 3 -2 4 -24 39.1380 13.2700 2 -2 -4 -24 29.7155 11.3944 2 2 4 24 26.3861 6.24763 3 2 -4 24 31.8989 6.39544 3 -2 4 -25-12.2047 14.1292 2 -2 -4 -25 1.74151 11.2673 2 2 4 25 5.37501 4.91085 3 2 -4 25 9.29074 5.13944 3 -2 4 -26-10.7745 14.1631 2 -2 -4 -26-12.5483 12.5279 2 2 -4 26-0.58651 4.51611 3 2 4 26 4.87471 4.84325 3 -2 4 -27 1.83533 14.7250 2 -2 -4 -27-2.74989 12.5516 2 2 4 27 22.4701 6.00674 3 2 -4 27 23.0774 6.15375 3 -2 4 -28 0.93748 14.7777 2 -2 -4 -28-0.93622 12.9434 2 2 4 28 17.0733 5.98139 3 2 -4 28 17.2595 6.22442 3 -2 4 -29-9.58367 15.5387 2 -2 -4 -29 12.4468 13.1972 2 2 4 29 7.96396 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13.2108 3.30760 1 -3 -6 1 22.5181 2.85015 10 -3 6 0 124.809 17.1074 6 3 6 0 118.354 14.2269 6 3 6 0 87.5898 11.8702 2 3 -6 0 100.554 11.1653 2 -3 -6 0 122.029 17.3856 5 -3 -6 0 97.1284 9.54748 1 -3 6 0 108.443 9.65010 1 -3 -6 0 85.9006 9.15539 10 -3 -6 -1 120.605 15.4797 5 -3 -6 -1 91.4454 9.31610 1 -3 6 -1 95.2335 9.43334 1 -3 -6 -1 79.2785 8.59091 10 3 -6 1 93.3100 10.7483 2 3 6 1 116.372 11.7338 2 3 6 1 85.6735 11.8756 6 -3 6 -1 138.573 18.4967 6 3 6 2 140.669 16.7350 6 -3 -6 -2 171.547 18.9038 5 3 6 2 185.550 17.2301 2 3 -6 2 170.916 16.3706 2 -3 -6 -2 164.548 15.5104 1 -3 6 -2 159.471 15.5692 1 -3 -6 -2 150.621 14.5818 10 3 -6 3 13.3295 6.86873 2 3 6 3 9.67987 8.24452 2 -3 -6 -3 23.0078 7.81900 5 -3 -6 -3 5.28263 1.59050 10 -3 6 -3 16.0020 6.14494 1 -3 -6 -3 7.13623 5.06254 1 3 -6 4 34.4482 8.91495 2 3 6 4 33.7583 10.2192 2 -3 -6 -4 38.3519 4.29650 10 -3 6 -4 37.8046 7.84095 4 -3 -6 -4 43.1191 7.22282 4 -3 -6 -4 57.2462 8.36696 5 3 6 4 40.3848 6.65050 6 -3 -6 -4 51.0946 8.03998 1 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2 -3 -6 -14 19.5777 10.4856 2 -3 6 -15 36.0688 13.7903 2 -3 -6 -15 26.9221 11.3406 2 3 6 15 57.2923 15.2118 8 -3 6 -16 76.1980 15.8623 2 -3 -6 -16 81.9904 13.9920 2 3 6 16 68.3751 19.0851 8 -3 6 -17 6.36031 12.6880 2 -3 -6 -17 11.9417 9.66234 2 3 6 17 13.0731 16.2857 8 -3 6 -18-0.72568 12.2044 2 -3 -6 -18 2.88215 9.99564 2 3 6 18-6.24512 17.2930 8 -3 6 -19-1.49967 13.1635 2 -3 -6 -19 19.3529 11.1556 2 3 6 19 2.18893 19.1962 8 -3 6 -20 40.6250 14.5657 2 -3 -6 -20 22.2448 11.8731 2 3 6 20 52.1268 22.8460 8 3 6 21-3.29406 4.91135 3 -3 6 -21-14.1986 15.0024 2 -3 -6 -21 2.36835 11.3899 2 3 6 21-11.3316 19.6084 8 3 6 22-3.93979 5.06157 3 3 -6 22-1.06353 4.57742 3 -3 6 -22-8.10352 14.2039 2 -3 -6 -22-9.73379 11.7558 2 3 6 22 2.26774 19.6199 8 3 6 23-1.68220 4.75549 3 3 -6 23 0.53699 4.58479 3 -3 6 -23 6.64837 15.0851 2 -3 -6 -23-0.83161 12.5147 2 3 6 23 15.7951 21.9094 8 3 6 24-0.56590 4.89825 3 3 -6 24-4.26205 4.87343 3 -3 6 -24 5.10434 14.6242 2 -3 -6 -24 11.0707 11.6041 2 3 6 24 2.24001 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3.83339 1 3 -7 -10-2.15300 4.89235 2 3 7 -10-4.58662 5.48085 2 3 7 -10 9.27070 8.87146 7 -3 -7 10 1.68413 2.10830 10 3 -7 -10 0.26931 0.76637 10 3 7 -9 4.46777 9.03551 5 3 -7 -9 0.80863 3.75352 1 3 -7 -9-1.78635 4.80576 2 3 7 -9-3.93094 4.65347 2 -3 -7 9 3.67017 2.15184 10 3 -7 -9 2.63475 1.03447 10 3 7 -9 7.50236 8.23795 7 3 7 -8 7.22025 7.11831 7 -3 7 8-1.27006 7.27418 6 3 -7 -8-3.49494 4.01536 1 3 7 -8 4.00841 4.35154 1 3 -7 -8-0.69724 3.41985 2 3 7 -8-4.88046 3.91556 2 3 -7 -8 0.68326 1.34746 10 -3 -7 8 1.74744 2.08800 10 3 7 -7 22.0669 6.85736 7 -3 7 7 30.9257 8.37844 6 3 7 -7 21.9341 5.63733 1 3 -7 -7 19.6215 4.80924 1 3 7 -7 21.1374 6.00289 5 3 -7 -7 16.0389 3.76400 2 3 -7 -7 17.4935 4.79777 4 3 7 -7 18.2961 5.44969 4 3 -7 -7 16.1296 2.49964 10 -3 -7 7 20.3833 3.11122 10 3 7 -6 65.1268 9.77914 7 -3 7 6 67.7322 10.9717 6 3 7 -6 59.3295 7.61937 5 3 7 -6 52.2998 7.92711 2 3 7 -6 53.8769 8.02280 4 3 -7 -6 49.4147 7.14734 4 3 7 -6 59.9808 7.84797 1 3 -7 -6 50.1584 6.98850 1 3 -7 -6 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4.27169 9 -4 -5 27 9.13883 6.08324 9 -4 -5 27 4.18235 4.75560 10 4 -5 -26 11.7541 11.0350 2 4 5 -26 24.8379 13.4382 2 -4 -5 26 5.25026 5.67104 9 -4 5 26 3.56998 4.08179 9 -4 -5 26-1.00111 4.01862 10 4 -5 -25 1.56818 9.79264 2 4 5 -25 18.7029 12.3041 2 -4 -5 25 6.68996 5.49485 9 -4 5 25 5.20525 3.90273 9 -4 -5 25 6.74894 4.33687 10 4 -5 -24 19.8875 11.2835 2 4 5 -24 22.8067 13.4894 2 -4 -5 24 18.0839 6.13844 9 -4 5 24 14.4505 4.12142 9 -4 -5 24 20.3811 4.93369 10 4 -5 -23 5.84188 9.87651 2 4 5 -23 11.6117 11.0890 2 -4 -5 23 4.55964 4.50720 9 -4 5 23 2.43660 3.39207 9 -4 -5 23 3.90861 3.64781 10 4 -5 -22 7.14143 9.76946 2 4 5 -22 18.4521 11.9704 2 -4 -5 22 30.8599 6.42218 9 -4 5 22 34.5878 4.89237 9 -4 -5 22 28.6724 5.42015 10 4 -5 -21-2.63475 8.71664 2 4 5 -21-11.7705 10.2376 2 -4 -5 21-1.37493 3.99982 9 4 -5 -20 3.62175 7.05017 2 -4 -5 20 14.4504 4.56201 9 4 -5 -19 1.08723 6.54151 2 4 5 -19 2.15808 8.04903 2 -4 -5 19 9.97397 4.27122 9 4 -5 -18-3.76842 6.63523 2 4 5 -18-8.40207 7.59162 2 -4 -5 18 1.97859 3.64305 9 4 -5 -17 5.57041 5.31247 2 4 5 -17 15.7751 7.03824 2 4 5 -17 20.7871 9.66872 7 -4 -5 17 20.9297 4.05955 10 -4 -5 17 25.1456 4.77184 9 4 -5 -16-3.45321 5.14205 2 4 5 -16-8.89652 6.03579 2 -4 -5 16 2.78684 2.66417 10 4 5 -16-4.32098 9.44983 7 -4 -5 15 89.3029 8.65615 10 4 -5 -15 51.1094 10.3248 8 4 5 -15 77.5648 13.1768 7 -4 -5 14 243.463 18.7276 10 4 5 -14 199.418 21.8957 7 -4 -5 13 151.976 13.4162 10 4 5 -13 154.568 16.2904 7 -4 -5 12 24.9230 3.97164 10 4 -5 -12 26.6477 2.80382 10 4 -5 -12 13.3680 6.30447 8 4 5 -12 26.9979 6.82666 7 4 -5 -11 1.83543 5.48858 8 -4 5 11 3.81026 2.47988 1 -4 -5 11 3.25562 2.44455 1 -4 -5 11-0.72925 1.94714 10 4 -5 -11-0.71275 1.28224 10 4 5 -11 0.88171 4.85936 7 4 5 -10 210.345 24.0150 5 -4 5 10 261.187 21.1600 1 -4 -5 10 251.399 21.2359 1 -4 -5 10 226.240 21.4203 10 4 -5 -10 243.880 20.7296 10 4 5 -10 251.121 22.8455 7 -4 5 9-1.38574 6.11420 5 4 5 -9 8.62331 7.63810 5 4 5 -9 12.0861 4.75501 7 4 -5 -9 6.28751 2.15307 7 4 -5 -9 3.20053 4.42185 8 -4 5 9 1.88000 2.23465 1 -4 -5 9 3.79936 2.41056 1 4 -5 -9 1.68824 1.46535 10 -4 -5 9 0.46027 1.93951 10 -4 5 8-0.79200 2.36917 1 -4 -5 8 2.00027 2.38796 1 4 -5 -8 2.23114 2.90684 7 -4 5 8 3.74117 5.72172 5 4 5 -8-2.30558 4.86742 5 -4 -5 8 0.65706 1.71505 10 4 -5 -8 0.69047 1.52955 10 4 -5 -7 8.75572 1.54507 3 4 -5 -7 8.17223 4.44282 7 -4 5 7 6.84472 5.55523 6 -4 -5 7 8.80242 2.18625 10 4 5 -7 11.6078 1.62814 3 -4 5 7 4.39278 7.75663 5 4 5 -7 11.6741 2.43355 5 4 -5 -7 5.82790 4.92626 1 -4 5 7 8.89935 2.69918 1 -4 -5 7 9.23685 2.80497 1 4 -5 -7 8.59763 1.94852 10 4 -5 -6 81.2506 7.12057 10 -4 -5 6 65.7771 7.13576 10 -4 5 6 59.6317 10.7998 5 -4 -5 6 67.0606 7.25599 1 -4 5 6 70.0258 7.24315 1 4 -5 -6 70.6825 8.62049 1 -4 5 6 76.9234 9.93589 6 4 -5 -6 48.5840 8.44771 7 -4 5 5-2.07479 6.56880 6 4 -5 -5-5.27778 6.26345 7 4 -5 -5 0.35346 1.67173 10 4 -5 -5 0.08609 0.78706 9 -4 5 5 4.20511 7.82498 5 4 -5 -5 3.77086 5.06412 1 4 -5 -5-1.64334 5.53397 4 -4 5 5 3.60304 2.90555 1 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7.96361 1 -4 5 -4 12.5613 9.79468 1 4 5 4 1.32771 1.36602 10 -4 -5 -4-1.74593 7.34324 4 -4 5 -4 12.8563 8.56403 4 -4 -5 -4-4.09770 4.31341 5 -4 5 -4-9.95372 23.2091 5 4 -5 4 19.7805 8.86134 2 -4 -5 -4-0.48564 1.46288 10 4 -5 5 219.419 27.2049 8 -4 5 -5 281.625 25.4188 4 -4 -5 -5 249.982 24.7290 4 -4 -5 -5 258.402 23.2244 5 -4 5 -5 262.118 38.9305 5 4 -5 5 262.715 25.5073 2 -4 5 -5 267.811 26.2065 2 -4 -5 -5 258.500 25.6012 2 -4 -5 -5 212.887 22.4365 10 4 5 5 280.846 22.3395 10 -4 -5 -6 287.794 26.4307 5 -4 5 -6 302.258 42.0805 5 4 5 6 300.552 25.5669 10 -4 5 -6 287.689 29.5441 2 -4 -5 -6 279.778 29.3262 2 4 -5 6 239.837 30.7253 8 -4 -5 -7 84.5871 9.32782 5 4 5 7 84.2988 7.81603 10 -4 -5 -7 66.7663 13.4269 2 -4 5 -7 87.2212 15.4929 2 4 -5 7 56.5001 14.6196 8 -4 5 -8 17.7195 12.9191 2 -4 -5 -8 14.8081 11.3508 2 4 -5 8 16.7613 11.3523 8 4 5 8 17.0302 2.43419 10 4 -5 9 12.7278 11.9417 8 -4 5 -9 17.3078 13.9437 2 -4 -5 -9 12.0811 11.2604 2 4 5 9 10.1348 2.01995 10 -4 -5 -9 38.5446 10.4579 6 4 -5 10 33.7143 14.7296 8 4 5 10 56.3013 5.57313 10 -4 5 -10 67.0716 15.3874 2 -4 -5 -10 52.7636 12.6646 2 4 -5 11 2.84346 11.6616 8 4 5 11 7.38123 1.93476 10 -4 5 -11 27.8694 14.1524 2 -4 -5 -11 12.6592 11.1668 2 4 -5 12 28.3187 13.8653 8 4 5 12 29.4322 3.51573 10 -4 5 -12 31.6034 13.6528 2 -4 -5 -12 44.3694 12.1314 2 4 -5 13 1.55790 13.5647 8 4 5 13 0.11707 1.53130 10 -4 5 -13 5.72368 13.4388 2 -4 -5 -13 3.56649 11.1412 2 4 -5 14 14.6412 13.8212 8 4 5 14 9.32527 2.10099 10 -4 5 -14 12.4970 13.0913 2 -4 -5 -14 16.2382 11.8520 2 4 5 15 86.3510 8.12699 10 -4 5 -15 78.6082 16.7545 2 -4 -5 -15 53.8059 14.8684 2 -4 5 -16 43.8092 14.8826 2 -4 -5 -16 21.0380 11.7625 2 4 -5 16 44.3299 16.7311 8 -4 5 -17 34.5201 14.2611 2 -4 -5 -17 23.1423 12.7055 2 4 5 17 38.5175 18.2960 8 -4 5 -18 31.2043 14.5429 2 -4 -5 -18 17.2504 12.1123 2 4 5 18 31.8775 19.6542 8 -4 5 -19 26.1698 14.7810 2 -4 -5 -19 20.1992 12.1509 2 4 5 19 23.1896 19.6292 8 -4 5 -20 6.05033 13.7988 2 -4 -5 -20 12.0867 12.9983 2 4 5 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34.6466 10.4166 6 -4 9 1 12.7597 16.2667 6 -4 9 0 20.1762 13.2056 5 4 9 0 26.9206 7.27638 7 4 9 0 17.8113 1.81885 3 -4 -9 0 9.22950 2.86412 10 4 9 0 3.33755 8.67642 6 -4 9 0-1.04928 14.9827 6 -4 9 -1 28.5440 12.8548 5 -4 9 -1 12.6341 14.3236 6 -4 -9 -1 5.68962 2.39217 10 4 9 1 26.4311 6.78190 7 -4 9 -1 8.65300 1.47496 1 -4 9 -2 10.8447 15.5303 6 4 9 2-13.8724 8.40007 6 -4 -9 -2 0.20359 1.65563 10 -4 9 -2 0.06178 1.45863 1 -4 -9 -2 1.52797 1.68264 1 4 9 2 6.39631 6.01473 7 -4 9 -3 2.27924 16.0864 6 4 9 3 0.96386 5.68170 6 -4 -9 -3 1.49962 1.66337 10 -4 9 -3 0.52133 1.98516 1 -4 -9 -3-0.75968 2.19017 1 4 -9 3-0.50165 1.30673 9 4 9 4 24.1845 6.99785 6 -4 9 -4 63.6414 18.6706 6 -4 9 -4 75.3042 19.0683 5 -4 -9 -4 34.2935 4.57074 1 -4 -9 -4 30.0797 4.21085 10 4 -9 4 40.9992 3.99569 9 -4 9 -4 38.4575 4.58647 1 -4 9 -5 21.4774 19.3361 6 4 -9 5 0.73052 1.71748 9 -4 -9 -5 0.80425 1.49952 10 -4 9 -5-2.61429 20.3761 5 4 9 5-0.44073 5.26904 6 -4 9 -5 3.01325 3.33617 1 -4 -9 -5 3.20663 3.04709 1 4 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46.2067 11.4220 1 -5 7 -8 25.4583 11.1518 1 -5 -7 -8 24.8564 10.0838 1 -5 -7 -9 22.1571 10.4386 2 -5 -7 -9 31.5149 10.5307 1 -5 7 -9 32.8769 12.3782 1 -5 7 -10 0.59826 12.1462 2 -5 -7 -10 3.12069 10.2978 2 -5 7 -11 8.36792 12.8649 2 -5 -7 -11 35.6045 11.5462 2 -5 7 -12-6.70675 13.0744 2 -5 -7 -12 4.81747 11.0866 2 -5 7 -13 7.06216 13.1271 2 -5 -7 -13 12.2483 11.7668 2 -5 7 -14 14.7493 14.6314 2 -5 -7 -14 25.6531 12.9849 2 -5 -7 -15 22.0355 13.4165 2 -5 7 -15 7.66880 15.3309 2 -5 7 -16 28.8829 16.2542 2 -5 -7 -16 12.2959 13.7650 2 5 7 17 17.9802 18.0208 8 -5 7 -17 24.1913 16.2015 2 -5 -7 -17 16.8289 14.3451 2 5 7 18 16.6368 19.3607 8 -5 7 -18 17.0971 16.6015 2 -5 -7 -18 1.72184 13.8432 2 5 7 19-9.21136 20.3085 8 -5 7 -19 5.23771 16.0113 2 -5 -7 -19 8.85456 13.8609 2 5 7 20 2.48036 21.9175 8 -5 7 -20 16.1304 17.0759 2 -5 -7 -20 24.1990 14.8796 2 5 7 21 13.3568 23.5515 8 -5 7 -21 30.7823 17.8616 2 -5 -7 -21 37.5574 15.2529 2 5 7 22 2.74999 25.0342 8 -5 7 -22 12.9231 16.5901 2 -5 -7 -22 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5 -6 31.9367 10.9203 4 -8 -5 6 36.4673 5.69437 10 -8 5 6 60.1973 13.5250 5 -8 5 6 58.2847 9.17173 1 -8 -5 6 47.1006 8.78718 1 -8 5 5 5.15729 11.6501 5 8 5 -5 9.14454 8.99797 4 8 -5 -5-3.96714 8.05836 4 -8 -5 5-1.74031 2.35334 10 -8 5 5 0.51126 6.76265 1 -8 -5 5-0.52076 6.90738 1 8 5 -5 18.4655 5.51935 6 -8 5 4 24.6472 13.0896 5 8 5 -4 4.17876 9.74679 4 8 -5 -4 13.6060 9.24517 4 -8 -5 4 7.09999 2.84717 10 -8 -5 4 7.07683 7.23086 1 -8 5 4 6.42196 7.67446 1 8 5 -4 7.73219 3.39679 6 -8 5 3 34.1828 14.0753 5 8 5 -3 12.7421 10.4998 4 -8 -5 3 23.6154 3.82792 10 8 5 -3 12.8235 2.18594 6 -8 5 3 22.5789 8.46647 1 -8 -5 3 33.5763 8.61753 1 -8 -5 2 2.99297 2.52570 10 -8 5 2 18.6945 15.8966 5 -8 5 2-1.60620 6.70028 6 -8 5 2-1.71739 7.82262 1 -8 -5 2 1.16197 7.64423 1 -8 -5 1 19.0519 3.90260 10 -8 5 1 41.8978 17.3990 5 -8 5 1 34.6876 8.01769 6 -8 5 1 24.1490 9.85139 1 -8 -5 1 30.5901 9.41515 1 -8 -5 0 2.58322 2.52476 10 -8 5 0 10.2538 19.1244 5 -8 5 0-1.15242 7.60628 6 -8 5 0 16.4810 9.86589 1 -8 -5 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38.6305 16.7503 1 8 -5 9 3.15710 13.8557 8 -8 5 -10 61.7749 41.5707 5 -8 5 -10 42.3911 15.4375 6 -8 5 -10 6.13699 16.3268 1 -8 -5 -10 6.07855 14.7526 1 8 -5 10-3.42947 15.0645 8 -8 5 -11 61.4073 42.8497 5 -8 5 -11 76.0351 18.0133 6 -8 -5 -11 39.3049 16.9854 1 -8 5 -11 23.7723 17.5930 1 8 -5 11 11.3171 16.0898 8 -8 5 -12 55.1482 43.8071 5 -8 5 -12 34.3795 17.5197 6 8 -5 12 2.08551 17.3827 8 -8 5 -12 26.8075 18.8065 1 -8 -5 -12 4.41474 15.8691 1 -8 -5 -13 19.3199 15.9632 1 -8 5 -13 62.2689 19.7057 6 8 -5 13 13.4086 19.0516 8 -8 5 -13 75.2462 46.4618 5 -8 5 -13 15.6888 17.4546 2 -8 -5 -13 5.28378 16.5865 2 -8 5 -14-7.48542 18.5668 2 -8 -5 -14-1.07900 16.1384 2 8 -5 14-7.12168 21.4541 8 -8 5 -15 31.7003 19.7278 2 -8 -5 -15 28.6826 17.5723 2 8 -5 15 5.01744 21.3606 8 -8 5 -16 10.0717 18.7057 2 -8 -5 -16 36.0854 18.8156 2 8 -5 16-2.58461 20.8997 8 -8 5 -17 18.1434 19.6965 2 -8 -5 -17 14.8482 17.8186 2 8 -5 17-10.5080 21.3688 8 -8 5 -18 11.5344 19.9866 2 -8 -5 -18 9.19946 17.2651 2 8 -5 18 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1.92442 14.1445 1 -8 6 -10 7.75293 16.3907 1 -8 6 -10 43.2686 17.3328 6 8 -6 10 5.67350 16.7119 8 -8 6 -10 23.9097 40.2946 5 -8 -6 -11 14.7808 14.5553 1 -8 6 -11 12.7950 16.1637 1 -8 6 -11 33.2685 18.4452 6 8 -6 11-1.99132 17.9246 8 -8 6 -11 20.2280 40.2124 5 -8 6 -12-10.5406 42.7024 5 -8 6 -12 42.9293 18.1788 6 -8 6 -12 19.4183 16.8958 1 -8 -6 -12 9.10388 16.1486 1 8 -6 12-10.5837 19.1578 8 -8 6 -13-13.7333 43.0109 5 -8 6 -13 52.6518 19.8723 6 -8 6 -13 23.6347 17.8142 1 -8 -6 -13 13.7207 16.6475 1 8 -6 13-4.39104 20.5862 8 -8 6 -14 76.3026 48.5362 5 -8 6 -14 97.5681 21.9860 6 8 -6 14 11.2381 19.8625 8 -8 6 -14 30.9744 19.4694 1 -8 -6 -14 29.4779 16.9146 1 -8 -6 -15 27.9858 16.7495 1 -8 6 -15 20.4234 19.7665 1 8 -6 15 18.3517 21.5496 8 -8 6 -15 83.5582 51.0920 5 -8 -6 -15 18.7926 16.1056 2 8 -6 16 11.6104 19.9692 8 -8 6 -16 61.5565 49.4711 5 -8 6 -16-1.05443 17.9884 2 -8 -6 -16 7.43122 16.7924 2 8 -6 17-2.36766 21.7728 8 -8 6 -17-4.27735 18.8301 2 -8 -6 -17 1.07958 16.0721 2 8 -6 18 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11.7683 1 -13 7 -4 3.74807 12.5008 1 -14 0 14 6.74396 9.20671 1 14 0 -14 11.3133 12.8049 4 -14 0 13 0.86901 9.10786 1 14 0 -13 2.06900 12.4079 4 -14 0 12 1.78850 9.61737 1 14 0 -12-2.06271 11.9012 4 -14 0 11 4.63107 9.79308 1 14 0 -11 22.4924 13.4415 4 -14 0 10 13.1963 10.9744 1 -14 0 9 3.93475 11.3146 1 -14 0 8 1.02086 11.6941 1 -14 0 7-10.5667 13.4118 1 -14 0 6-3.32042 13.0059 1 -14 0 5-12.5405 14.5205 1 -14 0 4 33.0937 15.8433 1 -14 0 3-7.24391 14.1971 1 -14 0 2-6.19772 14.3654 1 -14 0 1 13.9593 14.0383 1 -14 0 0-2.54184 14.7206 1 -14 0 -1 2.58752 15.2542 1 -14 0 -2 5.28858 15.0955 1 -14 0 -3 10.7970 16.4300 1 -14 0 -4 5.44865 16.6175 1 -14 0 -5 33.4324 17.1703 1 -14 -1 14 3.36002 8.96533 1 14 -1 -14 6.16661 12.2906 4 -14 -1 13-8.65799 9.91766 1 14 -1 -13 20.7377 13.6767 4 -14 -1 12 0.89087 9.54746 1 14 -1 -12 10.3001 12.4006 4 -14 -1 11 20.8066 11.0567 1 14 -1 -11 12.2603 12.7852 4 -14 -1 10 1.87744 10.2651 1 -14 -1 9 9.79472 10.7853 1 -14 -1 8 9.15297 12.0569 1 -14 -1 7-4.20709 12.2303 1 -14 -1 6 18.4012 13.4207 1 -14 -1 5 1.13435 12.8975 1 -14 -1 4 1.17580 13.4690 1 -14 -1 3-7.20517 14.3183 1 -14 -1 2 12.3270 14.8717 1 -14 -1 1 1.26267 15.0932 1 -14 -1 0-2.53012 14.9158 1 -14 -1 -1 1.28601 15.3722 1 -14 -1 -2 14.3396 16.7521 1 -14 -1 -3 4.02594 16.4219 1 -14 -1 -4 20.3008 16.8079 1 -14 -1 -5 16.4346 18.0180 1 -14 2 13 1.67890 9.12163 1 -14 -2 13 8.42338 9.48591 1 14 2 -13 11.3680 13.4133 4 14 -2 -13 9.30205 12.4929 4 -14 2 12 5.18999 9.98167 1 -14 -2 12-10.4150 9.71856 1 14 2 -12-3.08040 12.6437 4 14 -2 -12 11.1794 12.4743 4 -14 2 11-7.11812 10.0042 1 -14 -2 11-2.67848 9.92214 1 14 2 -11 13.2497 14.1050 4 14 -2 -11 26.4958 13.4810 4 -14 2 10 3.69249 9.71711 1 -14 -2 10-2.77819 9.79074 1 -14 2 9-0.94279 10.6875 1 -14 -2 9 10.6327 10.3168 1 -14 2 8 1.97678 10.9821 1 -14 -2 8-4.95628 11.0140 1 -14 2 7-3.05597 12.6875 1 -14 -2 7-14.3001 12.8015 1 -14 2 6-6.38574 13.4821 1 -14 -2 6-1.06611 12.9625 1 -14 -2 5-4.46709 13.3077 1 -14 2 5 15.6014 13.9444 1 -14 2 4-4.59526 13.6438 1 -14 -2 4-4.60094 13.8940 1 -14 2 3-3.51665 14.1583 1 -14 -2 3-4.69651 13.7496 1 -14 2 2 12.1056 14.3281 1 -14 -2 2-1.21218 13.6328 1 -14 2 1 12.2978 14.7162 1 -14 -2 1 3.69318 14.7814 1 -14 2 0 13.6720 15.8938 1 -14 -2 0 1.24384 14.8799 1 -14 2 -1 1.25575 14.8563 1 -14 -2 -1-2.51256 15.2195 1 -14 2 -2 12.8080 16.1347 1 -14 -2 -2 20.4949 15.9375 1 -14 2 -3 16.9640 16.7184 1 -14 -2 -3 11.7416 15.4279 1 -14 2 -4 14.6191 16.0105 1 -14 -2 -4 2.65654 16.0551 1 -14 3 12 0.83228 9.67443 1 -14 -3 12 0.83650 9.47551 1 14 3 -12-2.01933 12.3932 4 14 -3 -12 6.06120 12.3597 4 -14 3 11 6.85304 10.0286 1 -14 -3 11-4.30702 9.72030 1 -14 3 10 3.55194 9.91685 1 -14 -3 10 8.03034 9.88651 1 -14 3 9 10.8468 10.8843 1 -14 -3 9-0.92280 9.97325 1 -14 3 8 1.88821 10.7049 1 -14 -3 8-12.3249 11.1095 1 -14 3 7-8.81800 11.9124 1 -14 -3 7 1.96893 11.1546 1 -14 3 6-5.07143 13.4531 1 -14 -3 6 6.11177 12.2171 1 -14 -3 5-7.46539 12.4406 1 -14 3 5 8.49819 12.6543 1 -14 3 4 1.09399 13.9794 1 -14 -3 4-1.09794 12.9891 1 -14 3 3 5.67308 14.0261 1 -14 -3 3 6.82542 13.3750 1 -14 3 2-1.15867 13.9055 1 -14 -3 2 12.7706 13.9330 1 -14 3 1 2.37620 14.2978 1 -14 -3 1-1.19094 14.1870 1 -14 3 0 3.64979 14.9326 1 -14 -3 0-3.65610 14.7151 1 -14 3 -1 12.1898 15.7293 1 -14 -3 -1 3.66004 15.4645 1 -14 3 -2 22.2893 16.7905 1 -14 -3 -2 9.91017 15.0649 1 -14 3 -3-2.50717 15.1874 1 -14 -3 -3 6.27109 15.1447 1 -14 4 10-2.48569 8.98977 1 -14 -4 10-4.17249 9.77310 1 -14 4 9 3.43650 10.1692 1 -14 -4 9-8.65101 10.5201 1 -14 4 8 2.66842 10.5594 1 -14 -4 8-1.78983 9.74509 1 -14 4 7 5.59422 11.0408 1 -14 -4 7 5.62991 10.8382 1 -14 4 6-8.54220 13.0678 1 -14 -4 6 3.86490 11.5898 1 -14 4 5 1.96482 12.2131 1 -14 -4 5-3.95183 12.0874 1 -14 4 4 5.14587 13.9120 1 -14 -4 4-3.10275 12.4463 1 -14 4 3-2.16345 13.6604 1 -14 -4 3 9.78167 13.3863 1 -14 4 2-1.09863 13.7865 1 -14 -4 2-2.20653 13.6293 1 -14 4 1 6.72799 14.6672 1 -14 -4 1-10.1290 13.8595 1 -14 4 0 3.45091 15.0915 1 -14 -4 0 4.61426 14.6125 1 -14 4 -1 2.35262 15.1950 1 -14 -4 -1 20.0420 15.2288 1 -14 5 5-10.8767 12.8589 1 -14 5 4-10.3177 13.6817 1 -14 5 3-4.91287 13.2533 1 0 0 0 0.00 0.00 0 TITL MK_SB4_auto in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 0.71073 8.750058 8.951009 21.225478 90.0000 97.4459 90.0000 ZERR 4.00 0.001014 0.000720 0.001341 0.0000 0.0078 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O Cl UNIT 64.00 48.00 12.00 4.00 4.00 REM CrysAlisPro recorded range (K): Min=294.9; max=295.1; aver:295.0 TEMP 22 TREF HKLF 4 END ; _shelx_hkl_checksum 67814 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O3 O 0.5191(3) 0.6949(3) 0.85695(10) 0.0615(7) Uani 1 1 d . . . . . O1 O 0.3604(3) 0.3077(2) 0.57149(10) 0.0593(6) Uani 1 1 d . . . . . N2 N 0.3332(3) 0.5445(2) 0.53228(10) 0.0372(5) Uani 1 1 d . . . . . O2 O 0.3565(3) 0.5587(3) 0.75613(10) 0.0690(7) Uani 1 1 d . . . . . O4 O 0.2049(3) 0.5585(3) 0.85805(11) 0.0646(7) Uani 1 1 d . . . . . N1 N 0.1619(3) 0.6066(2) 0.44214(10) 0.0411(6) Uani 1 1 d . . . . . N3 N 0.4542(3) 0.6010(2) 0.57751(11) 0.0446(6) Uani 1 1 d . . . . . C1 C 0.2681(3) 0.6443(3) 0.48743(12) 0.0381(6) Uani 1 1 d . . . . . C8 C 0.1142(3) 0.4580(3) 0.43749(12) 0.0399(6) Uani 1 1 d . . . . . C10 C 0.4302(3) 0.5809(3) 0.63497(13) 0.0411(7) Uani 1 1 d . . . . . H10 H 0.343639 0.527367 0.642901 0.049 Uiso 1 1 calc R U . . . C13 C 0.5749(3) 0.7028(3) 0.80015(13) 0.0451(7) Uani 1 1 d . . . . . C11 C 0.5335(3) 0.6390(3) 0.68824(13) 0.0419(7) Uani 1 1 d . . . . . C2 C 0.2958(3) 0.3929(3) 0.53140(13) 0.0419(7) Uani 1 1 d . . . . . C3 C 0.1778(3) 0.3507(3) 0.48021(12) 0.0383(6) Uani 1 1 d . . . . . C12 C 0.4877(3) 0.6328(3) 0.74873(13) 0.0445(7) Uani 1 1 d . . . . . C7 C 0.0020(3) 0.4162(3) 0.38793(15) 0.0506(7) Uani 1 1 d . . . . . H7 H -0.042290 0.487436 0.359304 0.061 Uiso 1 1 calc R U . . . C16 C 0.6700(3) 0.7141(3) 0.68002(14) 0.0527(8) Uani 1 1 d . . . . . H16 H 0.702505 0.718182 0.640034 0.063 Uiso 1 1 calc R U . . . C9 C 0.3215(4) 0.8026(3) 0.49299(15) 0.0525(8) Uani 1 1 d . . . . . H9A H 0.265411 0.860928 0.459763 0.079 Uiso 1 1 calc R U . . . H9B H 0.429620 0.806854 0.489258 0.079 Uiso 1 1 calc R U . . . H9C H 0.303959 0.841809 0.533528 0.079 Uiso 1 1 calc R U . . . C14 C 0.7075(4) 0.7770(3) 0.79062(15) 0.0539(8) Uani 1 1 d . . . . . H14 H 0.765662 0.824713 0.824537 0.065 Uiso 1 1 calc R U . . . C4 C 0.1302(4) 0.2016(3) 0.47303(15) 0.0526(8) Uani 1 1 d . . . . . H4 H 0.172999 0.129771 0.501705 0.063 Uiso 1 1 calc R U . . . C15 C 0.7555(4) 0.7813(4) 0.73056(16) 0.0591(9) Uani 1 1 d . . . . . H15 H 0.846414 0.830268 0.724858 0.071 Uiso 1 1 calc R U . . . C5 C 0.0206(4) 0.1612(3) 0.42381(17) 0.0608(9) Uani 1 1 d . . . . . H5 H -0.010785 0.062128 0.418888 0.073 Uiso 1 1 calc R U . . . C6 C -0.0428(4) 0.2690(4) 0.38154(17) 0.0603(9) Uani 1 1 d . . . . . H6 H -0.117154 0.241455 0.348210 0.072 Uiso 1 1 calc R U . . . C17 C 0.0546(5) 0.5345(5) 0.8298(3) 0.1061(16) Uani 1 1 d . . . . . H17A H -0.010966 0.519435 0.862222 0.159 Uiso 1 1 calc R U . . . H17B H 0.051310 0.447597 0.803185 0.159 Uiso 1 1 calc R U . . . H17C H 0.019547 0.619848 0.804637 0.159 Uiso 1 1 calc R U . . . H2O H 0.567(4) 0.751(4) 0.886(2) 0.076(11) Uiso 1 1 d . . . . . H1O H 0.334(4) 0.576(4) 0.796(2) 0.088(12) Uiso 1 1 d . . . . . H3O H 0.194(5) 0.651(5) 0.881(2) 0.123(16) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O3 0.0818(18) 0.0713(14) 0.0300(11) -0.0097(10) 0.0019(11) -0.0280(12) O1 0.0754(16) 0.0523(12) 0.0463(13) 0.0108(9) -0.0067(12) 0.0100(10) N2 0.0399(13) 0.0456(12) 0.0245(11) -0.0016(9) -0.0022(10) 0.0034(9) O2 0.0764(17) 0.0938(16) 0.0380(13) -0.0189(12) 0.0115(12) -0.0380(13) O4 0.0609(16) 0.0718(14) 0.0600(15) -0.0153(11) 0.0039(12) -0.0028(11) N1 0.0443(14) 0.0448(12) 0.0333(13) 0.0006(9) 0.0013(11) 0.0054(10) N3 0.0459(15) 0.0542(13) 0.0319(13) -0.0031(10) -0.0021(11) 0.0014(10) C1 0.0404(16) 0.0441(13) 0.0299(14) -0.0005(11) 0.0047(13) 0.0051(11) C8 0.0361(16) 0.0498(14) 0.0339(14) -0.0052(12) 0.0055(13) 0.0045(11) C10 0.0383(16) 0.0509(14) 0.0332(14) -0.0049(11) 0.0008(13) 0.0039(11) C13 0.0507(18) 0.0482(15) 0.0340(15) -0.0035(12) -0.0033(14) -0.0024(12) C11 0.0369(16) 0.0530(15) 0.0338(15) -0.0056(12) -0.0035(13) 0.0070(12) C2 0.0519(18) 0.0404(14) 0.0345(15) 0.0015(11) 0.0089(14) 0.0081(12) C3 0.0395(16) 0.0446(14) 0.0311(14) -0.0034(11) 0.0053(13) 0.0037(11) C12 0.0462(17) 0.0484(15) 0.0372(16) -0.0030(11) -0.0011(14) -0.0024(12) C7 0.0402(17) 0.0633(18) 0.0465(18) -0.0078(14) -0.0009(14) 0.0053(13) C16 0.0425(18) 0.076(2) 0.0396(16) -0.0107(14) 0.0059(14) 0.0023(14) C9 0.059(2) 0.0463(15) 0.0509(18) 0.0024(13) 0.0013(16) 0.0015(13) C14 0.0468(19) 0.0655(18) 0.0461(18) -0.0145(14) -0.0070(15) -0.0044(14) C4 0.061(2) 0.0459(15) 0.0520(19) -0.0030(13) 0.0104(17) -0.0007(13) C15 0.0407(19) 0.084(2) 0.052(2) -0.0138(17) 0.0042(16) -0.0105(15) C5 0.058(2) 0.0545(18) 0.071(2) -0.0150(17) 0.012(2) -0.0095(15) C6 0.0420(18) 0.077(2) 0.060(2) -0.0243(17) 0.0022(16) -0.0052(15) C17 0.066(3) 0.123(4) 0.125(4) -0.049(3) -0.003(3) -0.014(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 N2 C2 123.2(2) . . ? C1 N2 N3 116.1(2) . . ? C2 N2 N3 120.4(2) . . ? C1 N1 C8 118.8(2) . . ? C10 N3 N2 113.2(2) . . ? N1 C1 N2 122.6(2) . . ? N1 C1 C9 119.6(3) . . ? N2 C1 C9 117.7(3) . . ? C3 C8 C7 119.5(3) . . ? C3 C8 N1 121.6(3) . . ? C7 C8 N1 119.0(3) . . ? N3 C10 C11 122.1(2) . . ? O3 C13 C14 124.2(3) . . ? O3 C13 C12 116.5(2) . . ? C14 C13 C12 119.2(2) . . ? C12 C11 C16 119.0(3) . . ? C12 C11 C10 118.6(2) . . ? C16 C11 C10 122.0(2) . . ? O1 C2 N2 120.6(3) . . ? O1 C2 C3 125.3(2) . . ? N2 C2 C3 114.0(2) . . ? C8 C3 C4 120.0(3) . . ? C8 C3 C2 119.8(2) . . ? C4 C3 C2 120.2(3) . . ? O2 C12 C11 118.4(3) . . ? O2 C12 C13 121.0(2) . . ? C11 C12 C13 120.5(2) . . ? C6 C7 C8 119.7(3) . . ? C15 C16 C11 120.2(3) . . ? C13 C14 C15 120.5(3) . . ? C5 C4 C3 120.2(3) . . ? C16 C15 C14 120.5(3) . . ? C4 C5 C6 119.5(3) . . ? C7 C6 C5 121.2(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O3 C13 1.360(3) . ? O1 C2 1.226(3) . ? N2 C1 1.374(3) . ? N2 C2 1.395(3) . ? N2 N3 1.426(3) . ? O2 C12 1.352(3) . ? O4 C17 1.390(5) . ? N1 C1 1.293(4) . ? N1 C8 1.394(3) . ? N3 C10 1.277(3) . ? C1 C9 1.491(4) . ? C8 C3 1.387(4) . ? C8 C7 1.394(4) . ? C10 C11 1.450(4) . ? C13 C14 1.374(4) . ? C13 C12 1.397(4) . ? C11 C12 1.395(3) . ? C11 C16 1.401(4) . ? C2 C3 1.448(4) . ? C3 C4 1.401(4) . ? C7 C6 1.377(4) . ? C16 C15 1.365(4) . ? C14 C15 1.394(4) . ? C4 C5 1.372(5) . ? C5 C6 1.384(5) . ?