#------------------------------------------------------------------------------ #$Date: 2024-12-26 01:02:16 +0200 (Thu, 26 Dec 2024) $ #$Revision: 296971 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/35/1573541.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573541 loop_ _publ_author_name 'Zhang, Yan' 'Apostol, Petru' 'Rambabu, Darsi' 'Guo, Xiaolong' 'Liu, Xuelian' 'Lin, Xiaodong' 'Xie, Haijiao' 'Chen, Xiaohua' 'Robeyns, Koen' 'Wang, Jiande' 'Wang, Junzhong' 'Vlad, Alexandru' _publ_section_title ; Ionically conducting Li- and Na-phosphonates as organic electrode materials for rechargeable batteries. ; _journal_name_full 'Chemical science' _journal_paper_doi 10.1039/d4sc07732f _journal_year 2024 _chemical_formula_moiety 'C18 H12 O6 P2, Na4, 4 (C H4 O)' _chemical_formula_sum 'C22 H28 Na4 O10 P2' _chemical_formula_weight 606.34 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_method SHELXL-2019/3 _audit_update_record ; 2024-11-11 deposited with the CCDC. 2024-12-09 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 106.967(12) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 12.6672(14) _cell_length_b 6.1624(6) _cell_length_c 18.016(2) _cell_measurement_reflns_used 1321 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 22.9720 _cell_measurement_theta_min 2.4390 _cell_volume 1345.1(3) _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_collection MAR _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_molecular_graphics 'MERCURY (Macrae et al., 2008)' _computing_publication_material ; 'MERCURY (Macrae et al., 2008), Platon (Spek, 2009)' ; _computing_structure_refinement 'SHELXL-2019/3 (Sheldrick, 2019)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 150(2) _diffrn_measured_fraction_theta_full 0.973 _diffrn_measured_fraction_theta_max 0.973 _diffrn_measurement_device_type 'MAR345 image plate' _diffrn_measurement_method ; '102 images, \D\F 2.0\% ' ; _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1125 _diffrn_reflns_av_unetI/netI 0.1003 _diffrn_reflns_Laue_measured_fraction_full 0.973 _diffrn_reflns_Laue_measured_fraction_max 0.973 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 7054 _diffrn_reflns_point_group_measured_fraction_full 0.973 _diffrn_reflns_point_group_measured_fraction_max 0.973 _diffrn_reflns_theta_full 23.287 _diffrn_reflns_theta_max 23.287 _diffrn_reflns_theta_min 2.469 _diffrn_source 'Incoatec microfocus source' _exptl_absorpt_coefficient_mu 0.279 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.70698 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.497 _exptl_crystal_description needle _exptl_crystal_F_000 628 _exptl_crystal_recrystallization_method 'diffusion of diethyl ether into a methanol solution of the compound' _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.01 _refine_diff_density_max 0.464 _refine_diff_density_min -0.510 _refine_diff_density_rms 0.091 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.116 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 175 _refine_ls_number_reflns 1879 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.116 _refine_ls_R_factor_all 0.1318 _refine_ls_R_factor_gt 0.0878 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0550P)^2^+5.6721P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1694 _refine_ls_wR_factor_ref 0.1881 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1331 _reflns_number_total 1879 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc07732f2.cif _cod_data_source_block av_pa_Na4PhPh _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 1573541 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL av_pa_Na4PhPh in P2(1)/c av_pa_Na4PhPh.res created by SHELXL-2019/3 at 10:28:43 on 07-Jun-2024 REM P2(1)/c (#14 in standard setting) CELL 0.71073 12.667246 6.162371 18.015660 90.0000 106.9670 90.0000 ZERR 2.00 0.001418 0.000568 0.001996 0.0000 0.0116 0.0000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N O P NA UNIT 44 56 0 20 4 8 L.S. 10 BOND $H CONF TEMP -123 ACTA LIST 4 FMAP 2 PLAN 20 WGHT 0.055000 5.672100 FVAR 0.24817 0.64406 NA1 6 0.449191 0.709134 0.771359 11.00000 0.04186 0.02136 = 0.02919 -0.00151 0.01591 0.00048 NA2 6 0.335213 0.403652 0.636597 11.00000 0.03901 0.03176 = 0.03493 0.00007 0.01189 0.00234 P3 5 0.595282 0.721254 0.658635 11.00000 0.03179 0.01981 = 0.02212 0.00197 0.01453 0.00060 C4 1 0.539799 0.878249 0.569344 11.00000 0.03137 0.01636 = 0.01903 -0.00259 0.00973 -0.00507 C5 1 0.584287 0.853995 0.507075 11.00000 0.02499 0.01761 = 0.02243 0.00092 0.00910 0.00128 AFIX 43 H5 2 0.642367 0.752267 0.512348 11.00000 -1.20000 AFIX 0 C6 1 0.547827 0.971893 0.436996 11.00000 0.02771 0.01755 = 0.02527 -0.00739 0.01210 -0.00680 O7 4 0.591206 0.937944 0.377549 11.00000 0.03959 0.02587 = 0.02280 0.00033 0.01940 0.00035 O8 4 0.514006 0.548849 0.666611 11.00000 0.03573 0.02158 = 0.03265 0.00921 0.01945 0.00341 O9 4 0.632779 0.872780 0.727891 11.00000 0.04562 0.02573 = 0.02312 -0.00344 0.01431 0.00468 C10 1 0.717681 0.582269 0.648248 11.00000 0.03449 0.02891 = 0.02138 0.00397 0.01430 -0.00235 C11 1 0.707360 0.379457 0.609846 11.00000 0.03223 0.02331 = 0.04118 0.00220 0.01529 0.00092 AFIX 43 H11 2 0.636062 0.321157 0.586059 11.00000 -1.20000 AFIX 0 C12 1 0.800426 0.264602 0.606550 11.00000 0.05438 0.03557 = 0.05294 -0.00663 0.02686 0.00736 AFIX 43 H12 2 0.792589 0.129335 0.580202 11.00000 -1.20000 AFIX 0 C13 1 0.904903 0.348320 0.641915 11.00000 0.04341 0.06059 = 0.06312 0.00319 0.03245 0.02293 AFIX 43 H13 2 0.968628 0.269059 0.640534 11.00000 -1.20000 AFIX 0 C14 1 0.916242 0.549055 0.679505 11.00000 0.03148 0.06562 = 0.06070 -0.00491 0.01860 -0.00218 AFIX 43 H14 2 0.987568 0.607606 0.703006 11.00000 -1.20000 AFIX 0 C15 1 0.823364 0.661933 0.682350 11.00000 0.03635 0.03881 = 0.04286 -0.00543 0.01958 -0.00543 AFIX 43 H15 2 0.831944 0.797815 0.708339 11.00000 -1.20000 AFIX 0 O21 4 0.290811 0.762790 0.654746 11.00000 0.05008 0.03095 = 0.08046 0.00943 0.04052 0.00084 AFIX 83 H21 2 0.325148 0.868813 0.643750 11.00000 -1.50000 AFIX 0 C22 1 0.190240 0.832711 0.661885 11.00000 0.04172 0.06809 = 0.09856 -0.01116 0.02622 0.00208 AFIX 137 H22A 2 0.132095 0.803860 0.613451 11.00000 -1.50000 H22B 2 0.193782 0.988859 0.672641 11.00000 -1.50000 H22C 2 0.173730 0.754855 0.704612 11.00000 -1.50000 AFIX 0 O23 4 0.167076 0.395413 0.536833 11.00000 0.07416 0.10221 = 0.11090 -0.01968 0.00193 -0.00756 AFIX 3 H23 2 0.185323 0.462059 0.501799 11.00000 -1.20000 AFIX 0 C24 1 0.099362 0.225755 0.504843 11.00000 0.10251 0.14071 = 0.07851 -0.00474 0.02452 -0.04185 AFIX 137 H24A 2 0.022443 0.266411 0.498532 11.00000 -1.50000 H24B 2 0.118627 0.099091 0.539028 11.00000 -1.50000 H24C 2 0.108521 0.190257 0.454056 11.00000 -1.50000 AFIX 0 HKLF 4 REM av_pa_Na4PhPh in P2(1)/c REM wR2 = 0.1881, GooF = S = 1.116, Restrained GooF = 1.116 for all data REM R1 = 0.0878 for 1331 Fo > 4sig(Fo) and 0.1318 for all 1879 data REM 175 parameters refined using 0 restraints END WGHT 0.0550 5.6720 REM Highest difference peak 0.464, deepest hole -0.510, 1-sigma level 0.091 Q1 1 0.5509 0.7380 0.6002 11.00000 0.05 0.46 Q2 1 0.6632 0.6543 0.6548 11.00000 0.05 0.36 Q3 1 0.1786 0.2799 0.6303 11.00000 0.05 0.35 Q4 1 0.2490 0.3749 0.6065 11.00000 0.05 0.35 Q5 1 0.5153 0.5075 0.6207 11.00000 0.05 0.31 Q6 1 0.3628 0.7206 0.7363 11.00000 0.05 0.30 Q7 1 0.1733 0.2348 0.5871 11.00000 0.05 0.29 Q8 1 0.6527 0.9595 0.4201 11.00000 0.05 0.29 Q9 1 0.5616 0.8546 0.6049 11.00000 0.05 0.28 Q10 1 0.2377 0.7489 0.5941 11.00000 0.05 0.28 Q11 1 0.7914 0.2736 0.5444 11.00000 0.05 0.28 Q12 1 0.4371 0.5551 0.6428 11.00000 0.05 0.27 Q13 1 0.1850 0.9646 0.7473 11.00000 0.05 0.27 Q14 1 0.7615 0.6484 0.6412 11.00000 0.05 0.26 Q15 1 0.7026 0.7014 0.4959 11.00000 0.05 0.26 Q16 1 0.6580 0.8598 0.5349 11.00000 0.05 0.26 Q17 1 0.4412 0.7570 0.5766 11.00000 0.05 0.26 Q18 1 0.6789 0.8587 0.7692 11.00000 0.05 0.26 Q19 1 0.1771 0.5774 0.6612 11.00000 0.05 0.25 Q20 1 0.9405 0.3611 0.7170 11.00000 0.05 0.25 ; _shelx_res_checksum 12130 _shelx_hkl_file ; 0 0 -3-1.13237 1.97057 1 0 0 3 1.99367 1.81574 1 0 0 -4 817.828 20.6551 1 0 0 4 815.266 20.4431 1 0 0 -5-0.67799 3.08778 1 0 0 5 0.64811 2.61662 1 0 0 6 581.263 21.5009 1 0 0 -6 591.244 21.8500 1 0 0 -7 3.53885 3.56125 1 0 0 7 10.7989 4.56764 1 0 0 8 123.840 12.1624 1 0 0 -8 129.076 12.6338 1 0 0 -9 7.45955 6.06497 1 0 0 9-1.00410 4.14521 1 0 0 10 199.060 17.0173 1 0 0 -10 228.872 18.3099 1 0 0 11 1.13062 4.06130 1 0 0 -11 0.77218 4.43139 1 0 0 -12 64.3113 12.4489 1 0 0 12 48.3043 9.54996 1 0 0 13 14.5974 6.72586 1 0 0 -13 7.17568 5.99874 1 0 0 -14 65.1670 13.3708 1 0 0 14 50.6057 12.1235 1 0 0 15 13.7359 7.60223 1 0 0 -15 21.7244 9.29033 1 0 0 -16 15.8405 9.46415 1 0 0 16 10.2659 9.84326 1 0 0 17 6.49917 3.34143 1 0 0 17 9.97703 9.11074 1 0 0 -17 9.12743 11.0274 1 0 0 18 48.7512 7.32081 1 0 0 -18 67.5843 15.8843 1 0 0 18 62.6761 15.8510 1 0 0 19 13.2918 5.05344 1 0 1 2 107.943 5.19916 1 0 -1 -2 107.592 4.97552 1 0 -1 2 112.014 5.47742 1 0 1 -2 109.841 5.61652 1 0 1 3 509.927 13.6285 1 0 -1 -3 499.311 13.3847 1 0 -1 3 497.119 14.0336 1 0 1 -3 494.338 14.2379 1 0 -1 -4 556.836 16.4475 1 0 -1 4 521.104 16.7379 1 0 1 -4 539.947 17.2294 1 0 1 4 548.467 16.3879 1 0 -1 5 8.42533 3.33475 1 0 1 -5 10.6148 4.10614 1 0 1 5 10.7916 3.26572 1 0 -1 -5 13.0053 4.04665 1 0 -1 6 21.9689 5.17282 1 0 1 6 29.1069 5.64609 1 0 -1 -6 35.0439 5.94246 1 0 1 -6 30.4014 5.67727 1 0 1 7 266.597 16.1653 1 0 -1 -7 272.311 16.3712 1 0 1 -7 283.402 16.7590 1 0 -1 7 263.419 16.1354 1 0 1 8 286.154 17.8439 1 0 1 -8 318.401 19.2536 1 0 -1 8 293.748 18.1214 1 0 -1 -8 304.766 18.4257 1 0 -1 -9 113.647 12.1218 1 0 -1 9 112.126 12.3373 1 0 1 9 101.249 12.0606 1 0 1 -9 109.572 12.1640 1 0 1 10 311.690 21.2839 1 0 1 -10 329.539 22.1793 1 0 -1 10 302.993 20.6288 1 0 -1 -10 317.790 21.1007 1 0 -1 -11 4.85235 5.39236 1 0 -1 11 0.27226 3.85908 1 0 1 -11 3.87518 5.88226 1 0 1 11 0.66799 4.35851 1 0 1 12 3.70350 4.85543 1 0 1 -12 2.43573 5.48949 1 0 -1 12 6.13987 5.01249 1 0 -1 -12 11.5712 7.36624 1 0 -1 -13 11.2242 7.83234 1 0 1 13 7.89747 6.87846 1 0 1 -13 19.2427 8.15504 1 0 -1 13 8.29462 6.43103 1 0 1 14 54.7470 11.7273 1 0 -1 -14 88.3267 15.4514 1 0 -1 14 45.0136 10.2544 1 0 1 -14 60.9206 12.8915 1 0 1 15 2.17649 2.20158 1 0 -1 -15 10.0983 9.04186 1 0 1 -15-2.69253 8.26308 1 0 -1 15-4.20513 4.60485 1 0 1 15 10.5349 8.22464 1 0 -1 -16 12.6242 8.80864 1 0 1 16-0.50259 3.06965 1 0 -1 16-4.12897 7.13561 1 0 1 -16-5.27526 7.44308 1 0 1 16 8.07837 6.99337 1 0 1 17 35.2872 6.33998 1 0 -1 17 37.0085 6.80128 1 0 1 17 27.2712 10.2574 1 0 -1 17 30.2809 10.4445 1 0 -1 -17 30.8088 11.1757 1 0 1 -17 28.2558 11.3305 1 0 1 18 14.4176 5.25068 1 0 -1 -18 9.98681 9.57066 1 0 1 -18 24.2559 12.6053 1 0 -1 18 11.9624 5.23395 1 0 -1 18 12.2229 10.5527 1 0 -2 1 6.43462 0.97621 1 0 2 -1 8.62683 1.36705 1 0 -2 2 84.1108 4.56410 1 0 2 -2 88.7538 5.05701 1 0 2 2 83.9384 4.46604 1 0 2 2 82.4028 2.75028 1 0 -2 -3 104.084 5.79775 1 0 -2 3 102.516 6.23537 1 0 2 -3 110.963 6.96170 1 0 2 3 117.675 6.50662 1 0 2 3 107.077 3.74417 1 0 -2 4 18.8655 3.31468 1 0 2 4 21.7772 3.63383 1 0 -2 -4 22.9086 3.61845 1 0 2 -4 24.2450 4.17891 1 0 2 4 20.7330 2.03817 1 0 2 -5 48.4570 6.77354 1 0 2 5 47.4190 3.25782 1 0 -2 -5 48.1395 5.46108 1 0 -2 5 42.7958 5.64079 1 0 2 5 43.1342 5.66526 1 0 -2 6 18.1854 4.48721 1 0 2 6 22.6357 2.59779 1 0 2 -6 21.2549 4.48735 1 0 -2 -6 22.7553 5.31857 1 0 2 6 21.2439 4.63509 1 0 -2 -7 44.7563 7.03662 1 0 2 7 45.0061 7.37574 1 0 2 -7 44.1827 7.62055 1 0 -2 7 33.0775 5.94035 1 0 2 8 29.5499 6.56697 1 0 -2 8 20.8001 5.62046 1 0 2 -8 22.9491 5.50702 1 0 -2 -8 21.9524 5.53678 1 0 2 -9 33.0717 7.79142 1 0 -2 -9 40.6397 7.96464 1 0 -2 9 25.9038 6.40177 1 0 2 9 33.8971 7.34735 1 0 -2 10 1.35807 4.59027 1 0 2 10 1.60517 1.61378 1 0 2 10 4.34850 4.60080 1 0 2 -10 0.68899 4.66518 1 0 -2 -10 10.0827 4.88151 1 0 2 11 14.3886 3.03864 1 0 2 11 12.4952 6.10301 1 0 -2 11 6.09002 4.32341 1 0 2 -11 14.1376 5.53996 1 0 -2 -11 8.98407 5.83819 1 0 -2 -12 56.6244 10.9410 1 0 2 12 35.6320 8.49419 1 0 -2 12 34.4370 8.42752 1 0 2 -12 55.1937 11.5442 1 0 2 12 54.0335 5.74149 1 0 2 13 15.2216 7.65409 1 0 -2 13 9.78700 4.77475 1 0 -2 -13 11.6504 7.02789 1 0 2 13 17.7258 3.88727 1 0 2 -13 18.1238 8.19644 1 0 2 14-0.10054 6.16973 1 0 2 14 5.13419 2.98300 1 0 -2 -14-8.24466 7.45746 1 0 2 -14 5.47742 5.65433 1 0 -2 14 10.7961 7.34817 1 0 2 15 2.46662 2.50753 1 0 2 -15 18.1391 10.9151 1 0 -2 15 2.58217 5.53562 1 0 -2 -15 7.27240 7.55723 1 0 -2 16 52.0451 12.6026 1 0 2 16 42.9362 11.8137 1 0 2 -16 32.9430 12.3323 1 0 -2 -16 61.6236 12.8066 1 0 2 16 47.9850 7.08547 1 0 2 17 13.1251 10.2895 1 0 2 17 12.1166 4.38605 1 0 -2 -17 13.4349 10.2032 1 0 -2 17 16.5739 5.19505 1 0 -2 17 16.4327 10.6545 1 0 2 -17 28.8782 11.9101 1 0 2 18 18.1385 5.10242 1 0 -2 18 28.4688 7.22048 1 0 2 18 26.5957 11.4569 1 0 -2 -18 31.4514 14.0523 1 0 2 -18 19.4049 11.9104 1 0 -2 18 22.3034 11.0458 1 0 -3 2 141.984 5.02233 1 0 3 2 125.143 3.48367 1 0 3 -2 134.346 6.12753 1 0 3 2 125.469 4.87644 1 0 -3 3 22.3064 2.74206 1 0 3 3 21.5152 3.05561 1 0 3 -3 19.6835 3.47635 1 0 3 3 21.3793 1.79267 1 0 3 -4 6.80122 3.04015 1 0 3 4 3.51748 2.46092 1 0 -3 4 4.61239 2.29605 1 0 3 4 2.53243 0.90028 1 0 -3 5 111.677 8.64802 1 0 3 5 120.687 9.02608 1 0 3 5 115.236 5.18992 1 0 3 -5 114.856 9.36290 1 0 -3 -6 189.586 11.2461 1 0 3 6 190.005 7.30395 1 0 3 6 180.076 12.0155 1 0 3 -6 198.746 13.5281 1 0 -3 6 167.052 11.4430 1 0 -3 7 41.5727 7.12604 1 0 -3 -7 38.4191 6.10815 1 0 3 -7 39.7528 6.94887 1 0 3 7 35.6898 6.20974 1 0 3 7 36.9042 3.59074 1 0 -3 8 167.765 13.4519 1 0 3 8 168.022 7.91520 1 0 -3 -8 146.128 11.8680 1 0 3 -8 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84.8201 8.38709 1 -3 -4 4 100.342 6.61277 1 -3 -4 3 1.81606 1.38372 1 3 4 -3 5.55287 3.36126 1 -3 -4 2 1.99986 1.74411 1 3 4 -2 0.58606 2.16449 1 3 4 -1 24.0755 3.46954 1 -3 -4 1 23.4385 2.87218 1 3 4 0 30.9531 3.89987 1 -3 -4 0 27.2200 2.91037 1 -3 -4 -1 0.22965 1.19372 1 3 -4 1-0.10686 0.81539 1 3 -4 1 2.42366 1.54906 1 3 4 1 0.48891 1.37371 1 -3 -4 -2 64.3142 4.61549 1 3 4 2 71.8627 7.39149 1 3 -4 2 57.9860 5.46389 1 3 4 2 70.5020 5.45657 1 3 -4 2 58.4464 3.47101 1 3 -4 3 80.7962 7.27348 1 -3 -4 -3 84.6189 5.42214 1 3 -4 3 81.9692 4.70194 1 3 4 3 94.7331 9.18503 1 3 4 3 91.4627 6.30083 1 3 4 4 31.1720 3.93131 1 3 -4 4 30.2751 3.21985 1 3 -4 4 33.8729 5.87549 1 3 4 4 37.1656 6.18715 1 3 4 5 14.3261 5.73796 1 3 -4 5 18.8092 5.01161 1 3 4 5 17.5650 3.35746 1 3 -4 5 13.6725 2.36489 1 3 -4 6 3.04575 2.14053 1 3 4 6-3.28955 4.66516 1 3 -4 6 0.47644 3.61204 1 3 4 6 5.01597 2.62529 1 3 -4 7 1.49053 1.50828 1 3 4 7 3.67716 5.73946 1 3 -4 7 8.34176 5.35300 1 3 4 7 3.82656 1.95867 1 3 4 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5.00127 1.54623 1 4 -4 -1 81.3370 4.56854 1 4 -4 -1 91.3189 5.73062 1 -4 -4 1 110.719 6.69500 1 4 4 -1 103.803 7.80615 1 4 -4 0 9.54856 2.83672 1 4 -4 0 11.4534 1.91992 1 4 4 0 14.7323 3.55102 1 -4 -4 0 10.8828 2.61871 1 -4 -4 -1 1.56355 1.31865 1 4 -4 1 2.57108 2.59690 1 4 4 1 4.38953 2.59866 1 4 -4 1 4.23477 1.56080 1 4 -4 2 28.1476 4.46487 1 4 4 2 31.9908 6.12858 1 4 4 2 36.6149 4.79492 1 -4 -4 -2 30.6174 3.67919 1 4 -4 2 24.1581 3.02448 1 4 4 3 136.100 11.9430 1 -4 -4 -3 123.258 7.31574 1 4 -4 3 111.232 9.95366 1 4 -4 3 108.484 6.19445 1 4 4 3 111.989 7.97459 1 4 4 4 45.5941 5.18648 1 4 4 4 54.3211 7.74479 1 4 -4 4 44.3143 4.30140 1 4 -4 4 46.5550 7.09832 1 -4 -4 -4 49.2201 4.77496 1 4 4 5 33.3313 4.62658 1 4 4 5 45.8178 9.03437 1 -4 -4 -5 41.3646 4.60061 1 4 -4 5 35.3034 3.84601 1 4 -4 5 28.1634 6.39668 1 4 4 6 2.48041 4.37836 1 4 4 6 0.70876 2.06367 1 4 -4 6-1.53419 4.10606 1 4 -4 6 0.68048 1.72749 1 4 -4 7 9.03680 3.07716 1 4 4 7 12.9616 3.80483 1 4 -4 7 11.0124 6.09395 1 4 4 7 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1.20178 0.92151 1 -4 5 7 9.26624 1.50408 1 4 -5 -7 16.2436 2.97616 1 4 5 -7 35.4641 7.98959 1 -4 -5 7 22.9836 4.49568 1 -4 5 7 14.3297 1.64281 1 4 5 -6 7.00914 3.56541 1 -4 -5 6 12.7745 3.50166 1 -4 -5 5 14.0087 3.10741 1 4 5 -5 14.5539 4.58652 1 -4 -5 4 6.33562 2.43611 1 4 5 -4 2.63600 3.99774 1 -4 -5 3 114.627 7.16513 1 4 5 -3 118.301 9.99241 1 -4 -5 2 5.33904 2.34325 1 4 5 -2 2.47550 2.53236 1 4 5 -1 5.61636 3.01779 1 -4 -5 1 10.5723 2.81690 1 4 5 0 4.89201 3.13241 1 -4 -5 0-0.37933 1.70548 1 4 5 1-0.20080 2.47797 1 -4 -5 -1-0.58707 1.38407 1 4 5 2 0.40759 3.98421 1 -4 -5 -2-0.50391 1.36574 1 4 -5 2 0.30633 1.10829 1 4 5 2-1.57663 2.32542 1 4 -5 2 0.76392 1.37920 1 -4 -5 -3-0.14977 1.49671 1 4 5 3 3.39496 4.78601 1 4 5 3-2.71952 2.06082 1 4 -5 3 1.37378 2.33935 1 4 -5 3 1.41166 1.15762 1 4 -5 4 12.7369 2.65010 1 4 5 4 11.8510 5.02379 1 4 -5 4 13.4748 4.28046 1 4 5 4 11.7667 3.08292 1 4 5 5 5.07367 5.31552 1 4 -5 5-1.69874 1.96087 1 4 -5 5 2.87783 3.65236 1 4 5 5 2.03954 2.28028 1 4 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3 8.86136 3.39006 1 4 6 3 9.27187 5.39919 1 4 6 4 1.30103 5.67947 1 4 6 4 0.33173 2.72991 1 4 6 5 17.9428 4.23512 1 4 -6 5 8.26872 1.81761 1 5 0 -19 16.0986 12.2854 1 -5 0 18 6.72109 6.28886 1 5 0 -18 9.25926 9.65507 1 -5 0 17 3.93724 4.51936 1 5 0 -17-4.43792 8.31186 1 -5 0 16 21.3625 7.22024 1 5 0 -16-8.46648 10.6874 1 -5 0 15 2.07031 6.24204 1 5 0 -15 1.13084 7.49034 1 -5 0 14 36.0944 8.56266 1 5 0 -14 56.6315 12.9573 1 -5 0 13-5.39124 4.10277 1 5 0 -13 7.97617 5.22502 1 -5 0 12 49.1454 8.73330 1 5 0 -12 64.3719 11.5253 1 -5 0 11 3.22006 3.05186 1 5 0 -11 0.46308 4.83555 1 -5 0 10 4.57444 3.54412 1 5 0 -10 4.18699 3.57702 1 -5 0 9-2.48628 2.61000 1 5 0 -9 3.38686 4.99279 1 -5 0 8 14.8701 3.88789 1 5 0 -8 23.7052 5.98695 1 5 0 -7-0.56021 2.81306 1 -5 0 7 2.42855 3.05928 1 5 0 -6 1.47723 2.83784 1 -5 0 6 0.54683 2.59901 1 5 0 -5-2.98607 2.43678 1 -5 0 5 0.71758 2.02599 1 5 0 -4 124.102 8.60684 1 -5 0 4 122.137 7.95692 1 5 0 -3 2.05974 1.93165 1 -5 0 3 0.83959 1.57648 1 -5 0 2 204.394 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12.1949 1 5 1 -18 7.15023 10.3969 1 -5 1 17-2.21446 4.90118 1 -5 -1 17-1.26346 6.02032 1 5 -1 -17 7.98385 10.3301 1 5 1 -17 17.3412 11.7897 1 -5 1 16 0.91886 4.59668 1 -5 -1 16-0.22745 4.70940 1 5 -1 -16 11.2944 10.6865 1 5 1 -16 4.46141 9.02820 1 -5 1 15-3.50940 4.66172 1 -5 -1 15-4.00030 4.22711 1 5 -1 -15 0.85858 6.67327 1 5 1 -15-4.55690 8.84941 1 -5 1 14 21.9172 7.14019 1 -5 -1 14 19.6981 7.08985 1 5 -1 -14 45.1758 12.8074 1 5 1 -14 35.8156 10.1904 1 -5 1 13 14.2563 6.24353 1 -5 -1 13 15.7438 6.15492 1 5 -1 -13 8.88354 5.54787 1 5 1 -13 16.3148 7.22816 1 -5 1 12-0.40261 3.10096 1 -5 -1 12-1.14648 3.02975 1 5 -1 -12 4.63425 5.15217 1 5 1 -12 6.05650 5.68462 1 -5 1 11 16.6339 5.32127 1 -5 -1 11 9.60266 4.62137 1 5 -1 -11 7.14593 3.82903 1 5 1 -11 9.84463 5.97118 1 -5 1 10-1.23819 3.45762 1 -5 -1 10 1.79775 3.77302 1 5 -1 -10 0.58670 4.46989 1 5 1 -10 9.13040 6.55463 1 5 -1 -9 94.9098 11.0579 1 -5 -1 9 84.8022 8.35944 1 -5 1 9 91.0700 8.86900 1 5 1 -9 99.9755 12.1944 1 -5 1 8 1.82343 2.46258 1 -5 -1 8-1.17556 2.10130 1 5 -1 -8 4.89211 4.31251 1 5 1 -8-4.35599 3.39916 1 5 1 -7 134.934 11.9904 1 -5 1 7 143.625 9.76331 1 -5 -1 7 136.907 9.87158 1 5 -1 -7 135.249 11.2771 1 5 -1 -6 27.8725 5.09965 1 5 1 -6 23.5597 5.19672 1 -5 1 6 26.8042 4.25344 1 -5 -1 6 33.6670 4.91942 1 5 -1 -5 54.7942 6.04991 1 5 1 -5 48.8222 6.05046 1 -5 1 5 46.7582 5.18735 1 -5 -1 5 54.9866 6.00927 1 5 -1 -4 265.977 12.3437 1 5 1 -4 278.662 13.1453 1 -5 -1 4 269.118 12.2667 1 -5 1 4 267.985 11.4160 1 5 -1 -3 107.800 7.39267 1 5 1 -3 113.585 8.08188 1 -5 -1 3 115.746 7.74283 1 -5 1 3 121.081 7.25244 1 -5 1 2 246.493 10.3813 1 -5 -1 2 270.688 11.3553 1 5 1 -2 245.210 11.4788 1 5 -1 -2 244.543 10.8510 1 -5 -1 1 433.587 14.0265 1 -5 1 1 428.141 12.9426 1 5 1 -1 420.024 14.3240 1 5 -1 -1 407.766 13.3449 1 5 1 0 104.298 7.37723 1 5 -1 0 99.7544 6.62690 1 -5 1 0 103.707 6.58649 1 -5 -1 0 115.294 7.47687 1 5 1 1 0.70009 1.54065 1 -5 1 -1 3.08765 1.84949 1 -5 -1 -1 1.67156 1.91280 1 5 -1 1-0.04450 2.04952 1 5 1 2 24.1249 3.74596 1 -5 -1 -2 23.6627 3.76209 1 -5 1 -2 21.2153 3.29662 1 5 -1 2 22.5591 3.34629 1 5 1 3 256.766 11.2550 1 5 -1 3 245.338 10.6841 1 -5 -1 -3 268.245 11.4516 1 5 -1 3 290.124 17.2977 1 -5 1 -3 276.353 11.0993 1 -5 -1 -4 4.44453 2.16123 1 5 -1 4 3.69779 4.09610 1 5 1 4 3.61918 3.65252 1 -5 1 -4 2.93412 1.57967 1 5 1 4 5.76146 2.37290 1 5 -1 4 4.20605 2.22346 1 5 -1 5 7.84483 2.48923 1 5 -1 5 10.7165 4.59957 1 5 1 5 3.56322 4.50993 1 -5 -1 -5 10.2340 2.79418 1 -5 1 -5 8.16750 2.44996 1 5 1 5 8.73317 2.71985 1 5 1 6 8.62081 2.91578 1 5 1 6 9.83290 5.00444 1 5 -1 6 10.0223 2.86198 1 -5 -1 -6 9.02636 2.72930 1 5 -1 6 12.5290 5.06190 1 -5 1 -6 13.1705 2.62962 1 5 1 7 23.1226 4.17496 1 -5 -1 -7 22.4590 3.93531 1 5 1 7 28.1489 7.68879 1 5 -1 7 24.4696 7.22372 1 5 -1 7 25.9087 4.54420 1 5 1 8 93.8834 13.4650 1 5 -1 8 71.6147 12.2378 1 -5 -1 -8 87.8968 7.49836 1 5 1 8 81.1248 7.60295 1 5 -1 8 79.6344 7.52953 1 5 1 9 5.92307 2.33482 1 5 1 9 13.7231 7.79279 1 5 -1 9 6.03842 2.96388 1 5 -1 9 13.0718 7.26102 1 5 1 10 7.09156 3.34264 1 5 1 10 5.75047 5.82362 1 5 -1 10 10.4088 6.78511 1 5 -1 10 5.87397 2.97224 1 5 1 11-2.29249 7.84128 1 5 1 11-3.28279 3.43976 1 5 -1 11 6.33361 2.84533 1 5 1 12 21.7386 4.60655 1 5 -1 12 20.1951 7.82286 1 5 -1 12 22.9259 4.94913 1 5 1 12 17.2770 9.14872 1 5 1 13 11.6847 4.68841 1 5 1 13 20.5107 12.7155 1 5 -1 13 7.03099 11.2926 1 5 -1 13 10.3657 4.14940 1 5 -1 14 17.6269 5.86381 1 5 1 14 15.1418 4.63804 1 5 -1 14 8.96024 10.2924 1 5 1 14 14.7888 11.5160 1 5 1 15 3.79794 11.0147 1 5 -1 15 4.63878 5.12173 1 -5 2 19 8.14024 7.07188 1 -5 -2 19 12.5325 8.92368 1 5 -2 -19 27.5799 12.7316 1 5 2 -19 0.70525 14.9106 1 -5 2 18 0.40238 6.09552 1 -5 -2 18 22.2650 10.0495 1 5 -2 -18 19.6376 11.4729 1 -5 2 17 1.73525 6.13742 1 -5 -2 17 3.07455 5.80623 1 5 -2 -17 14.4564 11.3395 1 5 2 -17 13.5968 13.0569 1 -5 2 16 24.4295 8.86149 1 -5 -2 16 9.38395 7.31060 1 5 -2 -16 23.6534 12.4336 1 5 2 -16 12.6245 11.7225 1 5 -2 -15 102.575 16.8850 1 -5 2 15 79.4790 11.9502 1 5 2 -15 84.9814 17.0480 1 -5 -2 15 75.7777 12.0672 1 -5 2 14 6.96913 4.16921 1 -5 -2 14 7.08056 3.90309 1 5 -2 -14 5.44926 8.09173 1 -5 2 13 4.48647 3.54457 1 -5 -2 13-2.52628 3.80700 1 5 -2 -13-6.48573 7.88413 1 5 2 -13-6.62516 6.54571 1 5 -2 -12 175.706 18.8895 1 -5 2 12 153.338 13.8610 1 -5 -2 12 139.485 13.8428 1 5 2 -12 202.661 19.8014 1 -5 2 11 3.17842 2.99804 1 -5 -2 11-1.48898 4.02225 1 5 -2 -11-1.25789 4.30020 1 5 2 -11 1.36521 4.63121 1 5 -2 -10 71.7853 10.2220 1 5 2 -10 66.5748 10.7765 1 -5 2 10 64.4853 7.72332 1 -5 -2 10 62.8460 8.33202 1 -5 2 9 35.2759 5.49831 1 -5 -2 9 45.8224 6.73397 1 5 -2 -9 42.9786 7.83512 1 5 2 -9 33.4078 7.19897 1 -5 2 8-0.40050 2.02470 1 -5 -2 8 6.66191 3.45282 1 5 -2 -8-0.46970 2.88474 1 5 2 -8 1.68092 3.63591 1 5 -2 -7 161.014 12.8126 1 5 2 -7 162.444 13.2150 1 -5 2 7 150.135 9.74543 1 -5 -2 7 156.691 10.7025 1 5 -2 -6 8.01952 3.54517 1 5 2 -6 4.93028 3.20917 1 -5 2 6 7.41375 2.51953 1 -5 -2 6 4.06500 2.58952 1 5 -2 -5 2.73403 2.22366 1 5 2 -5-4.86831 2.94240 1 -5 -2 5 5.42324 2.96475 1 -5 2 5 1.02838 1.51993 1 5 -2 -4 83.2631 6.84603 1 5 2 -4 73.8447 7.59011 1 -5 -2 4 88.9292 7.24627 1 -5 2 4 79.9528 5.99339 1 -5 2 3 39.3614 4.32702 1 5 -2 -3 30.4641 4.17668 1 5 2 -3 28.6999 4.46830 1 -5 -2 3 28.0928 4.19892 1 -5 -2 2 32.1879 4.17727 1 -5 2 2 32.7528 3.46645 1 5 -2 -2 26.7634 3.86031 1 5 2 -2 29.4184 4.54106 1 -5 -2 1 30.2702 4.15627 1 -5 2 1 29.2724 3.45632 1 5 2 -1 22.4563 3.94816 1 5 -2 -1 23.7392 3.40119 1 5 -2 0 114.857 6.91584 1 -5 -2 0 126.278 8.02244 1 -5 2 0 125.941 6.83427 1 5 2 0 123.377 8.10359 1 5 2 1 126.961 8.17145 1 5 -2 1 126.739 7.35035 1 -5 -2 -1 144.638 8.39098 1 -5 2 -1 141.903 7.34395 1 5 2 2 42.7517 4.86171 1 5 -2 2 50.3390 4.84043 1 -5 -2 -2 48.2713 5.08381 1 -5 2 -2 50.0453 4.51936 1 5 -2 3 63.4985 8.17444 1 -5 2 -3 55.5070 4.80961 1 5 2 3 58.8461 5.84743 1 5 -2 3 55.1032 5.22977 1 -5 -2 -3 54.4519 5.58209 1 -5 -2 -4 12.8211 2.72096 1 5 2 4 18.5699 5.81370 1 5 -2 4 12.3483 5.12839 1 -5 2 -4 15.9669 2.84663 1 5 2 4 13.0892 3.24563 1 5 -2 4 14.6832 2.91119 1 5 2 5 116.735 12.8382 1 -5 -2 -5 106.183 7.87422 1 -5 2 -5 113.248 7.33737 1 5 2 5 100.003 7.71108 1 5 -2 5 104.186 7.50758 1 5 -2 5 112.598 12.0615 1 5 -2 6 101.351 12.4409 1 5 2 6 114.798 13.2910 1 -5 -2 -6 102.070 7.67403 1 5 2 6 89.8653 7.64369 1 5 -2 6 93.5331 7.32799 1 -5 -2 -7 2.16258 2.34837 1 5 -2 7 5.37163 5.29950 1 5 -2 7 0.68022 1.85886 1 5 2 7 5.91991 5.74803 1 5 2 7 1.43718 2.12752 1 5 2 8 43.6230 9.62851 1 5 -2 8 56.6390 11.4061 1 5 2 8 55.8133 6.45056 1 -5 -2 -8 60.0301 6.26783 1 5 -2 8 52.8199 5.90597 1 5 2 9 6.47777 3.44489 1 5 2 9 15.6830 8.63293 1 5 -2 9 6.85916 2.89193 1 5 -2 9 0.68635 5.24165 1 5 2 10-1.05420 6.41387 1 5 2 10-1.95303 2.54983 1 5 -2 10 0.48039 5.54989 1 5 -2 10 9.48919 3.39905 1 5 2 11-1.54540 3.09179 1 5 2 11 4.68304 7.78762 1 5 -2 11 7.12128 7.13642 1 5 -2 11 3.99965 3.88296 1 5 2 12-4.42173 8.30042 1 5 -2 12 7.44732 3.42573 1 5 2 12 2.10633 2.92247 1 5 2 13 18.0911 5.17711 1 5 2 13 22.0187 10.8500 1 5 -2 13 40.6924 14.5513 1 5 -2 13 27.2898 6.28220 1 5 2 14 4.09593 3.39050 1 5 2 14 7.75194 10.6492 1 5 -2 14 3.99196 8.88690 1 5 -2 14 7.70134 4.05046 1 -5 3 17 7.77347 7.73120 1 -5 -3 17 2.59046 5.44440 1 5 3 -17 15.3894 15.0549 1 -5 3 16 3.94921 5.85643 1 -5 -3 16 4.56818 4.72564 1 5 -3 -16 15.9131 8.52835 1 -5 3 15 9.67759 5.85793 1 -5 -3 15 10.9297 5.84454 1 5 -3 -15 17.8725 8.04171 1 5 3 -15 16.6731 11.0759 1 -5 3 14 10.7918 4.61929 1 -5 -3 14 9.95599 4.85941 1 5 -3 -14 11.5129 8.80840 1 5 3 -14 17.9253 10.6507 1 -5 3 13 0.60786 3.89295 1 -5 -3 13 1.15064 3.71990 1 5 -3 -13-0.24504 7.32349 1 5 3 -13-3.46531 6.38313 1 -5 3 12 18.8673 5.58849 1 -5 -3 12 15.4899 5.01172 1 5 -3 -12 43.3849 10.0808 1 5 3 -12 19.0751 8.15378 1 -5 3 11 3.66877 3.12002 1 -5 -3 11-1.35767 3.17020 1 5 -3 -11-5.81990 5.48164 1 5 3 -11-4.40774 6.11356 1 -5 3 10 36.8153 5.95518 1 -5 -3 10 40.3772 6.70056 1 5 -3 -10 55.9469 9.24549 1 5 3 -10 32.9328 8.49396 1 5 3 -9 101.176 12.6400 1 -5 3 9 99.8950 8.65431 1 -5 -3 9 96.6091 9.90439 1 5 -3 -9 112.912 12.1158 1 5 -3 -8 143.310 12.4305 1 5 3 -8 152.358 14.2315 1 -5 -3 8 143.523 10.8543 1 -5 3 8 138.342 9.31917 1 -5 3 7 6.93055 2.40851 1 -5 -3 7 7.09102 2.90067 1 5 -3 -7 11.5489 3.79606 1 5 3 -7 9.63704 4.39709 1 5 3 -6 17.0301 4.70273 1 -5 3 6 18.7875 3.26261 1 -5 -3 6 12.7868 3.52847 1 5 -3 -6 8.94002 2.79150 1 -5 -3 5 25.1963 4.54577 1 5 3 -5 32.1074 6.17237 1 -5 3 5 21.5199 3.17958 1 5 -3 -5 25.3675 4.86360 1 -5 3 4 80.5662 5.49920 1 5 3 -4 84.3188 8.27039 1 5 -3 -4 84.0902 7.14203 1 -5 -3 4 85.8033 7.28228 1 -5 -3 3 29.6456 4.26879 1 -5 3 3 30.1967 3.41991 1 5 3 -3 32.5151 5.11254 1 5 -3 -3 28.9663 3.98348 1 -5 -3 2 43.3413 4.89300 1 -5 3 2 44.3579 3.89585 1 5 -3 -2 40.4325 4.26583 1 5 3 -2 36.7148 5.29786 1 -5 -3 1 40.8989 4.74617 1 -5 3 1 34.7068 3.42766 1 5 -3 -1 32.1689 3.95632 1 5 3 -1 38.7845 5.15671 1 -5 3 0 6.67407 1.85690 1 5 3 0 1.39540 2.15236 1 -5 -3 0 4.54030 2.70267 1 5 -3 0 5.32316 1.78567 1 5 -3 1 4.73312 1.95447 1 -5 -3 -1 7.84606 2.63314 1 5 -3 1 14.3265 4.67453 1 -5 3 -1 5.88857 1.83866 1 5 3 1 5.69990 2.30773 1 5 3 2 7.24512 2.34643 1 5 -3 2 7.89638 4.49389 1 5 -3 2 8.78372 2.30795 1 -5 -3 -2 8.77541 2.39207 1 -5 3 -2 9.65126 2.08698 1 5 3 3 26.0247 3.99152 1 5 -3 3 42.2786 7.27309 1 5 -3 3 24.9845 3.64299 1 -5 3 -3 27.4075 3.49164 1 -5 -3 -3 25.4258 3.89984 1 5 3 4 7.89495 5.02654 1 -5 -3 -4 2.11474 1.55835 1 5 -3 4-0.59078 3.76321 1 5 -3 4 0.86760 1.65230 1 5 3 4 1.85985 1.57705 1 5 3 5-7.89720 5.46662 1 5 -3 5 1.69903 4.87613 1 5 3 5 6.80119 2.53283 1 -5 -3 -5 1.59349 1.52929 1 5 -3 5 2.79809 1.98266 1 5 -3 6 3.40990 5.35137 1 -5 -3 -6 2.56211 1.93584 1 5 3 6 2.52998 2.19898 1 5 3 6 13.4847 6.45819 1 5 -3 6 6.41655 2.38178 1 5 -3 7-1.14685 1.83347 1 5 3 7 4.37474 5.11802 1 5 -3 7 2.86668 6.78126 1 5 3 7 3.16576 2.27379 1 -5 -3 -7-1.53676 2.32834 1 5 -3 8 11.3391 2.95297 1 5 3 8 2.61863 7.06199 1 5 -3 8 10.2297 6.03290 1 5 3 8 9.87516 3.20701 1 5 -3 9 13.8507 3.50633 1 5 3 9 6.26398 7.27241 1 5 -3 9 23.2548 8.52822 1 5 3 9 4.93774 2.59872 1 5 -3 10 14.9073 4.12365 1 5 3 10 7.20718 6.73818 1 5 -3 10-1.01318 7.34941 1 5 3 10 9.79212 3.60534 1 5 3 11 3.48006 2.95736 1 5 -3 11 11.0695 3.92943 1 5 3 11-3.27667 9.35647 1 5 -3 11-5.83995 8.08635 1 5 3 12 1.85216 3.44937 1 5 -3 12 3.58869 3.31964 1 5 -3 12 3.82454 7.50408 1 5 -4 -16 3.79687 9.27137 1 -5 4 15 2.03977 5.25494 1 -5 -4 15 4.83802 3.96021 1 5 -4 -15 21.3958 10.9390 1 5 4 -15 13.9680 12.2667 1 -5 4 14 19.7375 6.55367 1 -5 -4 14 22.9964 7.58260 1 5 -4 -14 31.2067 10.8289 1 5 4 -14 26.5147 11.7246 1 -5 4 13 19.8417 5.68504 1 5 -4 -13 45.4150 11.1767 1 5 4 -13 51.7652 14.7999 1 -5 -4 13 24.9105 6.31370 1 -5 -4 12 7.62792 5.23071 1 -5 4 12 2.75755 3.51576 1 5 -4 -12 10.3170 6.92201 1 5 4 -12-6.97647 9.10182 1 5 -4 -11 198.484 17.9367 1 5 4 -11 222.119 21.5579 1 -5 4 11 171.279 11.8689 1 -5 -4 11 174.755 13.9533 1 -5 4 10 24.0940 5.08297 1 -5 -4 10 23.9664 5.12880 1 5 -4 -10 18.6716 6.75107 1 5 4 -10 27.8869 8.18330 1 -5 4 9 20.0705 4.07085 1 -5 -4 9 22.2879 4.73367 1 5 -4 -9 33.7154 7.67885 1 5 4 -9 22.2954 7.57604 1 -5 -4 8 29.2251 5.04008 1 5 -4 -8 39.8843 7.22294 1 -5 4 8 37.3411 4.73374 1 5 4 -8 39.9340 8.76444 1 5 -4 -7 40.8655 7.35852 1 -5 -4 7 33.9900 5.59563 1 -5 4 7 39.0433 4.57089 1 5 4 -7 38.2032 7.65877 1 5 -4 -6 15.3318 4.20559 1 -5 -4 6 22.9473 4.47147 1 -5 4 6 13.7484 2.66850 1 5 4 -6 20.7222 5.88448 1 -5 4 5 49.2779 3.98123 1 5 4 -5 48.4256 7.64661 1 5 -4 -5 38.3150 5.11428 1 -5 -4 5 45.0309 5.52586 1 -5 -4 4 10.5516 3.05647 1 5 4 -4 8.96008 3.36284 1 -5 4 4 8.83987 1.86461 1 5 -4 -4 9.18429 2.70680 1 5 4 -3 15.7421 4.60628 1 -5 -4 3 7.33357 2.42768 1 -5 4 3 9.22281 1.61540 1 5 -4 -3 8.38132 2.40525 1 5 -4 -2 11.3701 2.99734 1 5 4 -2 4.31478 2.49962 1 -5 4 2 7.40511 1.60226 1 -5 -4 2 10.1024 2.60372 1 5 -4 -1 53.4364 4.65310 1 5 -4 -1 68.6974 6.31404 1 -5 -4 1 57.9221 5.58888 1 5 4 -1 55.1405 6.43490 1 -5 4 1 49.2057 3.28807 1 5 -4 0 8.23310 3.13091 1 5 -4 0 10.1938 2.46261 1 5 4 0 9.23348 2.98146 1 -5 4 0 7.82744 1.72203 1 -5 -4 0 7.40854 2.53928 1 -5 -4 -1 3.86082 2.12203 1 5 -4 1-0.56112 3.37587 1 5 4 1 4.13409 2.93058 1 5 -4 1 2.94977 1.73941 1 5 -4 2 28.9175 5.68455 1 -5 -4 -2 21.3009 3.63938 1 5 4 2 18.5828 3.83339 1 5 -4 2 18.9312 3.10513 1 -5 -4 -3 0.80367 1.76038 1 5 4 3-3.02064 3.87874 1 5 -4 3 2.07873 1.76131 1 5 -4 3-4.89286 4.71687 1 5 4 3 2.45810 1.89693 1 5 4 4 128.350 9.48372 1 5 4 4 137.645 13.9636 1 -5 -4 -4 142.219 8.79593 1 5 -4 4 127.420 7.82946 1 5 -4 4 122.459 12.1401 1 5 4 5 17.0445 3.96646 1 5 4 5 6.24919 5.28432 1 -5 -4 -5 12.7494 3.15737 1 5 -4 5 12.0754 6.16163 1 5 -4 5 13.4237 3.48694 1 -5 -4 -6 4.10204 2.30803 1 5 4 6 3.71851 2.98703 1 5 -4 6-2.01065 4.32747 1 5 4 6 2.38126 5.81352 1 5 -4 6 5.75836 2.30206 1 5 4 7 43.5454 5.82529 1 5 4 7 47.8061 11.0267 1 5 -4 7 54.6731 10.8597 1 5 -4 7 52.0149 6.16440 1 5 4 8 8.87483 6.75827 1 5 -4 8 8.07027 6.81538 1 5 4 8 8.26273 3.78634 1 5 -4 8 1.89801 2.23128 1 5 -4 9 0.23536 2.44896 1 5 4 9 2.34441 2.66276 1 5 4 10 6.17954 9.42249 1 5 4 10 0.84893 3.10378 1 5 4 11 15.8104 10.5246 1 5 -4 11 6.19300 9.83147 1 -5 5 13 9.72760 3.83049 1 -5 -5 13 7.77692 4.90248 1 5 5 -13 5.08857 8.53275 1 -5 5 12 1.24416 3.23616 1 -5 -5 12 3.00649 3.74685 1 5 -5 -11 10.7386 6.38250 1 5 -5 -10 20.6505 5.90889 1 -5 5 10 13.0650 3.67836 1 -5 -5 10 10.3442 4.10995 1 5 5 -10 28.6778 8.75420 1 5 -5 -9 7.30700 3.95736 1 -5 5 9 7.88426 2.69922 1 -5 -5 9 6.74913 2.80139 1 5 5 -9 22.9902 8.64391 1 5 -5 -8 2.34253 3.50490 1 -5 -5 8-0.35358 2.91474 1 -5 5 8 0.88324 1.54858 1 -5 5 7 4.98157 1.68429 1 5 -5 -7 4.85047 3.04126 1 -5 -5 7 3.96263 3.16628 1 5 -5 -6 9.03406 2.62861 1 -5 5 6 6.12535 1.20085 1 5 5 -6 8.50154 4.81376 1 -5 -5 6 5.93640 2.30120 1 -5 -5 5 1.60359 2.44024 1 5 5 -5 1.04899 3.70797 1 -5 -5 4 1.02633 2.48741 1 5 5 -4-2.49705 3.34675 1 -5 -5 3 128.781 8.24173 1 5 5 -3 120.393 10.6259 1 5 5 -2 58.1609 7.59951 1 -5 -5 2 53.8532 5.45360 1 5 5 -1 118.046 9.72759 1 -5 -5 1 123.493 8.05019 1 5 -5 0 2.64193 1.18197 1 -5 -5 0 3.47400 2.50536 1 5 -5 0-1.50694 1.45802 1 5 5 0 6.70929 3.73555 1 5 5 1 5.30210 3.83701 1 5 -5 1 1.28352 1.19569 1 5 5 1-0.99948 2.38631 1 5 -5 1-1.48968 2.13057 1 -5 -5 -1 0.31984 1.77765 1 -5 -5 -2 12.6458 3.09041 1 5 5 2 12.9268 5.06161 1 5 -5 2 7.08030 2.01902 1 5 -5 2 9.01043 4.04682 1 5 5 2 15.1966 4.05298 1 -5 -5 -3 15.4109 3.48231 1 5 5 3 22.1485 7.50403 1 5 -5 3 16.2593 4.59817 1 5 5 3 19.1538 4.90064 1 5 -5 3 9.08501 2.15397 1 -5 -5 -4 3.08013 2.26033 1 5 5 4-0.17957 4.90885 1 5 -5 4 3.32942 4.21824 1 5 5 4-1.28539 3.05475 1 5 -5 4 2.35099 2.17230 1 5 -5 5 0.60292 1.98500 1 5 5 5-4.62201 5.92954 1 5 -5 5 1.74801 5.74394 1 5 5 5 2.36021 2.38522 1 5 5 6 3.65544 3.24657 1 5 -5 6 3.63429 5.56581 1 5 5 7 35.3473 5.82679 1 5 5 7 43.6274 11.6566 1 5 -5 7 37.4137 5.30295 1 5 -5 7 17.6969 7.50033 1 5 5 8 7.08972 8.75946 1 5 -5 8 7.23540 6.30129 1 5 -5 8 0.23327 2.65783 1 5 5 9 19.3802 5.47533 1 5 5 9 27.9947 12.3394 1 5 -5 9 4.52272 7.32315 1 5 -5 9 15.8944 4.02847 1 -5 -6 8 7.71153 3.59463 1 -5 -6 7 3.95943 3.59376 1 5 6 -7 0.30538 6.36137 1 5 6 -6 13.3369 7.13770 1 -5 -6 5 2.80357 2.66814 1 5 6 -5 5.19414 7.25641 1 -5 -6 4 0.84458 2.22914 1 5 6 -3 6.28001 4.47869 1 -5 -6 3 15.3007 2.95938 1 5 6 -2 2.49836 4.24623 1 -5 -6 2 5.67263 2.17686 1 -5 -6 1 11.0096 3.00421 1 5 6 -1 10.7125 4.64038 1 5 6 0 0.02142 3.49887 1 5 6 0 4.77329 4.87590 1 5 6 1 6.62589 4.07060 1 5 6 1 0.91714 5.29716 1 -5 -6 -1 2.38536 2.09228 1 -5 -6 -2 10.7109 2.77892 1 5 6 2 11.1559 4.04882 1 5 6 2 11.2903 6.09746 1 5 6 3 4.80253 3.38430 1 5 -6 4 1.48413 1.53359 1 5 -6 4 1.84891 2.37318 1 6 0 -19 3.37045 10.6950 1 -6 0 18 9.01507 6.48401 1 -6 0 17-9.11720 6.26866 1 6 0 -17 15.6710 12.0383 1 -6 0 16-0.78296 5.43067 1 6 0 -16 1.32657 7.74233 1 -6 0 15 3.17624 4.02651 1 6 0 -15-0.37974 6.57797 1 -6 0 14 17.8373 5.61244 1 6 0 -14 15.0290 7.76834 1 -6 0 13 0.27169 3.84849 1 6 0 -13-4.63093 5.93164 1 -6 0 12 34.8496 7.06532 1 6 0 -12 48.7766 10.3084 1 -6 0 11-1.54241 2.90769 1 6 0 -11-3.82106 4.46812 1 -6 0 10 23.0358 5.21798 1 6 0 -10 22.4103 6.42781 1 -6 0 9-1.61629 2.60898 1 6 0 -9 1.90674 3.75637 1 -6 0 8 77.3576 7.98362 1 6 0 -8 74.0918 9.29415 1 6 0 -7 3.61663 2.91314 1 -6 0 7 0.73399 1.96828 1 6 0 -6 28.9926 5.71335 1 -6 0 6 26.5862 4.76182 1 6 0 -5-2.13780 2.61254 1 -6 0 5-2.12406 1.86211 1 6 0 -4-0.80086 1.82590 1 -6 0 4 3.38524 2.53758 1 -6 0 3 2.44068 1.59054 1 6 0 -3-2.18229 1.85563 1 -6 0 2-0.66388 1.90879 1 6 0 -2 1.31782 1.70142 1 -6 0 1 3.07532 2.18244 1 6 0 -1 1.96308 1.56676 1 6 0 0 7.48847 2.52579 1 -6 0 0 9.13274 2.92501 1 -6 0 -1-1.54163 1.89873 1 6 0 1-1.07258 1.76004 1 -6 0 -2 2.66400 2.05773 1 6 0 2 2.22913 1.91628 1 6 0 3 1.11869 1.66610 1 -6 0 -3 1.55939 1.90190 1 -6 0 -4-1.40863 1.90921 1 6 0 4 0.44151 1.71010 1 -6 0 -5 6.47487 2.48576 1 6 0 5 0.11590 1.89954 1 6 0 5-0.32886 3.82550 1 -6 0 -6 6.92294 2.74645 1 6 0 6 2.59272 5.59506 1 6 0 6 4.71320 2.55516 1 -6 0 -7 7.01203 2.68396 1 6 0 7 0.42979 2.01426 1 6 0 7 0.97206 5.91195 1 6 0 8-1.94908 2.61453 1 6 0 8-5.35253 5.68573 1 -6 0 -8-2.76987 2.61942 1 6 0 9-0.21288 2.13781 1 6 0 9 2.89413 7.06689 1 6 0 10 7.11901 7.31216 1 6 0 10 2.78276 2.71539 1 6 0 11 4.66969 3.34911 1 6 0 11 10.9808 8.99212 1 6 0 12 13.4080 4.74947 1 6 0 12 8.87268 9.45394 1 6 0 13 6.47801 3.86270 1 6 0 13 1.03505 9.59972 1 6 0 14 8.67673 4.55551 1 -6 -1 19 8.14592 6.93817 1 -6 1 19 3.37555 6.40556 1 6 1 -19 3.78797 11.3686 1 -6 1 18 45.3073 11.6079 1 -6 -1 18 42.6471 10.8120 1 6 -1 -18 46.4402 15.3493 1 6 1 -18 62.0017 17.9777 1 -6 -1 17 3.77528 5.05917 1 6 -1 -17-12.8472 11.2508 1 6 1 -17 15.6563 14.2072 1 -6 1 17-9.14160 6.28191 1 -6 -1 16 43.3943 10.4361 1 6 -1 -16 44.3603 14.8366 1 -6 1 16 40.6655 9.01079 1 6 1 -16 36.4125 12.6923 1 -6 1 15 5.43290 5.00004 1 -6 -1 15 15.4407 5.99854 1 6 1 -15 7.70919 7.95165 1 -6 1 14-0.42486 4.60049 1 -6 -1 14 6.09388 5.88969 1 6 -1 -14 1.90786 5.39760 1 6 1 -14-0.70926 5.71788 1 -6 1 13 2.46389 3.30204 1 -6 -1 13 12.8094 5.75618 1 6 -1 -13 11.4533 7.38290 1 6 1 -13 11.3802 6.81964 1 -6 1 12 7.31593 3.78298 1 -6 -1 12 6.60566 3.46160 1 6 -1 -12 9.28973 6.45826 1 6 1 -12 2.25132 4.68277 1 -6 1 11 17.0084 4.50922 1 -6 -1 11 15.2797 5.25478 1 6 -1 -11 9.59795 6.45419 1 6 1 -11 16.5609 5.47822 1 -6 1 10 10.8800 4.37125 1 -6 -1 10 10.7232 3.76625 1 6 -1 -10 8.32011 5.35054 1 6 1 -10 13.6853 6.06606 1 6 1 -9 37.9725 8.23275 1 -6 1 9 33.5111 5.71221 1 -6 -1 9 25.5988 5.17228 1 6 -1 -9 24.4539 6.26460 1 6 -1 -8 17.3551 5.82173 1 6 1 -8 16.9414 5.81471 1 -6 1 8 12.4872 3.57579 1 -6 -1 8 14.8257 3.99237 1 6 -1 -7 39.4071 6.74294 1 -6 1 7 33.9781 5.31381 1 -6 -1 7 44.6151 6.13721 1 6 1 -7 41.4227 6.92646 1 6 -1 -6 43.7893 6.72020 1 6 1 -6 45.6023 6.44159 1 -6 1 6 47.0625 5.93391 1 -6 -1 6 46.5776 6.19126 1 6 1 -5 5.56288 3.11293 1 -6 -1 5 11.5940 3.17736 1 -6 1 5 9.42236 3.11430 1 6 -1 -5 6.41190 2.61415 1 6 -1 -4 6.13875 2.96674 1 6 1 -4 1.51945 1.98493 1 -6 -1 4 2.72703 2.03743 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5.45217 2.40777 1 6 1 6 4.97282 4.68055 1 6 -1 6 12.5700 5.68593 1 -6 1 -6 6.03948 2.54290 1 6 1 6 7.29982 3.15139 1 -6 -1 -6 13.6851 3.46551 1 6 -1 6 7.54784 2.62888 1 -6 1 -7 10.1379 2.81002 1 6 -1 7 12.9063 3.46120 1 6 1 7 15.4854 7.77909 1 6 -1 7 22.2534 6.97274 1 -6 -1 -7 15.5746 3.88418 1 6 1 7 24.8299 4.77604 1 6 1 8 100.161 14.8102 1 6 -1 8 107.437 14.6893 1 6 1 8 83.3140 8.16179 1 6 -1 8 90.6542 8.49945 1 -6 -1 -8 94.4321 8.45328 1 6 1 9 10.7561 4.01085 1 6 -1 9 3.93496 3.52040 1 6 -1 9 4.92143 6.82783 1 6 1 9 4.54068 7.34470 1 6 1 10 6.33286 2.79857 1 6 -1 10 12.6982 3.95591 1 6 -1 10 12.5694 8.02700 1 6 1 11 7.72001 3.51079 1 6 1 11-6.71051 7.27917 1 6 -1 11 6.14481 3.70109 1 6 -1 11-5.26836 7.81560 1 6 1 12 1.96781 3.44735 1 6 -1 12 4.63788 3.79303 1 6 1 12 11.1858 8.96058 1 6 -1 12-0.95692 7.74286 1 6 -1 13 9.40408 4.97678 1 6 1 13 11.5378 12.0965 1 6 -1 13 5.66871 10.5354 1 6 1 13 3.64792 4.73334 1 6 -1 14 14.1276 5.16107 1 6 -1 14 1.57830 9.54776 1 -6 2 17 7.26132 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418.619 22.1278 1 -7 0 8 408.043 18.5528 1 7 0 -7 0.65104 2.81344 1 -7 0 7 1.29632 2.72113 1 7 0 -6 13.8847 4.41625 1 -7 0 6 7.51531 3.09736 1 7 0 -5 1.86724 2.23843 1 -7 0 5 3.50093 2.53901 1 -7 0 4 27.8260 4.58694 1 7 0 -4 22.3127 4.54343 1 -7 0 3-2.28523 2.46816 1 7 0 -3-0.05756 1.92452 1 -7 0 2 102.145 8.08886 1 7 0 -2 101.581 8.34753 1 -7 0 1 2.75768 3.05946 1 7 0 -1 1.64013 2.29987 1 7 0 0 35.5431 5.20136 1 -7 0 0 40.9332 5.39829 1 -7 0 -1 0.38520 1.74432 1 7 0 1 3.59890 2.49600 1 -7 0 -2 16.4157 4.01610 1 7 0 2 16.6886 3.86833 1 7 0 3 1.90977 2.26983 1 -7 0 -3-0.33197 1.58694 1 7 0 4 6.30406 6.04691 1 7 0 4 4.85099 2.89658 1 -7 0 -4 5.97723 2.65291 1 7 0 5-0.75685 5.80354 1 -7 0 -5 2.01104 2.15540 1 7 0 5-2.49355 2.59610 1 7 0 6 10.3836 6.32725 1 7 0 6 10.9772 3.69098 1 -7 0 -6 11.5032 3.86094 1 7 0 7 0.98438 5.34895 1 -7 0 -7 0.67871 2.15320 1 7 0 7 4.18169 2.53237 1 7 0 8 74.9603 8.18323 1 -7 0 -8 73.5913 8.00546 1 7 0 8 69.6848 12.7628 1 -7 0 -9-0.87220 2.77943 1 7 0 9-0.52671 3.04782 1 7 0 10 4.04379 2.89966 1 7 0 10 3.03932 7.19793 1 7 0 11-3.66063 3.30450 1 7 0 11-5.04327 9.77160 1 7 0 12 22.7531 5.85786 1 7 0 12 21.4113 10.3705 1 7 0 13 1.35528 4.20737 1 -7 1 19 4.79675 7.25225 1 7 -1 -19 14.2685 14.2479 1 7 1 -19 9.51883 14.2749 1 7 -1 -18 150.831 24.7844 1 -7 1 18 107.582 15.1206 1 -7 -1 18 121.709 16.3005 1 7 1 -18 160.692 27.1781 1 -7 1 17 10.6516 6.67014 1 -7 -1 17 0.49282 5.86611 1 7 1 -17 9.74562 11.2514 1 7 -1 -16 131.580 20.7049 1 7 1 -16 133.210 20.8803 1 -7 1 16 119.170 14.5083 1 -7 -1 16 104.954 14.1016 1 -7 1 15 3.26098 4.66885 1 -7 -1 15 1.31770 4.66571 1 7 -1 -15 1.20710 6.52883 1 7 1 -15 4.42894 5.98714 1 -7 1 14 3.18398 3.29788 1 -7 -1 14-6.75552 4.48617 1 7 -1 -14 2.19239 7.17387 1 7 1 -14 8.66393 6.96589 1 -7 1 13 10.8134 4.96560 1 -7 -1 13 8.70319 4.89788 1 7 -1 -13 8.41735 7.29760 1 7 1 -13 12.8915 8.35958 1 -7 -1 12 51.5306 7.87466 1 -7 1 12 46.0861 7.74034 1 7 -1 -12 48.7593 11.2350 1 7 1 -12 47.8279 11.1137 1 -7 1 11 0.51167 2.80514 1 -7 -1 11-0.97367 3.15160 1 7 -1 -11 5.69898 4.27656 1 7 1 -11 7.24276 4.72110 1 7 1 -10 5.18863 3.72632 1 -7 1 10 11.3794 4.59698 1 -7 -1 10 10.2838 3.77249 1 7 -1 -10 10.1243 5.44522 1 7 -1 -9 61.6674 9.29314 1 7 1 -9 76.4575 11.2403 1 -7 1 9 72.3821 8.25588 1 -7 -1 9 52.5611 7.17204 1 7 -1 -8 18.6068 5.29565 1 7 1 -8 26.0161 6.82537 1 -7 1 8 22.1439 4.65245 1 -7 -1 8 21.2703 4.92070 1 7 -1 -7 55.0460 7.95385 1 7 1 -7 51.1478 7.90610 1 -7 -1 7 55.1375 6.82032 1 -7 1 7 55.6378 7.00976 1 7 -1 -6 129.266 11.1323 1 7 1 -6 139.334 11.8104 1 -7 -1 6 132.226 10.4117 1 -7 1 6 131.173 9.74126 1 7 -1 -5 12.9611 3.78638 1 7 1 -5 16.8675 4.30982 1 -7 -1 5 12.8133 3.83166 1 -7 1 5 15.1950 3.96910 1 -7 -1 4 16.9855 4.36984 1 -7 1 4 8.37710 3.24027 1 7 -1 -4 13.3910 3.63932 1 7 1 -4 10.4360 3.18468 1 -7 -1 3 69.8003 7.09822 1 -7 1 3 65.6666 6.57577 1 7 -1 -3 54.4759 6.51541 1 7 1 -3 54.2239 6.43118 1 -7 -1 2 169.096 10.6653 1 -7 1 2 161.570 9.72899 1 7 1 -2 152.347 10.6684 1 7 -1 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7.46726 1 -7 -1 -7 0.35225 2.15932 1 7 1 7-0.26202 2.06072 1 7 -1 7 0.80031 2.03855 1 7 -1 8 88.5688 15.2431 1 7 1 8 69.7658 13.1223 1 -7 -1 -8 85.2599 8.26553 1 7 1 8 59.6996 7.61184 1 7 -1 8 77.6061 8.11929 1 -7 1 -8 98.0506 8.89465 1 7 -1 9 3.46542 6.37051 1 7 1 9 5.88275 7.08720 1 -7 -1 -9 13.3753 4.18821 1 7 1 9 10.9682 4.03303 1 7 -1 9 9.10964 3.87584 1 7 -1 10 8.09815 3.63664 1 7 1 10 12.5923 6.90442 1 7 -1 10 24.5478 10.0344 1 7 1 10 14.2618 4.54483 1 7 -1 11-3.06911 3.69849 1 7 1 11 0.85067 8.14251 1 7 1 11 3.66992 3.02765 1 7 1 12 11.7933 5.06551 1 7 -1 12 13.4922 5.50276 1 7 1 12 10.3816 9.48244 1 7 -1 12 3.43946 9.22198 1 7 1 13 12.8590 5.98917 1 7 -1 13 13.9333 5.40884 1 7 -2 -18 34.5484 15.3756 1 7 2 -18 1.04671 13.1263 1 -7 -2 17 3.80275 5.79233 1 7 2 -17 4.56429 10.3005 1 -7 2 16 20.3620 6.96831 1 -7 -2 16 21.2786 6.46934 1 7 -2 -16 24.6506 12.2076 1 7 2 -16 18.2733 11.9688 1 -7 2 15 11.8736 5.78952 1 -7 -2 15 7.67264 5.41457 1 7 -2 -15 13.6634 6.49648 1 7 2 -15 30.3127 11.5869 1 -7 2 14 16.9198 5.88895 1 -7 -2 14 15.0009 6.04545 1 7 -2 -14 26.8340 9.38443 1 7 2 -14 18.9550 9.56822 1 -7 2 13 30.7154 7.12358 1 -7 -2 13 31.5694 7.20082 1 7 -2 -13 30.0845 10.1552 1 7 2 -13 33.4881 10.2927 1 -7 2 12 25.7489 6.59643 1 -7 -2 12 22.0273 6.29809 1 7 -2 -12 16.8176 6.59669 1 7 2 -12 42.2939 11.3361 1 -7 2 11 52.1679 7.65896 1 -7 -2 11 50.7710 7.92531 1 7 -2 -11 53.7721 9.95647 1 7 2 -11 55.5248 10.3424 1 7 -2 -10 112.039 13.4717 1 7 2 -10 113.928 13.7435 1 -7 2 10 109.941 10.0314 1 -7 -2 10 104.782 10.6398 1 7 -2 -9 125.344 13.2168 1 7 2 -9 130.530 14.6314 1 -7 2 9 131.170 10.7123 1 -7 -2 9 113.870 11.2562 1 7 -2 -8 58.4115 8.94647 1 7 2 -8 55.1657 9.36333 1 -7 2 8 54.7262 6.87623 1 -7 -2 8 54.8714 7.40797 1 7 -2 -7 2.32657 3.63152 1 7 2 -7 0.03079 3.04013 1 -7 -2 7 3.49583 2.21052 1 -7 2 7 5.06874 1.99672 1 7 -2 -6 5.82852 4.00912 1 7 2 -6 2.23893 2.68922 1 -7 -2 6 4.18658 3.02565 1 -7 2 6 0.48520 1.81830 1 -7 2 5 6.33815 2.83351 1 7 -2 -5 5.26137 2.85097 1 7 2 -5 1.42523 2.64796 1 -7 -2 5 1.35091 2.90178 1 -7 -2 4 39.1982 5.71089 1 -7 2 4 30.9984 4.47471 1 7 -2 -4 31.1079 5.03740 1 7 2 -4 29.1013 5.49207 1 -7 -2 3 63.9087 6.92714 1 -7 2 3 69.0327 6.57950 1 7 -2 -3 68.8120 7.32808 1 7 2 -3 65.7700 7.79093 1 -7 -2 2 17.9885 4.53598 1 -7 2 2 19.5192 3.96864 1 7 2 -2 17.9565 4.83314 1 7 -2 -2 18.7342 4.55247 1 -7 -2 1 151.637 10.2360 1 -7 2 1 138.932 8.69610 1 7 2 -1 136.423 10.3135 1 7 -2 -1 128.655 9.21626 1 -7 -2 0 42.5040 5.57232 1 -7 2 0 43.3219 5.06570 1 7 2 0 46.5089 6.41826 1 7 -2 0 40.1613 5.13996 1 -7 -2 -1 7.10879 3.13308 1 7 2 1-1.24294 1.79756 1 7 -2 1 2.60236 2.44091 1 -7 2 -1 2.77197 2.04141 1 7 2 2 79.5310 7.98934 1 7 -2 2 82.3208 7.40648 1 -7 -2 -2 90.5844 8.15545 1 -7 2 -2 91.8578 7.52312 1 -7 2 -3 7.09140 2.51864 1 7 -2 3-1.10176 4.30093 1 7 2 3 0.97210 2.50899 1 7 -2 3 5.77700 2.58448 1 -7 -2 -3 5.62570 2.75556 1 7 -2 4 8.49207 5.02791 1 7 2 4 9.06965 3.29184 1 7 -2 4 11.1906 3.25148 1 -7 2 -4 10.5968 2.78603 1 -7 -2 -4 10.6429 3.54981 1 7 2 5 23.6548 8.17364 1 -7 -2 -5 25.9488 4.96074 1 -7 2 -5 23.0214 4.10546 1 7 -2 5 31.7622 8.18997 1 7 2 5 23.3452 4.78480 1 7 -2 5 23.4083 4.53775 1 7 -2 6 76.0559 12.2021 1 -7 -2 -6 69.2610 7.47803 1 7 2 6 67.8295 12.0971 1 7 2 6 64.1364 7.56157 1 -7 2 -6 74.0293 6.95495 1 7 -2 6 67.3156 7.29355 1 7 2 7 22.1880 8.47009 1 -7 -2 -7 37.3036 5.98326 1 7 -2 7 46.8251 10.8088 1 7 -2 7 39.7115 6.03867 1 7 2 7 21.0161 4.72867 1 -7 2 -7 36.8465 5.65039 1 -7 -2 -8 35.3916 5.70610 1 7 2 8 33.1979 10.8443 1 7 -2 8 47.3868 11.4948 1 7 -2 8 42.8611 6.16840 1 7 2 8 29.3743 5.68159 1 7 2 9 4.92467 7.22921 1 7 -2 9 3.28258 7.12359 1 -7 -2 -9-1.71601 2.82090 1 7 2 9 0.27679 2.99312 1 7 -2 9 5.16196 3.27660 1 7 -2 10 4.58188 3.84280 1 7 2 10 10.8021 8.04922 1 7 -2 10-4.84366 7.33243 1 7 2 10-2.42584 3.29930 1 7 -2 11 4.84180 4.47701 1 7 -2 12 4.37638 4.43933 1 7 2 12 12.7878 11.6362 1 7 -2 12 22.8824 12.2726 1 7 2 12 15.5634 6.05514 1 -7 -3 17 12.0663 7.40138 1 7 -3 -17 9.64790 9.61101 1 -7 -3 16 6.42133 6.40783 1 7 -3 -16 7.54218 10.2944 1 7 3 -16 2.17256 9.90797 1 -7 -3 15 6.95831 5.90681 1 -7 3 14-1.16705 4.87320 1 -7 -3 14 3.97932 5.41259 1 7 -3 -14 18.8329 9.58003 1 7 3 -14 8.54712 7.02031 1 -7 3 13 12.5731 4.82835 1 -7 -3 13 11.5882 5.61141 1 7 -3 -13 16.6843 9.53062 1 7 3 -13 5.93318 8.65168 1 -7 3 12 1.61845 3.28484 1 -7 -3 12 5.92896 4.74058 1 7 -3 -12 9.82153 6.27134 1 7 3 -12 7.17236 9.03023 1 -7 3 11 25.7888 5.67334 1 -7 -3 11 24.7414 5.74907 1 7 -3 -11 31.8809 8.86885 1 7 3 -11 26.9156 9.27598 1 -7 3 10 16.0577 4.30054 1 -7 -3 10 26.6397 6.62296 1 7 -3 -10 8.05088 4.78582 1 7 3 -10 11.9541 5.90002 1 7 3 -9 15.4339 7.42207 1 -7 3 9-1.43547 2.41741 1 -7 -3 9 6.80933 3.49132 1 7 -3 -9 15.2316 5.98680 1 7 3 -8 11.2787 4.45929 1 -7 -3 8 7.10629 3.92208 1 -7 3 8 8.47901 3.43552 1 7 -3 -8 7.84657 4.48678 1 7 -3 -7 3.41374 4.12585 1 7 3 -7-1.74727 3.92585 1 -7 -3 7 2.37797 2.74160 1 -7 3 7-0.98901 2.31475 1 7 -3 -6 38.7755 6.39542 1 7 3 -6 38.3284 6.72549 1 -7 -3 6 29.4058 5.34851 1 -7 3 6 37.6536 5.37337 1 -7 -3 5 7.24067 3.30476 1 7 -3 -5 4.68709 3.56897 1 -7 3 5 1.46676 2.17101 1 7 3 -5 1.98944 2.85056 1 -7 -3 4 2.09435 2.97431 1 7 -3 -4 5.27430 3.14854 1 7 3 -4-1.36560 3.32526 1 -7 3 4-0.90355 1.90471 1 -7 -3 3 7.66436 3.54927 1 7 -3 -3 5.77761 3.04371 1 7 3 -3 6.23064 3.38681 1 -7 3 3 7.28049 2.67225 1 -7 -3 2 77.4220 7.63537 1 -7 3 2 66.4246 5.93624 1 7 -3 -2 65.1797 6.85249 1 7 3 -2 65.8749 7.86785 1 -7 3 1 25.9731 3.81565 1 7 3 -1 21.5487 5.43051 1 -7 -3 1 24.8048 4.85242 1 7 -3 -1 25.4429 4.79595 1 -7 -3 0 154.186 10.6646 1 -7 3 0 141.270 8.30274 1 7 3 0 130.470 10.5200 1 7 -3 0 117.109 8.70693 1 -7 -3 -1 11.7830 3.73579 1 -7 3 -1 3.13061 2.02560 1 7 3 1 5.46144 3.13176 1 7 -3 1 1.98764 2.06923 1 7 3 2 10.3993 3.33478 1 7 -3 2 2.54447 3.79762 1 -7 3 -2 6.13530 2.32674 1 -7 -3 -2 6.87413 2.62675 1 7 -3 2 13.8345 3.13298 1 7 3 3 23.2573 5.08838 1 7 -3 3 18.6531 5.50523 1 7 -3 3 16.8757 3.61114 1 -7 -3 -3 22.2793 4.50300 1 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6.25316 1 -7 -4 15 3.86774 6.15582 1 7 -4 -15 6.16784 8.25373 1 -7 4 14 19.0175 6.15606 1 -7 -4 14 5.74394 5.16272 1 7 -4 -14 24.8333 9.96428 1 7 4 -14 23.6064 13.5425 1 -7 4 13 19.2195 5.55564 1 -7 -4 13 35.3462 8.16689 1 7 -4 -13 26.0321 10.3799 1 7 4 -13 19.2467 9.67649 1 -7 4 12 1.92808 3.39884 1 7 4 -12 14.1881 9.48336 1 -7 4 11 2.16509 2.91830 1 -7 -4 11 12.2897 5.23784 1 7 -4 -11 6.44718 7.35293 1 7 4 -11-2.89113 6.98876 1 7 -4 -10 230.376 18.9269 1 7 4 -10 209.438 19.9631 1 -7 -4 10 203.909 15.3119 1 -7 4 10 189.465 12.6406 1 -7 -4 9 0.97384 3.51244 1 7 -4 -9-4.55355 5.03261 1 -7 4 9 2.74795 3.24326 1 7 4 -9 1.95494 5.21548 1 7 -4 -8-1.63504 4.93013 1 -7 -4 8 8.24835 3.44147 1 -7 4 8 4.96358 3.04151 1 7 4 -8-0.08337 4.63540 1 7 4 -7 15.1613 5.02234 1 -7 4 7 18.0892 4.12316 1 7 -4 -7 11.8418 4.78948 1 -7 -4 7 17.1586 4.79009 1 -7 -4 6 3.34202 3.05134 1 7 4 -6 5.17342 4.81537 1 -7 4 6 4.22277 2.12862 1 7 -4 -6 6.56345 4.10409 1 7 4 -5 10.7338 4.22804 1 -7 -4 5 14.5887 3.59634 1 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-1 5.69891 4.86182 1 12 2 1 7.86463 4.76079 1 12 -2 1 6.70098 5.04781 1 -12 2 -2 2.65486 4.21029 1 12 -2 2 14.4233 5.90441 1 -12 -2 -3 6.99636 5.16166 1 12 2 3 5.35609 5.08095 1 12 -3 -10 38.1582 11.3957 1 -12 -3 10 25.0751 7.11788 1 12 3 -10 36.2654 11.5182 1 -12 3 10 52.9175 9.33047 1 12 -3 -9 10.9461 7.23655 1 12 3 -9 10.6519 8.17328 1 -12 -3 9 9.22567 6.18249 1 -12 3 9 6.62998 6.23767 1 12 3 -8 5.10960 8.61511 1 -12 3 8 3.76348 4.43232 1 12 3 -7 2.08352 5.31166 1 -12 -3 7 1.14672 3.93866 1 -12 3 7 0.91812 3.63189 1 12 -3 -6 25.5458 8.54599 1 -12 -3 6 26.0232 7.57984 1 -12 3 6 7.08184 3.87004 1 12 -3 -5 11.0761 6.65343 1 12 3 -5 10.4226 7.09472 1 -12 -3 5 8.94674 6.16144 1 -12 3 5 5.85430 4.32226 1 12 3 -4 12.1497 7.71663 1 -12 -3 4 4.30304 4.85697 1 -12 3 3 26.9082 7.30145 1 12 -3 -3 14.3130 7.16249 1 12 3 -3 24.6138 8.41924 1 -12 -3 3 17.0623 6.84570 1 -12 3 2 46.5882 7.99904 1 12 -3 -2 35.6413 8.90137 1 12 3 -2 30.1893 8.45830 1 -12 -3 2 31.1252 7.11441 1 -12 -3 1 7.04007 5.27906 1 -12 3 1 6.95937 4.10095 1 -12 -3 0 12.1372 5.89722 1 -12 3 0 5.87599 4.51806 1 12 3 0 3.24974 5.70299 1 12 -3 0 19.6500 7.23016 1 13 0 -12 6.18266 7.54735 1 13 0 -11 1.14591 8.19515 1 -13 0 10 96.6906 12.0766 1 13 0 -10 105.208 15.9476 1 -13 0 9 23.4116 8.38639 1 13 0 -9 8.09675 8.09451 1 -13 0 8 130.041 13.6106 1 13 0 -8 120.402 15.9159 1 13 0 -7 22.8826 10.0721 1 -13 0 7 18.3555 8.04345 1 13 0 -6 17.1012 8.00860 1 -13 0 6 28.2713 7.35644 1 13 0 -5 17.0414 7.12821 1 -13 0 5 15.6428 7.38668 1 13 0 -4 42.2381 9.38289 1 -13 0 4 48.5430 8.95969 1 13 0 -3 0.35458 4.49768 1 -13 0 3 5.51469 5.34655 1 13 0 -2 5.36978 4.74206 1 -13 0 2 10.6326 5.71296 1 -13 0 1 6.10941 4.40816 1 13 0 -1 6.62392 5.07169 1 13 0 0 2.88716 5.61413 1 -13 1 12 11.7360 5.88726 1 13 -1 -12 9.11970 11.0446 1 13 1 -12 2.81232 8.38064 1 -13 -1 12 11.2448 5.36302 1 -13 -1 11 1.14292 5.14942 1 -13 1 11 8.27759 6.08579 1 13 -1 -11 6.18274 7.23725 1 -13 -1 10 8.62966 5.77592 1 -13 1 10 10.2928 4.82110 1 13 -1 -10 15.4669 7.91377 1 -13 -1 9 8.18499 6.08007 1 13 1 -9 1.23825 6.48485 1 -13 1 9 9.19240 5.34793 1 13 -1 -8 21.7695 8.95483 1 13 1 -8 3.33526 5.68301 1 13 -1 -7 8.17472 6.72808 1 -13 -1 7 11.4083 6.32320 1 13 -1 -6 7.69084 4.96167 1 13 1 -6 5.65618 5.43863 1 -13 -1 6 2.85361 4.93653 1 -13 1 6 5.52733 4.89167 1 13 -1 -5 3.54269 5.49636 1 -13 -1 5 3.35708 5.11405 1 -13 1 5 0.68444 5.21859 1 13 1 -4 7.92452 5.55084 1 -13 -1 4 13.3463 6.01011 1 13 -1 -3 13.0613 7.02399 1 13 1 -3 23.5374 8.14312 1 -13 -1 3 13.4333 6.22217 1 -13 1 3 5.04490 4.27447 1 -13 1 2 17.7311 5.40984 1 13 -1 -2 2.43246 5.13928 1 13 1 -2 11.0818 5.37816 1 -13 -1 2 5.37644 5.82526 1 -13 1 1 10.2400 5.30937 1 13 1 -1 12.7572 7.89895 1 13 -1 -1 14.0345 6.73032 1 -13 -1 0 56.5923 10.0733 1 -13 1 0 74.4445 10.6687 1 13 1 0 55.2480 10.1569 1 13 -1 0 51.0241 9.90312 1 -13 -1 -1 6.88635 6.40618 1 -13 1 -1 14.6427 5.74571 1 13 1 1 11.3878 6.37521 1 13 -1 1 3.48954 6.07838 1 -13 2 10 1.30113 4.86810 1 -13 -2 9 7.99956 5.93374 1 -13 2 9 4.64482 5.43517 1 13 -2 -8 5.84020 5.99449 1 13 2 -8 1.92162 5.82128 1 -13 -2 8 18.0557 7.58778 1 -13 2 8 9.96851 4.90786 1 -13 -2 7 9.52502 6.10635 1 -13 2 7 2.95240 5.71158 1 13 -2 -6 3.40529 5.12404 1 13 2 -6 3.62234 5.54022 1 -13 -2 6 9.56504 5.47824 1 -13 2 6 18.1010 6.72456 1 13 -2 -5 2.29752 5.13109 1 -13 -2 5 9.64210 6.00586 1 -13 2 5 2.07865 5.07507 1 13 2 -4 12.2822 7.46347 1 -13 -2 4 12.7540 5.85327 1 -13 2 4 11.5813 5.91737 1 -13 2 3 22.7586 7.09700 1 13 -2 -3 5.22433 5.01790 1 13 2 -3 5.63927 5.13387 1 -13 -2 3 11.0670 6.31089 1 -13 2 2 28.4053 6.87158 1 13 -2 -2 15.0142 7.09042 1 13 2 -2 8.22271 6.03999 1 -13 -2 2 24.7016 7.71179 1 -13 -2 1 5.12111 4.56578 1 -13 2 1 3.77790 4.23500 1 13 -2 -1 1.11761 5.18764 1 13 2 -1 12.5788 7.52914 1 14 0 -7 5.85959 7.12114 1 -14 0 7 16.3970 7.78208 1 14 0 -6 6.00466 6.29958 1 -14 0 6 5.54063 5.64278 1 0 0 0 0.00 0.00 0 TITL av_pa_Na4PhPh in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 12.667246 6.162371 18.015660 90.0000 106.9670 90.0000 ZERR 6.00 0.001418 0.000568 0.001996 0.0000 0.0116 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 66.00 60.00 6.00 6.00 TREF HKLF 4 END ; _shelx_hkl_checksum 29383 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Na1 Na 0.4492(2) 0.7091(4) 0.77136(16) 0.0296(8) Uani 1 1 d . . . . . Na2 Na 0.3352(2) 0.4037(4) 0.63660(17) 0.0350(8) Uani 1 1 d . . . . . P3 P 0.59528(15) 0.7213(3) 0.65864(11) 0.0232(5) Uani 1 1 d . . . . . C4 C 0.5398(5) 0.8782(10) 0.5693(4) 0.0218(17) Uani 1 1 d . . . . . C5 C 0.5843(5) 0.8540(10) 0.5071(4) 0.0212(16) Uani 1 1 d . . . . . H5 H 0.642367 0.752267 0.512348 0.025 Uiso 1 1 calc R U . . . C6 C 0.5478(5) 0.9719(10) 0.4370(4) 0.0226(17) Uani 1 1 d . . . . . O7 O 0.5912(4) 0.9379(7) 0.3775(3) 0.0272(12) Uani 1 1 d . . . . . O8 O 0.5140(4) 0.5488(7) 0.6666(3) 0.0280(12) Uani 1 1 d . . . . . O9 O 0.6328(4) 0.8728(7) 0.7279(3) 0.0306(13) Uani 1 1 d . . . . . C10 C 0.7177(6) 0.5823(11) 0.6482(4) 0.0270(17) Uani 1 1 d . . . . . C11 C 0.7074(6) 0.3795(11) 0.6098(4) 0.0313(19) Uani 1 1 d . . . . . H11 H 0.636062 0.321157 0.586059 0.038 Uiso 1 1 calc R U . . . C12 C 0.8004(7) 0.2646(13) 0.6066(5) 0.045(2) Uani 1 1 d . . . . . H12 H 0.792589 0.129335 0.580202 0.054 Uiso 1 1 calc R U . . . C13 C 0.9049(7) 0.3483(15) 0.6419(5) 0.052(2) Uani 1 1 d . . . . . H13 H 0.968628 0.269059 0.640534 0.063 Uiso 1 1 calc R U . . . C14 C 0.9162(7) 0.5491(15) 0.6795(5) 0.052(2) Uani 1 1 d . . . . . H14 H 0.987568 0.607606 0.703006 0.062 Uiso 1 1 calc R U . . . C15 C 0.8234(6) 0.6619(13) 0.6824(5) 0.038(2) Uani 1 1 d . . . . . H15 H 0.831944 0.797815 0.708339 0.045 Uiso 1 1 calc R U . . . O21 O 0.2908(4) 0.7628(8) 0.6547(3) 0.0493(16) Uani 1 1 d . . . . . H21 H 0.325148 0.868813 0.643750 0.074 Uiso 1 1 calc R U . . . C22 C 0.1902(7) 0.8327(16) 0.6619(6) 0.068(3) Uani 1 1 d . . . . . H22A H 0.132095 0.803860 0.613451 0.102 Uiso 1 1 calc R U . . . H22B H 0.193782 0.988859 0.672641 0.102 Uiso 1 1 calc R U . . . H22C H 0.173730 0.754855 0.704612 0.102 Uiso 1 1 calc R U . . . O23 O 0.1671(6) 0.3954(14) 0.5368(5) 0.101(3) Uani 1 1 d . . . . . H23 H 0.185323 0.462059 0.501799 0.121 Uiso 1 1 d R U . . . C24 C 0.0994(10) 0.226(2) 0.5048(7) 0.108(5) Uani 1 1 d . . . . . H24A H 0.022443 0.266411 0.498532 0.161 Uiso 1 1 calc R U . . . H24B H 0.118627 0.099091 0.539028 0.161 Uiso 1 1 calc R U . . . H24C H 0.108521 0.190257 0.454056 0.161 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Na1 0.0419(17) 0.0214(15) 0.0292(18) -0.0015(12) 0.0159(13) 0.0005(12) Na2 0.0390(18) 0.0318(16) 0.0349(19) 0.0001(13) 0.0119(14) 0.0023(13) P3 0.0318(11) 0.0198(10) 0.0221(11) 0.0020(8) 0.0145(8) 0.0006(8) C4 0.031(4) 0.016(4) 0.019(4) -0.003(3) 0.010(3) -0.005(3) C5 0.025(4) 0.018(4) 0.022(4) 0.001(3) 0.009(3) 0.001(3) C6 0.028(4) 0.018(4) 0.025(4) -0.007(3) 0.012(3) -0.007(3) O7 0.040(3) 0.026(3) 0.023(3) 0.000(2) 0.019(2) 0.000(2) O8 0.036(3) 0.022(3) 0.033(3) 0.009(2) 0.019(2) 0.003(2) O9 0.046(3) 0.026(3) 0.023(3) -0.003(2) 0.014(2) 0.005(2) C10 0.034(4) 0.029(4) 0.021(4) 0.004(3) 0.014(3) -0.002(3) C11 0.032(4) 0.023(4) 0.041(5) 0.002(3) 0.015(4) 0.001(3) C12 0.054(6) 0.036(5) 0.053(6) -0.007(4) 0.027(5) 0.007(4) C13 0.043(6) 0.061(6) 0.063(7) 0.003(5) 0.032(5) 0.023(5) C14 0.031(5) 0.066(6) 0.061(7) -0.005(5) 0.019(4) -0.002(4) C15 0.036(5) 0.039(5) 0.043(5) -0.005(4) 0.020(4) -0.005(4) O21 0.050(4) 0.031(3) 0.080(5) 0.009(3) 0.041(3) 0.001(3) C22 0.042(6) 0.068(7) 0.099(9) -0.011(6) 0.026(6) 0.002(5) O23 0.074(5) 0.102(6) 0.111(7) -0.020(5) 0.002(5) -0.008(5) C24 0.103(10) 0.141(12) 0.079(9) -0.005(9) 0.025(8) -0.042(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O9 Na1 O8 144.9(2) 2_646 2_656 ? O9 Na1 O7 83.69(18) 2_646 4_576 ? O8 Na1 O7 87.63(18) 2_656 4_576 ? O9 Na1 O21 82.56(18) 2_646 . ? O8 Na1 O21 106.51(19) 2_656 . ? O7 Na1 O21 165.4(2) 4_576 . ? O9 Na1 O8 84.06(17) 2_646 . ? O8 Na1 O8 130.80(17) 2_656 . ? O7 Na1 O8 96.86(18) 4_576 . ? O21 Na1 O8 76.84(18) . . ? O9 Na1 O9 136.15(19) 2_646 . ? O8 Na1 O9 75.59(16) 2_656 . ? O7 Na1 O9 82.53(16) 4_576 . ? O21 Na1 O9 104.17(18) . . ? O8 Na1 O9 56.75(15) . . ? O9 Na1 Na2 133.67(16) 2_646 2_656 ? O8 Na1 Na2 50.23(13) 2_656 2_656 ? O7 Na1 Na2 50.04(13) 4_576 2_656 ? O21 Na1 Na2 143.12(17) . 2_656 ? O8 Na1 Na2 97.47(15) . 2_656 ? O9 Na1 Na2 47.58(12) . 2_656 ? O9 Na1 Na2 49.50(14) 2_646 . ? O8 Na1 Na2 154.19(17) 2_656 . ? O7 Na1 Na2 118.02(15) 4_576 . ? O21 Na1 Na2 48.15(14) . . ? O8 Na1 Na2 48.52(13) . . ? O9 Na1 Na2 103.44(14) . . ? Na2 Na1 Na2 145.28(11) 2_656 . ? O9 Na1 C6 74.17(18) 2_646 4_576 ? O8 Na1 C6 83.93(19) 2_656 4_576 ? O7 Na1 C6 24.69(16) 4_576 4_576 ? O21 Na1 C6 150.5(2) . 4_576 ? O8 Na1 C6 117.54(19) . 4_576 ? O9 Na1 C6 105.14(18) . 4_576 ? Na2 Na1 C6 64.14(15) 2_656 4_576 ? Na2 Na1 C6 120.37(16) . 4_576 ? O9 Na1 P3 112.11(16) 2_646 . ? O8 Na1 P3 102.39(15) 2_656 . ? O7 Na1 P3 94.54(14) 4_576 . ? O21 Na1 P3 86.10(15) . . ? O8 Na1 P3 28.52(11) . . ? O9 Na1 P3 29.03(10) . . ? Na2 Na1 P3 74.53(9) 2_656 . ? Na2 Na1 P3 74.47(9) . . ? C6 Na1 P3 119.19(15) 4_576 . ? O9 Na1 P3 22.63(12) 2_646 2_646 ? O8 Na1 P3 130.31(16) 2_656 2_646 ? O7 Na1 P3 62.04(12) 4_576 2_646 ? O21 Na1 P3 104.77(15) . 2_646 ? O8 Na1 P3 93.34(12) . 2_646 ? O9 Na1 P3 131.16(13) . 2_646 ? Na2 Na1 P3 111.97(10) 2_656 2_646 ? Na2 Na1 P3 70.03(8) . 2_646 ? C6 Na1 P3 51.75(13) 4_576 2_646 ? P3 Na1 P3 117.40(9) . 2_646 ? O9 Na1 Na1 53.88(12) 2_646 2_646 ? O8 Na1 Na1 148.21(18) 2_656 2_646 ? O7 Na1 Na1 66.67(13) 4_576 2_646 ? O21 Na1 Na1 100.95(17) . 2_646 ? O8 Na1 Na1 42.05(12) . 2_646 ? O9 Na1 Na1 82.49(14) . 2_646 ? Na2 Na1 Na1 97.99(12) 2_656 2_646 ? Na2 Na1 Na1 53.69(8) . 2_646 ? C6 Na1 Na1 79.86(15) 4_576 2_646 ? P3 Na1 Na1 63.48(10) . 2_646 ? P3 Na1 Na1 53.92(5) 2_646 2_646 ? O21 Na2 O7 170.9(2) . 3_666 ? O21 Na2 O8 82.05(19) . . ? O7 Na2 O8 88.85(18) 3_666 . ? O21 Na2 O23 85.8(3) . . ? O7 Na2 O23 101.4(3) 3_666 . ? O8 Na2 O23 141.4(3) . . ? O21 Na2 O9 84.7(2) . 2_646 ? O7 Na2 O9 94.94(19) 3_666 2_646 ? O8 Na2 O9 85.96(19) . 2_646 ? O23 Na2 O9 129.2(3) . 2_646 ? O21 Na2 Na1 121.33(18) . 2_646 ? O7 Na2 Na1 51.33(14) 3_666 2_646 ? O8 Na2 Na1 50.46(13) . 2_646 ? O23 Na2 Na1 152.7(2) . 2_646 ? O9 Na2 Na1 62.79(14) 2_646 2_646 ? O21 Na2 Na1 52.07(16) . . ? O7 Na2 Na1 121.64(16) 3_666 . ? O8 Na2 Na1 52.13(14) . . ? O23 Na2 Na1 136.7(2) . . ? O9 Na2 Na1 48.30(13) 2_646 . ? Na1 Na2 Na1 70.53(7) 2_646 . ? O21 Na2 H23 82.0 . . ? O7 Na2 H23 103.0 3_666 . ? O8 Na2 H23 123.2 . . ? O23 Na2 H23 18.3 . . ? O9 Na2 H23 145.4 2_646 . ? Na1 Na2 H23 149.2 2_646 . ? Na1 Na2 H23 133.6 . . ? O8 P3 O9 114.3(3) . . ? O8 P3 C10 107.5(3) . . ? O9 P3 C10 107.5(3) . . ? O8 P3 C4 110.9(3) . . ? O9 P3 C4 110.1(3) . . ? C10 P3 C4 106.1(3) . . ? O8 P3 Na1 51.20(19) . . ? O9 P3 Na1 65.4(2) . . ? C10 P3 Na1 137.5(2) . . ? C4 P3 Na1 115.8(2) . . ? O8 P3 Na1 113.43(19) . 2_656 ? O9 P3 Na1 35.99(18) . 2_656 ? C10 P3 Na1 134.1(2) . 2_656 ? C4 P3 Na1 78.1(2) . 2_656 ? Na1 P3 Na1 65.32(6) . 2_656 ? C5 C4 C6 119.4(6) . 3_676 ? C5 C4 P3 120.3(5) . . ? C6 C4 P3 120.2(5) 3_676 . ? C4 C5 C6 123.9(6) . . ? C4 C5 H5 118.1 . . ? C6 C5 H5 118.1 . . ? O7 C6 C5 121.7(6) . . ? O7 C6 C4 121.6(6) . 3_676 ? C5 C6 C4 116.7(6) . 3_676 ? O7 C6 Na1 47.4(3) . 4_575 ? C5 C6 Na1 127.8(4) . 4_575 ? C4 C6 Na1 94.1(4) 3_676 4_575 ? C6 O7 Na2 119.3(4) . 3_666 ? C6 O7 Na1 107.9(4) . 4_575 ? Na2 O7 Na1 78.63(17) 3_666 4_575 ? P3 O8 Na2 151.9(3) . . ? P3 O8 Na1 128.5(3) . 2_646 ? Na2 O8 Na1 79.31(16) . 2_646 ? P3 O8 Na1 100.3(2) . . ? Na2 O8 Na1 79.35(16) . . ? Na1 O8 Na1 93.26(17) 2_646 . ? P3 O9 Na1 121.4(3) . 2_656 ? P3 O9 Na2 144.7(3) . 2_656 ? Na1 O9 Na2 82.20(17) 2_656 2_656 ? P3 O9 Na1 85.6(2) . . ? Na1 O9 Na1 84.95(15) 2_656 . ? Na2 O9 Na1 69.63(15) 2_656 . ? C15 C10 C11 117.9(7) . . ? C15 C10 P3 121.7(6) . . ? C11 C10 P3 120.2(5) . . ? C12 C11 C10 120.8(7) . . ? C12 C11 H11 119.6 . . ? C10 C11 H11 119.6 . . ? C13 C12 C11 119.8(8) . . ? C13 C12 H12 120.1 . . ? C11 C12 H12 120.1 . . ? C12 C13 C14 120.0(8) . . ? C12 C13 H13 120.0 . . ? C14 C13 H13 120.0 . . ? C15 C14 C13 119.7(8) . . ? C15 C14 H14 120.1 . . ? C13 C14 H14 120.1 . . ? C14 C15 C10 121.8(8) . . ? C14 C15 H15 119.1 . . ? C10 C15 H15 119.1 . . ? C22 O21 Na2 125.1(5) . . ? C22 O21 Na1 120.2(6) . . ? Na2 O21 Na1 79.78(18) . . ? C22 O21 H21 109.5 . . ? Na2 O21 H21 122.9 . . ? Na1 O21 H21 87.5 . . ? O21 C22 H22A 109.5 . . ? O21 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? O21 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C24 O23 Na2 130.9(8) . . ? C24 O23 H23 109.5 . . ? Na2 O23 H23 100.2 . . ? O23 C24 H24A 109.5 . . ? O23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? O23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Na1 O9 2.320(5) 2_646 ? Na1 O8 2.355(5) 2_656 ? Na1 O7 2.389(5) 4_576 ? Na1 O21 2.467(6) . ? Na1 O8 2.473(5) . ? Na1 O9 2.846(6) . ? Na1 Na2 3.000(4) 2_656 ? Na1 Na2 3.078(4) . ? Na1 C6 3.088(7) 4_576 ? Na1 P3 3.122(3) . ? Na1 P3 3.371(3) 2_646 ? Na1 Na1 3.510(3) 2_646 ? Na2 O21 2.330(6) . ? Na2 O7 2.346(5) 3_666 ? Na2 O8 2.347(5) . ? Na2 O23 2.353(8) . ? Na2 O9 2.363(6) 2_646 ? Na2 H23 2.6346 . ? P3 O8 1.515(5) . ? P3 O9 1.519(5) . ? P3 C10 1.828(7) . ? P3 C4 1.832(7) . ? C4 C5 1.403(9) . ? C4 C6 1.423(9) 3_676 ? C5 C6 1.412(9) . ? C5 H5 0.9500 . ? C6 O7 1.355(8) . ? C10 C15 1.389(10) . ? C10 C11 1.416(10) . ? C11 C12 1.391(10) . ? C11 H11 0.9500 . ? C12 C13 1.390(11) . ? C12 H12 0.9500 . ? C13 C14 1.397(12) . ? C13 H13 0.9500 . ? C14 C15 1.381(11) . ? C14 H14 0.9500 . ? C15 H15 0.9500 . ? O21 C22 1.386(9) . ? O21 H21 0.8400 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? O23 C24 1.368(13) . ? O23 H23 0.8400 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O8 P3 C4 C5 -109.1(5) . . . . ? O9 P3 C4 C5 123.4(5) . . . . ? C10 P3 C4 C5 7.4(6) . . . . ? Na1 P3 C4 C5 -165.0(4) . . . . ? Na1 P3 C4 C5 140.1(5) 2_656 . . . ? O8 P3 C4 C6 71.8(6) . . . 3_676 ? O9 P3 C4 C6 -55.7(6) . . . 3_676 ? C10 P3 C4 C6 -171.8(5) . . . 3_676 ? Na1 P3 C4 C6 15.9(6) . . . 3_676 ? Na1 P3 C4 C6 -39.0(5) 2_656 . . 3_676 ? C6 C4 C5 C6 0.5(11) 3_676 . . . ? P3 C4 C5 C6 -178.7(5) . . . . ? C4 C5 C6 O7 -178.0(6) . . . . ? C4 C5 C6 C4 -0.5(10) . . . 3_676 ? C4 C5 C6 Na1 -119.8(6) . . . 4_575 ? C5 C6 O7 Na2 27.5(8) . . . 3_666 ? C4 C6 O7 Na2 -149.9(5) 3_676 . . 3_666 ? Na1 C6 O7 Na2 -86.8(3) 4_575 . . 3_666 ? C5 C6 O7 Na1 114.3(6) . . . 4_575 ? C4 C6 O7 Na1 -63.1(6) 3_676 . . 4_575 ? O9 P3 O8 Na2 104.9(6) . . . . ? C10 P3 O8 Na2 -135.9(6) . . . . ? C4 P3 O8 Na2 -20.3(7) . . . . ? Na1 P3 O8 Na2 86.6(6) . . . . ? Na1 P3 O8 Na2 65.4(7) 2_656 . . . ? O9 P3 O8 Na1 -84.3(4) . . . 2_646 ? C10 P3 O8 Na1 34.9(5) . . . 2_646 ? C4 P3 O8 Na1 150.5(3) . . . 2_646 ? Na1 P3 O8 Na1 -102.6(4) . . . 2_646 ? Na1 P3 O8 Na1 -123.8(3) 2_656 . . 2_646 ? O9 P3 O8 Na1 18.3(3) . . . . ? C10 P3 O8 Na1 137.5(3) . . . . ? C4 P3 O8 Na1 -106.9(3) . . . . ? Na1 P3 O8 Na1 -21.2(2) 2_656 . . . ? O8 P3 O9 Na1 -96.9(3) . . . 2_656 ? C10 P3 O9 Na1 143.8(3) . . . 2_656 ? C4 P3 O9 Na1 28.6(4) . . . 2_656 ? Na1 P3 O9 Na1 -81.4(3) . . . 2_656 ? O8 P3 O9 Na2 28.9(6) . . . 2_656 ? C10 P3 O9 Na2 -90.3(5) . . . 2_656 ? C4 P3 O9 Na2 154.5(5) . . . 2_656 ? Na1 P3 O9 Na2 44.5(4) . . . 2_656 ? Na1 P3 O9 Na2 125.9(7) 2_656 . . 2_656 ? O8 P3 O9 Na1 -15.6(3) . . . . ? C10 P3 O9 Na1 -134.9(2) . . . . ? C4 P3 O9 Na1 110.0(3) . . . . ? Na1 P3 O9 Na1 81.4(3) 2_656 . . . ? O8 P3 C10 C15 -142.2(6) . . . . ? O9 P3 C10 C15 -18.7(7) . . . . ? C4 P3 C10 C15 99.1(6) . . . . ? Na1 P3 C10 C15 -91.1(7) . . . . ? Na1 P3 C10 C15 10.2(8) 2_656 . . . ? O8 P3 C10 C11 32.8(7) . . . . ? O9 P3 C10 C11 156.3(6) . . . . ? C4 P3 C10 C11 -85.9(6) . . . . ? Na1 P3 C10 C11 83.9(7) . . . . ? Na1 P3 C10 C11 -174.8(4) 2_656 . . . ? C15 C10 C11 C12 0.0(11) . . . . ? P3 C10 C11 C12 -175.2(6) . . . . ? C10 C11 C12 C13 0.6(12) . . . . ? C11 C12 C13 C14 -1.1(13) . . . . ? C12 C13 C14 C15 1.0(14) . . . . ? C13 C14 C15 C10 -0.4(13) . . . . ? C11 C10 C15 C14 -0.1(11) . . . . ? P3 C10 C15 C14 175.1(7) . . . . ?