#------------------------------------------------------------------------------ #$Date: 2024-12-21 04:46:35 +0200 (Sat, 21 Dec 2024) $ #$Revision: 296941 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/35/1573523.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1573523 loop_ _publ_author_name 'Patyk-Kaźmierczak, Ewa' 'Szymańska, Kornelia' 'Kaźmierczak, Michał' _publ_section_title ; Managing negative linear compressibility and thermal expansion through steric hindrance: a case study of 1,2-bis(4'-pyridyl)ethane cocrystals. ; _journal_issue 1 _journal_name_full IUCrJ _journal_paper_doi 10.1107/S2052252524011734 _journal_volume 12 _journal_year 2025 _chemical_formula_moiety 'C12 H12 N2, C4 H6 O4' _chemical_formula_sum 'C16 H18 N2 O4' _chemical_formula_weight 302.32 _chemical_name_systematic '4,4'-Ethane-1,2-diyldipyridine succinic acid' _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-I 2ya' _space_group_name_H-M_alt 'I 1 2/a 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2023-08-24 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.17 svn.r577a77a9 for OlexSys, GUI svn.r6817) ; _cell_angle_alpha 90 _cell_angle_beta 114.32(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 16.429(12) _cell_length_b 4.4214(3) _cell_length_c 19.020(4) _cell_measurement_reflns_used 1430 _cell_measurement_temperature 295(2) _cell_measurement_theta_max 24.4260 _cell_measurement_theta_min 4.6750 _cell_volume 1259.0(11) _computing_cell_refinement 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.49 (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2014/7 (Sheldrick, 2015)' _diffrn_ambient_pressure 3290000 _diffrn_ambient_temperature 295(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16.1544 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.292 _diffrn_measured_fraction_theta_max 0.260 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -4.00 56.00 1.00 15.00 -- -0.43 -43.00 179.00 60 2 \w -33.00 29.00 1.00 15.00 -- -0.43 43.00 -28.00 62 3 \w -21.00 29.00 1.00 35.00 -- 27.06 43.00 -28.00 50 4 \w 8.00 57.00 1.00 35.00 -- 27.06 -43.00 179.00 49 5 \w -33.00 29.00 1.00 35.00 -- -27.92 43.00 -28.00 62 6 \w -4.00 28.00 1.00 35.00 -- -27.92 -43.00 179.00 32 7 \w -16.00 9.00 1.00 35.00 -- 27.06 67.00 157.00 25 8 \w -8.00 27.00 1.00 35.00 -- 27.06 -37.00 30.00 35 9 \w -4.00 49.00 1.00 35.00 -- 27.06 -53.00 17.00 53 10 \w -6.00 44.00 1.00 35.00 -- 27.06 -39.00-167.00 50 11 \w -18.00 14.00 1.00 35.00 -- 27.06 53.00 162.00 32 12 \w -88.00 -25.00 1.00 35.00 -- -27.92 134.00 123.00 63 13 \w -8.00 27.00 1.00 35.00 -- -27.92 -37.00 0.00 35 14 \w 13.00 36.00 1.00 35.00 -- -27.92-114.00 44.00 23 15 \w -57.00 -19.00 1.00 35.00 -- -27.92 77.00 -30.00 38 16 \w -14.00 17.00 1.00 35.00 -- -27.92 -53.00-162.00 31 17 \w 13.00 36.00 1.00 35.00 -- -27.92-114.00-136.00 23 18 \w -57.00 -19.00 1.00 35.00 -- -27.92 77.00 150.00 38 19 \w -19.00 14.00 1.00 15.00 -- -0.43 -19.00-150.00 33 20 \w -18.00 14.00 1.00 35.00 -- 27.06 53.00 -17.00 32 21 \w -31.00 1.00 1.00 35.00 -- 27.06 0.00 30.00 32 22 \w -31.00 1.00 1.00 35.00 -- 27.06 0.00-150.00 32 23 \w -44.00 8.00 1.00 35.00 -- 27.06 37.00-180.00 52 24 \w 7.00 60.00 1.00 35.00 -- 27.06 -81.00 29.00 53 25 \w 8.00 53.00 1.00 35.00 -- 27.06 -99.00-120.00 45 26 \w -48.00 -24.00 1.00 35.00 -- 27.06 37.00 0.00 24 27 \w -31.00 1.00 1.00 35.00 -- -27.92 0.00-150.00 32 28 \w -31.00 1.00 1.00 35.00 -- -27.92 0.00 30.00 32 29 \w -44.00 17.00 1.00 15.00 -- -0.43 19.00-180.00 61 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0446270000 _diffrn_orient_matrix_UB_12 -0.0286494000 _diffrn_orient_matrix_UB_13 0.0055038000 _diffrn_orient_matrix_UB_21 0.0138116000 _diffrn_orient_matrix_UB_22 0.1362646000 _diffrn_orient_matrix_UB_23 0.0213972000 _diffrn_orient_matrix_UB_31 0.0074411000 _diffrn_orient_matrix_UB_32 -0.0798893000 _diffrn_orient_matrix_UB_33 0.0344915000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0822 _diffrn_reflns_av_unetI/netI 0.0453 _diffrn_reflns_Laue_measured_fraction_full 0.292 _diffrn_reflns_Laue_measured_fraction_max 0.260 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_k_max 5 _diffrn_reflns_limit_k_min -5 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 4135 _diffrn_reflns_point_group_measured_fraction_full 0.292 _diffrn_reflns_point_group_measured_fraction_max 0.260 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.832 _diffrn_reflns_theta_min 2.350 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.116 _exptl_absorpt_correction_T_max 0.997 _exptl_absorpt_correction_T_min 0.995 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.49 (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model (Absorb Angel (2004) J. Appl. Cryst. 37:486-492) ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.595 _exptl_crystal_description plate _exptl_crystal_F_000 640 _exptl_crystal_recrystallization_method ;Single crystals were grown by slow evaporation of a solution obtained dissolving 4,4'-ethane-1,2-diyldipyridine and succinic acid in 1:1 mol ratio in hot methanol 99.8%. ; _exptl_crystal_size_max 0.31 _exptl_crystal_size_mid 0.153 _exptl_crystal_size_min 0.034 _refine_diff_density_max 0.179 _refine_diff_density_min -0.235 _refine_diff_density_rms 0.044 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.069 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 46 _refine_ls_number_reflns 353 _refine_ls_number_restraints 4 _refine_ls_restrained_S_all 1.075 _refine_ls_R_factor_all 0.0977 _refine_ls_R_factor_gt 0.0616 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0646P)^2^+5.1287P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1393 _refine_ls_wR_factor_ref 0.1618 _reflns_Friedel_coverage 0.000 _reflns_number_gt 241 _reflns_number_total 353 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yc5049.cif _cod_data_source_block ETYSUC_329 _cod_original_cell_volume 1258.9(11) _cod_database_code 1573523 _shelx_shelxl_version_number 2014/7 _chemical_oxdiff_formula 'C11 H10 N O' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.996 _shelx_estimated_absorpt_t_min 0.965 _exptl_oxdiff_absorpt_process_details ; Gaussian integration over a grid of 16 x 16 x 16 points = 4096 total grid points Based upon method of Burnham (1966) ; _diffrn_ambient_pressure_su 20000 _diffrn_orient_matrix_axis[1] matrixX _diffrn_orient_matrix_axis[2] matrixY _diffrn_orient_matrix_axis[3] matrixZ _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All O(H) groups 2. Restrained distances O2A-C1A 1.214 with sigma of 0.02 O1A-C1A 1.308 with sigma of 0.02 N1-C6 1.337 with sigma of 0.02 N1-C2 1.337 with sigma of 0.02 3.a Secondary CH2 refined with riding coordinates: C2A(H2AA,H2AB), C7(H7A,H7B) 3.b Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C5(H5), C6(H6) 3.c Idealised tetrahedral OH refined as rotating group: O1A(H1A) ; _shelx_res_file ; etysuc_320_1.res created by SHELXL-2014/7 TITL ETYSUC_320_1 in I2/a #15 CELL 0.71073 16.428553 4.421444 19.019659 90 114.3249 90 ZERR 4 0.012398 0.000265 0.003579 0 0.0503 0 LATT 2 SYMM 0.5-X,+Y,-Z SFAC C H N O UNIT 64 72 8 16 DFIX 1.214 O2A C1A DFIX 1.308 O1A C1A DFIX 1.337 N1 C6 DFIX 1.337 N1 C2 L.S. 100 PLAN 5 SIZE 0.034 0.153 0.31 TEMP 22(2) CONF BOND MORE -1 BOND $H fmap 2 53 acta OMIT -5 1 20 OMIT -4 2 14 OMIT -3 4 5 OMIT -2 2 4 OMIT -1 1 8 OMIT 0 4 0 OMIT 0 4 2 REM REM REM WGHT 0.064600 5.128700 FVAR 2.02839 N1 3 0.392709 0.476916 0.148131 11.00000 0.03181 C2 1 0.334175 0.633537 0.087889 11.00000 0.03470 AFIX 43 H2 2 0.273130 0.601203 0.071251 11.00000 -1.20000 AFIX 0 C3 1 0.365666 0.845209 0.050445 11.00000 0.02958 AFIX 43 H3 2 0.324985 0.956512 0.009585 11.00000 -1.20000 AFIX 0 C4 1 0.456812 0.892538 0.073179 11.00000 0.02287 C5 1 0.515266 0.724735 0.135832 11.00000 0.02889 AFIX 43 H5 2 0.576793 0.748252 0.153744 11.00000 -1.20000 AFIX 0 C6 1 0.479030 0.523005 0.170373 11.00000 0.02898 AFIX 43 H6 2 0.518156 0.412053 0.212174 11.00000 -1.20000 AFIX 0 C1A 1 0.252918 0.038529 0.175538 11.00000 0.02286 O1A 4 0.334468 0.102858 0.212303 11.00000 0.04067 AFIX 147 H1A 2 0.346621 0.252889 0.193158 11.00000 -1.50000 AFIX 0 C2A 1 0.217441 -0.199905 0.210921 11.00000 0.03113 AFIX 23 H2AA 2 0.200018 -0.373951 0.176867 11.00000 -1.20000 H2AB 2 0.164265 -0.123269 0.215062 11.00000 -1.20000 AFIX 0 O2A 4 0.204023 0.162121 0.113677 11.00000 0.03480 C7 1 0.491125 1.095750 0.030179 11.00000 0.02526 AFIX 23 H7A 2 0.545967 1.191502 0.065257 11.00000 -1.20000 H7B 2 0.447683 1.252589 0.004597 11.00000 -1.20000 AFIX 0 HKLF 4 REM ETYSUC_320_1 in I2/a #15 REM R1 = 0.0616 for 241 Fo > 4sig(Fo) and 0.0977 for all 353 data REM 46 parameters refined using 4 restraints END WGHT 0.0646 5.1287 REM Highest difference peak 0.179, deepest hole -0.235, 1-sigma level 0.044 Q1 1 0.3814 0.0130 0.1978 11.00000 0.05 0.18 Q2 1 0.1324 -0.4158 0.1216 11.00000 0.05 0.15 Q3 1 0.6071 0.6890 0.1019 11.00000 0.05 0.15 Q4 1 0.1699 0.3282 0.1138 11.00000 0.05 0.13 Q5 1 0.1673 0.1680 0.1551 11.00000 0.05 0.13 ; _shelx_res_checksum 85872 _shelx_hkl_file ; 0 0 2 4433.84 188.360 9 0 0 -2 4161.96 180.614 23 0 0 2 3911.97 164.758 8 0 0 -4 30596.2 642.939 13 0 0 4 31887.7 667.944 8 0 0 -4 31120.4 720.438 14 0 0 4 30219.1 722.555 24 0 0 4 30753.8 786.002 12 0 0 4 30856.5 812.811 18 0 0 4 31599.3 708.267 9 0 0 4 30704.3 530.380 15 0 0 4 28500.3 938.940 29 0 0 -4 30654.3 703.974 23 0 0 -4 32066.4 1005.06 29 0 0 -6 2786.62 273.233 14 0 0 -6 2666.58 257.280 23 0 0 6 2697.12 244.996 8 0 0 6 2884.61 262.930 9 0 0 -6 2687.39 237.775 13 0 0 6 2601.03 262.763 24 0 0 6 2828.04 376.755 29 0 0 6 2478.36 280.782 18 0 0 6 3004.19 207.307 15 0 0 -6 2833.07 363.835 29 0 0 6 2988.03 297.044 12 0 0 -8 7311.99 496.681 23 0 0 8 7058.72 462.514 8 0 0 -8 7018.15 507.403 11 0 0 8 7553.68 703.035 29 0 0 8 6903.80 548.861 12 0 0 -8 7350.41 508.788 14 0 0 8 7704.49 586.283 18 0 0 -8 7942.16 725.035 29 0 0 8 7289.08 517.678 24 0 0 8 8187.83 524.864 9 0 0 -8 8490.00 406.679 22 0 0 8 8014.09 387.905 15 0 0 8 8210.38 380.714 21 0 0 -8 7751.99 467.292 13 0 0 10 31.2618 74.3679 8 0 0 -10 186.050 115.462 29 0 0 10 233.710 113.391 29 0 0 10 77.7926 97.7714 24 0 0 10 83.8841 88.8734 9 0 0 10 207.616 138.481 12 0 0 10 154.420 63.4870 15 0 0 10 117.026 64.8022 21 0 0 -10 94.9216 61.2037 22 0 0 10-16.9815 122.289 18 0 0 -10 25.5274 86.7410 23 0 0 -10-131.503 142.551 11 0 0 -10 103.403 96.2999 13 0 0 -10 98.6891 106.715 14 0 0 12 1967.78 389.943 18 0 0 12 2282.87 342.096 8 0 0 -12 2294.51 378.116 11 0 0 -12 2107.73 465.787 29 0 0 -12 2535.90 380.351 14 0 0 12 2181.77 471.807 29 0 0 12 2443.53 371.416 9 0 0 12 2447.43 396.775 24 0 0 -12 2252.48 356.430 23 0 0 -12 2077.46 323.713 13 0 0 12 1329.78 301.482 12 0 0 -14 763.499 263.511 7 0 0 14 1159.61 323.403 18 0 0 14 775.786 276.921 24 0 0 -14 1170.53 282.955 23 0 0 -14 1097.81 295.010 11 0 0 14 1051.10 289.493 9 0 0 -14 1004.67 256.256 14 0 0 14-26.0146 102.826 8 0 0 14 412.903 220.054 12 0 0 -14 1030.60 254.132 17 0 0 -16 1500.00 367.837 14 0 0 16 1291.57 324.389 9 0 0 16 1655.59 455.419 18 0 0 16 1131.04 287.788 24 0 0 -16 896.723 312.517 7 0 0 -16 1247.11 326.369 11 0 0 -18-1.54505 170.925 11 0 0 18-261.178 224.344 18 0 0 18-191.867 179.679 9 0 0 -18 126.057 234.523 7 0 0 18-439.608 355.448 24 0 1 1 13221.1 443.441 21 0 -1 1 12543.7 697.370 1 0 1 -1 13696.0 499.004 3 0 -1 1 12689.8 457.554 10 0 -1 -1 14169.9 398.997 25 0 -1 1 14527.5 764.936 19 0 -1 -1 14479.1 402.351 11 0 -1 1 14151.7 478.069 25 0 1 -1 13642.6 561.308 29 0 -1 -1 14393.6 473.109 28 0 -1 1 13264.3 483.300 4 0 1 1 13910.5 508.021 3 0 -1 -1 13632.7 475.153 22 0 -1 -1 13831.9 424.152 23 0 -1 -1 13342.3 696.145 29 0 -1 -1 12523.6 703.990 1 0 -1 1 13866.6 797.815 2 0 1 -1 13132.9 491.397 20 0 -1 1 13642.8 511.625 5 0 1 1 13607.5 390.841 8 0 -1 -1 12798.5 488.879 5 0 -1 -1 13282.9 469.891 10 0 -1 -1 12844.6 483.908 4 0 1 1 13374.0 689.043 29 0 1 -1 15076.3 444.607 21 0 -1 -1 13765.1 787.980 2 0 1 1 14039.2 802.634 2 0 1 1 14809.7 389.294 9 0 1 1 12960.7 718.542 19 0 1 -1 13333.9 390.895 14 0 -1 -1 13562.3 746.296 19 0 1 1 13742.1 478.285 20 0 -1 1 14463.5 525.653 12 0 1 -1 14025.1 733.573 19 0 1 -1 13438.5 775.909 2 0 -1 1 14423.0 451.801 22 0 1 1 13146.8 450.193 27 0 1 -1 13499.0 408.413 27 0 1 -1 14384.7 756.295 1 0 -1 1 13838.6 409.786 28 0 1 3 9350.88 381.457 18 0 1 3 10300.9 413.759 9 0 -1 -3 9081.46 396.866 5 0 -1 3 8910.94 272.735 9 0 -1 -3 10340.3 443.073 4 0 1 -3 11593.0 361.370 27 0 -1 -3 9524.24 638.094 1 0 -1 -3 10324.9 418.900 7 0 -1 -3 10228.7 435.499 11 0 1 3 9837.73 354.520 24 0 -1 3 9894.20 613.833 1 0 -1 -3 9051.43 439.011 22 0 1 3 9129.43 414.158 21 0 -1 3 9904.83 676.305 2 0 -1 -3 9354.62 395.259 10 0 1 -3 10873.8 728.390 19 0 -1 -3 8532.76 593.733 2 0 -1 -3 9495.81 411.279 13 0 1 3 9634.28 687.020 2 0 1 -3 9393.86 616.695 1 0 1 3 10011.1 370.507 16 0 -1 3 9841.16 540.028 12 0 1 3 9395.29 437.763 3 0 1 -3 10311.6 475.236 14 0 -1 3 10308.4 421.487 4 0 -1 3 8374.35 489.705 25 0 1 3 9416.96 593.594 1 0 -1 3 8986.48 416.521 5 0 1 -3 9750.55 661.813 2 0 -1 3 11065.6 337.154 28 0 -1 -3 9237.75 323.735 15 0 1 -3 9933.88 428.046 3 0 -1 -3 9477.47 695.092 29 0 1 3 10073.1 425.231 8 0 1 3 9201.39 382.542 20 0 -1 3 10723.5 455.762 10 0 1 -3 9886.87 476.772 20 0 1 3 9627.27 682.754 29 0 -1 3 9744.43 381.776 24 0 -1 -3 10110.2 459.088 23 0 -1 -3 10032.0 686.620 19 0 1 -5 8577.38 509.099 14 0 -1 -5 7908.04 653.225 19 0 1 -5 8412.88 305.760 23 0 1 5 7732.26 537.035 1 0 -1 5 7784.54 559.388 12 0 -1 5 7475.01 552.956 1 0 -1 -5 7609.52 713.503 29 0 1 -5 8271.49 379.115 6 0 1 5 9204.22 460.908 3 0 -1 5 7877.74 434.786 24 0 -1 5 8365.15 613.388 2 0 -1 5 7729.28 390.405 5 0 -1 5 7189.71 482.183 15 0 1 5 7701.08 402.539 24 0 1 -5 8678.60 429.460 3 0 1 5 7392.70 438.254 18 0 1 5 8051.79 325.024 16 0 -1 -5 8734.02 429.351 4 0 1 5 8006.62 342.671 20 0 -1 -5 8227.04 627.908 1 0 1 -5 8624.87 670.839 2 0 1 -5 7539.09 510.232 20 0 1 5 7713.02 428.624 9 0 -1 5 7982.02 268.387 8 0 1 5 7777.36 350.159 6 0 -1 -5 7277.07 440.060 22 0 -1 -5 8014.50 346.108 14 0 -1 5 8609.10 381.456 9 0 -1 -5 7748.31 563.054 2 0 1 -5 7154.36 307.670 29 0 1 5 9596.07 742.147 2 0 1 5 7720.11 447.587 8 0 -1 5 7765.84 381.393 4 0 1 5 8439.36 736.575 29 0 -1 -5 7869.60 370.140 5 0 1 5 7867.59 429.305 21 0 -1 -5 7680.11 447.749 7 0 -1 5 7797.07 471.798 18 0 -1 -5 7854.47 480.317 23 0 -1 -5 8202.39 467.333 11 0 1 5 8666.46 350.043 12 0 1 -5 8225.63 585.507 1 0 -1 -5 7928.83 376.124 10 0 -1 -5 7409.08 435.595 13 0 1 -7 23558.9 802.045 29 0 1 -7 21391.4 897.272 1 0 1 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305.924 11 1 -3 -18-243.836 241.197 11 -1 3 18-89.6864 181.694 9 1 -3 -18-131.852 304.609 13 1 -3 -16 0.29789 214.632 13 1 -3 -16-524.147 323.987 23 1 -3 -16 237.804 289.820 11 -1 3 16 22.8042 166.739 21 -1 3 16 74.4654 179.937 9 1 -3 -16 17.5476 237.978 22 -1 3 16-13.4890 143.507 8 1 -3 -14 337.012 237.947 11 1 -3 -14 215.148 252.244 22 1 -3 -14 381.868 298.612 23 -1 3 14 185.648 222.846 9 -1 3 14-362.886 278.082 8 1 -3 -14 173.787 152.420 13 -1 3 14-349.180 260.436 21 1 -3 -12 335.573 206.527 23 1 -3 -12 721.231 270.880 11 -1 3 12 737.926 255.852 9 1 3 -12 136.356 138.222 16 1 3 -12 64.5673 146.727 17 1 -3 -12 554.962 185.738 13 -1 -3 12 110.455 217.658 15 1 -3 -12 508.120 200.411 22 -1 3 12 240.659 177.387 21 -1 3 12 1080.62 348.474 8 -1 -3 12 79.5093 144.865 12 1 -3 -10 8190.11 737.788 5 1 -3 -10 7705.85 783.755 23 -1 -3 10 1558.04 413.528 12 1 -3 -10 7191.47 684.459 11 1 -3 -10 8977.65 901.617 22 -1 3 10 10271.6 901.153 21 1 3 -10 2510.16 525.247 3 -1 3 10 2029.36 364.135 9 1 3 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2655.53 484.433 29 -1 -3 2 2366.88 375.879 4 1 -3 -2 1527.00 261.539 25 -1 3 0 456.787 226.360 27 -1 -3 0 1646.30 283.737 25 1 3 0 1785.25 298.198 21 1 -3 0 175.267 134.255 10 1 3 0 1684.95 312.582 20 -1 -3 0 1318.57 282.881 10 -1 3 0 134.824 118.816 20 -1 -3 0 1347.40 307.406 5 1 3 0 2266.09 279.688 17 1 3 0 1904.72 347.085 3 1 -3 0 687.701 236.669 28 1 3 0 1802.61 309.892 16 1 -3 0 192.366 131.990 25 1 -3 0 134.995 153.879 15 -1 -3 0 1784.21 357.413 15 -1 -3 0 1050.21 367.031 29 1 3 0 1500.06 295.994 6 -1 3 0 476.780 332.590 29 1 3 0 2137.97 459.118 29 -1 -3 0 1706.99 331.580 4 -1 -3 0 2057.64 340.639 22 1 3 2 7110.85 648.644 6 -1 -3 -2 6224.11 488.419 25 1 3 2 6390.45 565.039 21 1 3 2 6190.78 622.923 20 -1 -3 -2 6749.31 538.512 23 -1 -3 -2 5837.16 587.734 10 -1 -3 -2 6516.77 644.067 4 1 3 2 6273.77 566.342 16 -1 -3 -2 6318.70 607.498 22 -1 -3 -2 6940.44 626.042 15 1 3 2 6725.00 486.776 8 1 3 2 6292.61 640.031 3 -1 -3 -2 6021.07 470.303 13 -1 -3 -2 6117.92 614.834 5 -1 -3 -4 2404.79 348.846 23 1 3 4 2010.69 358.523 6 -1 -3 -4 2705.41 428.065 22 1 3 4 2412.73 372.134 21 1 3 4 2540.14 411.754 20 -1 -3 -4 2256.05 393.559 10 1 3 4 2525.31 294.280 9 -1 -3 -4 2205.51 382.148 5 1 3 4 2694.13 446.243 3 1 3 4 2588.64 368.199 16 -1 -3 -4 2497.66 356.945 15 1 3 4 2388.72 328.886 8 -1 -3 -4 2616.95 345.800 13 -1 -3 -4 2416.10 409.703 4 -1 -3 -6 592.905 205.987 23 1 3 6 906.040 248.341 6 -1 -3 -6 1019.68 226.310 11 1 3 6 1053.07 266.194 21 1 3 6 1524.57 326.065 20 -1 -3 -6 633.334 196.448 10 1 3 6 1178.37 327.934 3 -1 -3 -6 944.726 264.868 22 -1 -3 -6 1132.18 295.745 5 1 3 6 937.486 223.860 9 1 3 6 1151.08 228.309 16 1 3 6 1161.95 252.101 8 -1 -3 -6 1043.60 294.162 4 -1 -3 -6 1017.07 246.552 13 -1 -3 -8 2067.90 378.266 23 -1 -3 -8 1585.08 353.759 22 1 3 8 1635.38 330.813 21 1 3 8 1132.02 318.980 3 -1 -3 -8 2268.72 402.600 10 -1 -3 -8 2505.60 402.171 11 -1 -3 -8 2271.30 392.767 5 -1 -3 -8 2412.09 396.003 13 1 3 8 1804.62 327.263 9 1 3 8 2249.99 386.313 8 -1 -3 -8 1147.03 277.600 4 1 3 8 1809.21 325.904 6 -1 -3 -10 2379.06 458.943 23 -1 -3 -10 2279.26 432.426 11 1 3 10 2923.45 489.292 21 -1 -3 -10 2423.58 469.795 22 -1 -3 -10 2630.84 410.509 13 1 3 10 3151.12 475.128 9 1 3 10 2459.02 433.563 8 -1 -3 -12 326.929 218.517 23 -1 -3 -12 587.517 281.813 22 -1 -3 -12 706.498 317.873 11 1 3 12 705.790 310.284 21 1 3 12 1036.82 292.177 9 1 3 12 840.574 313.032 8 -1 -3 -12 282.645 189.704 13 -1 -3 -14 371.699 298.671 23 -1 -3 -14-244.207 165.318 22 -1 -3 -14 85.5126 263.838 11 1 3 14-125.493 220.641 21 1 3 14 378.147 263.526 9 1 3 14-25.9119 179.428 8 -1 -3 -14-11.4649 182.850 13 -1 -3 -16 705.062 317.442 23 -1 -3 -16 31.1530 303.813 11 1 3 16 558.193 371.191 21 1 3 16 306.302 272.649 9 -1 -3 -16 185.839 218.815 22 1 3 16 357.570 267.073 8 -1 -3 -16 828.154 346.940 13 1 4 -7-119.685 243.729 16 -1 -4 7 221.614 282.358 15 -1 -4 7-224.165 197.480 4 1 4 -7-95.0245 249.413 17 1 4 -7-1.64835 98.1399 3 1 4 -5 5011.57 788.387 3 1 4 -5 4003.53 662.882 17 1 4 -5 4231.05 735.933 20 -1 -4 5 1828.14 463.312 10 1 4 -5 5865.06 850.289 16 -1 -4 5 4469.66 797.360 15 -1 -4 5 3199.30 583.597 4 1 4 -3 276.419 232.793 20 1 4 -3 572.005 302.777 6 -1 -4 3 572.806 303.618 10 1 4 -3 596.403 333.389 3 -1 -4 3 319.486 174.743 5 1 4 -3 1011.37 381.611 16 -1 -4 3 696.833 319.041 15 -1 -4 3 458.721 306.382 4 -1 -4 3 676.085 289.465 25 1 4 -1 365.605 280.356 6 1 4 -1-71.1753 248.273 20 -1 -4 1 95.9794 186.261 10 1 4 -1 313.938 214.243 3 -1 -4 1 269.012 169.767 5 1 4 -1 305.835 263.681 16 -1 -4 1-12.9906 254.741 15 -1 -4 1 306.748 262.254 4 -1 -4 1 18.2439 147.285 25 1 4 1 30.3059 209.952 6 1 4 1 22.5212 157.992 20 -1 -4 -1-41.7440 143.344 22 -1 -4 -1 265.199 243.149 10 1 4 1-136.584 155.556 3 -1 -4 -1-247.859 186.996 5 1 4 1 128.326 246.966 16 -1 -4 -1-158.367 277.690 15 1 4 1 88.7558 153.691 21 -1 -4 -1-318.474 280.848 4 1 4 3 370.708 231.199 6 1 4 3 529.084 249.535 21 1 4 3 78.2407 181.910 20 -1 -4 -3 63.4618 234.613 10 1 4 3 250.891 213.559 3 -1 -4 -3-199.858 253.560 5 -1 -4 -3 195.670 204.198 22 1 4 3 444.948 266.971 16 -1 -4 -3-100.081 169.743 4 1 4 5 962.257 337.231 6 1 4 5 761.320 278.605 21 1 4 5 1528.07 441.215 20 1 4 5 787.915 347.060 3 -1 -4 -5 1244.60 408.836 10 -1 -4 -5 1569.30 458.745 5 1 4 5 973.673 314.578 16 -1 -4 -5 1527.76 429.563 22 -1 -4 -5 333.219 190.568 4 -1 -4 -7 3265.39 565.105 23 -1 -4 -7 3315.51 590.340 22 1 4 7 3033.55 522.662 6 1 4 7 3067.82 551.222 21 -1 -4 -7 3650.60 652.472 10 -1 -4 -7 3120.04 573.228 5 -1 -4 -7 3312.23 519.751 13 1 4 7 3785.10 548.602 8 -1 -4 -9 352.115 329.984 22 1 4 9 485.783 276.225 21 -1 -4 -9 22.4949 227.987 10 -1 -4 -9 348.701 328.164 5 -1 -4 -9 160.489 169.185 13 1 4 9 559.482 286.348 8 -1 -4 -9 219.900 216.635 23 1 4 9 521.656 249.276 6 -1 -4 -11 170.333 219.647 22 1 4 11 327.466 276.512 21 -1 -4 -11 451.481 252.419 23 1 4 11 938.925 371.374 8 -1 -4 -11 488.866 269.828 13 -1 -4 -13 896.397 369.584 23 1 4 13 1015.90 410.488 21 1 4 13 1168.70 460.435 8 -1 -4 -13 590.542 357.254 13 -1 -4 -13 572.667 437.699 22 -1 -5 -4 435.092 456.341 5 -1 -5 -6 168.539 252.744 5 1 5 6-730.568 354.205 6 1 5 8 371.289 435.127 6 -1 -5 -8 360.843 387.361 5 2 0 -22 337.314 215.692 11 2 0 -22-140.300 251.112 7 -2 0 22-189.170 189.128 9 2 0 -22 49.2725 201.929 14 2 0 -20-220.557 322.382 11 -2 0 20-116.136 188.565 24 -2 0 20-121.954 417.293 18 -2 0 20 81.8235 232.918 9 2 0 -20 193.113 275.535 7 2 0 -20 114.064 552.535 14 -2 0 18 344.304 307.500 12 2 0 -18 813.380 321.137 11 -2 0 18 1287.35 382.416 24 2 0 -18 651.517 273.631 7 2 0 -18 709.195 264.823 13 -2 0 18 722.083 400.346 18 2 0 -18 818.998 335.290 23 -2 0 18 167.309 174.581 9 2 0 -18 206.855 235.041 14 -2 0 16 519.753 281.428 12 2 0 -16 852.320 278.227 23 -2 0 16 1313.17 474.511 18 2 0 -16 664.671 199.880 17 2 0 -16 1249.96 326.909 11 -2 0 16 1067.71 335.784 9 -2 0 16 136.622 116.795 8 2 0 -16 785.492 295.729 7 2 0 -16 665.004 271.286 14 -2 0 16 787.098 279.926 24 2 0 -16 747.197 226.892 13 -2 0 14 102.290 179.810 12 2 0 -14 87.5209 185.711 11 2 0 -14 58.8233 132.802 13 -2 0 14 127.682 185.110 18 2 0 -14-65.5558 139.206 23 2 0 -14-88.1208 135.456 17 -2 0 14 233.925 164.631 9 -2 0 14 152.656 187.784 8 -2 0 14-79.2011 189.075 24 2 0 -14-255.774 259.501 14 2 0 -14-92.0741 168.855 7 2 0 -12 13866.6 866.562 11 2 0 -12 13558.9 1229.19 29 -2 0 12 13894.9 967.634 18 -2 0 12 13922.0 809.018 9 2 0 -12 13846.2 758.795 17 2 0 -12 14958.9 908.304 23 -2 0 12 14015.7 949.006 12 -2 0 12 14672.3 871.268 8 2 0 -12 13791.9 874.995 14 2 0 -12 14325.9 897.988 7 2 0 -12 13962.7 759.901 13 -2 0 12 13254.1 1096.99 29 -2 0 12 11387.7 789.514 24 2 0 -10 11768.9 711.064 23 2 0 -10 10785.6 674.998 11 -2 0 10 10552.5 742.268 12 -2 0 10 10868.0 773.632 18 -2 0 10 10983.9 644.096 9 2 0 -10 11390.8 605.649 17 2 0 -10 12197.4 1025.78 29 -2 0 10 10880.2 677.405 8 2 0 -10 10633.5 597.045 13 2 0 -10 11010.5 703.918 7 -2 0 10 12016.3 937.557 29 -2 0 10 9334.50 625.893 24 -2 0 8-12.7181 61.0656 24 2 0 -8 144.601 91.3128 23 2 0 -8 179.214 73.3715 17 2 0 -8 89.7997 61.7407 11 2 0 -8 144.266 57.1160 28 -2 0 8-2.93345 94.5753 18 -2 0 8 89.5208 68.4231 9 -2 0 8 94.4783 75.6722 8 2 0 -8 83.4953 67.6551 13 2 0 -8 104.682 106.911 29 -2 0 8 140.361 113.058 29 -2 0 8 58.6796 35.8921 27 2 0 -8 37.1870 74.3968 7 -2 0 8 21.5433 69.9482 12 -2 0 6 1932.49 172.891 19 -2 0 6 1537.76 200.920 9 2 0 -6 1768.71 178.953 17 2 0 -6 1457.83 198.183 23 2 0 -6 1590.11 202.330 11 2 0 -6 2039.16 228.957 7 -2 0 6 2139.43 302.125 29 2 0 -6 1811.41 151.305 28 -2 0 6 1739.30 146.734 27 -2 0 6 2229.91 270.629 12 -2 0 6 1921.73 220.757 24 -2 1 21-229.854 295.652 24 2 -1 -21-32.9330 287.655 11 -2 1 21 380.178 320.208 18 -2 1 21 304.577 248.091 9 2 -1 -21 168.108 147.356 23 2 1 -21-229.014 254.635 14 2 -1 -21-123.320 236.752 7 2 1 -21-282.674 290.473 7 2 -1 -21 3.05122 188.189 13 -2 -1 21 489.993 306.599 24 -2 -1 19 1724.71 460.347 24 2 -1 -19 2263.37 527.942 23 -2 -1 19 2191.06 599.348 12 -2 -1 19 2333.04 555.222 18 2 -1 -19 2436.15 541.167 11 -2 1 19 1699.06 526.831 18 2 1 -19 2230.62 453.779 17 -2 1 19 2505.86 551.440 9 -2 1 19 2396.91 516.002 24 2 -1 -19 2207.31 462.284 13 2 1 -19 2972.73 620.668 14 2 -1 -19 3140.01 604.238 7 2 1 -19 2042.01 471.611 7 -2 -1 17 2260.43 532.459 12 2 -1 -17 2672.80 535.056 23 2 -1 -17 2426.98 487.451 7 -2 1 17 1743.21 412.818 24 2 -1 -17 2425.43 510.950 11 2 1 -17 2255.13 449.567 11 -2 1 17 2309.33 524.235 18 -2 -1 17 2041.11 527.594 18 2 1 -17 2296.72 453.756 17 -2 -1 17 1732.46 403.581 24 -2 1 17 2508.01 492.728 9 -2 -1 17 1994.99 389.524 9 2 -1 -17 1771.51 397.597 13 -2 1 17 1288.52 338.587 8 2 -1 -17 2102.25 428.315 14 2 1 -17 2365.62 501.583 14 2 1 -17 2130.90 483.202 7 -2 1 15 927.210 287.490 24 -2 -1 15 1830.42 471.436 12 2 -1 -15 1600.64 401.972 23 2 1 -15 888.388 284.613 11 2 -1 -15 1097.52 308.039 11 -2 1 15 927.744 358.904 18 -2 -1 15 952.514 284.812 18 2 1 -15 2355.87 474.043 17 -2 1 15 1158.63 325.859 9 -2 -1 15 950.530 263.718 9 -2 -1 15 1882.36 398.358 24 -2 1 15 1000.83 307.216 8 2 -1 -15 1491.23 345.042 14 2 1 -15 1196.50 357.586 14 2 -1 -15 1596.94 336.490 13 2 -1 -15 910.272 297.266 7 2 1 -15 322.102 210.547 7 -2 1 13 2781.96 419.040 12 -2 -1 13 2899.50 427.634 24 -2 -1 13 2991.79 525.879 12 2 -1 -13 2533.26 444.996 23 2 1 -13 3131.85 429.649 11 2 -1 -13 3541.83 466.653 22 2 -1 -13 3058.17 447.054 11 -2 1 13 2074.92 337.035 21 2 1 -13 2996.26 434.032 17 -2 1 13 2576.86 456.090 18 -2 -1 13 3363.42 507.092 18 -2 -1 13 3342.64 405.913 9 -2 1 13 2826.43 427.490 9 -2 -1 13 3078.19 399.529 15 -2 1 13 3051.78 435.680 24 2 -1 -13 2235.07 376.744 7 -2 1 13 3151.26 461.132 8 2 1 -13 2614.46 411.454 7 2 -1 -13 3545.31 446.711 14 2 1 -13 2796.80 458.768 14 2 -1 -13 3224.34 447.925 13 2 -1 -11 3332.92 547.147 19 -2 -1 11 3189.91 472.527 12 2 -1 -11 3182.90 435.381 23 2 1 -11 3274.97 374.163 11 2 -1 -11 3111.02 403.155 22 2 -1 -11 2511.37 371.238 11 -2 1 11 3090.38 368.164 21 2 1 -11 3449.57 366.533 20 -2 -1 11 2952.13 426.333 18 -2 1 11 2838.48 437.293 18 -2 -1 11 3000.42 340.167 9 2 1 -11 2745.15 380.597 17 -2 1 11 2401.17 347.364 9 2 1 -11 3248.71 281.114 16 -2 1 11 3065.22 413.806 8 -2 -1 11 2964.42 374.375 15 2 1 -11 2859.49 419.747 14 2 1 -11 3106.53 400.734 7 2 1 -11 3142.67 311.335 13 2 -1 -11 2430.16 361.247 13 2 -1 -11 3138.99 658.049 29 -2 1 11 3116.80 615.755 29 2 -1 -11 2204.46 359.084 7 -2 1 11 3094.34 393.697 12 -2 1 11 2559.38 350.319 24 -2 -1 11 2857.03 376.884 24 -2 1 9 1075.49 222.367 24 -2 -1 9 1071.64 180.126 29 -2 -1 9 1130.35 202.149 24 -2 -1 9 833.309 233.453 12 2 -1 -9 1072.07 226.740 23 2 -1 -9 1378.20 336.276 19 -2 1 9 585.847 197.338 1 2 -1 -9 1449.39 245.708 22 2 -1 -9 1065.31 223.209 11 2 -1 -9 1228.44 213.619 28 2 1 -9 1006.49 177.712 11 -2 1 9 1163.47 209.181 21 2 -1 -9 1249.84 274.161 2 2 1 -9 1218.33 185.217 20 2 -1 -9 1168.11 176.744 5 2 1 -9 1176.59 241.838 2 -2 1 9 887.877 185.168 12 -2 1 9 1110.89 238.200 18 -2 -1 9 1361.94 264.811 18 2 1 -9 1261.00 234.452 17 -2 -1 9 1284.88 240.762 1 -2 1 9 807.555 193.952 9 -2 -1 9 1258.48 192.370 9 2 1 -9 1228.85 174.265 16 -2 1 9 1004.91 313.041 29 -2 -1 9 1463.90 249.697 15 -2 -1 9 1157.30 154.257 4 2 1 -9 1195.36 157.105 3 -2 1 9 1316.99 237.410 8 2 -1 -9 1497.88 249.787 13 2 -1 -9 788.324 274.720 29 2 1 -9 1073.27 149.433 13 2 -1 -9 1070.18 221.479 7 -2 1 9 811.428 170.033 27 -2 -1 9 1404.14 163.266 10 2 1 -9 1070.38 196.390 7 2 1 -7 9720.12 684.545 2 2 -1 -7 8940.76 577.566 23 2 -1 -7 9207.68 567.107 11 2 1 -7 8824.13 441.750 11 2 -1 -7 9749.96 589.015 22 -2 1 7 8156.33 519.676 21 2 1 -7 9988.01 450.497 3 2 1 -7 9493.90 476.962 20 -2 -1 7 8653.59 629.323 12 -2 -1 7 9261.80 639.053 1 2 -1 -7 8928.50 794.416 19 -2 1 7 8890.95 735.216 19 -2 -1 7 9069.84 544.369 18 -2 1 7 8980.79 549.859 9 -2 -1 7 9372.73 427.224 9 2 1 -7 9218.57 544.375 17 2 1 -7 8649.08 441.429 16 -2 1 7 7650.43 488.005 24 -2 1 7 8831.46 485.702 12 -2 -1 7 7663.67 552.201 25 -2 1 7 8691.95 548.243 8 -2 -1 7 8928.62 559.157 15 -2 -1 7 9284.22 425.585 4 2 -1 -7 9418.18 564.044 7 2 1 -7 8955.26 485.709 7 2 1 -7 9367.55 346.449 13 2 -1 -7 7250.35 785.473 29 -2 1 7 9314.97 876.573 29 -2 -1 7 9514.32 359.600 29 -2 -1 7 8978.96 397.341 10 2 -1 -7 9445.85 528.208 28 -2 1 7 8005.08 488.195 27 -2 -1 7 8251.16 478.705 24 2 -1 -5 54438.9 1278.69 23 2 1 -5 65323.1 1173.62 6 2 1 -5 68269.5 1170.35 3 -2 -1 5 71090.3 1134.84 10 -2 -1 5 69745.3 1413.59 19 -2 -1 5 67492.5 1889.53 2 -2 -1 5 65265.4 1189.41 18 2 1 -5 68554.1 1813.79 2 -2 -1 5 67970.7 1718.97 1 2 1 -5 67757.1 1308.31 17 -2 -1 5 68154.2 1244.61 5 2 1 -5 64192.6 1154.37 16 -2 -1 5 69451.4 1429.26 15 -2 -1 5 69537.2 1148.49 4 2 1 -5 67968.4 1080.42 7 2 1 -5 62530.4 1782.66 1 -2 -1 5 69091.8 1392.97 25 -2 -1 5 69731.0 1558.71 12 -2 -1 5 68071.4 1170.98 24 2 1 -3 120450. 1549.54 6 2 1 -3 117466. 2409.04 2 -2 -1 3 116062. 2389.96 2 2 1 -3 117808. 1558.53 3 -2 -1 3 116821. 1473.42 10 -2 -1 3 115517. 1562.77 5 2 1 -3 120993. 1550.89 17 2 1 -3 121141. 1538.16 16 -2 -1 3 115798. 2258.13 1 -2 -1 3 118614. 1725.67 15 -2 -1 3 115969. 1492.10 4 2 1 -3 117419. 1488.90 26 -2 -1 3 117641. 1747.21 12 -2 -1 1 639.630 118.230 4 2 1 -1 706.584 125.409 6 2 1 -1 773.566 191.737 1 -2 -1 1 606.850 109.153 10 -2 -1 1 665.247 121.315 5 2 1 -1 617.939 110.452 16 2 1 -1 625.185 180.766 2 -2 -1 1 729.339 129.484 15 -2 -1 1 757.379 204.090 2 2 1 -1 643.130 119.806 3 -2 -1 1 618.309 180.278 1 -2 -1 1 679.934 162.098 29 2 1 -1 626.926 116.028 26 -2 -1 1 677.036 109.514 12 2 1 1 2322.03 212.318 6 2 1 1 2395.10 346.894 2 -2 -1 -1 2286.41 214.836 23 -2 -1 -1 2324.00 338.089 2 2 1 1 2514.06 226.239 3 -2 -1 -1 2349.00 219.484 5 2 1 1 2234.96 183.176 9 -2 -1 -1 1889.82 291.566 1 2 1 1 2344.14 212.723 16 -2 -1 -1 2200.91 211.246 10 -2 -1 -1 2291.49 213.165 4 2 1 1 2248.55 318.258 1 -2 -1 -1 2227.34 190.460 13 -2 -1 -1 2140.97 322.069 29 2 1 1 2269.92 354.060 29 2 1 1 2632.60 246.047 26 -2 -1 -3 28682.4 903.365 23 2 1 3 29887.6 1223.39 2 2 1 3 28755.9 761.317 6 -2 -1 -3 30414.4 1245.90 2 2 1 3 29554.2 783.959 3 -2 -1 -3 29902.8 802.033 10 2 1 3 26976.2 825.578 26 -2 -1 -3 29665.3 806.861 5 -2 -1 -3 28272.4 1134.18 1 2 1 3 24784.6 771.841 9 -2 -1 -3 28669.2 753.102 4 2 1 3 30258.4 1195.40 1 -2 -1 -3 29547.1 825.876 13 -2 -1 -3 30813.3 1414.20 29 2 1 3 24924.2 1301.85 29 2 1 5 839.611 160.068 24 -2 -1 -5 1108.39 234.480 1 -2 -1 -5 942.409 142.815 4 -2 -1 -5 819.974 181.373 23 -2 -1 -5 943.104 151.335 10 2 1 5 79.5056 63.4851 18 2 1 5 1212.27 240.552 2 2 1 5 1022.91 191.305 9 2 1 5 923.976 137.860 3 -2 -1 -5 796.784 274.349 29 2 1 5 1011.70 299.570 29 -2 -1 -5 889.036 168.866 13 2 1 7 146.078 97.4436 24 -2 -1 -7-15.6208 75.4654 23 2 1 7-38.1855 108.471 2 -2 -1 -7 26.8399 57.3361 10 2 1 7 22.2874 101.086 18 -2 -1 -7 33.6142 66.5499 1 2 1 7-141.310 120.603 9 2 1 7 59.6026 59.4110 3 -2 -1 -7 26.2763 49.4504 4 -2 -1 -7 70.6740 160.935 29 2 1 7-58.7556 128.235 29 -2 -1 -7 11.0853 79.3842 13 2 1 9 1199.20 237.136 24 -2 -1 -9 1550.69 291.957 23 2 1 9 815.656 251.391 18 -2 -1 -9 1987.08 215.939 10 -2 -1 -9 1410.51 253.593 13 2 1 9 1089.10 244.699 9 2 1 9 621.545 165.388 8 2 1 11 76.9090 118.581 24 -2 -1 -11 309.041 147.921 22 -2 -1 -11 63.8755 106.772 23 -2 -1 -11 203.122 138.442 11 2 1 11 92.9139 86.9571 21 2 1 11-37.3548 137.095 18 2 1 11 49.3579 117.756 9 -2 2 20 250.649 206.584 24 -2 2 20-84.5930 271.034 18 -2 2 20-63.2142 329.611 9 2 -2 -20 177.936 165.894 23 2 -2 -20-308.993 283.381 7 2 -2 -20 149.741 241.934 13 2 -2 -20 134.775 196.604 11 2 -2 -18 1050.64 430.956 23 -2 -2 18-2.29157 190.858 24 -2 -2 18 276.492 374.986 12 2 -2 -18 1085.81 414.294 11 -2 2 18 530.080 371.111 18 2 2 -18 476.270 253.906 17 -2 2 18 1008.01 356.637 9 -2 2 18 6.80784 237.196 8 2 -2 -18 730.826 310.206 13 -2 2 18 764.350 302.040 24 2 2 -18 565.204 334.651 14 2 -2 -18 318.545 247.965 7 -2 -2 16 1950.10 424.890 24 -2 2 16 1762.88 402.375 24 -2 -2 16 2720.35 623.763 12 2 -2 -16 2425.79 522.786 23 2 -2 -16 2683.60 516.590 11 -2 2 16 2721.70 550.747 18 2 2 -16 2029.55 418.782 17 -2 2 16 3320.09 540.924 9 -2 2 16 1511.36 380.093 8 2 2 -16 2872.10 528.330 14 2 -2 -16 2853.22 467.619 13 2 -2 -16 2404.84 500.013 7 -2 2 14 189.838 151.860 24 -2 -2 14 239.918 152.260 24 -2 -2 14 121.985 223.004 12 2 -2 -14 212.930 228.408 23 2 -2 -14 256.282 219.615 22 2 -2 -14 129.785 155.973 11 -2 2 14 196.705 164.584 21 -2 2 14-260.482 319.931 18 -2 -2 14 309.723 234.880 18 2 2 -14 176.669 125.658 17 -2 2 14 470.184 231.080 9 -2 -2 14 519.390 262.900 15 -2 2 14 181.843 192.294 8 2 2 -14 237.631 163.278 14 2 -2 -14 385.124 210.190 13 2 -2 -14 410.603 237.193 7 -2 -2 12 47.4675 147.235 24 -2 -2 12 174.000 203.253 12 2 -2 -12 182.377 151.745 23 2 -2 -12 159.822 160.806 22 2 -2 -12 212.582 149.556 11 -2 2 12 206.819 143.313 21 2 2 -12 199.214 85.1968 20 -2 2 12 54.3063 163.555 18 -2 -2 12 289.321 205.650 18 2 2 -12 151.797 165.502 17 -2 2 12 81.3454 151.807 9 2 2 -12 326.621 190.823 16 -2 -2 12 412.430 245.417 15 -2 2 12 180.912 170.475 8 2 2 -12 59.7799 161.389 14 2 -2 -12 268.844 194.478 13 2 -2 -12-6.54546 106.678 7 2 2 -12 68.4774 158.960 7 -2 2 12-56.8389 141.677 24 -2 -2 10-58.6764 113.828 24 -2 -2 10 239.575 189.792 12 2 -2 -10 19.9425 139.720 23 2 -2 -10-105.368 147.893 22 2 -2 -10-55.6366 115.975 11 -2 -2 10 58.6918 156.873 1 -2 2 10-294.671 184.671 21 2 2 -10 0.30842 176.639 2 2 2 -10-96.6735 140.692 20 -2 -2 10 16.9058 89.4911 10 -2 -2 10 50.9360 87.2063 4 2 -2 -10-217.052 168.786 5 -2 2 10 276.425 203.541 18 2 -2 -10 114.972 175.631 2 -2 -2 10-49.0799 130.850 18 2 2 -10-133.488 131.401 17 -2 2 10-210.407 151.927 9 2 2 -10 13.5861 103.206 3 2 2 -10-51.5074 157.346 16 -2 2 10-45.3532 205.894 1 -2 -2 10 111.551 120.984 5 -2 -2 10 99.2715 156.784 15 -2 2 10 64.6984 142.878 8 2 2 -10-26.9386 149.553 14 -2 -2 10 7.43143 109.136 2 2 -2 -10-172.487 147.241 13 2 -2 -10 19.5364 96.8638 7 -2 -2 10 4.25733 154.900 25 2 2 -10-231.430 156.862 7 -2 -2 8 1196.91 224.986 4 -2 -2 8 1099.85 196.429 24 -2 -2 8 884.475 246.644 12 2 -2 -8 1039.65 121.709 23 2 -2 -8 762.849 179.706 11 2 -2 -8 999.808 192.850 22 2 2 -8 901.750 189.512 6 -2 2 8 640.648 168.021 21 -2 -2 8 999.393 260.357 25 -2 -2 8 1704.41 395.477 1 -2 2 8 327.470 182.946 1 2 2 -8 1158.83 243.446 20 2 2 -8 1159.92 358.419 2 2 -2 -8 966.929 336.545 19 2 -2 -8 735.857 383.730 2 2 -2 -8 750.059 248.574 5 -2 2 8 915.671 220.514 18 -2 -2 8 1218.85 222.411 10 -2 -2 8 1010.36 207.535 18 2 2 -8 1353.75 267.244 17 -2 2 8 379.720 131.619 9 -2 -2 8 1174.82 230.821 5 2 2 -8 1119.81 220.951 16 2 2 -8 1046.51 224.338 3 -2 -2 8 1212.97 282.898 15 -2 2 8 614.182 191.133 8 -2 -2 8 1386.60 394.316 2 2 2 -8 949.866 207.114 14 2 -2 -8 947.167 199.777 13 2 -2 -8 935.756 184.431 28 -2 2 8 747.353 201.779 27 2 2 -8 992.408 305.733 1 2 2 -8 1045.18 198.101 7 -2 -2 6 21.2785 61.5637 24 -2 -2 6 134.825 137.646 12 -2 -2 6 159.714 102.346 4 2 -2 -6 119.570 70.8090 23 2 -2 -6-44.0215 112.540 22 -2 -2 6 187.820 150.412 25 -2 2 6-7.92763 68.0790 21 2 2 -6 76.1012 53.2221 21 2 2 -6 20.7007 78.5766 20 2 2 -6-1.37421 118.367 2 -2 -2 6 266.742 140.433 1 2 -2 -6-164.218 151.260 19 -2 -2 6 21.8301 163.632 19 -2 2 6 182.315 252.810 19 -2 -2 6 37.6027 75.4238 10 2 -2 -6 98.3957 97.2296 28 -2 -2 6 119.023 91.3728 18 2 2 -6 59.3297 109.611 17 -2 -2 6 140.905 118.501 5 -2 -2 6 187.246 83.3616 22 2 2 -6 114.821 112.048 16 2 2 -6-41.0070 170.290 1 -2 -2 6-11.4105 96.9538 15 2 2 -6 126.496 98.0654 3 -2 2 6 110.713 97.6376 8 -2 -2 6 386.947 225.186 2 2 2 -6 11.9350 85.9759 14 2 2 -6 146.998 97.1261 6 2 2 -6 60.1722 46.8028 7 -2 2 6-115.132 151.605 29 -2 2 6 97.9630 92.7821 27 2 2 -4 7217.78 519.749 6 -2 -2 4 8410.29 820.904 1 -2 -2 4 9247.68 477.360 22 -2 -2 4 8431.72 897.329 2 2 2 -4 8584.98 433.047 21 2 2 -4 8695.93 572.537 3 -2 -2 4 8514.17 555.496 10 2 2 -4 8592.80 593.449 20 -2 -2 4 9463.50 619.493 5 -2 -2 4 8402.58 796.769 19 2 2 -4 9067.96 545.487 17 2 2 -4 8250.71 549.757 16 -2 -2 4 8413.82 627.051 15 2 2 -4 7722.45 823.451 1 2 2 -4 8673.59 230.667 8 -2 -2 4 8067.21 541.526 4 2 2 -4 9448.83 506.960 14 -2 -2 4 9283.98 588.109 29 2 2 -4 9396.50 927.397 2 -2 -2 4 8586.01 594.037 25 -2 -2 4 8528.43 605.224 12 -2 -2 2 11740.4 414.986 23 2 2 -2 11134.6 631.615 6 -2 -2 2 11497.8 955.403 1 -2 -2 2 11472.3 567.401 22 -2 -2 2 12536.3 1077.30 2 2 2 -2 11402.1 536.770 21 2 2 -2 11545.9 662.156 3 2 2 -2 11790.1 1042.20 2 -2 -2 2 11921.0 613.729 12 -2 -2 2 11046.4 627.500 10 2 2 -2 11352.0 658.434 20 -2 -2 2 11497.7 669.667 5 -2 -2 2 11631.1 963.376 19 2 2 -2 12058.4 568.551 17 2 2 -2 11094.0 624.055 16 2 2 -2 12361.6 1016.68 1 -2 -2 2 11253.9 681.534 15 -2 -2 2 11583.1 644.359 4 2 2 -2 12262.7 478.253 14 -2 -2 2 12645.5 396.567 13 -2 -2 2 12562.4 795.154 29 2 2 -2 12476.4 840.904 29 -2 -2 2 10511.8 598.667 25 -2 -2 0 1402.56 170.499 12 -2 -2 0 1426.51 183.725 23 -2 -2 0 1574.70 158.380 11 2 2 0 1562.51 244.385 6 -2 -2 0 1160.99 218.640 22 2 2 0 1401.57 203.424 21 2 2 0 1382.98 227.306 20 -2 -2 0 1160.52 313.471 19 2 2 0 1898.86 426.611 2 -2 -2 0 1428.04 231.671 10 2 2 0 1530.68 143.155 9 -2 -2 0 1536.27 251.122 5 2 2 0 1389.34 168.011 17 2 2 0 1849.45 364.803 29 -2 -2 0 1408.48 230.049 4 -2 -2 0 1638.92 367.508 1 2 2 0 1651.97 237.481 16 -2 -2 0 1024.95 294.495 2 -2 -2 0 1716.79 255.906 15 2 2 0 1088.04 201.534 3 2 2 0 1708.64 376.238 1 2 2 0 1679.64 128.853 14 -2 -2 0 1517.93 110.284 7 -2 -2 0 1592.80 179.141 13 -2 -2 0 2210.10 381.501 29 -2 -2 0 863.185 147.917 25 2 2 2 7111.53 494.461 6 -2 -2 -2 7537.42 491.488 23 -2 -2 -2 7987.38 812.716 1 -2 -2 -2 8167.39 431.768 11 -2 -2 -2 7820.21 538.064 22 -2 -2 -2 7980.07 847.588 2 2 2 2 8140.67 566.182 3 2 2 2 7531.60 509.678 21 -2 -2 -2 7540.85 524.472 10 2 2 2 7883.63 538.242 20 -2 -2 -2 7707.10 267.482 12 -2 -2 -2 7708.71 842.771 19 2 2 2 7778.20 408.835 9 2 2 2 7984.82 515.241 16 2 2 2 7020.11 758.976 1 -2 -2 -2 8118.87 526.191 15 2 2 2 7991.75 487.817 8 -2 -2 -2 7457.58 528.236 4 2 2 2 7702.86 868.492 2 -2 -2 -2 7613.55 449.042 13 -2 -2 -2 7632.27 799.219 29 2 2 2 8081.92 851.484 29 -2 -2 -2 7396.33 529.459 5 2 2 2 7617.79 281.475 24 -2 -2 -4 1878.34 275.113 4 -2 -2 -4 2271.42 304.292 23 -2 -2 -4 2228.46 268.021 11 -2 -2 -4 2130.45 314.604 22 2 2 4 1843.86 255.361 6 2 2 4 2161.75 304.566 3 2 2 4 2161.17 298.341 21 -2 -2 -4 1862.19 273.392 10 2 2 4 1904.45 267.031 20 -2 -2 -4 2015.19 423.937 1 2 2 4 2372.80 455.999 1 2 2 4 2515.57 496.621 2 -2 -2 -4 1480.66 399.379 19 2 2 4 2134.54 259.670 9 -2 -2 -4 1713.82 258.448 5 2 2 4 2052.70 275.378 16 2 2 4 2216.65 285.902 8 -2 -2 -4 2019.88 430.091 2 -2 -2 -4 2179.81 276.712 13 -2 -2 -4 2240.21 480.067 29 2 2 4 2717.95 554.651 29 2 2 4 2057.57 203.666 24 2 2 6 2137.41 288.274 6 -2 -2 -6 2205.08 342.496 23 -2 -2 -6 1949.95 317.732 22 2 2 6 1866.76 299.672 21 -2 -2 -6 1748.40 292.732 11 -2 -2 -6 1949.76 401.953 1 2 2 6 2056.92 271.417 20 2 2 6 2578.13 511.023 2 -2 -2 -6 2097.95 298.411 5 -2 -2 -6 2617.83 553.355 19 -2 -2 -6 2037.69 292.491 10 2 2 6 2254.94 305.811 9 2 2 6 418.065 138.404 18 2 2 6 2058.14 293.010 3 -2 -2 -6 1999.87 282.922 4 2 2 6 1834.22 397.057 1 -2 -2 -6 2493.71 471.629 2 2 2 6 2313.51 333.673 8 -2 -2 -6 2233.07 306.991 13 2 2 6 2270.20 262.113 24 2 2 8-126.334 123.617 24 -2 -2 -8 95.8174 148.818 1 -2 -2 -8-14.3738 140.462 23 -2 -2 -8 311.078 181.205 22 -2 -2 -8-26.9596 116.721 11 2 2 8 23.1456 90.5276 6 2 2 8-53.5139 118.243 21 2 2 8 75.8397 196.571 2 -2 -2 -8 112.069 99.4534 10 2 2 8-140.798 144.841 18 -2 -2 -8 156.256 151.009 13 2 2 8-73.8877 90.4377 3 -2 -2 -8 98.6167 97.0597 5 2 2 8 58.7659 112.772 9 2 2 8-30.5791 144.205 1 -2 -2 -8 94.3644 175.364 2 2 2 8-22.7869 83.5023 8 -2 -2 -8 13.5167 99.0709 4 -2 -2 -10 1086.86 294.237 7 2 2 10 776.944 229.157 24 -2 -2 -10 832.480 271.732 23 -2 -2 -10 1065.49 294.186 22 -2 -2 -10 592.511 226.085 11 2 2 10 839.062 223.845 21 2 2 10 388.187 206.468 18 2 2 10 618.654 190.476 9 -2 -2 -10 1126.02 280.984 13 2 2 10 581.984 233.459 8 -2 -2 -12 689.438 252.615 7 2 2 12 789.965 249.122 24 -2 -2 -12 460.155 219.369 23 -2 -2 -12 421.956 173.774 22 -2 -2 -12 703.173 267.949 11 2 2 12 516.779 230.857 21 2 2 12 654.064 196.720 9 2 2 12 289.119 173.115 8 -2 -2 -12 232.538 205.014 13 -2 -2 -14-89.8834 190.051 23 -2 -2 -14-13.0617 163.364 11 -2 -2 -14 303.663 228.568 7 2 2 14 207.000 224.541 9 -2 -2 -14 172.781 191.762 13 2 -3 -15 1019.08 371.163 23 -2 -3 15 557.423 279.489 12 2 3 -15 1376.45 452.966 17 -2 3 15 209.223 183.799 8 2 3 -15 576.162 226.959 14 2 -3 -15 937.689 342.054 13 2 -3 -13 2070.36 474.732 23 -2 -3 13 2894.38 623.801 12 2 3 -13 2922.11 568.384 17 -2 3 13 701.164 272.414 8 -2 -3 13 2195.13 496.662 15 2 3 -13 2903.11 497.251 14 2 -3 -13 2537.03 487.393 13 2 -3 -11 7000.55 790.975 23 2 -3 -11 3164.37 567.083 22 -2 3 11 1418.61 377.181 21 2 3 -11 5705.06 799.194 20 2 3 -11 10191.3 959.472 17 2 3 -11 8340.88 753.328 16 -2 -3 11 9616.22 974.552 15 -2 3 11 1997.99 400.878 8 2 3 -11 8917.97 779.684 14 2 -3 -11 6011.43 701.339 13 -2 -3 11 7405.10 872.169 12 2 3 -9 12840.2 837.483 6 2 -3 -9 5745.11 733.836 22 2 3 -9 17663.2 1133.74 3 -2 -3 9 16429.8 1131.26 10 2 3 -9 16945.8 1225.37 20 -2 -3 9 9711.37 780.148 5 2 3 -9 17231.8 1158.46 17 2 3 -9 16495.2 1045.44 16 -2 -3 9 14748.8 1163.47 15 -2 -3 9 16525.6 1027.59 4 2 3 -9 15339.2 963.498 14 2 -3 -9 4489.47 598.100 13 -2 -3 9 4442.16 702.021 25 -2 -3 9 13704.5 1109.82 12 -2 -3 7 1733.76 355.650 12 2 3 -7 1671.70 328.775 6 2 3 -7 2600.61 471.597 20 -2 -3 7 1927.55 375.277 10 -2 -3 7 2084.32 373.674 5 2 3 -7 2184.59 403.297 17 2 3 -7 2230.44 383.794 3 2 3 -7 2172.80 406.812 16 -2 -3 7 1842.56 393.816 15 2 3 -7 2300.16 363.137 14 -2 -3 7 2297.51 400.983 4 -2 -3 7 2347.41 440.594 25 -2 -3 5 968.127 274.578 12 -2 -3 5 396.910 154.828 22 2 3 -5 754.313 242.602 6 2 3 -5 310.455 120.651 21 2 3 -5 439.953 164.498 20 -2 -3 5 609.881 209.430 10 -2 -3 5 692.148 228.852 5 2 3 -5 568.689 179.226 17 2 3 -5 399.052 187.535 3 2 3 -5 586.960 232.884 16 -2 -3 5 640.993 237.381 15 2 3 -5 695.972 177.981 14 -2 -3 5 631.441 236.099 25 -2 -3 5 642.675 210.008 4 -2 -3 3-165.885 134.536 12 -2 -3 3 164.602 134.742 22 2 3 -3 34.3197 98.1412 21 2 3 -3 138.035 160.418 20 -2 -3 3 42.6858 108.797 10 -2 -3 3 98.0612 152.103 5 2 3 -3-108.510 97.9845 17 2 3 -3-57.0666 140.862 16 2 3 -3 248.616 175.898 6 2 3 -3 116.610 131.879 3 -2 -3 3 4.56938 144.601 15 -2 -3 3-179.579 130.203 25 -2 -3 3 227.684 134.862 4 2 3 -1-25.0733 101.484 6 -2 -3 1 24.4300 85.2709 22 2 3 -1 64.0720 91.8512 21 2 3 -1 61.3036 114.685 20 -2 -3 1 43.8607 114.197 10 -2 -3 1 221.613 161.858 5 2 3 -1 229.905 133.387 17 2 3 -1 11.4016 117.064 16 2 3 -1-97.3120 97.6116 3 -2 -3 1 51.3318 121.383 15 -2 -3 1 375.039 210.905 29 2 3 -1 209.262 253.037 29 -2 -3 1 152.388 121.694 4 -2 -3 1 1.91048 90.3920 25 -2 -3 -1 916.492 200.920 23 2 3 1 1070.12 269.271 6 -2 -3 -1 767.306 211.739 22 2 3 1 913.905 239.207 21 2 3 1 820.151 232.639 20 -2 -3 -1 994.585 258.791 10 -2 -3 -1 619.157 210.248 5 2 3 1 677.929 198.586 16 2 3 1 638.237 195.384 3 -2 -3 -1 1078.54 276.244 15 2 3 1 988.667 181.257 8 -2 -3 -1 739.714 306.541 29 -2 -3 -1 882.894 176.735 13 2 3 1 668.685 248.805 29 -2 -3 -1 927.936 207.703 25 -2 -3 -1 1057.91 277.272 4 -2 -3 -3 80.1213 118.937 23 2 3 3-128.488 135.100 6 -2 -3 -3-58.6339 104.621 22 2 3 3-280.338 148.799 21 2 3 3-142.144 113.356 20 -2 -3 -3 149.371 163.252 10 -2 -3 -3-142.712 138.975 5 2 3 3 295.220 130.595 3 2 3 3 69.6413 145.355 16 -2 -3 -3-7.30520 112.885 15 2 3 3-125.756 122.412 8 -2 -3 -3-76.1816 95.6428 13 -2 -3 -3 29.1079 120.836 4 -2 -3 -3-23.6429 79.6821 25 -2 -3 -5 23.0368 105.019 23 -2 -3 -5 518.671 214.967 22 -2 -3 -5 449.529 170.756 11 2 3 5 115.330 127.050 21 2 3 5 217.559 158.139 6 2 3 5 382.335 148.365 20 -2 -3 -5 465.296 183.764 10 -2 -3 -5 359.189 197.788 5 2 3 5 137.691 138.879 3 2 3 5 355.857 123.800 9 2 3 5 160.366 131.930 16 2 3 5 353.908 153.031 8 -2 -3 -5 509.300 177.273 13 -2 -3 -5 220.119 131.931 4 -2 -3 -7 2795.60 444.507 23 -2 -3 -7 2788.76 454.646 22 2 3 7 2551.85 382.078 6 -2 -3 -7 2528.67 402.064 11 2 3 7 2191.45 395.850 21 2 3 7 3069.16 417.345 20 -2 -3 -7 2576.05 390.802 10 2 3 7 2615.78 428.855 3 -2 -3 -7 2834.02 421.538 5 2 3 7 2821.39 387.943 9 2 3 7 2606.91 413.214 16 2 3 7 2504.43 385.906 8 -2 -3 -7 2786.73 425.030 4 -2 -3 -7 2892.93 413.515 13 -2 -3 -9 1456.24 346.586 23 -2 -3 -9 1773.28 389.026 22 -2 -3 -9 1586.88 356.594 11 2 3 9 2180.75 405.431 21 -2 -3 -9 1772.54 364.398 10 2 3 9 1697.07 330.460 9 2 3 9 1751.46 358.994 8 -2 -3 -9 1660.88 344.692 13 -2 -3 -11 350.673 176.866 23 -2 -3 -11 164.392 179.996 22 -2 -3 -11 490.439 302.273 11 2 3 11 182.161 197.972 21 2 3 11 300.338 187.234 9 2 3 11-104.024 164.417 8 -2 -3 -11 291.502 204.253 13 -2 -3 -13 182.319 207.606 23 -2 -3 -13 443.967 278.823 22 -2 -3 -13-227.174 228.848 11 2 3 13-25.1943 162.077 21 2 3 13-88.4963 164.304 9 -2 -3 -13-265.641 201.412 13 2 3 13 10.3232 277.897 8 2 4 -10 79.4318 122.080 3 2 4 -10-122.531 217.030 17 2 4 -10-191.092 296.266 16 -2 -4 10-61.1458 279.802 15 -2 -4 10-179.014 261.042 4 -2 -4 8-24.7201 222.991 10 2 4 -8-141.652 229.800 20 2 4 -8 29.5300 171.657 3 2 4 -8-5.46256 181.787 17 2 4 -8 162.874 245.063 16 -2 -4 8-43.0105 251.958 15 -2 -4 8-394.847 292.722 4 2 4 -6 2592.62 498.673 6 2 4 -6 3328.07 667.776 20 -2 -4 6 3306.92 609.189 10 2 4 -6 3092.70 595.182 3 -2 -4 6 1734.88 426.013 5 2 4 -6 3770.05 604.054 17 2 4 -6 2496.88 540.976 16 -2 -4 6 3191.85 646.926 15 -2 -4 6 2486.22 486.122 4 -2 -4 6 2309.29 516.989 25 2 4 -4 66.3323 180.617 6 2 4 -4 66.1680 220.761 20 -2 -4 4 205.732 173.827 10 -2 -4 4 11.9411 190.504 4 2 4 -4 164.444 190.372 3 -2 -4 4 236.093 198.983 5 2 4 -4 347.022 214.127 16 -2 -4 4 316.880 319.472 15 -2 -4 4 33.3060 175.549 25 -2 -4 2 418.554 275.492 22 2 4 -2 426.533 245.664 6 2 4 -2-2.34486 150.899 21 2 4 -2 320.752 248.563 20 -2 -4 2 462.382 288.176 10 -2 -4 2 138.731 172.034 25 2 4 -2-34.3971 206.980 3 -2 -4 2 140.647 162.411 5 2 4 -2-25.6775 203.778 16 -2 -4 2 22.8766 224.409 15 -2 -4 2 294.084 246.448 4 -2 -4 0 449.516 237.746 22 2 4 0 224.906 222.115 6 2 4 0 432.740 220.826 21 2 4 0 411.151 252.294 20 -2 -4 0 243.774 178.298 10 2 4 0 211.356 214.602 3 -2 -4 0 638.776 274.923 5 2 4 0 248.925 159.661 16 -2 -4 0 951.335 347.912 15 -2 -4 0 157.781 184.994 4 -2 -4 -2 964.161 331.700 22 2 4 2 708.681 269.373 6 2 4 2 849.457 270.629 21 2 4 2 1240.13 366.037 20 -2 -4 -2 1315.78 369.698 10 2 4 2 1372.73 385.949 3 -2 -4 -2 1090.54 352.893 5 2 4 2 1142.78 315.390 16 -2 -4 -2 1005.68 318.070 15 -2 -4 -2 768.226 264.160 4 -2 -4 -4 5126.90 680.293 22 2 4 4 5275.27 769.608 3 2 4 4 4244.32 602.464 6 2 4 4 3477.92 523.058 21 2 4 4 5587.55 748.983 20 -2 -4 -4 4869.99 668.723 5 -2 -4 -4 4255.25 624.108 10 2 4 4 4719.52 600.789 16 -2 -4 -4 6205.94 791.533 4 -2 -4 -6 264.332 224.380 22 2 4 6 704.616 281.245 6 2 4 6 1010.53 313.381 21 2 4 6 708.325 328.085 20 -2 -4 -6 957.442 346.411 10 2 4 6 1617.40 479.154 3 -2 -4 -6 900.958 332.339 5 2 4 6 1290.06 385.708 16 -2 -4 -6 1248.01 392.041 4 -2 -4 -8 4046.38 627.716 23 -2 -4 -8 3267.70 614.396 22 2 4 8 2660.70 482.841 6 2 4 8 3015.83 540.413 21 -2 -4 -8 3922.23 653.942 10 -2 -4 -8 2827.82 519.027 5 2 4 8 3242.42 543.039 8 -2 -4 -8 3257.16 537.575 13 -2 -4 -10 132.561 188.166 23 -2 -4 -10 334.901 267.559 22 2 4 10 27.4236 177.716 21 2 4 10 296.697 246.843 8 -2 -4 -10 78.5902 202.898 13 -2 -4 -12 559.812 392.975 23 -2 -4 -12-189.496 300.358 22 2 4 12-306.980 250.083 21 -2 -4 -12-54.2407 215.596 13 2 4 12 158.623 286.165 8 2 5 -3 16.7173 324.490 20 -2 -5 3 239.902 317.515 10 2 5 -3 14.0161 250.349 3 2 5 -3 333.847 497.487 16 -2 -5 3 789.987 471.170 15 -2 -5 3-89.1081 196.728 4 2 5 -1 13.7729 413.630 6 2 5 -1-114.381 248.531 20 -2 -5 1 267.263 262.006 10 2 5 -1 72.5034 261.009 3 -2 -5 1 257.730 349.402 5 2 5 -1 544.881 458.205 16 -2 -5 1 21.4681 387.478 15 -2 -5 1-120.042 206.946 4 2 5 1 4869.18 878.236 6 2 5 1 3997.09 813.025 20 2 5 1 1703.30 494.347 3 -2 -5 -1 4558.33 848.858 10 -2 -5 -1 5446.18 951.467 5 2 5 1 3557.74 767.329 16 -2 -5 -1 1667.59 519.319 4 -2 -5 -3 235.449 236.478 22 2 5 3-22.7186 355.764 6 2 5 3 580.708 347.444 21 2 5 3-394.016 295.511 3 2 5 3-66.2171 184.568 20 -2 -5 -3 288.303 292.880 10 -2 -5 -3 680.697 406.393 5 2 5 3 239.677 306.597 16 -2 -5 -5-250.784 337.031 22 2 5 5-133.666 386.870 6 2 5 5-317.932 375.345 21 2 5 5-16.9277 192.448 20 -2 -5 -5-160.461 225.400 10 -2 -5 -5 367.151 397.271 5 2 5 5-832.224 393.105 16 -2 -5 -7-446.268 388.832 22 2 5 7-35.9429 251.319 21 2 5 7 663.412 438.886 6 -2 -5 -7-89.1140 255.890 10 -2 -5 -7 549.348 423.246 5 3 0 -23-49.7098 241.280 11 -3 0 23 29.6968 183.930 9 3 0 -23 642.535 385.353 14 -3 0 21 86.1162 284.547 24 3 0 -21-275.625 233.843 11 -3 0 21-239.997 339.622 18 -3 0 21 204.440 220.415 9 3 0 -21-95.7750 262.488 14 3 0 -21 407.815 309.473 7 -3 0 19-146.884 199.324 24 -3 0 19-13.2424 278.206 12 3 0 -19 538.379 282.938 11 -3 0 19-297.932 300.813 18 -3 0 19 298.085 226.218 9 3 0 -19 244.492 216.466 14 3 0 -19 141.288 226.578 7 -3 0 17-83.5730 211.328 12 3 0 -17-253.782 263.442 11 -3 0 17 217.420 227.350 24 -3 0 17-180.759 302.029 18 -3 0 17 51.5223 183.124 9 3 0 -17-205.741 181.519 14 3 0 -17 36.3921 124.532 13 3 0 -17-489.145 280.412 7 -3 0 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653.962 29 -3 -3 0 2477.17 334.582 25 -3 -3 -2-275.536 184.455 4 -3 -3 -2 18.2494 104.447 23 -3 -3 -2 235.117 138.801 22 3 3 2 130.366 149.357 6 3 3 2 82.8126 121.689 21 3 3 2-69.5726 123.448 20 -3 -3 -2-47.9668 152.168 10 -3 -3 -2-114.438 138.891 5 3 3 2-61.0883 120.162 16 3 3 2-213.273 186.435 3 -3 -3 -2-111.713 163.722 15 3 3 2 278.433 155.859 8 -3 -3 -2 147.435 108.577 13 -3 -3 -4 1183.22 292.085 4 -3 -3 -4 1063.36 260.181 23 -3 -3 -4 1237.23 313.626 22 3 3 4 1032.24 267.977 6 3 3 4 1140.84 260.233 21 3 3 4 1185.99 257.579 20 -3 -3 -4 1221.15 283.457 10 -3 -3 -4 454.930 172.147 5 3 3 4 1472.98 300.571 16 3 3 4 1431.57 310.432 3 3 3 4 872.539 205.859 8 -3 -3 -4 1104.21 228.823 13 -3 -3 -6 701.458 252.505 23 -3 -3 -6 391.949 192.516 22 -3 -3 -6 274.093 129.750 11 3 3 6 368.948 165.315 6 3 3 6 500.067 199.989 21 3 3 6 400.970 177.319 20 -3 -3 -6 513.333 214.054 10 3 3 6 311.593 122.680 3 -3 -3 -6 236.385 193.900 5 3 3 6 677.383 210.166 9 -3 -3 -6 243.672 181.683 4 3 3 6 611.940 202.132 8 -3 -3 -6 386.820 161.749 13 -3 -3 -8 165.126 207.448 23 -3 -3 -8-213.311 173.397 22 -3 -3 -8 109.256 167.607 11 3 3 8-197.697 157.801 21 3 3 8 154.572 175.487 6 -3 -3 -8-95.3013 126.511 10 3 3 8-27.9133 145.830 9 -3 -3 -8-108.985 159.115 5 3 3 8-200.505 197.745 8 -3 -3 -8 11.5395 162.811 13 -3 -3 -10 1974.36 424.352 23 -3 -3 -10 1931.53 431.900 22 -3 -3 -10 1739.43 386.408 11 3 3 10 1586.10 375.066 21 3 3 10 442.828 178.404 9 3 3 10 916.917 281.763 8 -3 -3 -10 1169.11 313.069 13 3 4 -15 70.0522 349.998 17 3 4 -13 268.079 215.810 17 3 4 -13-298.054 274.254 16 -3 -4 13-7.71865 222.316 15 -3 -4 11 56.1544 151.599 12 3 4 -11 3.06144 174.779 20 3 4 -11 210.310 272.122 17 -3 -4 11 180.396 331.915 15 -3 -4 11-211.654 215.921 4 -3 -4 9 333.420 283.583 12 3 4 -9 97.8964 160.882 6 3 4 -9 358.655 286.652 20 -3 -4 9 452.585 270.745 10 3 4 -9 726.481 298.540 3 3 4 -9 25.9321 262.987 17 -3 -4 9 67.9580 125.126 5 3 4 -9-35.8141 266.158 16 -3 -4 9 86.9332 262.628 15 -3 -4 9 330.588 261.978 4 -3 -4 9 5.50214 149.228 25 3 4 -7 1358.99 394.746 6 3 4 -7 864.553 353.295 20 -3 -4 7 1223.34 397.402 10 3 4 -7 1365.74 371.145 3 3 4 -7 926.657 322.602 17 -3 -4 7 1010.58 344.437 5 3 4 -7 979.831 315.543 16 -3 -4 7 815.706 421.834 15 -3 -4 7 1168.39 334.507 4 -3 -4 7 1325.81 396.753 25 3 4 -5 144.631 206.453 6 3 4 -5 539.042 276.215 20 -3 -4 5 163.689 166.899 10 3 4 -5 249.505 222.423 3 3 4 -5 761.205 313.036 17 -3 -4 5 412.699 225.995 5 3 4 -5 455.352 277.325 16 -3 -4 5-234.273 321.854 15 -3 -4 5 150.905 200.222 4 -3 -4 5 58.3661 180.521 25 3 4 -3-485.553 305.373 6 3 4 -3 89.8658 166.414 20 -3 -4 3 112.793 187.662 10 -3 -4 3-33.2288 163.047 5 3 4 -3 390.205 278.096 3 3 4 -3 82.6040 200.110 16 -3 -4 3 491.169 295.398 15 -3 -4 3 156.871 182.287 4 -3 -4 3-411.849 262.219 25 -3 -4 1 280.347 197.351 22 3 4 -1 111.524 250.580 6 3 4 -1 58.2227 171.042 21 3 4 -1 82.7531 148.013 20 -3 -4 1 544.192 278.389 10 -3 -4 1 439.894 186.507 5 3 4 -1-88.5302 168.805 3 3 4 -1-258.576 262.927 16 -3 -4 1-250.070 218.820 15 -3 -4 1-44.3120 161.348 4 -3 -4 1 172.197 159.058 25 -3 -4 -1 80.7667 183.948 22 3 4 1 70.2604 204.807 6 3 4 1 144.686 203.888 21 3 4 1-8.61782 159.829 20 -3 -4 -1 284.499 220.048 10 3 4 1-31.6288 137.826 3 -3 -4 -1 190.465 249.027 5 3 4 1 156.556 204.338 16 -3 -4 -1 376.127 269.100 15 -3 -4 -1 137.563 224.711 4 -3 -4 -3 1929.60 434.944 22 3 4 3 1782.93 393.373 6 3 4 3 2221.26 432.974 21 3 4 3 1345.89 340.313 20 -3 -4 -3 1794.08 385.098 10 3 4 3 1870.32 439.544 3 -3 -4 -3 1630.41 408.026 5 3 4 3 1519.11 385.449 16 -3 -4 -3 1773.78 434.018 4 -3 -4 -5 655.432 256.069 22 3 4 5 800.546 320.533 6 3 4 5 1129.39 312.305 21 3 4 5 953.353 336.255 20 -3 -4 -5 1245.02 359.820 10 3 4 5 1457.11 419.506 3 -3 -4 -5 407.102 208.495 5 3 4 5 1233.72 369.680 16 -3 -4 -5 1082.38 367.743 4 -3 -4 -7 75.8716 237.951 23 -3 -4 -7 138.970 196.046 22 3 4 7-0.24017 179.245 6 3 4 7 194.580 179.188 21 -3 -4 -7 350.764 196.028 10 -3 -4 -7 201.123 193.096 5 3 4 7 45.7462 189.274 8 -3 -4 -7 297.052 205.871 13 -3 -4 -9 244.574 185.943 23 -3 -4 -9 86.5239 185.056 22 3 4 9 198.668 237.740 21 3 4 9-33.1174 209.844 8 -3 -4 -9 188.953 192.887 13 -3 -4 -11-646.941 422.035 23 -3 -4 -11-260.929 284.769 22 3 5 -8-500.272 327.653 20 3 5 -8 426.213 330.935 3 3 5 -8-90.1814 309.639 16 -3 -5 8-19.3780 307.632 15 -3 -5 8 429.712 250.533 4 3 5 -6-146.270 296.399 20 -3 -5 6 262.976 254.999 10 3 5 -6 238.955 203.950 3 3 5 -6 292.248 410.326 16 -3 -5 6 256.093 413.120 15 -3 -5 6 110.863 304.943 4 -3 -5 6-174.530 239.303 25 3 5 -4 131.092 411.439 6 3 5 -4 300.043 286.986 20 -3 -5 4 242.724 370.042 10 3 5 -4 174.201 326.458 3 -3 -5 4 162.268 373.736 5 3 5 -4 797.986 459.079 16 -3 -5 4 217.919 276.103 15 -3 -5 4 232.061 252.099 4 3 5 -2 560.436 374.539 6 3 5 -2 1298.75 491.791 20 -3 -5 2 1064.75 426.185 10 3 5 -2-39.7326 1689.39 3 -3 -5 2 1010.61 501.877 5 3 5 -2 24.7666 361.553 16 -3 -5 2 981.396 483.934 15 -3 -5 2 745.986 405.276 4 -3 -5 0 401.024 251.490 22 3 5 0 125.013 255.006 6 3 5 0-268.877 229.286 21 3 5 0-102.081 297.787 20 -3 -5 0 785.103 391.330 10 3 5 0-194.593 288.899 3 -3 -5 0-164.094 310.050 5 3 5 0 185.498 299.141 16 -3 -5 0 98.2931 293.347 4 -3 -5 -2 4633.30 774.690 22 3 5 2 3523.29 693.749 6 3 5 2 3817.49 711.264 21 3 5 2 4233.82 865.773 20 -3 -5 -2 3160.02 666.339 10 3 5 2 3181.84 771.901 3 -3 -5 -2 2466.50 574.411 5 3 5 2 2394.40 598.905 16 -3 -5 -2 3412.24 731.270 4 -3 -5 -4 82.9824 257.492 22 3 5 4-38.0599 199.741 21 3 5 4-320.898 338.390 6 3 5 4-158.912 321.871 20 3 5 4 101.231 186.235 3 -3 -5 -4 404.246 368.999 10 -3 -5 -4 262.019 405.258 5 3 5 4-230.217 304.072 16 -3 -5 -4 313.381 216.660 4 -3 -5 -6 49.8248 305.939 22 3 5 6 1001.54 438.320 21 3 5 6 327.185 308.210 6 -3 -5 -6 1228.79 516.648 10 -3 -5 -6 735.671 356.310 5 -4 0 22 303.363 225.611 24 -4 0 22-14.5193 274.828 18 4 0 -22 19.8794 238.790 14 4 0 -22 241.328 241.780 7 4 0 -20 10532.7 1022.76 11 -4 0 20 11694.2 1245.32 18 4 0 -20 11770.5 1095.30 14 4 0 -20 11555.2 1126.04 7 -4 0 20 11956.8 1144.06 24 -4 0 18 1109.42 341.445 24 -4 0 18 1197.02 432.282 12 4 0 -18 812.391 323.944 11 -4 0 18 660.930 294.622 18 -4 0 18 488.961 227.167 9 4 0 -18 720.175 318.926 14 4 0 -18 784.963 330.526 7 -4 0 16 2326.25 439.653 24 -4 0 16 2552.68 525.658 12 4 0 -16 2170.89 405.174 11 -4 0 16 2153.32 450.093 18 -4 0 16 2466.08 426.490 9 4 0 -16 2282.78 335.526 13 4 0 -16 2618.60 487.801 7 -4 0 14 2941.70 498.322 12 -4 0 14 3095.67 443.470 24 4 0 -14 2564.56 416.268 11 -4 0 14 2610.52 453.558 18 -4 0 14 2533.34 396.967 9 4 0 -14 3512.18 470.982 7 4 0 -14 2991.86 360.410 13 -4 0 14 3436.35 600.445 29 -4 0 12 156.056 135.237 24 4 0 -12 58.6539 60.1236 11 -4 0 12 334.658 182.347 18 -4 0 12 145.624 89.5786 9 4 0 -12 140.520 124.884 13 4 0 -12 94.6522 90.2551 7 -4 0 12-202.845 138.021 29 4 0 -12 28.4248 48.5067 28 -4 0 12 78.4619 63.5011 27 -4 0 12 148.233 175.392 12 -4 -1 23 34.3468 298.778 12 -4 -1 21 123.562 292.175 24 -4 -1 21 545.551 396.908 12 -4 -1 21-114.167 307.733 18 4 1 -21 63.9159 224.818 14 4 1 -21 300.762 215.588 7 -4 -1 19 678.094 297.898 24 -4 -1 19 1678.64 550.051 12 4 -1 -19 861.020 309.382 11 -4 1 19 290.347 284.625 18 -4 -1 19 1179.47 353.606 18 -4 1 19 106.675 137.870 9 4 1 -19 856.176 314.920 17 4 1 -19 1412.40 460.441 14 4 -1 -19 832.593 289.975 7 4 1 -19 1111.93 374.751 7 -4 -1 17 2728.96 490.381 24 -4 -1 17 3110.16 652.352 12 4 1 -17 2604.33 470.451 11 4 -1 -17 2407.13 474.283 11 -4 1 17 1087.82 350.504 18 -4 -1 17 2877.76 565.876 18 -4 -1 17 870.522 259.932 9 -4 1 17 816.591 287.159 9 4 1 -17 2684.41 452.473 17 4 -1 -17 2062.72 427.659 14 4 1 -17 2297.72 468.648 14 4 -1 -17 2532.56 458.051 7 4 1 -17 2529.14 501.043 7 -4 1 17 771.304 268.516 24 -4 -1 15-126.702 166.999 24 -4 -1 15 210.923 234.642 12 4 1 -15 76.9008 122.259 11 4 -1 -15-5.81320 113.752 11 -4 1 15-140.736 214.214 18 -4 -1 15 55.4512 171.992 18 -4 -1 15 73.0970 88.3533 9 -4 1 15 12.7678 110.437 9 4 1 -15 155.991 147.817 17 4 1 -15 34.4617 149.722 14 4 -1 -15 206.504 154.965 7 4 1 -15 10.6095 144.490 7 -4 -1 13 65.4223 127.895 24 -4 -1 13-83.9860 213.881 12 -4 -1 13 119.226 198.376 18 4 1 -13 95.3665 136.747 17 4 1 -13-10.7683 118.386 7 -4 -1 11 99.9555 163.217 12 -4 -1 11-13.7507 120.818 24 -4 -1 11 4.28300 59.0660 4 4 1 -11-4.83595 64.9677 20 -4 -1 11-135.427 157.984 18 4 1 -11 11.9068 86.3829 17 4 1 -11 118.174 125.209 2 -4 -1 11-20.7606 79.9423 1 4 1 -11-75.8439 86.3987 3 4 1 -11 62.6790 83.5628 7 4 1 -11 106.453 73.8803 13 -4 -1 9 121.346 66.3889 19 -4 -1 9 208.119 127.468 18 -4 -1 9 156.316 70.1763 10 4 1 -9 58.7363 74.8933 17 4 1 -9 110.579 52.9753 13 -4 -1 9 153.934 105.078 12 4 1 -7 25358.9 875.380 17 -4 -1 7 23937.5 1050.26 12 -4 -2 20 287.975 233.750 24 -4 -2 20-143.482 431.027 12 -4 -2 20 203.998 284.048 18 4 2 -20 868.855 362.327 17 4 2 -20 58.3944 256.534 14 -4 -2 18 1165.27 391.954 24 -4 -2 18 603.473 410.386 12 -4 -2 18 813.350 350.491 18 4 2 -18 671.048 316.122 17 4 2 -18 575.911 328.920 14 -4 -2 16 39.7997 172.621 24 -4 -2 16 196.838 365.525 12 -4 -2 16 50.2695 173.035 18 4 2 -16 161.312 214.997 17 -4 -2 16 198.471 159.210 15 4 2 -16 120.272 209.937 14 -4 -2 14 12274.8 955.093 18 4 2 -14 13568.3 1011.33 17 -4 -2 14 13897.7 1064.45 15 4 2 -14 13015.4 1003.20 14 -4 -2 14 11327.8 1108.55 12 -4 -2 14 12355.1 926.771 24 4 2 -12 7793.27 629.367 20 -4 -2 12 8006.24 710.801 18 4 2 -12 8962.32 763.202 17 4 2 -12 8391.83 655.318 16 -4 -2 12 8720.08 806.441 15 4 2 -12 8531.28 748.583 14 -4 -2 12 8528.85 871.630 12 -4 -2 12 8357.19 679.678 24 -4 -2 10 2219.33 421.911 12 -4 -2 10 1903.66 290.846 4 4 2 -10 1765.90 296.271 20 -4 -2 10 1949.19 277.477 10 -4 -2 10 1747.83 294.853 18 4 2 -10 1970.36 477.689 2 4 2 -10 2255.98 366.088 17 4 2 -10 1904.50 311.118 16 -4 -2 10 1924.25 420.097 1 -4 -2 10 2033.38 388.301 15 4 2 -10 1544.02 259.975 3 4 2 -8 26508.7 1633.68 2 4 2 -8 26523.8 1061.65 3 -4 -2 8 23892.9 956.837 10 4 2 -8 24434.6 1056.58 20 -4 -2 8 24901.6 1508.89 1 -4 -2 8 24882.0 1272.47 19 -4 -2 8 25822.7 936.093 18 4 2 -8 24660.4 1061.74 17 4 2 -8 25285.3 1083.98 16 -4 -2 8 25025.1 1196.80 15 -4 -2 8 25348.9 1006.93 4 -4 -2 8 24686.4 1232.57 12 -4 -2 6 2899.57 503.047 1 4 2 -6 2576.76 338.785 3 -4 -2 6 2699.07 320.417 10 -4 -2 6 2671.99 448.260 19 -4 -2 6 2477.39 242.883 18 4 2 -6 2152.83 288.093 17 4 2 -6 3043.89 561.937 2 4 2 -6 2570.83 329.674 16 -4 -2 6 2585.46 375.845 15 -4 -2 6 2529.77 320.455 4 -4 -2 6 2416.79 282.110 29 -4 -2 6 2546.11 354.545 12 4 2 -4 1723.85 284.925 6 -4 -2 4 1846.66 428.060 1 -4 -2 4 1848.02 383.663 19 -4 -2 4 1652.21 256.439 10 4 2 -4 2489.10 545.946 2 4 2 -4 1838.87 278.677 16 -4 -2 4 1605.65 305.485 5 -4 -2 4 2142.54 322.870 15 -4 -2 4 1947.99 288.516 4 4 2 -4 2037.05 296.945 3 -4 -2 4 1973.26 474.884 2 -4 -2 4 1639.61 290.671 29 4 2 -4 1894.51 285.502 26 -4 -2 4 1546.66 254.410 12 -4 -2 2-59.6698 111.456 4 4 2 -2-53.7547 106.747 6 -4 -2 2 206.250 118.821 10 -4 -2 2-84.6584 221.309 1 4 2 -2 3.87726 127.021 2 -4 -2 2 63.8139 91.5499 5 4 2 -2 111.645 111.775 16 4 2 -2 287.228 219.695 1 -4 -2 2 122.864 130.547 15 4 2 -2 69.7921 69.0415 3 -4 -2 2-31.3285 117.697 2 -4 -2 2-32.7340 115.181 29 4 2 -2 3.76665 71.1871 26 -4 -2 2-35.9978 81.1590 12 4 2 0 197.127 147.918 6 -4 -2 0 211.875 140.043 10 -4 -2 0 66.8166 95.1642 5 -4 -2 0 247.255 243.371 2 4 2 0 185.009 164.531 1 4 3 -19 128.179 248.140 17 4 3 -19 371.756 313.249 14 -4 -3 17-393.651 351.998 12 4 3 -17 321.894 290.245 17 -4 -3 17 46.4724 230.924 15 4 3 -17-220.846 331.361 14 -4 -3 15 297.643 245.953 12 4 3 -15-320.070 273.188 17 -4 -3 15-118.098 204.641 15 4 3 -15 295.246 242.727 14 -4 -3 13 371.054 265.071 12 4 3 -13 495.651 265.453 20 4 3 -13 544.681 296.431 17 4 3 -13 409.318 187.215 16 -4 -3 13 248.371 253.391 15 4 3 -13 828.117 292.057 14 -4 -3 11 955.605 268.377 4 -4 -3 11 356.763 248.283 12 4 3 -11 873.768 277.113 20 -4 -3 11 1076.56 285.466 10 4 3 -11 878.548 290.678 17 4 3 -11 860.583 289.157 16 4 3 -11 1195.25 278.283 3 -4 -3 11 1133.74 348.993 15 4 3 -11 1196.23 325.581 14 -4 -3 9 2662.77 491.573 12 -4 -3 9 2519.05 411.623 4 4 3 -9 2719.58 443.634 20 -4 -3 9 2618.09 417.528 10 4 3 -9 2700.55 445.399 17 4 3 -9 3099.72 485.587 16 -4 -3 9 2929.75 473.832 5 4 3 -9 2397.75 401.354 3 -4 -3 9 2252.60 456.880 15 4 3 -9 3121.33 432.453 14 -4 -3 9 1399.37 339.768 25 -4 -3 7 361.894 170.200 12 -4 -3 7-74.9572 123.487 4 4 3 -7 7.24938 186.122 6 4 3 -7-33.9191 142.071 20 -4 -3 7 29.9989 139.549 10 4 3 -7 26.9981 114.556 17 -4 -3 7-22.2005 131.252 5 4 3 -7-124.727 131.551 16 4 3 -7 328.106 211.586 3 -4 -3 7-18.9709 154.681 15 4 3 -7 149.114 172.901 14 -4 -3 7-46.1311 167.294 25 -4 -3 5 564.233 221.549 12 -4 -3 5 364.293 196.408 4 -4 -3 5 581.257 176.199 22 4 3 -5 350.271 191.619 6 4 3 -5 475.631 154.257 21 4 3 -5 284.293 148.428 20 -4 -3 5 379.437 188.680 10 4 3 -5 548.819 168.642 17 -4 -3 5 284.515 193.420 5 4 3 -5 309.795 186.776 16 -4 -3 5 263.527 170.456 15 4 3 -5 408.952 190.492 3 -4 -3 3 2464.52 396.321 4 -4 -3 3 2078.29 311.096 22 4 3 -3 2307.73 322.216 21 4 3 -3 1983.25 352.600 6 4 3 -3 2258.00 389.795 20 -4 -3 3 2183.32 355.008 10 -4 -3 3 2238.69 394.950 5 4 3 -3 1756.26 330.836 16 -4 -3 3 2315.35 388.115 15 4 3 -3 2090.20 378.032 3 4 3 -1 6778.70 637.900 6 -4 -3 1 5450.93 541.553 22 4 3 -1 5523.01 518.304 21 4 3 -1 6201.93 638.605 3 -4 -3 1 4572.02 523.633 10 4 3 -1 5330.27 563.751 20 -4 -3 1 5538.98 591.478 5 4 3 -1 5259.37 549.294 16 -4 -3 1 5844.48 607.147 15 -4 -3 1 5800.75 599.638 4 -4 -3 1 5252.94 747.168 29 -4 -3 -1 2543.72 348.310 23 -4 -3 -1 2482.57 404.391 4 -4 -3 -1 2346.93 391.971 22 4 3 1 2215.94 369.077 6 4 3 1 1668.94 312.496 21 4 3 1 2164.75 364.222 20 -4 -3 -1 2214.41 369.220 10 -4 -3 -1 2209.49 375.702 5 4 3 1 1961.23 349.483 16 4 3 1 2462.77 349.427 3 4 3 1 2412.36 265.819 8 -4 -3 -3 3767.61 465.680 23 4 3 3 3362.94 465.527 6 -4 -3 -3 3391.20 527.202 22 4 3 3 3713.92 468.243 21 4 3 3 3518.49 480.115 20 -4 -3 -3 3749.65 501.681 5 -4 -3 -3 3161.91 452.003 10 4 3 3 3515.86 432.746 8 4 3 3 3166.92 466.091 3 -4 -3 -3 3566.59 479.640 4 -4 -3 -5 1338.29 306.021 23 -4 -3 -5 1270.97 330.143 22 -4 -3 -5 1579.25 287.495 11 4 3 5 977.310 270.953 21 4 3 5 1420.29 307.306 6 4 3 5 1401.89 307.807 20 -4 -3 -5 945.853 267.080 10 4 3 5 1064.66 262.921 9 -4 -3 -5 1128.26 302.966 5 4 3 5 1030.14 250.490 8 -4 -4 16 316.142 393.598 12 -4 -4 16-208.241 270.431 15 -4 -4 14-77.8797 297.452 12 4 4 -14-218.214 355.387 17 -4 -4 14-237.628 311.082 15 -4 -4 12 401.619 312.309 12 4 4 -12 175.303 242.843 20 4 4 -12 475.897 340.062 17 4 4 -12 270.408 207.730 16 -4 -4 12 353.115 286.028 15 -4 -4 10 371.953 275.909 12 4 4 -10-58.4626 199.527 20 -4 -4 10 249.339 263.012 10 4 4 -10 443.214 262.721 3 4 4 -10-130.234 254.328 17 4 4 -10 270.387 252.021 16 -4 -4 10 129.208 213.835 5 -4 -4 10-71.6764 227.438 15 -4 -4 10 66.5310 194.127 4 -4 -4 10 309.929 305.616 25 4 4 -8 206.710 266.572 6 4 4 -8 562.140 322.213 20 -4 -4 8 76.3451 197.398 10 4 4 -8-276.961 237.173 17 4 4 -8 318.887 242.401 3 -4 -4 8 53.6141 170.096 5 4 4 -8 278.166 287.659 16 -4 -4 8 233.361 234.375 15 -4 -4 8 199.653 189.005 4 -4 -4 8 130.236 218.392 25 4 4 -6 132.724 205.650 6 4 4 -6 47.1917 229.794 20 -4 -4 6 305.871 187.780 10 4 4 -6 269.968 171.498 17 4 4 -6 428.543 254.758 3 -4 -4 6 233.037 190.739 5 4 4 -6 391.934 267.609 16 -4 -4 6 76.0235 195.636 15 -4 -4 6 361.463 254.621 25 -4 -4 6 320.349 240.795 4 4 4 -4 896.064 361.248 6 4 4 -4 552.230 228.262 20 -4 -4 4 811.359 285.375 10 -4 -4 4 777.373 278.425 5 4 4 -4 546.565 291.322 3 4 4 -4 583.272 276.784 16 -4 -4 4 470.788 313.540 15 -4 -4 4 638.186 261.635 25 -4 -4 4 656.953 288.623 4 -4 -4 2 616.663 189.643 22 4 4 -2 1023.86 357.375 6 4 4 -2 529.166 242.743 21 4 4 -2 948.868 367.314 20 -4 -4 2 738.019 280.708 10 -4 -4 2 1116.25 327.336 5 4 4 -2 754.997 303.106 3 4 4 -2 517.194 265.081 16 -4 -4 2 548.283 271.615 15 -4 -4 2 690.341 240.356 25 -4 -4 2 601.998 272.218 4 -4 -4 0 434.828 206.294 22 4 4 0 617.390 280.872 6 4 4 0 803.315 274.452 21 4 4 0 461.159 240.642 20 -4 -4 0 757.713 295.750 10 -4 -4 0 568.125 242.965 5 4 4 0 149.543 182.811 3 4 4 0 1172.92 328.588 16 -4 -4 0 333.576 227.913 15 -4 -4 0 600.508 244.899 4 -4 -4 -2 579.736 275.703 22 4 4 2 510.625 229.015 6 4 4 2 488.353 244.360 21 4 4 2 756.420 295.163 20 -4 -4 -2 455.102 251.456 10 4 4 2 580.796 264.499 3 -4 -4 -2 694.011 270.629 5 4 4 2 705.596 315.312 16 -4 -4 -2 192.137 153.624 4 -4 -4 -4 1032.95 354.414 22 4 4 4 1331.25 350.926 21 4 4 4 882.108 288.764 6 4 4 4 1008.62 371.789 20 -4 -4 -4 1671.16 426.586 10 -4 -4 -4 986.502 361.792 5 -4 -4 -6 397.837 309.771 22 4 4 6 534.040 197.543 21 4 4 6 748.072 299.504 6 -4 -4 -6 494.187 244.006 10 -4 -4 -6 488.267 257.269 5 4 4 6 454.572 224.943 8 -4 -5 11 604.835 359.256 4 4 5 -9 159.019 224.632 20 -4 -5 9-246.618 374.205 10 4 5 -9-347.878 434.654 3 4 5 -9-430.944 331.958 16 -4 -5 9-388.890 297.773 4 4 5 -7 289.590 311.761 6 4 5 -7-342.849 403.873 20 -4 -5 7-271.926 255.632 10 4 5 -7-631.247 485.891 3 -4 -5 7-405.452 330.009 5 4 5 -7 183.534 356.834 16 -4 -5 7-549.174 474.345 15 -4 -5 7-175.815 271.829 4 -4 -5 7 38.0789 197.888 25 4 5 -5 382.996 349.555 6 4 5 -5 613.062 421.872 20 -4 -5 5 539.160 341.975 10 4 5 -5 744.890 485.375 3 -4 -5 5-224.769 226.772 5 4 5 -5-120.549 331.020 16 -4 -5 5 123.741 349.398 15 -4 -5 5 307.502 262.821 4 -4 -5 5 127.520 233.103 25 4 5 -3-564.983 500.256 6 4 5 -3-353.103 315.575 20 -4 -5 3-1.44954 329.189 10 4 5 -3-293.317 295.821 3 -4 -5 3 258.015 292.883 5 4 5 -3-394.203 362.257 16 -4 -5 3 522.197 435.557 15 -4 -5 3 442.792 249.174 4 4 5 -1 869.909 487.376 6 4 5 -1 2164.66 626.998 20 -4 -5 1 1149.75 457.007 10 4 5 -1 292.856 309.958 3 -4 -5 1 1000.40 491.869 5 4 5 -1 757.312 475.346 16 -4 -5 1 1033.92 446.924 15 -4 -5 1 507.627 263.488 4 -4 -5 -1 754.076 388.853 22 4 5 1 419.298 343.586 21 4 5 1 619.439 322.599 6 4 5 1-2.50609 268.408 20 -4 -5 -1 150.687 273.114 10 4 5 1 457.977 409.960 3 -4 -5 -1 376.286 337.612 5 4 5 1 599.721 348.163 16 -4 -5 -1-610.977 366.193 4 -4 -5 -3 2110.05 548.940 22 4 5 3 2185.48 546.824 21 4 5 3 2548.53 606.563 6 4 5 3 1234.32 465.104 20 -4 -5 -3 1738.36 502.720 10 -4 -5 -3 2247.68 593.657 5 4 5 5 598.385 327.812 6 -4 -5 -5-238.824 234.295 5 -5 -1 20 13.4627 263.622 12 -5 -1 20 100.573 186.358 24 -5 -1 18 1580.58 433.788 12 -5 -1 18 1696.89 449.199 18 5 1 -18 1468.88 394.836 14 -5 -1 18 701.663 238.725 24 -5 -1 16 366.910 275.093 12 -5 -1 16 190.520 181.397 18 -5 -1 16 26.3385 113.272 24 -5 -1 14 1467.97 364.426 12 -5 -1 14 986.952 307.794 18 -5 -1 12 43.4434 101.599 18 -5 -1 12 131.052 139.117 12 -5 -2 21-326.585 470.437 12 5 2 -21-710.394 357.031 14 -5 -2 19 166.912 257.601 12 5 2 -19 606.922 340.046 17 5 2 -19 436.492 327.131 14 -5 -2 17 2269.44 568.238 12 -5 -2 17 1279.98 403.998 18 5 2 -17 976.159 331.824 17 5 2 -17 1774.72 431.382 14 -5 -2 15 250.291 220.482 12 -5 -2 15 20.5641 216.718 18 5 2 -15 78.8574 163.590 17 5 2 -15 60.9585 189.715 14 5 2 -13 4946.12 495.665 20 -5 -2 13 5495.36 611.827 18 5 2 -13 5578.92 618.670 17 -5 -2 13 5819.16 740.250 12 -5 -2 11 599.493 243.899 12 -5 -2 11 457.013 160.878 4 -5 -2 11-72.4683 182.633 1 5 2 -11 124.843 118.905 20 -5 -2 11 245.125 114.472 10 -5 -2 11 365.115 141.534 18 5 2 -11 140.176 196.692 2 5 2 -11 252.905 127.526 17 -5 -2 11 252.079 121.193 15 5 2 -11 97.8987 116.877 3 -5 -2 9 2068.90 303.817 4 -5 -2 9 2292.07 476.709 1 -5 -2 9 2051.16 292.113 18 -5 -2 9 2015.32 290.339 10 5 2 -9 1927.17 307.393 17 5 2 -9 2534.61 546.096 2 -5 -2 9 2420.90 397.824 15 5 2 -9 1952.62 315.715 3 -5 -2 9 1520.67 328.807 12 -5 -2 7 26235.8 1030.47 10 -5 -2 7 26614.4 1379.96 19 -5 -2 7 27733.3 887.594 18 -5 -2 7 28379.3 1269.19 12 -5 -3 18 353.065 382.258 12 5 3 -18 33.5049 235.908 17 5 3 -18 83.0936 232.517 14 -5 -3 16-78.4686 199.358 12 5 3 -16 21.4794 230.654 17 -5 -3 16-171.690 199.497 15 5 3 -16-473.153 346.374 14 -5 -3 14 2538.38 582.005 12 5 3 -14 3219.20 558.284 17 -5 -3 14 2621.25 568.888 15 5 3 -14 2646.04 518.006 14 -5 -3 12-105.854 236.612 12 -5 -3 12 308.562 175.661 4 5 3 -12 91.4779 146.778 20 5 3 -12 698.606 312.316 17 5 3 -12 601.125 279.091 16 5 3 -12 259.374 191.588 3 -5 -3 12 477.372 226.050 15 5 3 -12 460.707 191.361 14 -5 -3 10 2121.61 469.285 12 -5 -3 10 2078.48 384.944 4 5 3 -10 1629.99 356.176 20 -5 -3 10 1949.34 357.712 10 5 3 -10 1280.57 295.037 17 5 3 -10 2079.52 418.694 16 5 3 -10 1211.16 292.295 3 -5 -3 10 1560.84 414.340 15 5 3 -10 2233.87 407.810 14 -5 -3 8 651.237 250.487 12 -5 -3 8 569.488 210.042 4 5 3 -8 528.659 224.466 20 -5 -3 8 510.266 201.655 10 5 3 -8 380.136 171.936 17 5 3 -8 651.418 211.838 16 -5 -3 8 898.942 322.505 15 5 3 -8 537.368 214.124 3 5 3 -8 629.792 237.681 14 -5 -3 6 1452.66 347.452 12 -5 -3 6 898.236 253.544 4 5 3 -6 1012.01 292.189 20 -5 -3 6 876.142 238.153 10 5 3 -6 1227.13 313.669 16 -5 -3 6 1388.54 344.637 15 5 3 -6 886.833 258.049 3 -5 -3 4 151.194 139.733 12 -5 -3 4-226.856 169.028 4 -5 -3 4 203.125 120.973 22 5 3 -4 131.988 100.758 21 5 3 -4-135.526 176.313 20 -5 -3 4-1.05010 145.787 10 5 3 -4-187.597 187.690 16 -5 -3 4 110.231 180.082 5 -5 -3 4 247.817 166.326 15 5 3 -4 60.0567 142.187 3 -5 -3 2 216.401 141.330 22 5 3 -2 55.8912 134.655 21 5 3 -2 233.515 146.794 6 5 3 -2 227.279 168.338 20 -5 -3 2 203.231 149.537 10 5 3 -2 125.546 123.051 16 -5 -3 2 384.308 199.551 5 -5 -3 2 38.2400 154.442 29 -5 -4 15 331.225 291.157 12 5 4 -15 831.778 342.091 17 -5 -4 15 1168.88 471.538 15 -5 -4 13 929.783 485.644 12 5 4 -13 628.104 267.517 20 5 4 -13 1588.89 478.858 17 -5 -4 13 1390.43 536.273 15 -5 -4 11 262.657 268.818 12 5 4 -11 993.430 364.168 20 -5 -4 11 691.785 242.896 10 5 4 -11 1065.14 395.504 17 5 4 -11 245.475 258.739 3 5 4 -11-115.721 274.392 16 -5 -4 11 53.6831 232.484 15 -5 -4 11 711.267 278.405 4 5 4 -9 120.643 207.847 20 -5 -4 9-296.159 259.875 10 5 4 -9 14.6682 176.167 17 5 4 -9 73.6135 195.225 3 5 4 -9 441.951 248.053 16 -5 -4 9-224.804 309.452 15 -5 -4 9 222.244 208.024 4 -5 -4 7 75.1433 175.427 4 5 4 -7 624.729 248.643 20 -5 -4 7 888.271 322.941 10 5 4 -7 731.325 290.293 16 5 4 -7 749.843 312.905 3 -5 -4 7 511.121 222.274 15 -5 -4 5 32.1050 140.851 4 5 4 -5-66.9334 187.774 6 5 4 -5 39.4538 154.024 20 -5 -4 5-101.739 144.564 10 5 4 -5-106.867 179.681 16 -5 -4 5 258.188 223.676 5 5 4 -5-132.078 266.400 3 -5 -4 5 176.377 203.153 15 -5 -4 3 0.26049 183.732 4 -5 -4 3 94.5208 165.819 22 5 4 -3-110.458 175.217 21 5 4 -3 195.440 189.031 6 5 4 -3-211.990 275.557 20 -5 -4 3-283.826 268.046 10 -5 -4 3-621.972 361.085 5 5 4 -3 34.5985 228.534 16 5 4 -3 319.242 229.586 3 -5 -4 3 407.742 280.846 15 -5 -4 1 188.893 201.331 22 5 4 -1-132.507 175.216 21 5 4 -1 268.207 240.055 6 5 4 -1 328.834 240.312 20 -5 -4 1-153.184 259.809 10 -5 -4 1 298.451 252.868 5 5 4 -1 256.198 181.351 16 5 4 -1 241.335 270.969 3 -5 -4 -1 127.274 180.600 22 5 4 1-144.103 173.437 21 5 4 1-167.921 200.663 6 5 4 1-211.058 220.557 20 -5 -4 -1-184.458 205.991 10 -5 -4 -1 172.364 213.520 5 5 5 -10-480.057 349.028 3 -5 -5 10 3.79231 281.712 4 5 5 -8 780.365 432.320 20 -5 -5 8-161.538 228.625 10 5 5 -8-110.431 272.880 3 5 5 -8-164.085 422.642 16 -5 -5 8 910.931 459.223 15 -5 -5 8 813.466 422.791 4 5 5 -6-332.461 335.861 20 -5 -5 6 337.060 255.922 10 5 5 -6 5.47659 254.212 3 5 5 -6-40.9832 294.230 16 -5 -5 6-71.3407 282.005 15 -5 -5 6 864.085 447.320 4 5 5 -4 128.780 304.126 20 -5 -5 4 445.034 321.921 10 5 5 -4-66.9555 345.990 3 5 5 -4 338.986 374.179 16 -5 -5 4-398.381 378.936 15 -5 -5 4 395.097 345.072 4 5 5 -2 1006.38 490.452 20 -5 -5 2 624.529 400.518 10 5 5 -2 119.521 243.626 16 -5 -5 2 421.994 272.246 5 6 3 -17 278.683 232.387 17 -6 -3 15 1896.79 490.905 12 6 3 -15 1756.65 414.245 17 -6 -3 13 3126.00 612.247 12 6 3 -13 3044.29 490.482 17 -6 -3 11 958.402 343.363 12 -6 -3 11 1453.55 322.215 4 6 3 -11 1321.64 320.897 20 6 3 -11 1886.45 369.962 3 6 4 -12 358.846 266.015 3 -6 -4 12 248.413 310.273 15 -6 -4 12 148.959 177.745 4 -6 -4 10 85.2846 184.219 4 6 4 -10 1707.73 494.174 20 6 4 -10 1063.78 459.261 3 -6 -4 10 627.425 490.353 15 -6 -4 8-770.356 441.116 15 0 0 0 0.00 0.00 0 TITL ETYSUC_320_1 in I2/a REM I2/a (#15 in standard setting) CELL 0.71073 16.428553 4.421444 19.019659 90.0000 114.3249 90.0000 ZERR 5.00 0.012398 0.000265 0.003579 0.0000 0.0503 0.0000 LATT 2 SYMM -x+1/2, y,-z SFAC C H N O UNIT 55.00 50.00 5.00 5.00 SIZE 0.03 0.15 0.31 TREF HKLF 4 END ; _shelx_hkl_checksum 64776 _hp_anvil_anvil_thickness 1.95 _hp_anvil_material diamond _hp_cell_type 'Diamond anvil cell' _hp_open_angle 30.00 _ins_header ; TITL ETYSUC_320_1 in I2/a REM I2/a (#15 in standard setting) CELL 0.71073 16.428553 4.421444 19.019659 90.0000 114.3249 90.0000 ZERR 5.00 0.012398 0.000265 0.003579 0.0000 0.0503 0.0000 LATT 2 SYMM -x+1/2, y,-z SFAC C H N O UNIT 55.00 50.00 5.00 5.00 SIZE 0.03 0.15 0.31 TREF HKLF 4 END ; _olex2_exptl_crystal_mounting_method ;Single crystal grown at ambient conditions was mounted in Merrill-Bassett diamond anvil cell and compressed to 3.29(2) GPa. Daphne oil 7575 was used as hydrostatic medium. ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.184 _oxdiff_exptl_absorpt_empirical_full_min 0.736 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N 0.3927(10) 0.4769(11) 0.1481(4) 0.0318(18) Uiso 1 1 d D . . . . C2 C 0.3342(11) 0.6335(12) 0.0879(4) 0.0347(18) Uiso 1 1 d D . . . . H2 H 0.2731 0.6012 0.0713 0.042 Uiso 1 1 calc R U . . . C3 C 0.3657(15) 0.8452(14) 0.0504(4) 0.030(2) Uiso 1 1 d . . . . . H3 H 0.3250 0.9565 0.0096 0.035 Uiso 1 1 calc R U . . . C4 C 0.4568(13) 0.8925(13) 0.0732(4) 0.0229(18) Uiso 1 1 d . . . . . C5 C 0.5153(12) 0.7247(12) 0.1358(3) 0.0289(17) Uiso 1 1 d . . . . . H5 H 0.5768 0.7483 0.1537 0.035 Uiso 1 1 calc R U . . . C6 C 0.4790(11) 0.5230(14) 0.1704(4) 0.029(2) Uiso 1 1 d D . . . . H6 H 0.5182 0.4121 0.2122 0.035 Uiso 1 1 calc R U . . . C1A C 0.2529(10) 0.0385(12) 0.1755(4) 0.0229(16) Uiso 1 1 d D . . . . O1A O 0.3345(8) 0.1029(9) 0.2123(3) 0.0407(14) Uiso 1 1 d D . . . . H1A H 0.3466 0.2529 0.1932 0.061 Uiso 1 1 calc R U . . . C2A C 0.2174(12) -0.1999(12) 0.2109(4) 0.0311(16) Uiso 1 1 d . . . . . H2AA H 0.2000 -0.3740 0.1769 0.037 Uiso 1 1 calc R U . . . H2AB H 0.1643 -0.1233 0.2151 0.037 Uiso 1 1 calc R U . . . O2A O 0.2040(8) 0.1621(8) 0.1137(2) 0.0348(13) Uiso 1 1 d D . . . . C7 C 0.4911(11) 1.0957(12) 0.0302(3) 0.0253(15) Uiso 1 1 d . . . . . H7A H 0.5460 1.1915 0.0653 0.030 Uiso 1 1 calc R U . . . H7B H 0.4477 1.2526 0.0046 0.030 Uiso 1 1 calc R U . . . loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _axis.id _axis.type _axis.equipment _axis.parity _axis.depends_on _axis.zero _axis.vector[1] _axis.vector[2] _axis.vector[3] source . source . . . 0.99999925 0.00000000 -0.00122697 omega rotation goniometer -1 . -0.27905000 0.00000000 0.00000000 1.00000000 kappa rotation goniometer -1 omega -0.01185000 -0.76836295 0.00000000 0.64001436 phi rotation goniometer -1 kappa . -0.00017069 0.00000000 0.99999999 theta rotation goniometer -1 . -0.37252000 0.00000000 0.00000000 1.00000000 matrixX general general . phi . 1.00000000 0.00000000 0.00000000 matrixY general general . phi . 0.00000000 1.00000000 0.00000000 matrixZ general general . phi . 0.00000000 0.00000000 1.00000000 dacX translation general . phi . 0.00000000 1.00000000 0.00000000 dacY translation general . phi . -1.00000000 0.00000000 0.00000000 dacZ translation general . phi . 0.00000000 0.00000000 1.00000000 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -5 1 26 0.1171 5 -1 -26 0.0331 3 -5 -16 0.0631 6 3 -25 0.0708 -3 6 17 0.1314 -23 -1 4 0.0120 23 1 -4 0.0210 -5 -5 18 0.1541 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 N1 C2 119.4(10) . . ? N1 C2 H2 120.2 . . ? N1 C2 C3 119.6(14) . . ? C3 C2 H2 120.2 . . ? C2 C3 H3 119.4 . . ? C4 C3 C2 121.2(10) . . ? C4 C3 H3 119.4 . . ? C3 C4 C5 117.3(11) . . ? C3 C4 C7 121.8(10) . . ? C5 C4 C7 120.8(17) . . ? C4 C5 H5 121.0 . . ? C6 C5 C4 118.0(16) . . ? C6 C5 H5 121.0 . . ? N1 C6 C5 124.4(10) . . ? N1 C6 H6 117.8 . . ? C5 C6 H6 117.8 . . ? O1A C1A C2A 115.6(8) . . ? O2A C1A O1A 123.3(9) . . ? O2A C1A C2A 121.1(12) . . ? C1A O1A H1A 109.5 . . ? C1A C2A C2A 113.9(16) . 7_545 ? C1A C2A H2AA 108.8 . . ? C1A C2A H2AB 108.8 . . ? C2A C2A H2AA 108.8 7_545 . ? C2A C2A H2AB 108.8 7_545 . ? H2AA C2A H2AB 107.7 . . ? C4 C7 C7 108.1(7) . 5_675 ? C4 C7 H7A 110.1 . . ? C4 C7 H7B 110.1 . . ? C7 C7 H7A 110.1 5_675 . ? C7 C7 H7B 110.1 5_675 . ? H7A C7 H7B 108.4 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C2 1.345(12) . ? N1 C6 1.318(17) . ? C2 H2 0.9300 . ? C2 C3 1.398(16) . ? C3 H3 0.9300 . ? C3 C4 1.39(3) . ? C4 C5 1.396(14) . ? C4 C7 1.474(16) . ? C5 H5 0.9300 . ? C5 C6 1.380(16) . ? C6 H6 0.9300 . ? C1A O1A 1.262(15) . ? C1A C2A 1.492(14) . ? C1A O2A 1.245(9) . ? O1A H1A 0.8200 . ? C2A C2A 1.497(19) 7_545 ? C2A H2AA 0.9700 . ? C2A H2AB 0.9700 . ? C7 C7 1.548(18) 5_675 ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C2 C3 C4 1.5(12) . . . . ? C2 N1 C6 C5 0.0(12) . . . . ? C2 C3 C4 C5 -1.3(14) . . . . ? C2 C3 C4 C7 174.7(5) . . . . ? C3 C4 C5 C6 0.5(12) . . . . ? C3 C4 C7 C7 -92.2(17) . . . 5_675 ? C4 C5 C6 N1 0.2(11) . . . . ? C5 C4 C7 C7 83.7(14) . . . 5_675 ? C6 N1 C2 C3 -0.8(11) . . . . ? O1A C1A C2A C2A 6.3(15) . . . 7_545 ? O2A C1A C2A C2A -173.9(11) . . . 7_545 ? C7 C4 C5 C6 -175.6(6) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -5.0343 1.1615 25.7862 -0.1160 0.6405 0.7592 5.0956 -0.8725 -25.9931 0.1093 -0.6047 -0.7889 2.9249 -4.8391 -16.4500 0.1786 -0.9710 -0.1590 5.5245 3.3006 -24.6615 0.0163 -0.0016 -1.0732 -2.8306 5.6114 16.7775 -0.1947 1.0845 0.1093 -22.9982 -0.5564 4.1054 -0.9878 -0.3056 0.0149 23.1802 0.6659 -3.6052 0.9955 0.3337 -0.0051 -4.5482 -4.6679 17.6042 0.0276 -0.3222 0.9463 loop_ _hkl_oxdiff_h _hkl_oxdiff_k _hkl_oxdiff_l _hkl_oxdiff_f2 _hkl_oxdiff_sig _hkl_oxdiff_ba 0 0 2 4433.84 188.360 9 0 0 -2 4161.96 180.614 23 0 0 2 3911.97 164.758 8 0 0 -4 30596.2 642.939 13 0 0 4 31887.7 667.944 8 0 0 -4 31120.4 720.438 14 0 0 4 30219.1 722.555 24 0 0 4 30753.8 786.002 12 0 0 4 30856.5 812.811 18 0 0 4 31599.3 708.267 9 0 0 4 30704.3 530.380 15 0 0 4 28500.3 938.940 29 0 0 -4 30654.3 703.974 23 0 0 -4 32066.4 1005.06 29 0 0 -6 2786.62 273.233 14 0 0 -6 2666.58 257.280 23 0 0 6 2697.12 244.996 8 0 0 6 2884.61 262.930 9 0 0 -6 2687.39 237.775 13 0 0 6 2601.03 262.763 24 0 0 6 2828.04 376.755 29 0 0 6 2478.36 280.782 18 0 0 6 3004.19 207.307 15 0 0 -6 2833.07 363.835 29 0 0 6 2988.03 297.044 12 0 0 -8 7311.99 496.681 23 0 0 8 7058.72 462.514 8 0 0 -8 7018.15 507.403 11 0 0 8 7553.68 703.035 29 0 0 8 6903.80 548.861 12 0 0 -8 7350.41 508.788 14 0 0 8 7704.49 586.283 18 0 0 -8 7942.16 725.035 29 0 0 8 7289.08 517.678 24 0 0 8 8187.83 524.864 9 0 0 -8 8490.00 406.679 22 0 0 8 8014.09 387.905 15 0 0 8 8210.38 380.714 21 0 0 -8 7751.99 467.292 13 0 0 10 31.2618 74.3679 8 0 0 -10 186.050 115.462 29 0 0 10 233.710 113.391 29 0 0 10 77.7926 97.7714 24 0 0 10 83.8841 88.8734 9 0 0 10 207.616 138.481 12 0 0 10 154.420 63.4870 15 0 0 10 117.026 64.8022 21 0 0 -10 94.9216 61.2037 22 0 0 10 -16.9815 122.289 18 0 0 -10 25.5274 86.7410 23 0 0 -10 -131.503 142.551 11 0 0 -10 103.403 96.2999 13 0 0 -10 98.6891 106.715 14 0 0 12 1967.78 389.943 18 0 0 12 2282.87 342.096 8 0 0 -12 2294.51 378.116 11 0 0 -12 2107.73 465.787 29 0 0 -12 2535.90 380.351 14 0 0 12 2181.77 471.807 29 0 0 12 2443.53 371.416 9 0 0 12 2447.43 396.775 24 0 0 -12 2252.48 356.430 23 0 0 -12 2077.46 323.713 13 0 0 12 1329.78 301.482 12 0 0 -14 763.499 263.511 7 0 0 14 1159.61 323.403 18 0 0 14 775.786 276.921 24 0 0 -14 1170.53 282.955 23 0 0 -14 1097.81 295.010 11 0 0 14 1051.10 289.493 9 0 0 -14 1004.67 256.256 14 0 0 14 -26.0146 102.826 8 0 0 14 412.903 220.054 12 0 0 -14 1030.60 254.132 17 0 0 -16 1500.00 367.837 14 0 0 16 1291.57 324.389 9 0 0 16 1655.59 455.419 18 0 0 16 1131.04 287.788 24 0 0 -16 896.723 312.517 7 0 0 -16 1247.11 326.369 11 0 0 -18 -1.54505 170.925 11 0 0 18 -261.178 224.344 18 0 0 18 -191.867 179.679 9 0 0 -18 126.057 234.523 7 0 0 18 -439.608 355.448 24 0 1 1 13221.1 443.441 21 0 -1 1 12543.7 697.370 1 0 1 -1 13696.0 499.004 3 0 -1 1 12689.8 457.554 10 0 -1 -1 14169.9 398.997 25 0 -1 1 14527.5 764.936 19 0 -1 -1 14479.1 402.351 11 0 -1 1 14151.7 478.069 25 0 1 -1 13642.6 561.308 29 0 -1 -1 14393.6 473.109 28 0 -1 1 13264.3 483.300 4 0 1 1 13910.5 508.021 3 0 -1 -1 13632.7 475.153 22 0 -1 -1 13831.9 424.152 23 0 -1 -1 13342.3 696.145 29 0 -1 -1 12523.6 703.990 1 0 -1 1 13866.6 797.815 2 0 1 -1 13132.9 491.397 20 0 -1 1 13642.8 511.625 5 0 1 1 13607.5 390.841 8 0 -1 -1 12798.5 488.879 5 0 -1 -1 13282.9 469.891 10 0 -1 -1 12844.6 483.908 4 0 1 1 13374.0 689.043 29 0 1 -1 15076.3 444.607 21 0 -1 -1 13765.1 787.980 2 0 1 1 14039.2 802.634 2 0 1 1 14809.7 389.294 9 0 1 1 12960.7 718.542 19 0 1 -1 13333.9 390.895 14 0 -1 -1 13562.3 746.296 19 0 1 1 13742.1 478.285 20 0 -1 1 14463.5 525.653 12 0 1 -1 14025.1 733.573 19 0 1 -1 13438.5 775.909 2 0 -1 1 14423.0 451.801 22 0 1 1 13146.8 450.193 27 0 1 -1 13499.0 408.413 27 0 1 -1 14384.7 756.295 1 0 -1 1 13838.6 409.786 28 0 1 3 9350.88 381.457 18 0 1 3 10300.9 413.759 9 0 -1 -3 9081.46 396.866 5 0 -1 3 8910.94 272.735 9 0 -1 -3 10340.3 443.073 4 0 1 -3 11593.0 361.370 27 0 -1 -3 9524.24 638.094 1 0 -1 -3 10324.9 418.900 7 0 -1 -3 10228.7 435.499 11 0 1 3 9837.73 354.520 24 0 -1 3 9894.20 613.833 1 0 -1 -3 9051.43 439.011 22 0 1 3 9129.43 414.158 21 0 -1 3 9904.83 676.305 2 0 -1 -3 9354.62 395.259 10 0 1 -3 10873.8 728.390 19 0 -1 -3 8532.76 593.733 2 0 -1 -3 9495.81 411.279 13 0 1 3 9634.28 687.020 2 0 1 -3 9393.86 616.695 1 0 1 3 10011.1 370.507 16 0 -1 3 9841.16 540.028 12 0 1 3 9395.29 437.763 3 0 1 -3 10311.6 475.236 14 0 -1 3 10308.4 421.487 4 0 -1 3 8374.35 489.705 25 0 1 3 9416.96 593.594 1 0 -1 3 8986.48 416.521 5 0 1 -3 9750.55 661.813 2 0 -1 3 11065.6 337.154 28 0 -1 -3 9237.75 323.735 15 0 1 -3 9933.88 428.046 3 0 -1 -3 9477.47 695.092 29 0 1 3 10073.1 425.231 8 0 1 3 9201.39 382.542 20 0 -1 3 10723.5 455.762 10 0 1 -3 9886.87 476.772 20 0 1 3 9627.27 682.754 29 0 -1 3 9744.43 381.776 24 0 -1 -3 10110.2 459.088 23 0 -1 -3 10032.0 686.620 19 0 1 -5 8577.38 509.099 14 0 -1 -5 7908.04 653.225 19 0 1 -5 8412.88 305.760 23 0 1 5 7732.26 537.035 1 0 -1 5 7784.54 559.388 12 0 -1 5 7475.01 552.956 1 0 -1 -5 7609.52 713.503 29 0 1 -5 8271.49 379.115 6 0 1 5 9204.22 460.908 3 0 -1 5 7877.74 434.786 24 0 -1 5 8365.15 613.388 2 0 -1 5 7729.28 390.405 5 0 -1 5 7189.71 482.183 15 0 1 5 7701.08 402.539 24 0 1 -5 8678.60 429.460 3 0 1 5 7392.70 438.254 18 0 1 5 8051.79 325.024 16 0 -1 -5 8734.02 429.351 4 0 1 5 8006.62 342.671 20 0 -1 -5 8227.04 627.908 1 0 1 -5 8624.87 670.839 2 0 1 -5 7539.09 510.232 20 0 1 5 7713.02 428.624 9 0 -1 5 7982.02 268.387 8 0 1 5 7777.36 350.159 6 0 -1 -5 7277.07 440.060 22 0 -1 -5 8014.50 346.108 14 0 -1 5 8609.10 381.456 9 0 -1 -5 7748.31 563.054 2 0 1 -5 7154.36 307.670 29 0 1 5 9596.07 742.147 2 0 1 5 7720.11 447.587 8 0 -1 5 7765.84 381.393 4 0 1 5 8439.36 736.575 29 0 -1 -5 7869.60 370.140 5 0 1 5 7867.59 429.305 21 0 -1 -5 7680.11 447.749 7 0 -1 5 7797.07 471.798 18 0 -1 -5 7854.47 480.317 23 0 -1 -5 8202.39 467.333 11 0 1 5 8666.46 350.043 12 0 1 -5 8225.63 585.507 1 0 -1 -5 7928.83 376.124 10 0 -1 -5 7409.08 435.595 13 0 1 -7 23558.9 802.045 29 0 1 -7 21391.4 897.272 1 0 1 -7 22839.1 935.793 14 0 1 7 21915.1 901.846 1 0 1 7 21553.1 895.580 18 0 -1 7 23083.3 1013.70 2 0 1 7 22917.3 598.088 6 0 -1 -7 22823.2 639.658 5 0 -1 7 21306.9 927.352 18 0 1 7 20990.9 795.356 24 0 1 7 22495.5 793.638 21 0 1 7 23947.2 596.158 20 0 1 7 22269.8 854.738 9 0 -1 7 22414.7 741.494 9 0 -1 -7 22833.0 655.743 10 0 -1 -7 22792.6 899.096 7 0 -1 7 20601.2 889.844 15 0 -1 -7 21751.2 828.690 22 0 -1 7 22358.2 653.755 5 0 -1 -7 21933.5 928.517 23 0 -1 -7 21170.2 879.095 11 0 -1 7 20164.1 1009.26 12 0 -1 7 21238.2 841.499 24 0 1 -7 24177.3 698.308 23 0 -1 -7 23753.2 999.260 2 0 1 7 21786.8 1335.28 29 0 -1 -7 24220.8 1425.70 29 0 -1 7 21005.5 601.989 8 0 -1 -7 19772.8 451.467 17 0 1 -7 21623.3 593.721 6 0 -1 -7 21282.0 726.916 14 0 1 7 22890.0 789.131 12 0 1 7 22031.5 864.673 8 0 -1 -7 21602.2 1160.14 19 0 -1 -7 21428.2 836.827 13 0 1 9 4635.75 400.440 21 0 1 -9 3931.42 386.771 11 0 -1 9 3991.06 360.899 9 0 1 9 4632.03 411.251 1 0 1 -9 4503.50 443.168 29 0 -1 -9 4155.17 450.159 11 0 -1 -9 4171.06 559.575 19 0 1 9 4152.75 459.101 18 0 -1 9 3891.13 487.103 12 0 -1 -9 4385.53 273.968 5 0 1 -9 3867.00 429.728 14 0 1 9 4073.99 631.072 29 0 -1 -9 4300.64 389.552 14 0 -1 -9 4491.66 281.734 17 0 -1 -9 4806.12 442.486 13 0 -1 -9 5032.94 444.550 2 0 -1 9 3977.20 419.369 15 0 1 9 4297.42 426.899 8 0 -1 9 2419.57 254.388 8 0 -1 -9 4182.53 446.192 7 0 -1 9 4004.03 460.051 18 0 1 9 5034.27 447.105 24 0 -1 -9 4577.40 420.684 22 0 1 9 4414.02 264.123 6 0 1 9 4419.25 429.602 9 0 -1 9 4034.72 420.985 24 0 1 -9 4742.58 382.565 23 0 1 9 4281.57 428.256 12 0 -1 -9 4398.02 685.611 29 0 -1 -9 4278.61 465.579 23 0 -1 -9 4434.96 296.440 10 0 1 -11 414.054 174.978 14 0 -1 11 342.658 214.303 18 0 1 11 342.896 167.705 9 0 1 -11 490.010 165.991 11 0 -1 11 249.548 145.645 24 0 1 -11 499.723 159.461 23 0 -1 -11 244.700 163.619 11 0 -1 -11 455.599 185.050 22 0 -1 -11 734.484 280.473 19 0 1 11 445.094 165.312 24 0 -1 11 624.675 203.317 15 0 1 11 545.500 176.239 18 0 -1 -11 219.904 176.216 7 0 -1 -11 300.275 137.683 13 0 1 11 532.739 177.716 8 0 -1 11 477.829 156.384 9 0 -1 -11 577.691 179.873 14 0 1 11 452.974 202.521 12 0 1 11 513.716 170.605 21 0 -1 11 314.190 203.701 12 0 -1 -11 544.967 204.403 23 0 1 13 4508.83 538.919 9 0 -1 13 3921.02 507.871 24 0 -1 -13 4463.86 575.642 23 0 1 13 5132.95 663.103 18 0 -1 -13 4058.80 482.648 14 0 1 13 4394.87 540.693 24 0 -1 -13 4139.17 558.115 11 0 -1 -13 4633.28 498.395 22 0 -1 -13 4844.22 615.871 7 0 1 -13 3987.99 527.669 14 0 1 13 4650.80 555.744 8 0 -1 13 3200.74 409.988 9 0 -1 13 3294.33 558.716 12 0 1 13 4605.52 465.667 21 0 -1 13 1521.89 358.303 18 0 1 -13 3699.73 461.740 11 0 -1 -13 4637.84 533.885 13 0 -1 -15 -62.1078 181.786 23 0 1 15 311.689 224.531 24 0 1 -15 -19.1690 124.458 17 0 1 -15 38.3675 163.142 7 0 -1 -15 132.942 142.547 11 0 1 -15 2.05125 168.871 14 0 1 15 349.339 254.093 9 0 -1 -15 120.620 160.755 13 0 -1 15 154.426 176.806 9 0 1 15 -187.187 166.242 8 0 1 -15 60.8841 125.431 11 0 -1 -15 -71.4040 191.785 7 0 -1 15 -191.748 197.888 12 0 -1 15 293.038 221.665 24 0 -1 -15 102.979 119.720 14 0 1 15 -124.515 172.756 18 0 -1 -17 500.120 269.490 7 0 -1 -17 752.793 359.277 11 0 1 17 -123.315 176.329 8 0 1 17 -109.875 218.357 24 0 1 17 -600.934 373.514 18 0 1 17 297.871 228.503 9 0 -1 -17 -88.6058 242.420 23 0 -1 -17 549.389 250.228 13 0 1 19 169.661 212.185 24 0 -1 -19 -62.4659 199.736 7 0 1 19 508.176 401.332 18 0 1 19 -14.8133 225.662 9 0 -1 -19 90.4703 245.306 11 0 -2 0 1664.11 197.462 23 0 -2 0 1619.75 225.255 28 0 -2 0 1564.18 214.633 25 0 2 0 1489.19 388.117 1 0 -2 0 1790.20 366.917 29 0 -2 0 1627.83 398.921 2 0 2 0 1770.86 238.560 27 0 -2 0 1463.02 239.111 4 0 2 0 1807.36 389.100 19 0 -2 0 1703.68 395.256 19 0 -2 0 1459.48 236.538 10 0 -2 0 1614.81 258.996 5 0 -2 0 1487.05 255.937 15 0 2 0 1824.37 192.590 8 0 2 0 1673.99 321.876 29 0 2 0 1624.27 243.517 20 0 2 0 1693.99 263.587 3 0 -2 0 1790.57 254.205 22 0 2 0 1825.51 434.118 2 0 2 0 1575.81 223.238 21 0 -2 0 1685.35 401.441 1 0 -2 -2 2183.05 407.347 29 0 -2 -2 1916.82 416.290 19 0 -2 -2 1701.53 258.443 10 0 2 -2 1848.20 383.532 1 0 2 2 1333.59 339.374 19 0 -2 2 1442.79 257.764 5 0 2 -2 1125.68 230.148 20 0 2 -2 182.090 80.9070 21 0 -2 2 1656.94 131.631 24 0 2 -2 1475.97 237.718 3 0 2 2 1447.03 133.593 18 0 -2 2 1370.34 251.792 15 0 -2 2 793.128 298.043 19 0 -2 2 1568.68 247.304 4 0 -2 -2 1354.10 172.579 25 0 -2 2 1553.99 206.397 28 0 -2 2 1276.15 357.442 2 0 2 2 1588.23 198.338 8 0 2 2 1469.38 251.702 20 0 -2 -2 1300.31 225.209 5 0 -2 2 399.145 119.094 22 0 -2 -2 1680.18 268.087 4 0 2 2 1704.56 284.320 3 0 -2 2 1443.07 237.895 10 0 2 -2 1781.02 314.070 29 0 2 2 1714.39 394.065 1 0 2 -2 1578.24 390.075 2 0 -2 2 1272.73 340.610 1 0 2 -2 1385.24 196.298 27 0 -2 -2 1247.17 206.926 15 0 -2 -2 1310.02 347.689 1 0 2 2 1742.06 384.335 29 0 -2 -2 1652.37 215.380 23 0 -2 -2 1517.65 398.576 2 0 -2 2 1385.36 230.473 25 0 2 -2 1388.86 373.956 19 0 -2 -2 1606.57 253.739 22 0 2 2 1669.12 431.956 2 0 2 2 1309.34 206.952 21 0 2 2 1046.65 187.511 16 0 -2 -4 -52.7168 66.4168 15 0 -2 -4 161.654 107.233 10 0 2 4 23.6722 48.5628 18 0 -2 4 74.7101 103.893 1 0 -2 -4 4.34404 123.358 29 0 -2 4 58.8755 78.5470 10 0 -2 -4 83.9626 124.762 19 0 2 -4 -154.326 134.427 20 0 -2 -4 38.6186 53.7218 7 0 2 -4 -17.9014 188.903 1 0 2 -4 61.3687 82.9248 3 0 2 -4 -96.5084 105.742 29 0 2 -4 -45.2306 57.8380 27 0 -2 4 92.8000 103.795 5 0 2 4 -35.9618 152.888 29 0 -2 4 59.5547 59.7793 28 0 -2 4 -9.13875 81.5155 12 0 -2 4 -35.1699 30.9658 9 0 -2 -4 30.4108 165.746 1 0 -2 -4 -10.3269 70.5514 13 0 -2 4 -43.4485 161.581 2 0 2 4 11.3615 92.6131 6 0 2 4 -5.42202 208.882 2 0 -2 -4 -92.2223 111.628 22 0 -2 4 -72.5151 95.1405 25 0 -2 4 26.1474 99.2776 15 0 2 4 -30.9038 75.9652 9 0 2 4 1.42432 135.182 1 0 2 4 17.3268 87.8370 21 0 2 4 -28.6614 90.6595 20 0 2 4 82.7302 73.5025 8 0 -2 -4 -14.0203 97.8375 23 0 -2 4 65.1029 72.7671 24 0 2 -4 -175.314 244.801 2 0 2 4 -25.2539 30.6731 17 0 -2 -4 -79.0691 80.7546 5 0 -2 -4 -107.377 113.339 2 0 -2 -4 -44.7044 61.8733 11 0 -2 -4 60.5703 78.2898 4 0 2 -4 -358.358 234.088 19 0 2 4 1.83134 70.1827 16 0 2 4 38.6358 105.985 3 0 -2 -4 10.7453 44.2019 25 0 2 -4 -19.0339 87.7661 6 0 -2 4 50.0651 73.2527 4 0 -2 -6 10019.5 673.717 23 0 -2 6 8279.45 583.123 5 0 -2 -6 9947.01 621.643 11 0 2 6 9404.34 605.272 8 0 -2 6 10285.0 427.340 28 0 2 -6 6453.69 486.563 6 0 2 6 9053.81 499.387 24 0 -2 6 8196.44 701.136 12 0 2 -6 10798.6 459.328 27 0 -2 -6 9156.31 599.682 13 0 2 -6 6735.62 743.279 1 0 -2 6 8635.83 711.366 15 0 -2 -6 9533.50 1030.60 29 0 2 6 11224.7 792.752 3 0 -2 -6 8120.20 443.196 15 0 2 6 9551.40 623.071 21 0 -2 6 9555.59 623.905 4 0 -2 -6 9534.01 583.121 7 0 2 6 10243.1 897.713 1 0 2 -6 12301.1 1218.87 2 0 -2 -6 9299.38 968.712 19 0 -2 -6 9639.29 603.899 5 0 -2 6 9797.11 952.518 2 0 -2 6 9046.19 372.884 9 0 2 -6 8922.16 596.687 14 0 2 -6 6322.45 649.063 20 0 2 -6 10895.2 733.642 3 0 -2 -6 8799.34 646.244 22 0 2 6 9438.86 531.467 16 0 -2 -6 10029.6 631.684 10 0 2 6 10820.3 1213.74 2 0 -2 -6 9415.52 914.065 2 0 2 6 9440.86 571.183 18 0 2 6 10933.8 657.875 20 0 2 6 10466.0 612.503 9 0 -2 -6 9141.58 960.085 1 0 2 -6 11720.7 1074.96 19 0 -2 6 9530.10 530.062 24 0 2 6 9378.46 559.558 6 0 -2 -6 9591.40 675.562 4 0 -2 6 9601.86 937.235 1 0 2 6 8521.19 927.973 29 0 2 8 3749.74 358.365 6 0 -2 -8 3710.73 458.409 23 0 -2 8 6849.66 757.156 12 0 2 8 3446.65 520.562 1 0 -2 -8 3927.28 407.313 10 0 2 8 4040.96 381.660 24 0 2 -8 3356.14 343.337 6 0 2 -8 3645.36 569.271 19 0 -2 8 1225.23 350.737 2 0 -2 8 1606.21 269.469 5 0 -2 -8 3844.05 387.694 5 0 2 8 3905.58 402.824 9 0 2 8 4171.95 429.690 21 0 -2 -8 3862.05 662.965 19 0 -2 -8 3998.05 450.324 11 0 -2 -8 3906.76 424.731 7 0 -2 8 3878.93 398.114 24 0 -2 -8 3792.79 427.642 13 0 -2 -8 4274.79 487.396 22 0 2 -8 3935.47 575.482 1 0 2 8 3733.92 435.322 18 0 2 8 4549.67 446.968 20 0 -2 8 3125.28 455.317 15 0 2 8 4121.54 454.365 8 0 -2 -8 3792.37 577.378 2 0 2 -8 5695.71 556.032 14 0 2 8 3833.83 352.866 16 0 -2 10 376.600 243.215 12 0 2 -10 880.050 206.273 16 0 2 10 1244.08 257.181 21 0 -2 -10 1296.39 295.238 22 0 -2 -10 992.339 251.149 7 0 -2 -10 1083.06 280.569 13 0 2 10 1048.74 242.477 24 0 2 10 719.336 212.139 8 0 2 -10 1131.98 263.885 14 0 2 10 774.755 225.687 9 0 -2 -10 1013.09 265.874 23 0 -2 10 547.824 193.022 24 0 -2 10 477.409 215.792 15 0 2 10 1221.28 307.471 18 0 -2 -10 1579.36 318.838 11 0 -2 -12 5382.77 597.927 13 0 2 -12 4171.33 547.665 14 0 -2 -12 5455.05 665.421 23 0 2 12 5278.23 580.110 21 0 -2 -12 5006.41 602.592 22 0 2 12 5390.74 600.811 9 0 -2 12 603.465 286.470 12 0 2 12 4669.56 525.250 24 0 -2 -12 5689.50 657.078 11 0 2 12 5175.69 629.784 18 0 -2 -12 5116.79 610.482 7 0 2 12 5226.45 610.058 8 0 2 14 571.591 259.834 9 0 -2 -14 665.836 266.406 22 0 2 14 568.627 230.301 21 0 -2 -14 894.771 324.624 7 0 -2 -14 814.584 329.216 11 0 -2 -14 708.958 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477.360 22 -2 -2 4 8431.72 897.329 2 2 2 -4 8584.98 433.047 21 2 2 -4 8695.93 572.537 3 -2 -2 4 8514.17 555.496 10 2 2 -4 8592.80 593.449 20 -2 -2 4 9463.50 619.493 5 -2 -2 4 8402.58 796.769 19 2 2 -4 9067.96 545.487 17 2 2 -4 8250.71 549.757 16 -2 -2 4 8413.82 627.051 15 2 2 -4 7722.45 823.451 1 2 2 -4 8673.59 230.667 8 -2 -2 4 8067.21 541.526 4 2 2 -4 9448.83 506.960 14 -2 -2 4 9283.98 588.109 29 2 2 -4 9396.50 927.397 2 -2 -2 4 8586.01 594.037 25 -2 -2 4 8528.43 605.224 12 -2 -2 2 11740.4 414.986 23 2 2 -2 11134.6 631.615 6 -2 -2 2 11497.8 955.403 1 -2 -2 2 11472.3 567.401 22 -2 -2 2 12536.3 1077.30 2 2 2 -2 11402.1 536.770 21 2 2 -2 11545.9 662.156 3 2 2 -2 11790.1 1042.20 2 -2 -2 2 11921.0 613.729 12 -2 -2 2 11046.4 627.500 10 2 2 -2 11352.0 658.434 20 -2 -2 2 11497.7 669.667 5 -2 -2 2 11631.1 963.376 19 2 2 -2 12058.4 568.551 17 2 2 -2 11094.0 624.055 16 2 2 -2 12361.6 1016.68 1 -2 -2 2 11253.9 681.534 15 -2 -2 2 11583.1 644.359 4 2 2 -2 12262.7 478.253 14 -2 -2 2 12645.5 396.567 13 -2 -2 2 12562.4 795.154 29 2 2 -2 12476.4 840.904 29 -2 -2 2 10511.8 598.667 25 -2 -2 0 1402.56 170.499 12 -2 -2 0 1426.51 183.725 23 -2 -2 0 1574.70 158.380 11 2 2 0 1562.51 244.385 6 -2 -2 0 1160.99 218.640 22 2 2 0 1401.57 203.424 21 2 2 0 1382.98 227.306 20 -2 -2 0 1160.52 313.471 19 2 2 0 1898.86 426.611 2 -2 -2 0 1428.04 231.671 10 2 2 0 1530.68 143.155 9 -2 -2 0 1536.27 251.122 5 2 2 0 1389.34 168.011 17 2 2 0 1849.45 364.803 29 -2 -2 0 1408.48 230.049 4 -2 -2 0 1638.92 367.508 1 2 2 0 1651.97 237.481 16 -2 -2 0 1024.95 294.495 2 -2 -2 0 1716.79 255.906 15 2 2 0 1088.04 201.534 3 2 2 0 1708.64 376.238 1 2 2 0 1679.64 128.853 14 -2 -2 0 1517.93 110.284 7 -2 -2 0 1592.80 179.141 13 -2 -2 0 2210.10 381.501 29 -2 -2 0 863.185 147.917 25 2 2 2 7111.53 494.461 6 -2 -2 -2 7537.42 491.488 23 -2 -2 -2 7987.38 812.716 1 -2 -2 -2 8167.39 431.768 11 -2 -2 -2 7820.21 538.064 22 -2 -2 -2 7980.07 847.588 2 2 2 2 8140.67 566.182 3 2 2 2 7531.60 509.678 21 -2 -2 -2 7540.85 524.472 10 2 2 2 7883.63 538.242 20 -2 -2 -2 7707.10 267.482 12 -2 -2 -2 7708.71 842.771 19 2 2 2 7778.20 408.835 9 2 2 2 7984.82 515.241 16 2 2 2 7020.11 758.976 1 -2 -2 -2 8118.87 526.191 15 2 2 2 7991.75 487.817 8 -2 -2 -2 7457.58 528.236 4 2 2 2 7702.86 868.492 2 -2 -2 -2 7613.55 449.042 13 -2 -2 -2 7632.27 799.219 29 2 2 2 8081.92 851.484 29 -2 -2 -2 7396.33 529.459 5 2 2 2 7617.79 281.475 24 -2 -2 -4 1878.34 275.113 4 -2 -2 -4 2271.42 304.292 23 -2 -2 -4 2228.46 268.021 11 -2 -2 -4 2130.45 314.604 22 2 2 4 1843.86 255.361 6 2 2 4 2161.75 304.566 3 2 2 4 2161.17 298.341 21 -2 -2 -4 1862.19 273.392 10 2 2 4 1904.45 267.031 20 -2 -2 -4 2015.19 423.937 1 2 2 4 2372.80 455.999 1 2 2 4 2515.57 496.621 2 -2 -2 -4 1480.66 399.379 19 2 2 4 2134.54 259.670 9 -2 -2 -4 1713.82 258.448 5 2 2 4 2052.70 275.378 16 2 2 4 2216.65 285.902 8 -2 -2 -4 2019.88 430.091 2 -2 -2 -4 2179.81 276.712 13 -2 -2 -4 2240.21 480.067 29 2 2 4 2717.95 554.651 29 2 2 4 2057.57 203.666 24 2 2 6 2137.41 288.274 6 -2 -2 -6 2205.08 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62.6790 83.5628 7 4 1 -11 106.453 73.8803 13 -4 -1 9 121.346 66.3889 19 -4 -1 9 208.119 127.468 18 -4 -1 9 156.316 70.1763 10 4 1 -9 58.7363 74.8933 17 4 1 -9 110.579 52.9753 13 -4 -1 9 153.934 105.078 12 4 1 -7 25358.9 875.380 17 -4 -1 7 23937.5 1050.26 12 -4 -2 20 287.975 233.750 24 -4 -2 20 -143.482 431.027 12 -4 -2 20 203.998 284.048 18 4 2 -20 868.855 362.327 17 4 2 -20 58.3944 256.534 14 -4 -2 18 1165.27 391.954 24 -4 -2 18 603.473 410.386 12 -4 -2 18 813.350 350.491 18 4 2 -18 671.048 316.122 17 4 2 -18 575.911 328.920 14 -4 -2 16 39.7997 172.621 24 -4 -2 16 196.838 365.525 12 -4 -2 16 50.2695 173.035 18 4 2 -16 161.312 214.997 17 -4 -2 16 198.471 159.210 15 4 2 -16 120.272 209.937 14 -4 -2 14 12274.8 955.093 18 4 2 -14 13568.3 1011.33 17 -4 -2 14 13897.7 1064.45 15 4 2 -14 13015.4 1003.20 14 -4 -2 14 11327.8 1108.55 12 -4 -2 14 12355.1 926.771 24 4 2 -12 7793.27 629.367 20 -4 -2 12 8006.24 710.801 18 4 2 -12 8962.32 763.202 17 4 2 -12 8391.83 655.318 16 -4 -2 12 8720.08 806.441 15 4 2 -12 8531.28 748.583 14 -4 -2 12 8528.85 871.630 12 -4 -2 12 8357.19 679.678 24 -4 -2 10 2219.33 421.911 12 -4 -2 10 1903.66 290.846 4 4 2 -10 1765.90 296.271 20 -4 -2 10 1949.19 277.477 10 -4 -2 10 1747.83 294.853 18 4 2 -10 1970.36 477.689 2 4 2 -10 2255.98 366.088 17 4 2 -10 1904.50 311.118 16 -4 -2 10 1924.25 420.097 1 -4 -2 10 2033.38 388.301 15 4 2 -10 1544.02 259.975 3 4 2 -8 26508.7 1633.68 2 4 2 -8 26523.8 1061.65 3 -4 -2 8 23892.9 956.837 10 4 2 -8 24434.6 1056.58 20 -4 -2 8 24901.6 1508.89 1 -4 -2 8 24882.0 1272.47 19 -4 -2 8 25822.7 936.093 18 4 2 -8 24660.4 1061.74 17 4 2 -8 25285.3 1083.98 16 -4 -2 8 25025.1 1196.80 15 -4 -2 8 25348.9 1006.93 4 -4 -2 8 24686.4 1232.57 12 -4 -2 6 2899.57 503.047 1 4 2 -6 2576.76 338.785 3 -4 -2 6 2699.07 320.417 10 -4 -2 6 2671.99 448.260 19 -4 -2 6 2477.39 242.883 18 4 2 -6 2152.83 288.093 17 4 2 -6 3043.89 561.937 2 4 2 -6 2570.83 329.674 16 -4 -2 6 2585.46 375.845 15 -4 -2 6 2529.77 320.455 4 -4 -2 6 2416.79 282.110 29 -4 -2 6 2546.11 354.545 12 4 2 -4 1723.85 284.925 6 -4 -2 4 1846.66 428.060 1 -4 -2 4 1848.02 383.663 19 -4 -2 4 1652.21 256.439 10 4 2 -4 2489.10 545.946 2 4 2 -4 1838.87 278.677 16 -4 -2 4 1605.65 305.485 5 -4 -2 4 2142.54 322.870 15 -4 -2 4 1947.99 288.516 4 4 2 -4 2037.05 296.945 3 -4 -2 4 1973.26 474.884 2 -4 -2 4 1639.61 290.671 29 4 2 -4 1894.51 285.502 26 -4 -2 4 1546.66 254.410 12 -4 -2 2 -59.6698 111.456 4 4 2 -2 -53.7547 106.747 6 -4 -2 2 206.250 118.821 10 -4 -2 2 -84.6584 221.309 1 4 2 -2 3.87726 127.021 2 -4 -2 2 63.8139 91.5499 5 4 2 -2 111.645 111.775 16 4 2 -2 287.228 219.695 1 -4 -2 2 122.864 130.547 15 4 2 -2 69.7921 69.0415 3 -4 -2 2 -31.3285 117.697 2 -4 -2 2 -32.7340 115.181 29 4 2 -2 3.76665 71.1871 26 -4 -2 2 -35.9978 81.1590 12 4 2 0 197.127 147.918 6 -4 -2 0 211.875 140.043 10 -4 -2 0 66.8166 95.1642 5 -4 -2 0 247.255 243.371 2 4 2 0 185.009 164.531 1 4 3 -19 128.179 248.140 17 4 3 -19 371.756 313.249 14 -4 -3 17 -393.651 351.998 12 4 3 -17 321.894 290.245 17 -4 -3 17 46.4724 230.924 15 4 3 -17 -220.846 331.361 14 -4 -3 15 297.643 245.953 12 4 3 -15 -320.070 273.188 17 -4 -3 15 -118.098 204.641 15 4 3 -15 295.246 242.727 14 -4 -3 13 371.054 265.071 12 4 3 -13 495.651 265.453 20 4 3 -13 544.681 296.431 17 4 3 -13 409.318 187.215 16 -4 -3 13 248.371 253.391 15 4 3 -13 828.117 292.057 14 -4 -3 11 955.605 268.377 4 -4 -3 11 356.763 248.283 12 4 3 -11 873.768 277.113 20 -4 -3 11 1076.56 285.466 10 4 3 -11 878.548 290.678 17 4 3 -11 860.583 289.157 16 4 3 -11 1195.25 278.283 3 -4 -3 11 1133.74 348.993 15 4 3 -11 1196.23 325.581 14 -4 -3 9 2662.77 491.573 12 -4 -3 9 2519.05 411.623 4 4 3 -9 2719.58 443.634 20 -4 -3 9 2618.09 417.528 10 4 3 -9 2700.55 445.399 17 4 3 -9 3099.72 485.587 16 -4 -3 9 2929.75 473.832 5 4 3 -9 2397.75 401.354 3 -4 -3 9 2252.60 456.880 15 4 3 -9 3121.33 432.453 14 -4 -3 9 1399.37 339.768 25 -4 -3 7 361.894 170.200 12 -4 -3 7 -74.9572 123.487 4 4 3 -7 7.24938 186.122 6 4 3 -7 -33.9191 142.071 20 -4 -3 7 29.9989 139.549 10 4 3 -7 26.9981 114.556 17 -4 -3 7 -22.2005 131.252 5 4 3 -7 -124.727 131.551 16 4 3 -7 328.106 211.586 3 -4 -3 7 -18.9709 154.681 15 4 3 -7 149.114 172.901 14 -4 -3 7 -46.1311 167.294 25 -4 -3 5 564.233 221.549 12 -4 -3 5 364.293 196.408 4 -4 -3 5 581.257 176.199 22 4 3 -5 350.271 191.619 6 4 3 -5 475.631 154.257 21 4 3 -5 284.293 148.428 20 -4 -3 5 379.437 188.680 10 4 3 -5 548.819 168.642 17 -4 -3 5 284.515 193.420 5 4 3 -5 309.795 186.776 16 -4 -3 5 263.527 170.456 15 4 3 -5 408.952 190.492 3 -4 -3 3 2464.52 396.321 4 -4 -3 3 2078.29 311.096 22 4 3 -3 2307.73 322.216 21 4 3 -3 1983.25 352.600 6 4 3 -3 2258.00 389.795 20 -4 -3 3 2183.32 355.008 10 -4 -3 3 2238.69 394.950 5 4 3 -3 1756.26 330.836 16 -4 -3 3 2315.35 388.115 15 4 3 -3 2090.20 378.032 3 4 3 -1 6778.70 637.900 6 -4 -3 1 5450.93 541.553 22 4 3 -1 5523.01 518.304 21 4 3 -1 6201.93 638.605 3 -4 -3 1 4572.02 523.633 10 4 3 -1 5330.27 563.751 20 -4 -3 1 5538.98 591.478 5 4 3 -1 5259.37 549.294 16 -4 -3 1 5844.48 607.147 15 -4 -3 1 5800.75 599.638 4 -4 -3 1 5252.94 747.168 29 -4 -3 -1 2543.72 348.310 23 -4 -3 -1 2482.57 404.391 4 -4 -3 -1 2346.93 391.971 22 4 3 1 2215.94 369.077 6 4 3 1 1668.94 312.496 21 4 3 1 2164.75 364.222 20 -4 -3 -1 2214.41 369.220 10 -4 -3 -1 2209.49 375.702 5 4 3 1 1961.23 349.483 16 4 3 1 2462.77 349.427 3 4 3 1 2412.36 265.819 8 -4 -3 -3 3767.61 465.680 23 4 3 3 3362.94 465.527 6 -4 -3 -3 3391.20 527.202 22 4 3 3 3713.92 468.243 21 4 3 3 3518.49 480.115 20 -4 -3 -3 3749.65 501.681 5 -4 -3 -3 3161.91 452.003 10 4 3 3 3515.86 432.746 8 4 3 3 3166.92 466.091 3 -4 -3 -3 3566.59 479.640 4 -4 -3 -5 1338.29 306.021 23 -4 -3 -5 1270.97 330.143 22 -4 -3 -5 1579.25 287.495 11 4 3 5 977.310 270.953 21 4 3 5 1420.29 307.306 6 4 3 5 1401.89 307.807 20 -4 -3 -5 945.853 267.080 10 4 3 5 1064.66 262.921 9 -4 -3 -5 1128.26 302.966 5 4 3 5 1030.14 250.490 8 -4 -4 16 316.142 393.598 12 -4 -4 16 -208.241 270.431 15 -4 -4 14 -77.8797 297.452 12 4 4 -14 -218.214 355.387 17 -4 -4 14 -237.628 311.082 15 -4 -4 12 401.619 312.309 12 4 4 -12 175.303 242.843 20 4 4 -12 475.897 340.062 17 4 4 -12 270.408 207.730 16 -4 -4 12 353.115 286.028 15 -4 -4 10 371.953 275.909 12 4 4 -10 -58.4626 199.527 20 -4 -4 10 249.339 263.012 10 4 4 -10 443.214 262.721 3 4 4 -10 -130.234 254.328 17 4 4 -10 270.387 252.021 16 -4 -4 10 129.208 213.835 5 -4 -4 10 -71.6764 227.438 15 -4 -4 10 66.5310 194.127 4 -4 -4 10 309.929 305.616 25 4 4 -8 206.710 266.572 6 4 4 -8 562.140 322.213 20 -4 -4 8 76.3451 197.398 10 4 4 -8 -276.961 237.173 17 4 4 -8 318.887 242.401 3 -4 -4 8 53.6141 170.096 5 4 4 -8 278.166 287.659 16 -4 -4 8 233.361 234.375 15 -4 -4 8 199.653 189.005 4 -4 -4 8 130.236 218.392 25 4 4 -6 132.724 205.650 6 4 4 -6 47.1917 229.794 20 -4 -4 6 305.871 187.780 10 4 4 -6 269.968 171.498 17 4 4 -6 428.543 254.758 3 -4 -4 6 233.037 190.739 5 4 4 -6 391.934 267.609 16 -4 -4 6 76.0235 195.636 15 -4 -4 6 361.463 254.621 25 -4 -4 6 320.349 240.795 4 4 4 -4 896.064 361.248 6 4 4 -4 552.230 228.262 20 -4 -4 4 811.359 285.375 10 -4 -4 4 777.373 278.425 5 4 4 -4 546.565 291.322 3 4 4 -4 583.272 276.784 16 -4 -4 4 470.788 313.540 15 -4 -4 4 638.186 261.635 25 -4 -4 4 656.953 288.623 4 -4 -4 2 616.663 189.643 22 4 4 -2 1023.86 357.375 6 4 4 -2 529.166 242.743 21 4 4 -2 948.868 367.314 20 -4 -4 2 738.019 280.708 10 -4 -4 2 1116.25 327.336 5 4 4 -2 754.997 303.106 3 4 4 -2 517.194 265.081 16 -4 -4 2 548.283 271.615 15 -4 -4 2 690.341 240.356 25 -4 -4 2 601.998 272.218 4 -4 -4 0 434.828 206.294 22 4 4 0 617.390 280.872 6 4 4 0 803.315 274.452 21 4 4 0 461.159 240.642 20 -4 -4 0 757.713 295.750 10 -4 -4 0 568.125 242.965 5 4 4 0 149.543 182.811 3 4 4 0 1172.92 328.588 16 -4 -4 0 333.576 227.913 15 -4 -4 0 600.508 244.899 4 -4 -4 -2 579.736 275.703 22 4 4 2 510.625 229.015 6 4 4 2 488.353 244.360 21 4 4 2 756.420 295.163 20 -4 -4 -2 455.102 251.456 10 4 4 2 580.796 264.499 3 -4 -4 -2 694.011 270.629 5 4 4 2 705.596 315.312 16 -4 -4 -2 192.137 153.624 4 -4 -4 -4 1032.95 354.414 22 4 4 4 1331.25 350.926 21 4 4 4 882.108 288.764 6 4 4 4 1008.62 371.789 20 -4 -4 -4 1671.16 426.586 10 -4 -4 -4 986.502 361.792 5 -4 -4 -6 397.837 309.771 22 4 4 6 534.040 197.543 21 4 4 6 748.072 299.504 6 -4 -4 -6 494.187 244.006 10 -4 -4 -6 488.267 257.269 5 4 4 6 454.572 224.943 8 -4 -5 11 604.835 359.256 4 4 5 -9 159.019 224.632 20 -4 -5 9 -246.618 374.205 10 4 5 -9 -347.878 434.654 3 4 5 -9 -430.944 331.958 16 -4 -5 9 -388.890 297.773 4 4 5 -7 289.590 311.761 6 4 5 -7 -342.849 403.873 20 -4 -5 7 -271.926 255.632 10 4 5 -7 -631.247 485.891 3 -4 -5 7 -405.452 330.009 5 4 5 -7 183.534 356.834 16 -4 -5 7 -549.174 474.345 15 -4 -5 7 -175.815 271.829 4 -4 -5 7 38.0789 197.888 25 4 5 -5 382.996 349.555 6 4 5 -5 613.062 421.872 20 -4 -5 5 539.160 341.975 10 4 5 -5 744.890 485.375 3 -4 -5 5 -224.769 226.772 5 4 5 -5 -120.549 331.020 16 -4 -5 5 123.741 349.398 15 -4 -5 5 307.502 262.821 4 -4 -5 5 127.520 233.103 25 4 5 -3 -564.983 500.256 6 4 5 -3 -353.103 315.575 20 -4 -5 3 -1.44954 329.189 10 4 5 -3 -293.317 295.821 3 -4 -5 3 258.015 292.883 5 4 5 -3 -394.203 362.257 16 -4 -5 3 522.197 435.557 15 -4 -5 3 442.792 249.174 4 4 5 -1 869.909 487.376 6 4 5 -1 2164.66 626.998 20 -4 -5 1 1149.75 457.007 10 4 5 -1 292.856 309.958 3 -4 -5 1 1000.40 491.869 5 4 5 -1 757.312 475.346 16 -4 -5 1 1033.92 446.924 15 -4 -5 1 507.627 263.488 4 -4 -5 -1 754.076 388.853 22 4 5 1 419.298 343.586 21 4 5 1 619.439 322.599 6 4 5 1 -2.50609 268.408 20 -4 -5 -1 150.687 273.114 10 4 5 1 457.977 409.960 3 -4 -5 -1 376.286 337.612 5 4 5 1 599.721 348.163 16 -4 -5 -1 -610.977 366.193 4 -4 -5 -3 2110.05 548.940 22 4 5 3 2185.48 546.824 21 4 5 3 2548.53 606.563 6 4 5 3 1234.32 465.104 20 -4 -5 -3 1738.36 502.720 10 -4 -5 -3 2247.68 593.657 5 4 5 5 598.385 327.812 6 -4 -5 -5 -238.824 234.295 5 -5 -1 20 13.4627 263.622 12 -5 -1 20 100.573 186.358 24 -5 -1 18 1580.58 433.788 12 -5 -1 18 1696.89 449.199 18 5 1 -18 1468.88 394.836 14 -5 -1 18 701.663 238.725 24 -5 -1 16 366.910 275.093 12 -5 -1 16 190.520 181.397 18 -5 -1 16 26.3385 113.272 24 -5 -1 14 1467.97 364.426 12 -5 -1 14 986.952 307.794 18 -5 -1 12 43.4434 101.599 18 -5 -1 12 131.052 139.117 12 -5 -2 21 -326.585 470.437 12 5 2 -21 -710.394 357.031 14 -5 -2 19 166.912 257.601 12 5 2 -19 606.922 340.046 17 5 2 -19 436.492 327.131 14 -5 -2 17 2269.44 568.238 12 -5 -2 17 1279.98 403.998 18 5 2 -17 976.159 331.824 17 5 2 -17 1774.72 431.382 14 -5 -2 15 250.291 220.482 12 -5 -2 15 20.5641 216.718 18 5 2 -15 78.8574 163.590 17 5 2 -15 60.9585 189.715 14 5 2 -13 4946.12 495.665 20 -5 -2 13 5495.36 611.827 18 5 2 -13 5578.92 618.670 17 -5 -2 13 5819.16 740.250 12 -5 -2 11 599.493 243.899 12 -5 -2 11 457.013 160.878 4 -5 -2 11 -72.4683 182.633 1 5 2 -11 124.843 118.905 20 -5 -2 11 245.125 114.472 10 -5 -2 11 365.115 141.534 18 5 2 -11 140.176 196.692 2 5 2 -11 252.905 127.526 17 -5 -2 11 252.079 121.193 15 5 2 -11 97.8987 116.877 3 -5 -2 9 2068.90 303.817 4 -5 -2 9 2292.07 476.709 1 -5 -2 9 2051.16 292.113 18 -5 -2 9 2015.32 290.339 10 5 2 -9 1927.17 307.393 17 5 2 -9 2534.61 546.096 2 -5 -2 9 2420.90 397.824 15 5 2 -9 1952.62 315.715 3 -5 -2 9 1520.67 328.807 12 -5 -2 7 26235.8 1030.47 10 -5 -2 7 26614.4 1379.96 19 -5 -2 7 27733.3 887.594 18 -5 -2 7 28379.3 1269.19 12 -5 -3 18 353.065 382.258 12 5 3 -18 33.5049 235.908 17 5 3 -18 83.0936 232.517 14 -5 -3 16 -78.4686 199.358 12 5 3 -16 21.4794 230.654 17 -5 -3 16 -171.690 199.497 15 5 3 -16 -473.153 346.374 14 -5 -3 14 2538.38 582.005 12 5 3 -14 3219.20 558.284 17 -5 -3 14 2621.25 568.888 15 5 3 -14 2646.04 518.006 14 -5 -3 12 -105.854 236.612 12 -5 -3 12 308.562 175.661 4 5 3 -12 91.4779 146.778 20 5 3 -12 698.606 312.316 17 5 3 -12 601.125 279.091 16 5 3 -12 259.374 191.588 3 -5 -3 12 477.372 226.050 15 5 3 -12 460.707 191.361 14 -5 -3 10 2121.61 469.285 12 -5 -3 10 2078.48 384.944 4 5 3 -10 1629.99 356.176 20 -5 -3 10 1949.34 357.712 10 5 3 -10 1280.57 295.037 17 5 3 -10 2079.52 418.694 16 5 3 -10 1211.16 292.295 3 -5 -3 10 1560.84 414.340 15 5 3 -10 2233.87 407.810 14 -5 -3 8 651.237 250.487 12 -5 -3 8 569.488 210.042 4 5 3 -8 528.659 224.466 20 -5 -3 8 510.266 201.655 10 5 3 -8 380.136 171.936 17 5 3 -8 651.418 211.838 16 -5 -3 8 898.942 322.505 15 5 3 -8 537.368 214.124 3 5 3 -8 629.792 237.681 14 -5 -3 6 1452.66 347.452 12 -5 -3 6 898.236 253.544 4 5 3 -6 1012.01 292.189 20 -5 -3 6 876.142 238.153 10 5 3 -6 1227.13 313.669 16 -5 -3 6 1388.54 344.637 15 5 3 -6 886.833 258.049 3 -5 -3 4 151.194 139.733 12 -5 -3 4 -226.856 169.028 4 -5 -3 4 203.125 120.973 22 5 3 -4 131.988 100.758 21 5 3 -4 -135.526 176.313 20 -5 -3 4 -1.05010 145.787 10 5 3 -4 -187.597 187.690 16 -5 -3 4 110.231 180.082 5 -5 -3 4 247.817 166.326 15 5 3 -4 60.0567 142.187 3 -5 -3 2 216.401 141.330 22 5 3 -2 55.8912 134.655 21 5 3 -2 233.515 146.794 6 5 3 -2 227.279 168.338 20 -5 -3 2 203.231 149.537 10 5 3 -2 125.546 123.051 16 -5 -3 2 384.308 199.551 5 -5 -3 2 38.2400 154.442 29 -5 -4 15 331.225 291.157 12 5 4 -15 831.778 342.091 17 -5 -4 15 1168.88 471.538 15 -5 -4 13 929.783 485.644 12 5 4 -13 628.104 267.517 20 5 4 -13 1588.89 478.858 17 -5 -4 13 1390.43 536.273 15 -5 -4 11 262.657 268.818 12 5 4 -11 993.430 364.168 20 -5 -4 11 691.785 242.896 10 5 4 -11 1065.14 395.504 17 5 4 -11 245.475 258.739 3 5 4 -11 -115.721 274.392 16 -5 -4 11 53.6831 232.484 15 -5 -4 11 711.267 278.405 4 5 4 -9 120.643 207.847 20 -5 -4 9 -296.159 259.875 10 5 4 -9 14.6682 176.167 17 5 4 -9 73.6135 195.225 3 5 4 -9 441.951 248.053 16 -5 -4 9 -224.804 309.452 15 -5 -4 9 222.244 208.024 4 -5 -4 7 75.1433 175.427 4 5 4 -7 624.729 248.643 20 -5 -4 7 888.271 322.941 10 5 4 -7 731.325 290.293 16 5 4 -7 749.843 312.905 3 -5 -4 7 511.121 222.274 15 -5 -4 5 32.1050 140.851 4 5 4 -5 -66.9334 187.774 6 5 4 -5 39.4538 154.024 20 -5 -4 5 -101.739 144.564 10 5 4 -5 -106.867 179.681 16 -5 -4 5 258.188 223.676 5 5 4 -5 -132.078 266.400 3 -5 -4 5 176.377 203.153 15 -5 -4 3 0.26049 183.732 4 -5 -4 3 94.5208 165.819 22 5 4 -3 -110.458 175.217 21 5 4 -3 195.440 189.031 6 5 4 -3 -211.990 275.557 20 -5 -4 3 -283.826 268.046 10 -5 -4 3 -621.972 361.085 5 5 4 -3 34.5985 228.534 16 5 4 -3 319.242 229.586 3 -5 -4 3 407.742 280.846 15 -5 -4 1 188.893 201.331 22 5 4 -1 -132.507 175.216 21 5 4 -1 268.207 240.055 6 5 4 -1 328.834 240.312 20 -5 -4 1 -153.184 259.809 10 -5 -4 1 298.451 252.868 5 5 4 -1 256.198 181.351 16 5 4 -1 241.335 270.969 3 -5 -4 -1 127.274 180.600 22 5 4 1 -144.103 173.437 21 5 4 1 -167.921 200.663 6 5 4 1 -211.058 220.557 20 -5 -4 -1 -184.458 205.991 10 -5 -4 -1 172.364 213.520 5 5 5 -10 -480.057 349.028 3 -5 -5 10 3.79231 281.712 4 5 5 -8 780.365 432.320 20 -5 -5 8 -161.538 228.625 10 5 5 -8 -110.431 272.880 3 5 5 -8 -164.085 422.642 16 -5 -5 8 910.931 459.223 15 -5 -5 8 813.466 422.791 4 5 5 -6 -332.461 335.861 20 -5 -5 6 337.060 255.922 10 5 5 -6 5.47659 254.212 3 5 5 -6 -40.9832 294.230 16 -5 -5 6 -71.3407 282.005 15 -5 -5 6 864.085 447.320 4 5 5 -4 128.780 304.126 20 -5 -5 4 445.034 321.921 10 5 5 -4 -66.9555 345.990 3 5 5 -4 338.986 374.179 16 -5 -5 4 -398.381 378.936 15 -5 -5 4 395.097 345.072 4 5 5 -2 1006.38 490.452 20 -5 -5 2 624.529 400.518 10 5 5 -2 119.521 243.626 16 -5 -5 2 421.994 272.246 5 6 3 -17 278.683 232.387 17 -6 -3 15 1896.79 490.905 12 6 3 -15 1756.65 414.245 17 -6 -3 13 3126.00 612.247 12 6 3 -13 3044.29 490.482 17 -6 -3 11 958.402 343.363 12 -6 -3 11 1453.55 322.215 4 6 3 -11 1321.64 320.897 20 6 3 -11 1886.45 369.962 3 6 4 -12 358.846 266.015 3 -6 -4 12 248.413 310.273 15 -6 -4 12 148.959 177.745 4 -6 -4 10 85.2846 184.219 4 6 4 -10 1707.73 494.174 20 6 4 -10 1063.78 459.261 3 -6 -4 10 627.425 490.353 15 -6 -4 8 -770.356 441.116 15