#------------------------------------------------------------------------------ #$Date: 2024-11-23 05:14:18 +0200 (Sat, 23 Nov 2024) $ #$Revision: 296089 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/32/1573264.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1573264 loop_ _publ_author_name 'Setifi, Fatima' 'Setifi, Zouaoui' 'Reuter, Hans' 'Al-Douh, Mohammad Hadi' 'Addala, Abderezak' _publ_section_title ; Bis(azido-\kN 1)bis(2,2′-dipyridylamine-\k2 N 1,N 1′)iron(II) monohydrate ; _journal_coeditor_code WM4222 _journal_issue 11 _journal_name_full IUCrData _journal_paper_doi 10.1107/S2414314624011167 _journal_volume 9 _journal_year 2024 _chemical_formula_iupac '[Fe (N3)2 (C10 H9 N3)2], H2 O' _chemical_formula_moiety 'C20 H18 Fe N12, H2 O' _chemical_formula_sum 'C20 H20 Fe N12 O' _chemical_formula_weight 500.33 _chemical_name_systematic 'Bis(azido-\kN^1^)bis(2,2'-dipyridylamine-\k^2^N^1^,N^1'^)iron(II) monohydrate' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 79.516(3) _cell_angle_beta 83.962(3) _cell_angle_gamma 69.520(3) _cell_formula_units_Z 2 _cell_length_a 7.7496(5) _cell_length_b 9.3778(6) _cell_length_c 16.6178(10) _cell_measurement_reflns_used 2459 _cell_measurement_temperature 300(2) _cell_measurement_theta_max 28.207 _cell_measurement_theta_min 2.681 _cell_volume 1111.33(12) _computing_cell_refinement ; SAINT (Bruker, 2019) ; _computing_data_collection ; APEX2 (Bruker, 2019) ; _computing_data_reduction ; SAINT (Bruker, 2019) ; _computing_molecular_graphics ; DIAMOND (Brandenburg, 2006) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick 2015a) ; _diffrn_ambient_temperature 300(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0568 _diffrn_reflns_av_unetI/netI 0.0348 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 93449 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 36.442 _diffrn_reflns_theta_min 2.347 _exptl_absorpt_coefficient_mu 0.720 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.495 _exptl_crystal_description block _exptl_crystal_F_000 516 _exptl_crystal_size_max 0.38 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.382 _refine_diff_density_min -0.651 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.094 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 315 _refine_ls_number_reflns 10836 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.094 _refine_ls_R_factor_all 0.0736 _refine_ls_R_factor_gt 0.0373 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0356P)^2^+0.3320P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0854 _refine_ls_wR_factor_ref 0.1085 _reflns_number_gt 7610 _reflns_number_total 10836 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file wm4222.cif _cod_data_source_block I _cod_original_cell_volume 1111.34(12) _cod_database_code 1573264 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; -1 0 0 2123.09 103.09 1 0 0 2079.59 103.29 -2 0 0 108.99 5.50 -2 0 0 107.39 5.50 -2 0 0 109.29 6.90 -2 0 0 110.59 5.00 -2 0 0 106.99 4.70 -2 0 0 112.19 5.30 -2 0 0 109.29 6.10 -2 0 0 107.79 6.90 -2 0 0 104.99 6.30 -2 0 0 114.09 6.70 2 0 0 105.69 6.80 2 0 0 105.19 6.50 2 0 0 108.69 4.70 2 0 0 103.89 5.40 2 0 0 105.79 5.50 2 0 0 110.09 6.70 2 0 0 105.79 6.30 2 0 0 109.09 6.10 2 0 0 110.59 6.40 -3 0 0 17.70 1.80 -3 0 0 20.20 4.50 -3 0 0 18.50 2.40 -3 0 0 17.60 3.50 -3 0 0 22.00 3.60 -3 0 0 16.10 3.50 -3 0 0 17.40 3.50 -3 0 0 20.40 3.20 3 0 0 20.70 2.80 3 0 0 13.80 3.20 3 0 0 16.30 3.50 3 0 0 16.60 3.60 3 0 0 15.40 3.30 3 0 0 15.80 2.40 3 0 0 18.70 3.10 3 0 0 18.10 2.80 -4 0 0 1898.91 74.29 -4 0 0 1877.11 72.69 -4 0 0 1905.01 74.19 -4 0 0 1915.81 68.29 -4 0 0 1905.11 72.19 -4 0 0 1909.61 70.39 -4 0 0 1985.00 73.19 4 0 0 1884.81 71.79 4 0 0 1895.41 70.39 4 0 0 1884.01 73.09 4 0 0 2003.70 70.39 4 0 0 1970.50 72.69 4 0 0 1974.70 69.99 4 0 0 1946.51 73.79 4 0 0 1976.70 72.79 -5 0 0 85.49 5.00 -5 0 0 82.19 8.20 -5 0 0 93.19 8.80 -5 0 0 89.69 9.30 -5 0 0 85.39 9.30 -5 0 0 88.09 6.80 5 0 0 91.19 8.90 5 0 0 101.39 9.90 5 0 0 85.49 6.80 5 0 0 97.19 8.60 5 0 0 87.99 8.00 5 0 0 92.59 7.10 5 0 0 90.99 6.30 -6 0 0 3.50 4.80 -6 0 0 4.00 1.40 -6 0 0 4.60 3.80 -6 0 0 5.00 4.10 -6 0 0 5.00 3.60 6 0 0 0.00 3.20 6 0 0 5.70 4.40 6 0 0 1.30 2.60 6 0 0 6.00 3.30 6 0 0 2.70 2.40 6 0 0 5.40 3.00 6 0 0 -0.30 2.40 -7 0 0 233.08 18.60 -7 0 0 234.58 17.20 -7 0 0 216.58 16.00 -7 0 0 232.98 16.60 7 0 0 231.38 17.00 7 0 0 263.87 19.00 7 0 0 242.78 14.20 7 0 0 250.27 15.70 7 0 0 269.07 16.70 7 0 0 247.48 14.80 -8 0 0 121.09 13.00 -8 0 0 85.39 9.70 -8 0 0 99.49 16.10 -8 0 0 128.99 12.70 8 0 0 116.79 11.00 8 0 0 98.89 10.40 8 0 0 113.09 9.60 8 0 0 130.59 10.90 8 0 0 113.59 12.50 -9 0 0 36.60 11.60 -9 0 0 18.50 6.80 -9 0 0 22.60 7.10 9 0 0 27.10 8.00 9 0 0 25.30 6.10 9 0 0 23.00 6.60 9 0 0 38.20 8.80 9 0 0 20.50 5.50 -10 0 0 64.09 12.20 -10 0 0 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4.40 7 -1 0 3.50 3.30 7 -1 0 8.40 4.20 7 -1 0 -2.40 2.00 7 -1 0 2.00 2.80 -7 1 0 3.30 4.40 -7 1 0 7.90 5.30 -7 1 0 2.90 1.10 -7 1 0 9.40 6.70 6 -1 0 281.67 15.10 6 -1 0 282.07 16.70 6 -1 0 304.17 16.90 6 -1 0 308.47 18.30 6 -1 0 297.87 15.50 6 -1 0 280.07 14.60 6 -1 0 301.57 19.50 -6 1 0 280.17 12.00 -6 1 0 291.57 19.60 -6 1 0 284.97 18.10 -6 1 0 286.67 18.00 5 -1 0 140.99 11.20 5 -1 0 111.79 9.20 5 -1 0 138.69 9.70 5 -1 0 131.59 9.60 5 -1 0 129.69 10.40 5 -1 0 138.39 8.70 5 -1 0 131.59 8.60 5 -1 0 116.99 10.70 5 -1 0 117.69 7.70 -5 1 0 125.49 10.20 -5 1 0 129.09 8.20 -5 1 0 111.19 10.10 -5 1 0 120.39 12.40 -5 1 0 119.99 9.80 -5 1 0 137.29 11.60 -5 1 0 122.09 6.20 4 -1 0 224.08 10.90 4 -1 0 222.98 11.30 4 -1 0 219.28 12.30 4 -1 0 237.38 13.00 4 -1 0 212.28 13.30 4 -1 0 236.48 11.90 4 -1 0 232.88 13.30 4 -1 0 243.78 14.20 4 -1 0 228.48 12.50 -4 1 0 221.18 13.00 -4 1 0 236.28 13.40 -4 1 0 233.78 9.70 -4 1 0 257.17 14.00 -4 1 0 223.68 14.10 -4 1 0 196.38 13.50 -4 1 0 230.18 11.30 -4 1 0 213.58 9.60 3 -1 0 25.20 3.80 3 -1 0 39.30 5.20 3 -1 0 30.50 4.50 3 -1 0 30.00 3.90 3 -1 0 35.60 4.70 3 -1 0 31.80 4.10 3 -1 0 31.60 3.30 3 -1 0 32.30 3.00 3 -1 0 40.80 5.00 -3 1 0 35.70 4.80 -3 1 0 27.50 3.30 -3 1 0 29.80 5.50 -3 1 0 31.20 4.80 -3 1 0 27.80 4.20 -3 1 0 32.70 2.50 -3 1 0 31.60 2.30 -3 1 0 32.30 4.60 -3 1 0 31.20 2.90 2 -1 0 739.23 27.80 2 -1 0 764.62 29.80 2 -1 0 750.92 29.20 2 -1 0 758.22 28.90 2 -1 0 750.22 29.60 2 -1 0 782.02 31.40 2 -1 0 733.63 28.10 2 -1 0 799.92 30.00 2 -1 0 787.32 27.30 2 -1 0 753.02 29.60 -2 1 0 771.72 29.70 -2 1 0 739.33 29.50 -2 1 0 767.32 29.80 -2 1 0 758.02 27.20 -2 1 0 757.22 27.70 -2 1 0 763.52 29.90 -2 1 0 777.52 30.30 -2 1 0 751.42 28.00 1 -1 0 3233.58 150.48 -1 1 0 3109.49 148.59 0 -1 0 8454.45 316.57 0 1 0 8276.97 314.37 -1 -1 0 1064.69 37.90 -1 -1 0 1039.40 38.20 -1 -1 0 1059.89 37.90 -1 -1 0 1046.30 36.80 -1 -1 0 1051.09 37.90 1 1 0 1040.30 37.90 1 1 0 1016.90 38.10 -2 -1 0 12.60 2.80 -2 -1 0 12.00 2.40 -2 -1 0 6.30 1.80 -2 -1 0 11.30 1.70 -2 -1 0 12.30 2.60 -2 -1 0 13.60 2.40 -2 -1 0 10.30 2.00 -2 -1 0 9.30 2.40 2 1 0 9.40 2.30 2 1 0 9.50 2.60 2 1 0 13.40 1.70 2 1 0 10.80 2.00 2 1 0 13.70 2.40 2 1 0 12.10 2.00 2 1 0 9.10 2.30 2 1 0 8.90 1.90 -3 -1 0 1142.59 42.90 -3 -1 0 1153.68 44.10 -3 -1 0 1145.79 44.40 -3 -1 0 1150.78 41.60 -3 -1 0 1097.19 41.80 -3 -1 0 1165.58 43.50 -3 -1 0 1172.98 44.60 -3 -1 0 1081.59 45.20 3 1 0 1222.88 44.50 3 1 0 1170.48 42.90 3 1 0 1170.08 45.30 3 1 0 1191.98 43.10 3 1 0 1124.99 43.40 3 1 0 1170.38 44.60 3 1 0 1150.28 43.90 3 1 0 1133.69 41.60 -4 -1 0 1282.17 50.59 -4 -1 0 1274.37 49.50 -4 -1 0 1303.67 48.20 -4 -1 0 1273.37 46.60 -4 -1 0 1295.57 48.60 -4 -1 0 1256.87 50.49 -4 -1 0 1303.67 52.29 -4 -1 0 1337.77 51.99 4 1 0 1286.67 50.29 4 1 0 1292.07 46.60 4 1 0 1312.37 50.09 4 1 0 1284.67 48.50 4 1 0 1294.87 50.89 4 1 0 1326.57 51.79 4 1 0 1237.18 49.30 4 1 0 1229.18 48.30 -5 -1 0 211.88 15.20 -5 -1 0 225.58 14.30 -5 -1 0 226.98 10.30 -5 -1 0 231.18 14.50 -5 -1 0 220.98 15.00 -5 -1 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16.00 10 1 0 133.59 14.30 10 1 0 155.38 13.20 10 1 0 129.89 13.30 10 1 0 139.39 13.00 10 1 0 146.19 26.10 10 1 0 123.79 11.60 -11 -1 0 0.10 6.50 -11 -1 0 5.30 4.80 -11 -1 0 8.40 8.90 11 1 0 -3.20 4.90 11 1 0 3.60 4.60 11 1 0 1.80 5.50 11 1 0 3.60 3.50 11 1 0 2.90 4.40 11 1 0 1.90 5.10 -12 -1 0 20.00 9.00 -12 -1 0 -8.20 5.50 -12 -1 0 11.80 9.40 12 1 0 10.90 7.30 12 1 0 7.50 5.80 12 1 0 -1.70 4.60 12 1 0 0.30 6.80 12 1 0 4.40 5.30 12 1 0 -5.70 4.50 11 -2 0 2.90 6.40 11 -2 0 -9.80 4.90 11 -2 0 1.80 6.80 11 -2 0 -0.90 4.50 -11 2 0 -5.20 6.90 -11 2 0 3.20 7.70 10 -2 0 15.40 7.00 10 -2 0 19.20 7.40 10 -2 0 24.60 5.90 -10 2 0 14.90 7.40 -10 2 0 12.30 5.00 -10 2 0 20.90 10.50 9 -2 0 24.40 5.60 9 -2 0 14.50 3.90 9 -2 0 9.60 5.40 9 -2 0 16.50 9.00 -9 2 0 5.80 6.90 -9 2 0 8.90 3.90 -9 2 0 10.50 6.50 8 -2 0 6.10 3.10 8 -2 0 5.30 3.20 8 -2 0 1.80 4.20 8 -2 0 5.80 5.00 8 -2 0 8.10 3.10 8 -2 0 9.40 5.00 -8 2 0 7.30 3.40 -8 2 0 8.70 6.90 -8 2 0 6.80 5.60 -8 2 0 5.40 3.90 7 -2 0 12.30 4.90 7 -2 0 4.30 3.30 7 -2 0 7.50 3.00 7 -2 0 16.00 5.90 7 -2 0 8.40 5.30 7 -2 0 9.50 3.60 -7 2 0 8.40 5.20 -7 2 0 3.10 1.10 -7 2 0 7.80 6.20 -7 2 0 1.10 4.00 -7 2 0 6.60 4.80 6 -2 0 170.98 13.90 6 -2 0 191.78 13.10 6 -2 0 160.78 11.20 6 -2 0 165.48 10.90 6 -2 0 167.68 13.80 6 -2 0 179.98 10.10 -6 2 0 171.48 14.00 -6 2 0 147.79 7.50 -6 2 0 168.98 8.00 -6 2 0 158.08 11.40 -6 2 0 170.68 13.80 -6 2 0 169.78 14.40 5 -2 0 191.18 13.30 5 -2 0 156.88 12.60 5 -2 0 183.08 11.40 5 -2 0 179.38 11.80 5 -2 0 189.58 10.50 5 -2 0 198.28 12.40 5 -2 0 169.58 9.50 -5 2 0 164.68 7.70 -5 2 0 171.88 8.20 -5 2 0 177.88 12.90 -5 2 0 176.18 12.90 -5 2 0 160.48 9.80 4 -2 0 246.08 11.40 4 -2 0 236.68 14.30 4 -2 0 243.68 12.10 4 -2 0 249.38 13.30 4 -2 0 248.88 14.80 4 -2 0 235.78 13.90 4 -2 0 243.18 13.40 4 -2 0 240.88 13.60 -4 2 0 249.08 14.70 -4 2 0 219.88 13.70 -4 2 0 249.08 11.20 -4 2 0 252.37 10.80 -4 2 0 259.37 12.00 -4 2 0 246.58 15.20 -4 2 0 251.47 14.60 -4 2 0 248.98 14.90 3 -2 0 344.27 14.20 3 -2 0 351.06 16.80 3 -2 0 352.76 17.20 3 -2 0 338.57 16.30 3 -2 0 321.97 13.80 3 -2 0 323.37 16.70 3 -2 0 349.67 14.80 3 -2 0 350.16 15.90 -3 2 0 362.66 17.30 -3 2 0 341.67 16.70 -3 2 0 357.46 15.00 -3 2 0 346.87 15.40 -3 2 0 346.27 13.90 -3 2 0 320.47 13.10 -3 2 0 351.26 17.10 -3 2 0 356.06 17.70 -3 2 0 347.37 17.10 2 -2 0 6061.99 285.77 -2 2 0 5608.44 277.77 1 -2 0 1360.96 51.19 1 -2 0 1452.75 49.40 1 -2 0 1391.96 50.09 1 -2 0 1415.06 50.19 1 -2 0 1386.26 51.29 1 -2 0 1379.36 51.49 -1 2 0 1384.46 51.39 -1 2 0 1414.46 49.40 -1 2 0 1432.66 50.49 -1 2 0 1436.26 50.09 -1 2 0 1403.26 49.60 -1 2 0 1378.66 50.99 -1 2 0 1367.66 51.39 -1 2 0 1362.66 50.99 0 -2 0 975.30 36.90 0 -2 0 996.50 35.60 0 -2 0 976.80 36.70 0 -2 0 1044.10 37.20 0 -2 0 1026.30 36.30 0 -2 0 994.70 36.90 0 -2 0 971.00 36.60 0 -2 0 984.80 36.90 0 2 0 983.40 36.60 0 2 0 1014.10 36.80 0 2 0 1026.50 37.00 0 2 0 993.40 35.50 0 2 0 1001.70 37.30 0 2 0 1004.70 37.30 -1 -2 0 -0.90 1.30 -1 -2 0 2.20 1.60 -1 -2 0 -0.10 1.50 -1 -2 0 -0.50 0.90 -1 -2 0 0.70 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106.09 9.20 4 4 0 100.79 7.20 4 4 0 92.49 8.90 4 4 0 114.69 6.70 4 4 0 102.39 8.30 4 4 0 102.99 7.20 -5 -4 0 113.89 9.10 -5 -4 0 128.99 10.90 -5 -4 0 135.59 10.70 -5 -4 0 142.49 11.40 -5 -4 0 141.69 10.90 -5 -4 0 135.99 12.00 5 4 0 126.49 9.50 5 4 0 128.99 8.60 5 4 0 128.99 8.90 5 4 0 139.59 11.90 5 4 0 117.09 7.90 5 4 0 148.69 11.50 5 4 0 122.79 9.30 5 4 0 131.49 9.60 -6 -4 0 30.20 7.00 -6 -4 0 22.90 3.90 -6 -4 0 19.10 5.80 -6 -4 0 29.90 6.50 -6 -4 0 20.20 5.20 -6 -4 0 35.50 6.00 -6 -4 0 35.70 7.00 6 4 0 19.60 5.60 6 4 0 38.60 5.30 6 4 0 24.70 6.30 6 4 0 20.00 4.60 6 4 0 27.50 4.90 6 4 0 34.50 5.60 6 4 0 24.20 5.70 6 4 0 24.10 5.80 6 4 0 24.60 5.10 6 4 0 29.40 6.80 -7 -4 0 29.90 6.60 -7 -4 0 34.60 6.90 -7 -4 0 22.20 7.20 -7 -4 0 21.10 3.90 7 4 0 28.50 5.40 7 4 0 23.70 6.30 7 4 0 22.10 6.50 7 4 0 25.90 6.00 7 4 0 19.40 6.70 7 4 0 21.00 4.40 -8 -4 0 186.98 16.10 -8 -4 0 165.88 16.60 -8 -4 0 135.09 8.80 -8 -4 0 161.58 13.50 8 4 0 165.38 13.00 8 4 0 161.88 14.70 8 4 0 177.48 16.10 8 4 0 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489.75 26.80 -4 -6 0 571.94 27.70 -4 -6 0 548.45 24.30 -4 -6 0 546.35 25.40 -4 -6 0 526.75 27.40 -4 -6 0 587.54 27.10 4 6 0 517.15 26.30 4 6 0 547.95 27.40 4 6 0 564.44 23.40 4 6 0 567.94 25.30 4 6 0 551.94 27.40 4 6 0 520.45 26.20 4 6 0 563.44 25.50 4 6 0 551.24 27.00 4 6 0 513.65 24.30 -5 -6 0 63.79 9.90 -5 -6 0 78.49 8.10 -5 -6 0 68.19 10.40 -5 -6 0 72.39 9.40 -5 -6 0 79.09 12.00 -5 -6 0 72.79 6.80 5 6 0 74.59 7.80 5 6 0 89.39 10.00 5 6 0 86.09 8.50 5 6 0 74.39 10.90 5 6 0 78.89 6.50 5 6 0 73.39 9.70 5 6 0 66.59 6.70 -6 -6 0 224.18 14.60 -6 -6 0 235.58 17.30 -6 -6 0 225.08 13.60 -6 -6 0 248.48 16.90 6 6 0 205.58 12.40 6 6 0 247.38 17.30 6 6 0 238.18 14.80 6 6 0 191.78 13.00 6 6 0 204.68 19.10 6 6 0 214.78 13.80 6 6 0 244.38 15.90 -7 -6 0 155.78 13.50 -7 -6 0 186.38 15.50 -7 -6 0 205.38 16.70 -7 -6 0 175.88 13.50 7 6 0 188.48 12.60 7 6 0 157.78 11.90 7 6 0 173.18 13.70 7 6 0 178.88 11.50 7 6 0 188.28 15.80 7 6 0 179.38 13.60 7 6 0 189.28 16.70 -8 -6 0 61.19 8.50 -8 -6 0 61.99 9.60 -8 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347.77 17.20 4 8 0 341.07 20.00 4 8 0 344.47 21.70 4 8 0 336.97 21.80 4 8 0 358.66 21.50 4 8 0 353.46 18.60 -5 -8 0 76.29 11.70 -5 -8 0 48.90 8.70 -5 -8 0 72.99 11.10 -5 -8 0 68.09 7.40 -5 -8 0 68.59 9.50 5 8 0 66.79 9.50 5 8 0 72.79 10.10 5 8 0 70.79 9.20 5 8 0 69.59 6.90 5 8 0 94.69 10.10 5 8 0 88.29 12.10 5 8 0 71.59 6.70 -6 -8 0 28.60 7.70 -6 -8 0 27.00 5.40 -6 -8 0 32.20 8.20 -6 -8 0 30.80 6.90 6 8 0 29.60 7.20 6 8 0 38.10 7.50 6 8 0 34.50 8.00 6 8 0 32.30 5.80 6 8 0 24.40 6.30 -7 -8 0 9.10 5.30 -7 -8 0 9.10 4.70 -7 -8 0 4.80 5.00 -7 -8 0 5.80 3.80 7 8 0 6.70 4.90 7 8 0 6.60 6.00 7 8 0 4.50 4.60 7 8 0 6.10 4.00 7 8 0 5.70 5.30 7 8 0 18.70 4.50 -8 -8 0 47.60 8.60 -8 -8 0 27.10 6.60 -8 -8 0 43.70 9.70 -8 -8 0 37.70 9.40 8 8 0 42.40 9.70 8 8 0 43.70 9.90 8 8 0 32.10 7.10 8 8 0 44.00 9.80 8 8 0 27.00 5.80 8 8 0 40.60 7.80 -9 -8 0 1.90 5.90 -9 -8 0 3.10 3.90 -9 -8 0 8.20 5.50 -9 -8 0 3.60 3.50 9 8 0 4.30 4.20 9 8 0 -5.30 4.20 9 8 0 -4.10 4.90 9 8 0 0.60 5.50 9 8 0 -1.90 2.40 9 8 0 3.90 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16.10 5.80 3 13 0 13.90 8.30 3 13 0 16.90 6.60 3 13 0 5.20 5.20 3 13 0 23.50 8.90 -4 -13 0 7.90 6.20 -4 -13 0 8.00 7.00 -4 -13 0 10.60 6.10 4 13 0 4.90 4.40 4 13 0 18.00 8.50 4 13 0 5.10 4.30 4 13 0 5.00 5.90 4 13 0 -2.60 4.70 4 13 0 -3.00 3.20 -5 -13 0 6.00 5.90 -5 -13 0 16.50 7.00 -5 -13 0 9.80 7.60 5 13 0 7.90 6.10 5 13 0 -7.10 5.30 5 13 0 2.70 5.00 5 13 0 2.40 5.20 -6 -13 0 -5.10 4.80 -6 -13 0 -7.00 3.90 -6 -13 0 0.40 6.10 6 13 0 4.30 4.80 6 13 0 -4.30 4.60 6 13 0 -1.50 4.70 6 13 0 -1.90 4.50 6 13 0 -6.00 5.60 -7 -13 0 51.89 12.40 -7 -13 0 38.30 9.70 -7 -13 0 50.19 12.00 7 13 0 38.00 9.00 7 13 0 24.30 8.90 7 13 0 33.90 8.80 7 13 0 34.90 9.80 -8 -13 0 -1.60 6.00 -8 -13 0 6.50 7.40 -8 -13 0 0.50 5.70 8 13 0 -9.50 3.00 8 13 0 -7.00 5.30 8 13 0 -11.10 6.10 8 13 0 -3.20 4.80 8 13 0 -1.70 5.10 8 13 0 -10.80 5.00 -9 -13 0 -0.40 4.90 -9 -13 0 -6.30 6.50 -9 -13 0 -8.60 5.10 9 13 0 -2.90 6.70 9 13 0 -12.70 4.60 9 13 0 10.70 6.60 9 13 0 -4.40 6.20 9 13 0 -1.40 5.60 -10 -13 0 -2.00 8.90 -10 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1.10 4.60 -5 -14 0 7.90 7.20 -5 -14 0 18.20 7.20 -5 -14 0 5.50 5.90 -5 -14 0 4.60 6.40 5 14 0 -1.60 4.40 5 14 0 -3.70 9.30 5 14 0 11.00 6.50 5 14 0 -9.10 5.10 -6 -14 0 3.40 7.40 -6 -14 0 7.20 6.10 -6 -14 0 6.30 7.40 6 14 0 6.10 6.60 6 14 0 6.30 6.80 6 14 0 2.10 5.30 6 14 0 -2.40 7.50 6 14 0 5.60 6.00 -7 -14 0 21.90 8.20 -7 -14 0 -1.80 7.00 -7 -14 0 6.90 6.30 7 14 0 16.60 7.50 7 14 0 5.00 5.10 7 14 0 -14.90 5.60 7 14 0 5.40 7.00 -8 -14 0 8.70 7.90 -8 -14 0 5.80 6.40 -8 -14 0 14.70 8.00 8 14 0 -1.60 5.80 8 14 0 -12.30 6.30 8 14 0 -1.00 7.20 8 14 0 15.20 9.30 8 14 0 1.00 5.80 -9 -14 0 1.80 8.70 -2 -15 0 17.80 8.70 -2 -15 0 -4.10 5.80 -2 -15 0 -4.50 4.20 2 15 0 -7.40 5.50 2 15 0 2.90 6.20 2 15 0 -6.70 8.90 2 15 0 -3.40 6.80 2 15 0 -4.00 6.50 -3 -15 0 11.00 8.00 -3 -15 0 22.00 11.20 -3 -15 0 14.20 7.40 3 15 0 -7.00 5.60 3 15 0 5.60 9.40 3 15 0 -0.40 6.90 3 15 0 -1.90 5.30 -4 -15 0 9.80 7.50 -4 -15 0 3.20 6.90 -4 -15 0 -7.80 5.30 -4 -15 0 -4.90 5.40 4 15 0 -6.90 5.30 4 15 0 -1.90 4.70 4 15 0 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13.20 9.10 -2 -15 1 -8.00 4.40 -2 -15 1 -4.00 5.80 8 14 -1 6.30 9.30 8 14 -1 1.30 7.20 8 14 -1 -4.30 6.00 8 14 -1 -12.70 7.20 8 14 -1 16.20 8.50 -8 -14 1 -0.80 6.30 -8 -14 1 21.30 11.10 7 14 -1 -11.90 5.50 7 14 -1 -5.20 5.80 7 14 -1 -5.40 5.50 7 14 -1 -7.90 6.30 -7 -14 1 -0.80 6.20 -7 -14 1 8.10 6.00 -7 -14 1 3.60 7.00 6 14 -1 -1.30 6.20 6 14 -1 -5.90 4.00 6 14 -1 -0.50 6.80 6 14 -1 -9.10 5.00 6 14 -1 -13.50 4.90 -6 -14 1 -8.20 4.50 -6 -14 1 -2.10 5.80 -6 -14 1 0.60 6.60 5 14 -1 -0.80 5.50 5 14 -1 8.60 5.90 5 14 -1 13.00 8.20 5 14 -1 -5.70 7.10 5 14 -1 20.50 7.30 -5 -14 1 6.80 8.20 -5 -14 1 5.10 7.10 -5 -14 1 6.80 6.90 4 14 -1 30.00 8.30 4 14 -1 36.10 9.90 4 14 -1 37.10 8.50 4 14 -1 33.90 9.10 4 14 -1 47.00 13.50 -4 -14 1 31.70 9.40 -4 -14 1 39.40 10.50 -4 -14 1 27.60 9.50 -4 -14 1 52.19 13.60 -4 -14 1 34.10 10.00 3 14 -1 -6.80 5.30 3 14 -1 -10.30 4.60 3 14 -1 -9.30 4.10 3 14 -1 -13.10 6.60 -3 -14 1 -6.10 5.60 -3 -14 1 -6.50 5.70 -3 -14 1 2.90 5.30 -3 -14 1 2.00 5.40 -3 -14 1 -1.90 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12 -3 30.30 8.40 4 12 -3 38.00 6.80 4 12 -3 51.79 13.80 4 12 -3 42.10 8.70 -4 -12 3 28.10 11.00 -4 -12 3 34.10 9.20 -4 -12 3 24.30 8.70 -4 -12 3 33.70 8.00 3 12 -3 0.30 6.90 3 12 -3 -1.80 3.70 3 12 -3 4.20 3.90 3 12 -3 -0.70 5.50 3 12 -3 -3.10 5.20 -3 -12 3 0.10 4.60 -3 -12 3 3.70 5.50 -3 -12 3 -1.00 4.50 -3 -12 3 -2.50 4.20 2 12 -3 140.09 19.90 2 12 -3 158.98 16.90 2 12 -3 150.98 14.20 2 12 -3 138.79 12.80 -2 -12 3 133.19 15.30 -2 -12 3 122.19 16.70 -2 -12 3 128.79 19.20 -2 -12 3 160.78 15.20 1 12 -3 30.20 7.80 1 12 -3 18.50 5.70 1 12 -3 26.80 9.90 1 12 -3 35.70 9.40 -1 -12 3 27.80 7.80 -1 -12 3 34.20 9.70 -1 -12 3 35.60 9.60 -1 -12 3 48.40 11.80 0 12 -3 15.90 9.00 0 12 -3 20.20 7.70 0 12 -3 6.10 4.70 0 12 -3 20.30 7.00 0 -12 3 16.70 7.70 0 -12 3 20.50 6.20 0 -12 3 19.50 7.60 -1 12 -3 -4.90 5.20 -1 12 -3 2.80 5.30 -1 12 -3 8.20 8.40 -1 12 -3 3.70 5.70 1 -12 3 1.50 6.20 1 -12 3 2.50 4.40 1 -12 3 14.00 6.50 1 -12 3 6.20 6.90 -2 12 -3 43.80 12.30 -2 12 -3 31.50 8.70 -2 12 -3 31.80 10.80 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14.50 -6 -8 3 303.47 20.90 -6 -8 3 291.57 17.90 -6 -8 3 302.37 21.80 5 8 -3 34.50 8.60 5 8 -3 43.20 9.40 5 8 -3 44.60 7.00 5 8 -3 45.90 8.10 5 8 -3 40.00 9.60 -5 -8 3 29.40 8.50 -5 -8 3 40.70 8.70 -5 -8 3 46.00 7.20 -5 -8 3 34.70 5.10 4 8 -3 6.90 4.60 4 8 -3 5.30 5.50 4 8 -3 20.20 7.20 -4 -8 3 4.80 3.40 -4 -8 3 8.30 5.60 -4 -8 3 9.80 5.50 -4 -8 3 5.30 4.40 3 8 -3 -2.20 4.00 3 8 -3 2.50 3.60 3 8 -3 2.60 2.40 3 8 -3 -2.30 3.60 3 8 -3 -0.60 2.20 -3 -8 3 0.20 3.70 -3 -8 3 5.20 4.10 -3 -8 3 3.80 3.70 2 8 -3 341.87 18.60 2 8 -3 334.77 16.70 2 8 -3 324.87 20.40 2 8 -3 338.87 22.30 -2 -8 3 341.87 20.60 -2 -8 3 345.57 22.10 -2 -8 3 338.37 20.40 1 8 -3 3.50 2.00 1 8 -3 3.80 3.60 1 8 -3 1.80 2.80 1 8 -3 -1.10 4.20 1 8 -3 0.80 5.70 -1 -8 3 0.60 3.70 -1 -8 3 3.50 2.80 -1 -8 3 -2.50 3.20 -1 -8 3 4.40 4.90 -1 -8 3 -1.30 2.70 0 8 -3 378.26 22.20 0 8 -3 354.36 22.70 0 8 -3 329.27 17.10 0 8 -3 341.77 20.80 0 8 -3 371.46 23.90 0 -8 3 412.66 22.40 0 -8 3 367.26 19.90 0 -8 3 376.76 23.50 0 -8 3 371.26 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3 87.59 14.60 -7 8 -3 9.90 8.90 -7 8 -3 7.30 8.40 7 -8 3 6.50 6.40 7 -8 3 0.50 5.70 7 -8 3 1.30 6.00 7 -8 3 2.20 7.10 12 7 -3 16.00 4.80 12 7 -3 -8.90 4.20 12 7 -3 10.50 6.80 12 7 -3 6.30 6.20 12 7 -3 13.40 8.60 12 7 -3 12.00 7.60 -12 -7 3 7.20 7.50 -12 -7 3 8.40 5.40 -12 -7 3 21.50 12.10 11 7 -3 1.90 3.80 11 7 -3 1.20 5.90 11 7 -3 -4.50 2.80 11 7 -3 9.30 6.60 11 7 -3 2.00 4.90 11 7 -3 14.90 8.00 -11 -7 3 -3.70 5.10 -11 -7 3 15.70 10.40 -11 -7 3 -4.10 5.20 10 7 -3 12.60 7.30 10 7 -3 12.40 4.30 10 7 -3 13.20 6.30 10 7 -3 12.80 7.70 10 7 -3 22.30 4.90 10 7 -3 13.10 8.00 -10 -7 3 7.70 3.90 -10 -7 3 11.60 5.80 -10 -7 3 9.10 6.70 -10 -7 3 8.30 9.30 9 7 -3 4.30 4.90 9 7 -3 6.10 5.20 9 7 -3 9.80 5.50 9 7 -3 10.10 6.20 9 7 -3 8.40 5.70 9 7 -3 5.50 3.70 -9 -7 3 -0.10 3.80 -9 -7 3 12.90 6.50 -9 -7 3 8.80 6.70 -9 -7 3 6.00 4.10 -9 -7 3 16.40 7.40 8 7 -3 20.60 6.80 8 7 -3 30.90 8.80 8 7 -3 23.80 6.00 8 7 -3 29.40 7.20 8 7 -3 20.60 7.20 8 7 -3 21.00 4.00 -8 -7 3 25.80 6.20 -8 -7 3 26.00 8.30 -8 -7 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57.29 11.60 7 12 -4 58.79 12.10 7 12 -4 51.49 10.70 7 12 -4 78.99 12.50 -7 -12 4 66.49 13.60 -7 -12 4 30.00 7.30 -7 -12 4 58.29 12.20 6 12 -4 -1.30 5.60 6 12 -4 -2.30 3.60 6 12 -4 -1.20 5.30 6 12 -4 4.20 6.80 -6 -12 4 0.50 5.60 -6 -12 4 4.10 4.70 -6 -12 4 4.70 5.40 5 12 -4 32.20 9.90 5 12 -4 34.10 9.60 5 12 -4 31.00 8.60 5 12 -4 28.70 9.70 -5 -12 4 21.70 8.70 -5 -12 4 39.20 10.20 -5 -12 4 38.50 8.10 4 12 -4 79.09 12.90 4 12 -4 60.09 11.80 4 12 -4 59.49 10.70 4 12 -4 50.09 12.50 -4 -12 4 68.69 14.10 -4 -12 4 85.49 16.00 -4 -12 4 53.29 12.60 -4 -12 4 60.79 10.10 -4 -12 4 82.89 13.90 3 12 -4 19.20 6.20 3 12 -4 25.90 9.90 3 12 -4 25.10 6.00 -3 -12 4 36.80 9.40 -3 -12 4 20.80 6.60 -3 -12 4 28.20 8.60 -3 -12 4 19.00 8.00 -3 -12 4 30.30 8.80 2 12 -4 13.90 5.60 2 12 -4 1.90 6.60 2 12 -4 14.80 5.50 2 12 -4 31.00 9.30 -2 -12 4 7.30 7.80 -2 -12 4 11.00 6.70 -2 -12 4 24.80 7.90 -2 -12 4 11.10 6.20 1 12 -4 7.10 4.70 1 12 -4 1.30 5.70 1 12 -4 -1.60 6.90 -1 -12 4 8.20 5.50 -1 -12 4 -3.90 5.40 -1 -12 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1.90 5.60 -8 -11 4 3.30 5.60 7 11 -4 2.80 6.00 7 11 -4 6.00 5.80 7 11 -4 5.20 5.90 -7 -11 4 16.30 6.70 -7 -11 4 7.80 5.20 -7 -11 4 12.90 11.20 6 11 -4 0.10 4.90 6 11 -4 10.70 6.00 6 11 -4 -3.90 4.20 6 11 -4 -2.30 5.30 -6 -11 4 0.40 3.80 -6 -11 4 8.50 5.60 -6 -11 4 0.90 5.40 5 11 -4 35.50 9.60 5 11 -4 49.30 10.60 5 11 -4 24.20 7.80 5 11 -4 38.10 10.50 -5 -11 4 26.20 8.90 -5 -11 4 38.50 9.80 -5 -11 4 27.80 7.20 4 11 -4 51.49 10.50 4 11 -4 35.30 10.40 4 11 -4 38.40 10.40 4 11 -4 40.70 6.50 -4 -11 4 40.70 8.40 -4 -11 4 56.79 10.70 -4 -11 4 51.79 10.40 -4 -11 4 38.70 10.50 3 11 -4 91.09 14.20 3 11 -4 107.29 11.90 3 11 -4 98.79 12.00 3 11 -4 97.79 16.20 -3 -11 4 91.99 14.80 -3 -11 4 101.29 14.40 -3 -11 4 82.79 13.40 -3 -11 4 120.09 13.30 2 11 -4 34.60 9.50 2 11 -4 42.20 10.60 2 11 -4 34.70 10.70 2 11 -4 34.30 6.90 -2 -11 4 52.19 10.40 -2 -11 4 28.20 9.00 -2 -11 4 40.00 9.40 -2 -11 4 37.20 9.50 1 11 -4 -0.50 5.40 1 11 -4 10.40 5.10 1 11 -4 1.80 3.50 1 11 -4 1.90 5.90 -1 -11 4 5.80 4.50 -1 -11 4 8.50 6.30 -1 -11 4 9.00 6.10 -1 -11 4 4.00 5.50 0 11 -4 3.60 5.30 0 11 -4 -1.70 3.30 0 11 -4 4.80 6.10 0 11 -4 -3.10 3.70 0 -11 4 7.90 6.70 0 -11 4 -0.60 4.90 0 -11 4 3.70 4.20 -1 11 -4 27.60 6.70 -1 11 -4 39.80 11.40 -1 11 -4 29.20 8.40 -1 11 -4 25.10 8.30 1 -11 4 35.00 7.50 1 -11 4 32.30 9.00 1 -11 4 37.00 6.90 1 -11 4 30.10 9.10 1 -11 4 42.70 11.00 -2 11 -4 5.30 7.50 -2 11 -4 12.00 6.90 2 -11 4 8.30 4.10 2 -11 4 10.30 6.50 2 -11 4 17.90 5.80 2 -11 4 7.00 5.50 2 -11 4 10.50 6.20 -3 11 -4 -1.20 8.30 -3 11 -4 18.00 7.20 -3 11 -4 2.30 6.90 -3 11 -4 8.40 6.20 3 -11 4 8.70 6.80 3 -11 4 7.70 6.80 3 -11 4 14.50 8.20 3 -11 4 14.00 4.30 3 -11 4 12.50 5.20 -4 11 -4 6.00 7.70 -4 11 -4 1.90 7.70 -4 11 -4 -9.90 6.50 4 -11 4 7.50 6.80 4 -11 4 -8.60 5.70 4 -11 4 -2.90 7.30 11 10 -4 -4.60 6.00 11 10 -4 -9.60 7.20 11 10 -4 -3.00 5.30 11 10 -4 1.00 4.50 11 10 -4 -7.10 7.90 -11 -10 4 -6.70 7.80 -11 -10 4 8.50 6.40 -11 -10 4 6.90 6.50 -11 -10 4 6.10 5.40 10 10 -4 -2.70 7.00 10 10 -4 11.70 6.20 10 10 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0.40 4.50 -3 10 -4 50.09 10.20 -3 10 -4 24.10 7.90 -3 10 -4 27.00 9.80 3 -10 4 34.40 9.40 3 -10 4 42.70 10.30 3 -10 4 38.60 11.30 3 -10 4 33.10 5.80 3 -10 4 32.50 7.30 -4 10 -4 5.90 8.90 -4 10 -4 12.60 6.50 -4 10 -4 -3.80 4.90 4 -10 4 10.20 6.40 4 -10 4 14.30 6.40 4 -10 4 10.70 6.60 -5 10 -4 13.20 8.90 -5 10 -4 1.50 6.60 -5 10 -4 3.20 6.60 5 -10 4 2.30 5.60 5 -10 4 12.10 6.70 5 -10 4 -3.00 4.50 5 -10 4 8.20 7.00 6 -10 4 -4.10 7.10 11 9 -4 4.80 7.70 11 9 -4 13.80 10.20 11 9 -4 18.70 8.20 11 9 -4 5.50 6.80 11 9 -4 5.30 4.40 -11 -9 4 10.40 5.50 -11 -9 4 12.10 8.80 -11 -9 4 20.00 11.00 -11 -9 4 16.60 7.20 10 9 -4 5.10 6.00 10 9 -4 7.30 7.20 10 9 -4 19.50 7.30 10 9 -4 0.50 4.30 10 9 -4 9.80 6.80 -10 -9 4 7.10 5.70 -10 -9 4 11.50 7.70 -10 -9 4 20.10 9.90 -10 -9 4 6.60 5.60 -10 -9 4 2.70 7.40 9 9 -4 124.39 17.10 9 9 -4 90.99 13.70 9 9 -4 88.59 16.10 9 9 -4 121.99 12.10 9 9 -4 101.59 18.70 -9 -9 4 110.29 16.90 -9 -9 4 122.49 11.90 -9 -9 4 80.29 12.10 8 9 -4 13.40 8.10 8 9 -4 10.00 5.70 8 9 -4 17.70 6.10 8 9 -4 22.20 6.80 8 9 -4 5.80 6.10 -8 -9 4 10.40 7.00 -8 -9 4 15.20 5.00 -8 -9 4 5.70 5.60 7 9 -4 57.49 11.60 7 9 -4 49.20 8.80 7 9 -4 48.60 9.30 -7 -9 4 45.90 10.50 -7 -9 4 42.10 10.70 -7 -9 4 46.10 7.70 6 9 -4 6.80 5.80 6 9 -4 4.00 6.40 6 9 -4 4.00 3.60 6 9 -4 14.70 6.70 6 9 -4 8.80 5.20 -6 -9 4 0.90 3.50 -6 -9 4 9.40 6.10 -6 -9 4 3.30 5.30 5 9 -4 146.89 15.90 5 9 -4 153.98 16.60 5 9 -4 151.78 15.90 -5 -9 4 133.79 15.00 -5 -9 4 162.58 14.90 -5 -9 4 153.38 12.40 4 9 -4 27.50 5.40 4 9 -4 31.20 8.80 4 9 -4 19.60 7.70 4 9 -4 22.10 7.10 -4 -9 4 19.20 6.30 -4 -9 4 28.80 7.70 -4 -9 4 29.60 8.50 -4 -9 4 7.80 4.60 3 9 -4 9.30 5.00 3 9 -4 11.80 5.80 3 9 -4 6.60 5.90 3 9 -4 9.30 3.40 3 9 -4 6.50 3.40 -3 -9 4 3.70 4.30 -3 -9 4 6.90 5.80 -3 -9 4 7.10 4.70 2 9 -4 2.70 4.00 2 9 -4 4.80 3.20 2 9 -4 3.10 3.60 2 9 -4 -0.20 4.70 2 9 -4 3.90 5.00 -2 -9 4 6.60 4.10 -2 -9 4 9.50 5.40 -2 -9 4 4.80 4.50 -2 -9 4 4.00 4.80 1 9 -4 29.70 7.20 1 9 -4 26.20 4.90 1 9 -4 17.30 5.30 1 9 -4 22.50 7.60 1 9 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19.70 6.80 -4 -6 8 30.00 7.70 -4 -6 8 22.40 3.70 -4 -6 8 31.30 7.80 3 6 -8 149.39 15.50 3 6 -8 138.79 14.00 3 6 -8 140.69 11.50 3 6 -8 167.38 15.10 3 6 -8 151.58 12.80 -3 -6 8 160.38 13.00 -3 -6 8 156.58 12.00 -3 -6 8 182.78 14.50 -3 -6 8 172.58 9.30 2 6 -8 146.89 7.90 2 6 -8 154.78 12.40 2 6 -8 145.09 12.60 2 6 -8 152.98 14.30 2 6 -8 158.68 15.60 2 6 -8 156.18 14.50 -2 -6 8 133.29 11.70 -2 -6 8 176.48 14.20 -2 -6 8 142.69 7.00 -2 -6 8 156.98 11.20 -2 -6 8 151.48 9.10 1 6 -8 85.09 12.50 1 6 -8 82.39 12.00 1 6 -8 91.29 8.00 1 6 -8 84.39 8.90 1 6 -8 105.29 13.70 1 6 -8 85.69 8.30 1 6 -8 90.49 7.30 -1 -6 8 88.99 9.00 -1 -6 8 92.39 10.60 -1 -6 8 105.09 8.50 -1 -6 8 64.69 9.60 -1 -6 8 92.79 6.70 -1 -6 8 80.79 10.60 0 6 -8 74.29 7.70 0 6 -8 71.59 11.40 0 6 -8 64.29 10.60 0 6 -8 69.59 10.90 0 -6 8 65.49 9.70 0 -6 8 70.39 7.00 0 -6 8 74.19 9.60 0 -6 8 83.39 10.70 0 -6 8 59.89 9.70 0 -6 8 69.69 6.30 -1 6 -8 190.18 16.20 -1 6 -8 165.18 15.50 1 -6 8 176.18 12.80 1 -6 8 183.78 14.00 1 -6 8 163.78 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5 -8 43.30 10.90 -6 5 -8 47.90 9.90 6 -5 8 54.49 11.30 6 -5 8 27.70 5.40 6 -5 8 25.80 8.90 6 -5 8 49.00 8.80 6 -5 8 22.30 5.80 -7 5 -8 76.19 3.90 -7 5 -8 68.79 14.00 -7 5 -8 56.39 11.10 7 -5 8 59.29 9.60 7 -5 8 69.29 12.40 7 -5 8 63.49 13.00 7 -5 8 44.90 6.90 -8 5 -8 6.50 7.20 -8 5 -8 -2.90 5.00 8 -5 8 12.50 7.10 8 -5 8 11.00 5.50 8 -5 8 6.80 6.90 11 4 -8 -5.40 3.40 11 4 -8 7.70 7.50 11 4 -8 8.80 4.10 11 4 -8 -6.60 4.20 11 4 -8 0.60 5.80 -11 -4 8 -6.60 5.20 -11 -4 8 3.80 7.30 -11 -4 8 -10.60 4.10 -11 -4 8 -2.80 4.20 -11 -4 8 -0.70 8.30 -11 -4 8 -2.90 5.30 10 4 -8 26.50 8.10 10 4 -8 15.20 8.30 10 4 -8 5.00 6.10 10 4 -8 25.90 7.60 10 4 -8 19.60 4.20 -10 -4 8 6.80 4.90 -10 -4 8 22.10 6.80 -10 -4 8 19.40 6.30 -10 -4 8 18.20 7.50 -10 -4 8 31.20 8.00 -10 -4 8 7.40 9.80 9 4 -8 13.00 10.20 9 4 -8 13.10 3.60 9 4 -8 21.30 6.30 9 4 -8 15.50 2.80 9 4 -8 8.10 5.30 -9 -4 8 16.60 7.00 -9 -4 8 12.70 4.00 -9 -4 8 14.10 6.20 -9 -4 8 17.90 5.70 -9 -4 8 8.00 5.80 -9 -4 8 13.90 7.80 8 4 -8 15.40 3.20 8 4 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6 -4 8 11.60 5.00 6 -4 8 5.00 3.30 6 -4 8 4.70 3.80 -7 4 -8 84.79 12.80 -7 4 -8 80.39 8.70 -7 4 -8 90.69 14.40 7 -4 8 89.59 8.40 7 -4 8 91.59 10.00 7 -4 8 94.19 14.00 7 -4 8 99.29 15.00 -8 4 -8 43.00 9.50 -8 4 -8 39.40 8.00 -8 4 -8 55.69 12.80 8 -4 8 51.19 11.80 8 -4 8 33.30 9.30 8 -4 8 39.10 7.80 -9 4 -8 19.80 10.10 -9 4 -8 13.50 6.30 9 -4 8 -3.90 6.00 9 -4 8 21.80 6.20 9 -4 8 14.00 7.10 11 3 -8 14.30 8.10 11 3 -8 4.50 4.90 11 3 -8 11.40 7.80 11 3 -8 7.80 3.50 11 3 -8 19.60 9.30 -11 -3 8 15.80 6.20 -11 -3 8 4.60 8.40 -11 -3 8 21.50 10.70 -11 -3 8 6.80 6.60 10 3 -8 -4.80 3.00 10 3 -8 3.90 6.30 10 3 -8 -7.60 2.60 10 3 -8 2.30 3.90 10 3 -8 0.70 5.10 -10 -3 8 1.40 8.20 -10 -3 8 0.10 3.90 -10 -3 8 -2.10 4.50 -10 -3 8 1.40 4.10 -10 -3 8 -0.30 3.90 9 3 -8 21.70 8.40 9 3 -8 17.50 4.30 9 3 -8 20.30 7.40 9 3 -8 14.30 5.20 9 3 -8 14.90 5.90 -9 -3 8 22.30 7.60 -9 -3 8 24.90 5.70 -9 -3 8 13.30 5.60 -9 -3 8 16.50 12.00 -9 -3 8 10.60 5.20 -9 -3 8 22.10 6.40 8 3 -8 6.00 5.50 8 3 -8 -2.10 2.00 8 3 -8 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19.30 8.90 -6 -9 9 27.30 8.30 -6 -9 9 25.10 7.60 -6 -9 9 18.40 4.30 5 9 -9 0.00 5.60 5 9 -9 13.80 8.20 5 9 -9 1.30 6.30 -5 -9 9 11.70 6.20 -5 -9 9 6.60 3.20 -5 -9 9 4.60 5.50 -5 -9 9 7.10 5.10 4 9 -9 16.00 7.80 4 9 -9 1.30 5.50 4 9 -9 18.70 7.30 -4 -9 9 12.40 6.70 -4 -9 9 5.00 5.80 -4 -9 9 9.00 3.40 -4 -9 9 13.70 6.10 3 9 -9 22.70 9.40 3 9 -9 35.00 10.50 3 9 -9 21.00 8.50 -3 -9 9 32.80 9.30 -3 -9 9 15.00 5.90 -3 -9 9 14.30 4.40 -3 -9 9 14.90 7.10 2 9 -9 63.49 13.30 2 9 -9 54.09 12.20 2 9 -9 57.59 5.90 2 9 -9 66.49 13.10 -2 -9 9 61.59 11.80 -2 -9 9 56.69 7.30 -2 -9 9 61.99 11.20 -2 -9 9 53.69 11.10 -2 -9 9 73.39 10.50 1 9 -9 201.38 20.00 1 9 -9 211.88 14.50 1 9 -9 210.98 20.30 1 9 -9 236.38 21.30 -1 -9 9 224.28 17.50 -1 -9 9 241.98 20.40 -1 -9 9 213.58 15.70 -1 -9 9 225.18 18.70 0 9 -9 6.00 6.20 0 9 -9 18.20 8.70 0 9 -9 11.90 4.80 0 9 -9 13.70 7.00 0 -9 9 13.50 4.80 0 -9 9 4.80 5.20 0 -9 9 13.80 6.10 0 -9 9 20.30 7.40 0 -9 9 13.10 5.60 -1 9 -9 40.90 10.10 -1 9 -9 39.70 11.00 -1 9 -9 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3 -8 9 82.09 12.80 3 -8 9 62.39 9.00 3 -8 9 67.49 11.80 -4 8 -9 0.10 5.90 -4 8 -9 8.80 7.30 -4 8 -9 5.60 6.90 4 -8 9 15.20 6.60 4 -8 9 -0.90 4.70 4 -8 9 10.10 7.00 4 -8 9 4.20 4.20 4 -8 9 6.90 4.10 -5 8 -9 49.20 18.20 -5 8 -9 50.19 13.50 -5 8 -9 32.50 10.30 5 -8 9 35.60 6.50 5 -8 9 42.70 10.30 5 -8 9 67.19 11.70 5 -8 9 52.69 12.60 5 -8 9 45.80 8.70 -6 8 -9 5.50 8.80 -6 8 -9 -9.60 5.90 -6 8 -9 10.30 5.90 6 -8 9 9.50 8.20 6 -8 9 -7.00 4.50 6 -8 9 -2.50 4.60 6 -8 9 -1.80 5.80 6 -8 9 -4.40 3.00 11 7 -9 8.00 6.00 11 7 -9 12.70 7.80 -11 -7 9 5.20 7.30 -11 -7 9 17.70 10.80 -11 -7 9 10.20 9.10 -11 -7 9 4.90 5.60 -11 -7 9 -3.10 5.90 10 7 -9 6.00 3.80 10 7 -9 18.00 9.40 10 7 -9 21.00 8.30 10 7 -9 9.20 7.80 10 7 -9 7.70 6.80 -10 -7 9 -1.10 7.60 -10 -7 9 13.20 5.40 -10 -7 9 7.90 6.60 -10 -7 9 30.90 9.40 -10 -7 9 32.90 10.30 9 7 -9 100.39 16.40 9 7 -9 100.19 18.40 9 7 -9 89.09 13.40 9 7 -9 94.89 9.80 9 7 -9 125.09 16.60 -9 -7 9 97.29 14.90 -9 -7 9 102.49 10.30 -9 -7 9 135.69 23.00 -9 -7 9 81.99 13.60 -9 -7 9 99.79 15.90 8 7 -9 -5.80 2.80 8 7 -9 6.20 5.30 -8 -7 9 9.00 6.80 -8 -7 9 0.10 2.80 -8 -7 9 -5.20 4.50 -8 -7 9 -5.50 2.40 7 7 -9 72.99 14.40 7 7 -9 54.09 8.70 7 7 -9 67.99 13.40 7 7 -9 67.19 12.80 -7 -7 9 64.79 6.80 -7 -7 9 56.99 10.80 -7 -7 9 46.10 10.80 -7 -7 9 46.30 12.40 -7 -7 9 58.99 11.40 -7 -7 9 53.79 11.00 6 7 -9 22.40 8.60 6 7 -9 35.90 9.60 6 7 -9 44.30 10.60 -6 -7 9 31.50 8.60 -6 -7 9 24.40 7.30 -6 -7 9 27.10 4.70 -6 -7 9 29.90 8.50 5 7 -9 135.99 15.20 5 7 -9 117.79 17.20 5 7 -9 104.99 15.30 -5 -7 9 102.69 14.10 -5 -7 9 109.09 7.70 -5 -7 9 121.39 12.60 -5 -7 9 102.19 14.80 4 7 -9 29.90 8.80 4 7 -9 27.30 8.40 4 7 -9 22.00 8.40 -4 -7 9 32.20 4.30 -4 -7 9 36.40 9.00 -4 -7 9 32.30 8.30 -4 -7 9 32.20 7.40 3 7 -9 261.27 21.20 3 7 -9 268.77 22.70 3 7 -9 295.77 22.30 -3 -7 9 302.07 19.80 -3 -7 9 282.47 14.00 -3 -7 9 270.67 17.70 -3 -7 9 284.47 20.10 2 7 -9 30.70 6.30 2 7 -9 44.10 10.10 2 7 -9 39.50 9.70 2 7 -9 43.00 4.00 2 7 -9 36.40 9.60 -2 -7 9 47.10 7.50 -2 -7 9 47.00 6.00 -2 -7 9 42.80 5.60 -2 -7 9 41.80 8.90 -2 -7 9 50.89 9.80 -2 -7 9 44.10 4.70 1 7 -9 11.90 6.60 1 7 -9 11.80 6.50 1 7 -9 14.90 7.40 1 7 -9 13.90 3.70 -1 -7 9 12.70 6.00 -1 -7 9 18.70 6.40 -1 -7 9 18.60 3.80 -1 -7 9 24.60 7.20 -1 -7 9 18.70 7.30 -1 -7 9 16.10 4.90 0 7 -9 159.18 16.60 0 7 -9 168.08 16.40 0 7 -9 155.38 12.20 0 7 -9 142.59 15.40 0 -7 9 157.88 13.40 0 -7 9 156.78 11.30 0 -7 9 172.08 14.20 0 -7 9 143.79 14.70 0 -7 9 141.29 13.30 -1 7 -9 52.69 11.00 -1 7 -9 44.60 8.30 -1 7 -9 44.70 10.30 1 -7 9 52.89 9.30 1 -7 9 39.60 6.40 1 -7 9 44.00 6.90 1 -7 9 40.50 8.10 1 -7 9 54.39 10.50 1 -7 9 58.39 9.90 -2 7 -9 126.99 14.60 -2 7 -9 135.59 17.70 2 -7 9 99.39 10.10 2 -7 9 104.29 13.70 2 -7 9 114.39 9.60 2 -7 9 143.79 15.30 2 -7 9 123.19 12.60 -3 7 -9 33.40 9.30 -3 7 -9 27.30 8.80 3 -7 9 43.60 9.30 3 -7 9 37.90 7.30 3 -7 9 30.20 5.90 3 -7 9 45.00 10.70 3 -7 9 47.70 9.40 -4 7 -9 7.00 7.10 -4 7 -9 3.20 4.70 4 -7 9 9.40 4.90 4 -7 9 -3.30 4.10 4 -7 9 1.70 4.90 4 -7 9 6.60 3.50 -5 7 -9 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15.70 -8 -7 10 99.29 14.80 -8 -7 10 55.99 13.90 -8 -7 10 61.69 12.20 7 7 -10 14.30 6.60 7 7 -10 14.50 6.80 7 7 -10 16.00 8.90 -7 -7 10 11.50 6.50 -7 -7 10 6.20 5.40 -7 -7 10 8.30 3.30 -7 -7 10 13.20 7.10 -7 -7 10 12.10 6.00 6 7 -10 -3.10 4.90 6 7 -10 1.20 5.10 6 7 -10 1.10 5.90 -6 -7 10 2.10 4.90 -6 -7 10 1.00 2.10 -6 -7 10 -0.50 5.20 -6 -7 10 -1.50 5.10 -6 -7 10 -2.90 4.50 5 7 -10 -1.20 4.80 5 7 -10 0.20 5.80 5 7 -10 4.80 4.90 -5 -7 10 -2.10 4.70 -5 -7 10 11.50 5.90 -5 -7 10 4.10 2.00 -5 -7 10 2.80 4.20 4 7 -10 189.68 18.20 4 7 -10 161.08 16.90 4 7 -10 174.78 19.00 -4 -7 10 175.38 15.70 -4 -7 10 180.38 16.50 -4 -7 10 184.28 14.60 -4 -7 10 177.68 9.30 3 7 -10 94.69 14.20 3 7 -10 96.89 14.50 3 7 -10 98.19 15.40 -3 -7 10 72.79 11.30 -3 -7 10 111.99 14.70 -3 -7 10 120.39 11.20 -3 -7 10 94.09 6.40 2 7 -10 342.27 24.40 2 7 -10 359.46 26.20 2 7 -10 273.87 18.00 2 7 -10 341.27 24.40 -2 -7 10 377.76 23.60 -2 -7 10 351.06 15.90 -2 -7 10 317.07 20.60 -2 -7 10 314.97 15.10 -2 -7 10 331.07 19.00 1 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-7 -6 10 23.50 4.60 -7 -6 10 33.20 9.30 -7 -6 10 31.80 10.80 6 6 -10 57.69 11.50 6 6 -10 38.40 11.00 -6 -6 10 64.79 5.70 -6 -6 10 50.29 10.10 -6 -6 10 43.00 9.80 -6 -6 10 46.60 10.50 -6 -6 10 59.49 12.90 5 6 -10 22.60 8.50 5 6 -10 33.20 9.50 5 6 -10 32.70 10.00 -5 -6 10 38.20 9.90 -5 -6 10 43.20 8.50 -5 -6 10 35.30 4.10 -5 -6 10 27.00 7.80 4 6 -10 426.06 26.90 4 6 -10 394.46 26.00 4 6 -10 391.36 28.90 -4 -6 10 442.16 23.70 -4 -6 10 406.36 24.30 -4 -6 10 382.26 16.40 -4 -6 10 405.86 24.70 3 6 -10 298.57 21.40 3 6 -10 245.68 21.80 3 6 -10 254.17 19.80 3 6 -10 226.88 15.30 -3 -6 10 246.38 10.90 -3 -6 10 225.18 16.70 -3 -6 10 259.47 16.20 -3 -6 10 245.08 18.00 2 6 -10 202.68 19.00 2 6 -10 201.58 17.20 2 6 -10 195.68 17.30 -2 -6 10 173.48 14.40 -2 -6 10 206.78 15.90 -2 -6 10 172.38 9.10 -2 -6 10 190.08 12.80 -2 -6 10 180.98 9.30 1 6 -10 12.50 6.30 1 6 -10 7.50 5.50 1 6 -10 10.20 5.90 1 6 -10 8.10 2.80 1 6 -10 3.40 2.90 -1 -6 10 10.10 2.70 -1 -6 10 11.20 3.60 -1 -6 10 6.70 5.20 -1 -6 10 7.90 4.50 -1 -6 10 9.40 5.20 -1 -6 10 11.40 2.70 0 6 -10 22.10 7.90 0 6 -10 24.30 7.90 0 6 -10 6.20 5.90 0 -6 10 22.20 4.00 0 -6 10 22.90 6.80 0 -6 10 13.20 5.40 0 -6 10 19.60 6.40 0 -6 10 24.20 6.80 0 -6 10 24.90 4.60 -1 6 -10 100.69 14.20 -1 6 -10 84.59 13.40 1 -6 10 65.19 10.70 1 -6 10 94.59 13.00 1 -6 10 75.69 10.50 1 -6 10 93.19 7.40 1 -6 10 68.29 6.90 1 -6 10 105.29 12.60 -2 6 -10 115.09 15.70 -2 6 -10 138.69 14.70 2 -6 10 107.09 8.30 2 -6 10 123.39 11.80 2 -6 10 105.59 14.10 2 -6 10 104.49 10.40 2 -6 10 91.39 12.60 -3 6 -10 -0.50 5.40 -3 6 -10 0.10 3.70 3 -6 10 13.00 5.70 3 -6 10 -1.10 3.30 3 -6 10 1.00 1.90 3 -6 10 2.00 3.90 3 -6 10 9.40 5.80 -4 6 -10 -5.20 3.60 -4 6 -10 1.80 5.00 4 -6 10 5.50 4.00 4 -6 10 0.60 4.40 4 -6 10 -3.20 3.50 4 -6 10 1.60 2.70 4 -6 10 -0.90 3.40 -5 6 -10 41.80 9.80 -5 6 -10 25.30 9.20 5 -6 10 16.60 4.50 5 -6 10 27.20 6.40 5 -6 10 21.90 6.90 5 -6 10 25.00 7.30 5 -6 10 36.20 9.20 -6 6 -10 51.69 12.50 -6 6 -10 51.59 11.30 6 -6 10 40.10 10.00 6 -6 10 56.79 9.90 6 -6 10 39.20 7.10 6 -6 10 44.90 10.40 6 -6 10 51.99 12.50 -7 6 -10 -0.90 5.70 -7 6 -10 7.30 8.00 7 -6 10 6.90 6.60 7 -6 10 -8.70 3.60 7 -6 10 -7.00 4.50 7 -6 10 -7.50 3.00 -8 6 -10 12.10 9.90 -8 6 -10 28.90 9.80 8 -6 10 14.80 7.80 8 -6 10 10.40 8.60 8 -6 10 -4.50 5.70 11 5 -10 -2.40 5.20 11 5 -10 -13.10 5.10 11 5 -10 5.70 9.60 11 5 -10 -7.50 4.20 -11 -5 10 8.30 7.70 -11 -5 10 -8.50 7.20 -11 -5 10 0.60 5.10 -11 -5 10 -6.80 5.60 10 5 -10 -3.70 4.50 10 5 -10 9.20 7.80 10 5 -10 8.30 6.20 10 5 -10 3.70 7.80 -10 -5 10 6.10 5.20 -10 -5 10 1.90 7.20 -10 -5 10 6.00 5.80 -10 -5 10 -4.10 6.60 9 5 -10 8.50 5.90 9 5 -10 8.10 6.80 9 5 -10 5.40 7.10 9 5 -10 9.10 2.70 -9 -5 10 6.10 4.00 -9 -5 10 17.60 10.70 -9 -5 10 15.60 6.70 -9 -5 10 12.50 6.60 -9 -5 10 5.10 6.10 8 5 -10 2.80 2.60 8 5 -10 4.20 4.00 8 5 -10 -4.60 4.80 8 5 -10 1.60 3.90 -8 -5 10 -0.80 5.30 -8 -5 10 -5.60 3.10 -8 -5 10 1.10 3.00 -8 -5 10 1.10 5.90 -8 -5 10 -0.10 4.30 7 5 -10 12.40 4.10 7 5 -10 22.60 8.90 7 5 -10 18.50 7.00 7 5 -10 10.70 6.80 7 5 -10 6.40 5.20 -7 -5 10 5.80 3.00 -7 -5 10 -0.30 4.40 -7 -5 10 7.90 8.60 -7 -5 10 5.40 5.60 -7 -5 10 10.40 6.20 6 5 -10 129.09 13.80 6 5 -10 138.79 15.00 6 5 -10 129.59 18.80 -6 -5 10 144.29 15.20 -6 -5 10 144.99 13.80 -6 -5 10 131.39 15.00 -6 -5 10 130.99 12.80 -6 -5 10 130.69 8.60 5 5 -10 239.18 19.40 5 5 -10 270.07 23.30 5 5 -10 259.47 19.90 -5 -5 10 248.58 12.10 -5 -5 10 265.57 20.50 -5 -5 10 287.87 21.20 -5 -5 10 255.67 18.20 -5 -5 10 287.57 19.20 4 5 -10 296.17 20.50 4 5 -10 222.78 17.20 4 5 -10 242.38 22.00 4 5 -10 270.17 20.10 -4 -5 10 279.27 11.80 -4 -5 10 271.67 18.50 -4 -5 10 290.97 18.50 -4 -5 10 286.87 19.40 3 5 -10 13.10 6.00 3 5 -10 9.00 3.90 3 5 -10 13.90 6.30 3 5 -10 5.40 5.40 3 5 -10 10.10 3.60 -3 -5 10 18.70 5.10 -3 -5 10 7.30 5.10 -3 -5 10 11.20 1.40 -3 -5 10 7.90 4.80 2 5 -10 304.17 21.10 2 5 -10 289.77 16.40 2 5 -10 334.97 23.90 2 5 -10 298.27 20.40 -2 -5 10 292.67 11.90 -2 -5 10 316.07 19.00 -2 -5 10 295.47 12.00 -2 -5 10 336.57 19.80 -2 -5 10 322.57 17.00 1 5 -10 14.80 2.90 1 5 -10 20.20 6.30 1 5 -10 6.20 4.90 1 5 -10 17.30 5.20 1 5 -10 15.00 3.80 1 5 -10 15.40 6.20 -1 -5 10 19.50 2.80 -1 -5 10 16.30 3.90 -1 -5 10 5.50 4.60 -1 -5 10 16.40 2.50 -1 -5 10 12.80 4.70 -1 -5 10 13.20 5.20 0 5 -10 14.50 6.10 0 5 -10 10.30 4.00 0 5 -10 8.00 5.90 0 -5 10 18.40 5.60 0 -5 10 12.10 5.30 0 -5 10 17.20 5.90 0 -5 10 15.50 5.30 0 -5 10 12.50 3.00 0 -5 10 13.90 3.30 -1 5 -10 3.00 4.80 -1 5 -10 -5.60 2.60 -1 5 -10 -1.70 3.50 1 -5 10 -4.10 1.60 1 -5 10 2.90 4.00 1 -5 10 1.10 3.30 1 -5 10 2.30 3.80 1 -5 10 -0.10 1.40 1 -5 10 2.20 3.30 -2 5 -10 365.76 23.10 -2 5 -10 329.17 22.60 2 -5 10 324.47 19.50 2 -5 10 339.17 19.30 2 -5 10 308.47 20.60 2 -5 10 324.77 15.40 2 -5 10 322.17 16.80 2 -5 10 357.66 21.70 -3 5 -10 158.38 15.40 -3 5 -10 151.68 15.40 3 -5 10 144.19 13.50 3 -5 10 144.39 12.20 3 -5 10 130.49 11.30 3 -5 10 133.59 13.60 3 -5 10 142.09 8.80 -4 5 -10 68.39 11.80 -4 5 -10 97.99 14.10 4 -5 10 96.69 13.00 4 -5 10 81.39 12.20 4 -5 10 87.29 9.20 4 -5 10 97.29 10.20 4 -5 10 84.49 7.10 -5 5 -10 -0.10 5.30 -5 5 -10 11.50 6.50 5 -5 10 5.70 3.20 5 -5 10 9.10 4.60 5 -5 10 -2.10 3.60 5 -5 10 6.30 6.00 5 -5 10 7.40 4.30 5 -5 10 5.50 3.30 -6 5 -10 100.79 15.10 6 -5 10 102.89 9.70 6 -5 10 98.89 11.10 6 -5 10 122.29 16.20 6 -5 10 99.29 15.30 6 -5 10 97.39 8.80 -7 5 -10 13.10 7.10 -7 5 -10 18.90 8.30 7 -5 10 14.30 5.00 7 -5 10 17.20 7.70 7 -5 10 19.80 5.60 7 -5 10 20.30 5.60 -8 5 -10 26.40 9.00 -8 5 -10 16.20 9.70 8 -5 10 26.10 8.70 8 -5 10 10.70 5.40 8 -5 10 11.90 5.80 8 -5 10 12.40 7.20 8 -5 10 16.30 8.10 -9 5 -10 3.40 8.30 -9 5 -10 -4.50 7.20 9 -5 10 -8.80 5.40 9 -5 10 -5.30 6.00 9 -5 10 4.60 5.40 9 -5 10 -7.00 6.80 11 4 -10 0.80 5.20 11 4 -10 5.30 5.60 11 4 -10 8.80 6.70 11 4 -10 -8.00 7.30 -11 -4 10 3.00 7.80 -11 -4 10 -4.90 7.70 -11 -4 10 9.00 6.40 10 4 -10 10.60 7.20 10 4 -10 4.40 6.60 10 4 -10 11.80 5.90 10 4 -10 5.20 6.40 -10 -4 10 4.10 6.70 -10 -4 10 12.10 6.50 -10 -4 10 3.30 5.20 -10 -4 10 10.00 10.80 9 4 -10 5.80 5.00 9 4 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5.00 -4 -4 10 6.50 4.90 3 4 -10 48.80 10.00 3 4 -10 39.30 9.30 3 4 -10 45.40 7.60 3 4 -10 38.60 8.00 3 4 -10 43.50 6.50 -3 -4 10 38.90 7.30 -3 -4 10 57.29 9.60 -3 -4 10 59.69 8.50 -3 -4 10 44.90 6.90 2 4 -10 353.36 23.30 2 4 -10 304.67 16.30 2 4 -10 310.17 18.20 2 4 -10 293.57 25.20 2 4 -10 299.47 20.30 -2 -4 10 325.27 17.90 -2 -4 10 321.97 18.50 -2 -4 10 308.67 18.30 -2 -4 10 325.97 16.80 1 4 -10 111.59 11.20 1 4 -10 113.29 9.40 1 4 -10 110.59 7.90 1 4 -10 116.59 11.90 1 4 -10 134.89 11.70 1 4 -10 106.99 9.50 1 4 -10 108.09 13.00 -1 -4 10 119.79 10.50 -1 -4 10 114.49 6.10 -1 -4 10 104.69 10.30 -1 -4 10 133.29 10.90 -1 -4 10 113.59 8.00 -1 -4 10 117.49 5.00 -1 -4 10 111.49 5.10 -1 -4 10 113.69 10.90 0 4 -10 26.70 5.20 0 4 -10 39.50 9.20 0 4 -10 15.80 4.40 0 -4 10 40.20 7.20 0 -4 10 29.20 4.00 0 -4 10 27.10 4.00 0 -4 10 21.00 5.80 0 -4 10 25.60 6.30 0 -4 10 21.80 3.00 -1 4 -10 59.69 6.60 -1 4 -10 62.09 9.90 -1 4 -10 53.49 7.70 -1 4 -10 69.49 10.00 1 -4 10 58.79 8.10 1 -4 10 71.59 4.90 1 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8 -4 10 56.79 11.30 8 -4 10 45.00 8.10 8 -4 10 23.30 6.00 8 -4 10 43.20 10.00 8 -4 10 39.50 9.90 -9 4 -10 -8.20 5.40 -9 4 -10 -5.20 6.60 9 -4 10 -9.90 5.70 9 -4 10 11.00 7.90 9 -4 10 -5.50 5.00 9 -4 10 2.70 6.10 9 -4 10 -1.00 7.00 11 3 -10 -5.50 4.50 11 3 -10 10.00 7.10 11 3 -10 -11.70 6.20 11 3 -10 -8.60 5.30 -11 -3 10 -17.50 7.10 -11 -3 10 -9.70 5.60 -11 -3 10 9.30 9.70 10 3 -10 23.00 8.10 10 3 -10 2.50 3.10 10 3 -10 7.40 8.20 10 3 -10 1.30 4.90 10 3 -10 -0.40 4.00 -10 -3 10 9.90 6.30 -10 -3 10 2.10 4.70 -10 -3 10 6.70 5.00 -10 -3 10 17.40 10.70 9 3 -10 16.40 5.80 9 3 -10 15.40 6.10 9 3 -10 9.60 3.80 9 3 -10 11.60 5.80 9 3 -10 16.90 8.30 -9 -3 10 13.90 5.90 -9 -3 10 18.20 6.30 -9 -3 10 22.70 11.10 -9 -3 10 13.80 4.60 8 3 -10 47.30 2.50 8 3 -10 44.60 8.40 8 3 -10 69.49 14.00 8 3 -10 70.19 11.80 8 3 -10 52.89 4.90 -8 -3 10 56.09 13.10 -8 -3 10 60.49 10.00 -8 -3 10 60.09 10.70 -8 -3 10 39.50 5.40 -8 -3 10 60.09 11.00 7 3 -10 61.39 5.10 7 3 -10 54.89 4.20 7 3 -10 47.90 7.40 7 3 -10 58.49 9.00 7 3 -10 48.60 11.40 7 3 -10 50.59 10.40 -7 -3 10 59.09 10.10 -7 -3 10 78.79 15.30 -7 -3 10 50.89 4.90 -7 -3 10 54.39 10.50 -7 -3 10 62.29 7.60 -7 -3 10 58.79 9.40 6 3 -10 4.00 6.00 6 3 -10 8.60 2.90 6 3 -10 3.20 3.90 6 3 -10 19.20 6.90 6 3 -10 4.00 4.60 -6 -3 10 20.50 8.30 -6 -3 10 6.00 5.40 -6 -3 10 7.90 3.10 -6 -3 10 14.00 5.40 -6 -3 10 8.70 4.10 5 3 -10 30.70 6.80 5 3 -10 36.60 8.20 5 3 -10 32.10 4.30 5 3 -10 31.00 8.80 5 3 -10 24.60 6.70 -5 -3 10 34.90 4.40 -5 -3 10 32.50 7.80 -5 -3 10 38.30 7.70 -5 -3 10 42.30 9.90 -5 -3 10 45.90 8.30 -5 -3 10 25.20 7.30 4 3 -10 81.59 10.50 4 3 -10 113.89 11.30 4 3 -10 88.49 13.40 4 3 -10 100.79 9.10 4 3 -10 110.09 11.00 -4 -3 10 93.29 10.90 -4 -3 10 93.79 10.60 -4 -3 10 110.69 9.90 -4 -3 10 85.39 9.10 -4 -3 10 91.79 9.40 3 3 -10 356.26 21.30 3 3 -10 340.77 24.50 3 3 -10 356.26 19.80 3 3 -10 326.87 18.20 3 3 -10 380.06 21.20 -3 -3 10 345.57 19.10 -3 -3 10 385.96 19.70 -3 -3 10 372.06 21.20 -3 -3 10 356.46 22.40 -3 -3 10 372.36 20.20 -3 -3 10 387.66 20.20 2 3 -10 174.78 13.70 2 3 -10 169.78 11.80 2 3 -10 189.38 13.50 2 3 -10 146.99 11.10 2 3 -10 164.58 10.30 2 3 -10 171.88 12.40 2 3 -10 156.08 14.80 -2 -3 10 170.58 12.10 -2 -3 10 179.38 12.00 -2 -3 10 155.48 10.90 -2 -3 10 151.38 11.70 -2 -3 10 165.78 11.70 1 3 -10 1.90 2.00 1 3 -10 0.80 1.20 1 3 -10 -0.40 2.40 1 3 -10 2.70 3.90 1 3 -10 -1.10 2.50 1 3 -10 1.10 1.50 1 3 -10 1.00 2.20 -1 -3 10 -0.10 1.70 -1 -3 10 3.60 2.20 -1 -3 10 3.70 2.90 -1 -3 10 -2.60 1.60 -1 -3 10 -0.60 2.10 -1 -3 10 0.10 1.10 -1 -3 10 3.20 2.70 -1 -3 10 -2.30 2.50 0 3 -10 82.89 5.50 0 3 -10 92.49 8.00 0 3 -10 85.29 7.70 0 3 -10 93.79 8.30 0 3 -10 90.29 8.20 0 3 -10 106.79 9.80 0 3 -10 73.19 7.10 0 3 -10 90.69 10.20 0 -3 10 94.79 5.80 0 -3 10 87.99 4.70 0 -3 10 88.09 5.90 0 -3 10 84.09 9.10 0 -3 10 88.59 5.90 0 -3 10 85.49 8.10 0 -3 10 91.79 7.30 0 -3 10 84.99 8.30 0 -3 10 75.19 7.50 -1 3 -10 250.17 15.50 -1 3 -10 300.27 16.30 -1 3 -10 275.37 17.00 -1 3 -10 252.77 17.40 -1 3 -10 231.08 14.80 -1 3 -10 256.57 14.50 -1 3 -10 250.67 15.00 1 -3 10 267.17 11.00 1 -3 10 288.17 13.60 1 -3 10 264.87 12.40 1 -3 10 266.87 17.00 1 -3 10 277.57 15.70 1 -3 10 253.37 14.70 1 -3 10 285.67 16.10 1 -3 10 290.17 15.80 -2 3 -10 9.90 6.50 -2 3 -10 5.70 3.60 -2 3 -10 3.40 2.30 -2 3 -10 6.30 3.00 2 -3 10 3.70 4.00 2 -3 10 6.30 3.90 2 -3 10 6.70 3.20 2 -3 10 7.00 2.80 2 -3 10 1.20 3.20 2 -3 10 4.90 1.00 2 -3 10 5.50 2.90 -3 3 -10 6.30 4.10 -3 3 -10 3.60 2.30 -3 3 -10 8.10 4.00 -3 3 -10 6.80 4.50 3 -3 10 8.10 1.60 3 -3 10 2.40 3.50 3 -3 10 2.50 3.30 3 -3 10 2.70 2.50 3 -3 10 10.00 4.60 3 -3 10 3.80 3.00 -4 3 -10 70.99 10.60 -4 3 -10 65.39 10.90 4 -3 10 59.99 4.80 4 -3 10 76.09 7.50 4 -3 10 47.60 8.90 4 -3 10 60.89 4.60 4 -3 10 54.39 9.70 4 -3 10 74.99 9.20 -5 3 -10 91.49 12.60 -5 3 -10 72.39 7.80 -5 3 -10 80.29 12.10 5 -3 10 82.69 6.50 5 -3 10 100.69 11.30 5 -3 10 83.29 8.20 5 -3 10 81.29 8.40 5 -3 10 82.89 12.20 5 -3 10 90.49 6.50 -6 3 -10 13.70 6.40 -6 3 -10 25.60 8.40 6 -3 10 13.20 4.00 6 -3 10 18.90 5.30 6 -3 10 37.40 9.00 6 -3 10 20.40 7.50 -7 3 -10 20.90 7.20 -7 3 -10 34.70 9.60 -7 3 -10 33.40 2.80 7 -3 10 21.50 5.70 7 -3 10 34.20 9.40 7 -3 10 31.00 6.20 7 -3 10 44.30 10.40 7 -3 10 33.70 6.50 7 -3 10 28.10 8.70 -8 3 -10 108.69 8.10 -8 3 -10 95.59 14.70 -8 3 -10 110.49 16.80 8 -3 10 108.39 15.00 8 -3 10 112.49 16.20 8 -3 10 91.29 14.80 -9 3 -10 39.90 10.50 -9 3 -10 41.50 10.20 9 -3 10 17.10 8.00 9 -3 10 20.70 7.80 9 -3 10 15.30 5.40 9 -3 10 32.30 9.90 -10 3 -10 -5.40 6.80 10 -3 10 5.00 8.00 10 -3 10 -12.20 6.20 10 -3 10 10.30 7.30 11 2 -10 3.80 6.60 11 2 -10 -0.60 6.30 11 2 -10 1.20 3.60 11 2 -10 6.30 7.20 11 2 -10 -0.40 3.40 -11 -2 10 -4.80 7.20 -11 -2 10 -16.70 8.10 10 2 -10 0.60 3.20 10 2 -10 0.30 5.90 10 2 -10 6.40 4.20 10 2 -10 1.50 3.50 10 2 -10 8.90 7.20 -10 -2 10 8.10 6.10 -10 -2 10 0.60 4.10 -10 -2 10 -1.30 4.40 -10 -2 10 0.00 8.30 9 2 -10 28.40 5.50 9 2 -10 37.50 9.90 9 2 -10 23.40 6.30 9 2 -10 15.40 5.60 9 2 -10 26.50 9.00 -9 -2 10 28.80 8.30 -9 -2 10 23.20 5.50 -9 -2 10 22.20 7.60 -9 -2 10 18.40 5.60 -9 -2 10 32.90 12.10 8 2 -10 8.30 6.40 8 2 -10 15.10 5.70 8 2 -10 5.80 5.30 8 2 -10 7.60 4.30 -8 -2 10 9.30 4.60 -8 -2 10 12.70 8.10 -8 -2 10 6.70 4.90 -8 -2 10 7.90 4.10 -8 -2 10 9.90 5.60 7 2 -10 75.99 9.60 7 2 -10 110.29 14.10 7 2 -10 55.79 12.20 7 2 -10 70.39 3.50 -7 -2 10 76.09 11.90 -7 -2 10 105.89 9.40 -7 -2 10 78.89 11.20 -7 -2 10 87.69 15.80 -7 -2 10 74.99 7.30 6 2 -10 261.27 15.10 6 2 -10 318.47 18.30 6 2 -10 297.67 19.90 6 2 -10 308.87 24.00 6 2 -10 296.27 17.60 6 2 -10 245.68 18.40 -6 -2 10 268.37 17.10 -6 -2 10 317.77 21.60 -6 -2 10 292.07 14.80 -6 -2 10 291.37 18.50 -6 -2 10 293.87 22.70 -6 -2 10 292.27 17.20 5 2 -10 0.10 3.00 5 2 -10 -5.20 2.50 5 2 -10 1.80 3.40 5 2 -10 -1.10 1.70 5 2 -10 -1.50 3.20 -5 -2 10 1.10 2.60 -5 -2 10 -1.10 2.70 -5 -2 10 3.90 4.50 -5 -2 10 -3.90 3.00 -5 -2 10 0.30 1.40 -5 -2 10 0.00 2.90 4 2 -10 442.36 23.20 4 2 -10 440.36 18.70 4 2 -10 465.75 23.90 4 2 -10 486.05 24.50 4 2 -10 433.66 28.20 -4 -2 10 444.76 25.90 -4 -2 10 460.25 18.20 -4 -2 10 507.95 23.50 -4 -2 10 428.76 22.90 -4 -2 10 497.85 27.50 -4 -2 10 415.76 24.30 -4 -2 10 481.25 23.00 3 2 -10 102.59 8.90 3 2 -10 90.19 8.00 3 2 -10 117.49 13.00 3 2 -10 100.99 9.90 3 2 -10 90.19 4.10 3 2 -10 99.19 9.30 3 2 -10 128.69 10.30 -3 -2 10 109.89 8.70 -3 -2 10 92.89 8.20 -3 -2 10 73.99 7.80 -3 -2 10 103.79 10.10 -3 -2 10 104.89 11.10 2 2 -10 495.55 25.10 2 2 -10 472.25 21.80 2 2 -10 497.85 24.80 2 2 -10 471.75 24.20 2 2 -10 528.05 29.00 2 2 -10 477.75 18.70 2 2 -10 517.65 24.40 -2 -2 10 494.15 22.60 -2 -2 10 482.05 26.40 -2 -2 10 504.45 23.60 -2 -2 10 449.36 21.90 -2 -2 10 502.55 24.10 -2 -2 10 479.75 23.60 1 2 -10 219.28 10.30 1 2 -10 210.48 12.70 1 2 -10 225.68 13.70 1 2 -10 221.88 16.90 1 2 -10 203.98 12.30 1 2 -10 216.28 14.40 1 2 -10 191.58 10.40 -1 -2 10 199.08 11.80 -1 -2 10 225.68 13.10 -1 -2 10 204.68 11.50 -1 -2 10 212.98 12.20 -1 -2 10 205.68 13.00 -1 -2 10 191.18 13.40 -1 -2 10 208.38 9.50 0 2 -10 309.67 12.90 0 2 -10 302.77 16.80 0 2 -10 329.57 18.50 0 2 -10 302.47 15.70 0 -2 10 315.47 17.90 0 -2 10 288.07 14.80 0 -2 10 274.17 16.00 0 -2 10 317.57 13.60 0 -2 10 299.77 13.70 0 -2 10 305.17 15.70 -1 2 -10 667.23 29.30 -1 2 -10 690.43 31.90 -1 2 -10 656.03 29.90 -1 2 -10 739.23 30.70 -1 2 -10 614.54 27.90 -1 2 -10 661.13 29.90 -1 2 -10 627.64 28.50 1 -2 10 690.03 31.10 1 -2 10 660.33 27.30 1 -2 10 707.43 29.40 1 -2 10 676.63 28.30 1 -2 10 671.63 25.90 1 -2 10 644.04 29.50 -2 2 -10 421.86 21.10 -2 2 -10 430.16 19.10 -2 2 -10 410.86 21.20 -2 2 -10 387.06 20.20 -2 2 -10 411.66 19.20 -2 2 -10 427.76 23.20 -2 2 -10 438.46 22.00 -2 2 -10 415.96 20.70 2 -2 10 434.96 22.50 2 -2 10 393.76 20.70 2 -2 10 460.45 20.30 2 -2 10 428.76 21.00 2 -2 10 431.06 19.70 2 -2 10 409.86 20.10 2 -2 10 430.16 18.80 -3 2 -10 109.19 9.00 -3 2 -10 88.29 13.10 -3 2 -10 92.99 8.40 -3 2 -10 80.39 6.80 -3 2 -10 90.39 8.00 3 -2 10 100.49 7.70 3 -2 10 87.79 8.20 3 -2 10 95.49 8.90 3 -2 10 105.19 8.40 3 -2 10 100.59 7.70 -4 2 -10 6.60 2.90 -4 2 -10 5.40 3.70 -4 2 -10 6.00 4.40 -4 2 -10 1.90 4.00 -4 2 -10 2.30 2.90 4 -2 10 9.90 4.30 4 -2 10 7.10 3.50 4 -2 10 6.90 3.00 4 -2 10 2.90 4.50 4 -2 10 6.70 3.30 4 -2 10 5.20 1.40 4 -2 10 3.00 3.60 -5 2 -10 280.87 19.10 -5 2 -10 261.17 18.20 -5 2 -10 208.48 13.10 -5 2 -10 268.57 16.90 5 -2 10 248.98 17.00 5 -2 10 249.78 15.20 5 -2 10 257.27 14.10 5 -2 10 273.37 16.80 5 -2 10 234.48 14.80 5 -2 10 246.38 17.80 5 -2 10 236.28 16.80 -6 2 -10 192.28 15.90 -6 2 -10 135.99 8.50 -6 2 -10 144.89 13.40 -6 2 -10 193.68 15.90 6 -2 10 146.69 13.50 6 -2 10 157.28 14.10 6 -2 10 144.49 13.30 6 -2 10 152.18 10.60 6 -2 10 138.39 9.40 6 -2 10 174.28 12.20 6 -2 10 160.98 14.80 -7 2 -10 74.29 6.50 -7 2 -10 107.49 15.10 -7 2 -10 82.79 12.10 -7 2 -10 82.69 12.30 7 -2 10 78.09 5.90 7 -2 10 79.59 13.30 7 -2 10 68.59 7.30 7 -2 10 91.99 11.20 7 -2 10 79.99 12.30 7 -2 10 70.69 11.10 7 -2 10 93.69 13.50 -8 2 -10 5.90 6.50 -8 2 -10 -0.30 4.00 -8 2 -10 0.10 3.70 -8 2 -10 -3.50 3.70 8 -2 10 1.20 3.20 8 -2 10 -2.20 4.60 8 -2 10 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265.57 16.70 -3 -6 11 263.67 18.70 2 6 -11 5.70 3.10 2 6 -11 -2.70 4.80 2 6 -11 -4.30 3.00 2 6 -11 0.50 4.90 -2 -6 11 2.10 3.00 -2 -6 11 1.20 1.10 -2 -6 11 3.30 4.10 -2 -6 11 3.80 4.30 1 6 -11 10.80 3.60 1 6 -11 25.70 7.90 1 6 -11 25.90 8.60 1 6 -11 22.10 3.80 1 6 -11 26.10 8.90 -1 -6 11 25.10 7.20 -1 -6 11 25.70 3.60 -1 -6 11 16.40 4.50 -1 -6 11 19.40 6.80 -1 -6 11 26.10 7.90 0 6 -11 -4.60 4.30 0 6 -11 -4.00 3.90 0 6 -11 0.70 5.30 0 -6 11 -0.90 3.70 0 -6 11 3.50 4.90 0 -6 11 -1.20 2.00 0 -6 11 -6.50 2.90 0 -6 11 0.80 2.10 0 -6 11 -4.80 2.90 0 -6 11 -3.30 1.70 -1 6 -11 93.79 13.90 -1 6 -11 68.89 12.60 1 -6 11 82.79 12.50 1 -6 11 70.29 7.00 1 -6 11 85.19 12.10 1 -6 11 65.59 10.00 1 -6 11 70.19 6.30 1 -6 11 61.89 10.00 -2 6 -11 38.50 10.40 -2 6 -11 38.50 9.20 2 -6 11 43.20 8.70 2 -6 11 31.00 6.80 2 -6 11 43.00 8.40 2 -6 11 37.70 5.00 2 -6 11 47.00 9.70 2 -6 11 23.20 6.60 -3 6 -11 128.19 17.50 -3 6 -11 82.79 13.50 3 -6 11 110.79 11.60 3 -6 11 122.69 13.80 3 -6 11 88.19 13.40 3 -6 11 104.09 10.50 3 -6 11 96.39 7.50 -4 6 -11 4.30 5.40 -4 6 -11 1.30 5.90 4 -6 11 5.10 4.20 4 -6 11 1.80 4.20 4 -6 11 1.50 5.10 4 -6 11 4.20 2.70 4 -6 11 1.40 5.40 -5 6 -11 111.69 17.30 -5 6 -11 102.89 16.30 5 -6 11 90.69 14.40 5 -6 11 109.59 12.10 5 -6 11 87.59 7.90 5 -6 11 118.39 10.90 5 -6 11 117.29 16.60 -6 6 -11 -0.70 5.40 -6 6 -11 -7.80 7.90 6 -6 11 -1.50 3.50 6 -6 11 3.70 4.10 6 -6 11 -1.00 3.70 6 -6 11 -6.50 4.60 -7 6 -11 23.90 10.20 -7 6 -11 -4.30 7.30 7 -6 11 15.80 7.30 7 -6 11 19.60 7.70 7 -6 11 9.60 7.80 7 -6 11 23.30 5.80 -8 6 -11 -6.90 6.60 -8 6 -11 7.60 9.80 8 -6 11 -6.10 4.80 8 -6 11 -4.50 7.40 8 -6 11 -1.60 5.90 11 5 -11 -0.10 6.10 11 5 -11 -0.50 9.20 11 5 -11 12.80 6.70 11 5 -11 20.80 9.70 -11 -5 11 13.60 6.30 -11 -5 11 31.40 13.10 -11 -5 11 4.80 9.00 -11 -5 11 11.80 7.70 10 5 -11 -3.10 5.60 10 5 -11 2.30 5.40 10 5 -11 2.60 6.40 10 5 -11 -5.20 6.30 -10 -5 11 -12.20 5.80 -10 -5 11 4.30 7.70 -10 -5 11 -0.80 5.50 9 5 -11 16.90 3.80 9 5 -11 36.10 12.00 9 5 -11 22.30 7.40 9 5 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8.20 3 2 26 30.80 8.70 3 2 26 9.40 7.70 -4 -2 -26 -7.00 7.50 -4 -2 -26 -9.30 3.60 4 2 26 8.10 7.00 4 2 26 0.80 6.40 4 2 26 0.20 6.50 4 2 26 10.50 7.10 -5 -2 -26 -0.80 4.50 -5 -2 -26 3.30 9.80 5 2 26 7.40 6.40 5 2 26 -8.90 6.80 5 2 26 7.60 7.20 2 -3 -26 4.70 7.00 2 -3 -26 -14.10 5.80 -2 3 26 7.50 6.70 1 -3 -26 6.60 6.70 -1 3 26 1.00 8.60 0 -3 -26 4.10 7.80 0 -3 -26 -4.50 4.50 0 -3 -26 0.50 5.60 0 3 26 3.10 5.90 0 3 26 0.30 7.10 0 3 26 0.30 4.90 -1 -3 -26 23.30 9.00 -1 -3 -26 1.20 4.60 -1 -3 -26 24.90 10.90 1 3 26 17.30 7.50 1 3 26 21.10 9.60 1 3 26 2.90 7.70 -2 -3 -26 -4.20 5.80 -2 -3 -26 -5.60 8.50 2 3 26 9.20 6.30 2 3 26 0.90 5.90 2 3 26 -9.20 4.60 -3 -3 -26 11.70 8.00 -3 -3 -26 19.30 10.90 3 3 26 28.20 9.50 3 3 26 32.20 9.40 3 3 26 33.60 10.30 -4 -3 -26 4.10 7.00 4 3 26 6.90 7.70 4 3 26 9.80 8.30 4 3 26 -3.90 5.80 4 3 26 3.50 6.10 -5 -3 -26 4.70 4.10 5 3 26 5.70 7.00 5 3 26 7.10 6.30 5 3 26 7.40 7.50 2 -4 -26 -1.10 7.40 2 -4 -26 -1.20 6.90 -2 4 26 -4.90 7.00 -2 4 26 -13.50 4.70 1 -4 -26 -1.50 7.70 1 -4 -26 4.20 5.50 1 -4 -26 22.00 7.40 -1 4 26 8.70 6.90 -1 4 26 16.70 9.50 0 -4 -26 6.10 5.60 0 -4 -26 -10.20 6.70 0 4 26 25.60 8.70 0 4 26 -3.70 5.10 0 4 26 3.10 6.60 -1 -4 -26 0.30 3.90 -1 -4 -26 10.80 6.40 -1 -4 -26 -1.50 5.50 1 4 26 5.80 6.80 1 4 26 22.50 8.00 1 4 26 15.90 6.90 -2 -4 -26 -2.40 5.40 -2 -4 -26 7.30 8.50 2 4 26 3.80 5.60 2 4 26 -9.50 6.10 2 4 26 0.10 6.00 -3 -4 -26 19.40 9.70 -3 -4 -26 21.60 7.90 3 4 26 27.60 8.70 3 4 26 24.90 9.70 -4 -4 -26 16.30 9.30 4 4 26 2.90 7.40 4 4 26 2.40 5.90 -5 -4 -26 -3.10 6.30 5 4 26 11.90 8.30 5 4 26 2.80 6.60 5 4 26 7.20 7.00 1 -5 -26 14.80 6.00 1 -5 -26 13.40 9.00 -1 5 26 40.00 10.00 0 -5 -26 0.40 5.30 0 -5 -26 -9.30 3.60 0 -5 -26 -4.30 5.90 0 5 26 3.20 6.00 0 5 26 10.70 7.40 -1 -5 -26 6.20 7.20 -1 -5 -26 22.40 7.70 -1 -5 -26 5.60 5.00 1 5 26 22.70 9.10 1 5 26 19.10 7.60 -2 -5 -26 4.10 6.20 -2 -5 -26 0.60 7.30 2 5 26 -2.90 5.40 2 5 26 0.90 5.20 -3 -5 -26 -12.60 5.00 -3 -5 -26 2.50 7.70 3 5 26 7.70 8.00 3 5 26 5.70 6.70 -4 -5 -26 -0.60 7.80 -4 -5 -26 -11.30 5.50 4 5 26 9.50 6.40 4 5 26 -2.80 5.60 -5 -5 -26 -2.20 7.90 5 5 26 12.40 8.20 5 5 26 8.30 8.10 5 5 26 5.10 8.20 1 -6 -26 5.10 6.00 1 -6 -26 -2.40 7.80 1 -6 -26 1.90 5.60 -1 6 26 20.40 9.20 0 -6 -26 -7.60 4.00 0 -6 -26 -5.70 7.50 0 6 26 -13.80 4.80 -1 -6 -26 3.30 7.70 -1 -6 -26 21.00 5.80 -1 -6 -26 -1.70 4.60 1 6 26 4.50 5.50 1 6 26 5.50 7.20 -2 -6 -26 -7.90 6.70 -2 -6 -26 6.30 5.90 2 6 26 11.20 7.40 2 6 26 11.50 7.40 -3 -6 -26 -5.20 5.40 -3 -6 -26 -17.20 6.40 -3 -6 -26 -6.70 5.10 3 6 26 3.40 6.50 3 6 26 -1.30 4.70 -4 -6 -26 -6.80 3.70 -4 -6 -26 -12.90 7.50 -4 -6 -26 -16.40 5.60 4 6 26 -1.40 6.80 4 6 26 -8.00 4.50 -5 -6 -26 -9.20 4.80 -5 -6 -26 -5.70 5.70 5 6 26 17.50 9.00 5 6 26 9.50 8.30 0 -7 -26 -15.10 4.50 1 7 26 -4.20 5.40 1 7 26 -3.90 5.80 -2 -7 -26 -11.50 5.10 -2 -7 -26 1.10 7.20 -2 -7 -26 -13.10 4.40 2 7 26 -1.90 5.90 2 7 26 -4.50 5.70 -3 -7 -26 0.50 6.90 -3 -7 -26 3.70 7.60 3 7 26 -6.60 6.20 3 7 26 6.20 8.20 -4 -7 -26 -5.30 4.40 -4 -7 -26 5.10 7.90 -4 -7 -26 -15.20 6.10 4 7 26 11.50 8.10 4 7 26 -1.20 5.90 -3 -8 -26 -4.60 7.00 3 8 26 36.30 10.40 -1 0 27 0.70 6.10 -1 0 27 5.80 8.60 0 0 -27 -10.10 7.10 0 0 27 -2.30 4.50 -1 0 -27 10.50 9.00 -1 0 -27 7.10 3.60 1 0 27 4.70 5.70 1 0 27 9.20 7.10 1 0 27 2.50 8.00 -2 0 -27 -5.70 3.80 -2 0 -27 -15.40 9.00 2 0 27 -1.20 7.10 2 0 27 -18.70 7.00 2 0 27 -13.30 4.70 1 -1 -27 -0.60 9.50 -1 1 27 -0.40 5.90 -1 1 27 0.50 8.70 0 -1 -27 -1.50 8.80 0 -1 -27 3.40 8.00 0 1 27 -11.10 7.20 0 1 27 0.50 5.90 0 1 27 -5.40 4.60 -1 -1 -27 -2.60 6.50 -1 -1 -27 10.30 10.20 1 1 27 2.70 8.60 1 1 27 20.90 9.00 1 1 27 6.00 5.20 -2 -1 -27 13.30 8.30 -2 -1 -27 -2.30 9.80 2 1 27 5.80 5.90 2 1 27 20.30 10.30 2 1 27 -3.60 6.40 -3 -1 -27 3.90 10.20 -3 -1 -27 -8.70 3.30 3 1 27 2.40 7.10 3 1 27 8.40 7.70 3 1 27 8.20 6.90 1 -2 -27 12.90 6.70 1 -2 -27 14.40 9.50 -1 2 27 4.50 10.40 -1 2 27 6.10 7.10 0 -2 -27 7.80 9.20 0 -2 -27 -6.40 7.30 0 2 27 4.20 6.70 0 2 27 4.60 9.30 0 2 27 7.40 4.90 -1 -2 -27 1.00 7.20 -1 -2 -27 4.70 9.50 1 2 27 -3.60 4.70 1 2 27 15.40 9.80 1 2 27 5.60 7.90 -2 -2 -27 3.40 10.30 -2 -2 -27 11.50 8.10 2 2 27 1.50 7.20 2 2 27 4.90 8.00 2 2 27 -4.80 5.50 -3 -2 -27 -10.50 8.40 -3 -2 -27 -11.80 6.70 3 2 27 -0.30 5.70 3 2 27 1.70 7.90 3 2 27 3.10 6.80 0 -3 -27 -2.40 6.70 0 -3 -27 6.90 9.30 0 -3 -27 -2.70 4.90 0 3 27 -1.40 4.70 0 3 27 13.00 10.10 0 3 27 20.40 8.50 -1 -3 -27 -16.30 7.80 -1 -3 -27 -2.70 6.20 1 3 27 20.50 8.90 1 3 27 3.70 7.90 1 3 27 -5.20 4.30 -2 -3 -27 15.40 9.70 -2 -3 -27 6.90 6.90 2 3 27 -1.80 5.90 2 3 27 6.30 6.20 2 3 27 12.60 8.20 -3 -3 -27 5.20 8.30 -3 -3 -27 7.80 8.20 3 3 27 1.40 8.00 3 3 27 -9.40 4.20 3 3 27 3.60 6.30 -4 -3 -27 -28.40 12.70 4 3 27 9.20 7.60 4 3 27 9.20 7.00 4 3 27 -4.30 7.50 0 -4 -27 5.60 7.20 0 -4 -27 10.50 6.00 0 -4 -27 -13.00 8.80 0 4 27 2.20 5.40 0 4 27 20.40 8.10 -1 -4 -27 -14.60 7.30 -1 -4 -27 -2.60 5.60 1 4 27 -1.70 5.30 1 4 27 -9.50 6.40 1 4 27 6.70 8.00 -2 -4 -27 -1.00 6.20 -2 -4 -27 -1.10 9.20 2 4 27 8.50 7.70 2 4 27 12.70 7.10 2 4 27 3.90 7.90 -3 -4 -27 6.60 7.00 -3 -4 -27 2.90 8.40 3 4 27 8.10 7.10 3 4 27 8.70 7.30 -4 -4 -27 -0.70 7.10 -4 -4 -27 -19.30 7.50 4 4 27 0.60 7.30 4 4 27 8.60 7.10 0 -5 -27 9.70 10.10 0 -5 -27 25.40 10.90 0 -5 -27 28.60 7.20 0 5 27 21.70 8.50 -1 -5 -27 8.50 8.40 -1 -5 -27 -12.80 4.50 1 5 27 -4.10 6.80 1 5 27 12.40 6.40 -2 -5 -27 -15.60 7.90 -2 -5 -27 -0.80 7.10 2 5 27 -6.70 5.60 2 5 27 4.20 7.60 -3 -5 -27 9.10 8.30 -3 -5 -27 -12.40 6.10 3 5 27 -2.20 5.90 3 5 27 9.00 6.90 -4 -5 -27 -2.30 7.00 -4 -5 -27 2.50 10.30 4 5 27 9.80 8.20 4 5 27 -1.40 7.40 -2 -6 -27 -3.80 5.90 -2 -6 -27 -18.70 7.30 2 6 27 -0.20 7.10 2 6 27 3.60 5.40 -3 -6 -27 -5.80 5.60 -3 -6 -27 39.60 12.50 3 6 27 6.20 7.20 3 6 27 0.20 7.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 39830 _shelx_res_file ; TITL SETIFI_FedpaN3_Tamb_0m_a.res in P-1 wm4222_.res created by SHELXL-2019/3 at 09:40:07 on 23-Oct-2024 CELL 0.71073 7.7496 9.3778 16.6178 79.516 83.962 69.52 ZERR 2 0.0005 0.0006 0.001 0.003 0.003 0.003 LATT 1 SFAC C H Fe N O UNIT 40 40 2 24 2 LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!! L.S. 10 PLAN 5 0 0 TEMP 26.85 dfix 0.85 0.001 O1 H1 O1 H2 EQIV $1 x-1, y, z HTAB N2A N1_$1 HTAB N2B O1 EQIV $2 -x+1, -y+1, -z+2 HTAB O1 N6_$2 EQIV $3 x-1, y+1, z HTAB O1 N6_$3 BOND $H FMAP 2 ACTA conf WGHT 0.035600 0.332000 FVAR 0.89498 FE1 3 0.751821 0.517198 0.716417 11.00000 0.02457 0.02777 = 0.03363 -0.00701 -0.00253 -0.00780 N1 4 0.932262 0.601911 0.630270 11.00000 0.02889 0.04859 = 0.04606 -0.00327 -0.00180 -0.01691 REM REM First ligand A REM N1A 4 0.652143 0.428138 0.625846 11.00000 0.02601 0.02884 = 0.03448 -0.00838 -0.00303 -0.00655 N6 4 1.019809 0.141728 0.877716 11.00000 0.05788 0.05774 = 0.06417 0.01345 -0.00443 -0.02153 C1A 1 0.778832 0.313275 0.590702 11.00000 0.03167 0.03598 = 0.03754 -0.01122 -0.00142 -0.00503 AFIX 43 H1A 2 0.902781 0.300924 0.592767 11.00000 -1.20000 AFIX 0 C2A 1 0.734172 0.214348 0.552287 11.00000 0.04715 0.03762 = 0.04297 -0.01699 -0.00031 -0.00719 AFIX 43 H2A 2 0.825505 0.135541 0.529849 11.00000 -1.20000 AFIX 0 C3A 1 0.548687 0.234780 0.547695 11.00000 0.05521 0.03907 = 0.04454 -0.01493 -0.00387 -0.02117 AFIX 43 H3A 2 0.514078 0.167702 0.523344 11.00000 -1.20000 AFIX 0 C4A 1 0.417358 0.354592 0.579358 11.00000 0.03774 0.03849 = 0.04339 -0.00899 -0.00553 -0.01812 AFIX 43 H4A 2 0.292675 0.371479 0.575537 11.00000 -1.20000 AFIX 0 C5A 1 0.473999 0.451484 0.617669 11.00000 0.02865 0.02662 = 0.03167 -0.00353 -0.00307 -0.01010 N2A 4 0.338000 0.572353 0.648625 11.00000 0.02221 0.03182 = 0.04705 -0.01013 -0.00243 -0.00861 AFIX 3 H21 2 0.224127 0.575159 0.642404 11.00000 0.03962 AFIX 0 C6A 1 0.348403 0.710803 0.661905 11.00000 0.02477 0.02695 = 0.03177 -0.00442 -0.00085 -0.00610 C7A 1 0.184789 0.838462 0.657521 11.00000 0.02693 0.03480 = 0.04928 -0.00764 -0.00509 -0.00233 AFIX 43 H7A 2 0.074958 0.829053 0.645695 11.00000 -1.20000 AFIX 0 C8A 1 0.189092 0.976762 0.670866 11.00000 0.04074 0.03018 = 0.05590 -0.00706 -0.00484 0.00185 AFIX 43 H8A 2 0.081235 1.061619 0.669914 11.00000 -1.20000 AFIX 0 C9A 1 0.355054 0.989747 0.685813 11.00000 0.05201 0.02459 = 0.04858 -0.00493 -0.00386 -0.00973 AFIX 43 H9A 2 0.361499 1.083335 0.693806 11.00000 -1.20000 AFIX 0 C10A 1 0.509199 0.860859 0.688471 11.00000 0.03891 0.02870 = 0.04285 -0.00436 -0.00429 -0.01335 AFIX 43 H10A 2 0.621159 0.870158 0.697129 11.00000 -1.20000 AFIX 0 N3A 4 0.508502 0.720217 0.679227 11.00000 0.02602 0.02534 = 0.03783 -0.00524 -0.00235 -0.00810 REM REM Second Ligand B REM N1B 4 0.576667 0.430660 0.813835 11.00000 0.03365 0.02953 = 0.03721 -0.00506 -0.00046 -0.01254 C1B 1 0.549103 0.298467 0.807104 11.00000 0.04537 0.03171 = 0.04479 -0.00429 -0.00390 -0.01554 AFIX 43 H1B 2 0.628281 0.235554 0.771837 11.00000 -1.20000 AFIX 0 C2B 1 0.411550 0.252271 0.849191 11.00000 0.05355 0.04083 = 0.05421 0.00154 -0.00847 -0.02659 AFIX 43 H2B 2 0.396359 0.161449 0.841875 11.00000 -1.20000 AFIX 0 C3B 1 0.295239 0.344104 0.903047 11.00000 0.04490 0.05738 = 0.05231 0.00242 0.00048 -0.02911 AFIX 43 H3B 2 0.198122 0.317344 0.931310 11.00000 -1.20000 AFIX 0 C4B 1 0.325048 0.474660 0.914133 11.00000 0.03837 0.05224 = 0.04314 -0.00674 0.00483 -0.01892 AFIX 43 H4B 2 0.251129 0.535740 0.951412 11.00000 -1.20000 AFIX 0 C5B 1 0.468526 0.515045 0.868524 11.00000 0.03030 0.03457 = 0.03376 -0.00317 -0.00300 -0.01087 N2B 4 0.491313 0.649240 0.880672 11.00000 0.03602 0.03830 = 0.04478 -0.01626 0.00713 -0.01312 AFIX 3 H22 2 0.403667 0.703840 0.913001 11.00000 0.04389 AFIX 0 N2 4 0.875376 0.705407 0.575438 11.00000 0.02966 0.05220 = 0.03861 -0.00750 0.00033 -0.02025 C6B 1 0.643149 0.696407 0.865465 11.00000 0.03658 0.03151 = 0.03301 -0.00684 -0.00380 -0.01114 C7B 1 0.639879 0.821803 0.901588 11.00000 0.05428 0.04039 = 0.04528 -0.01646 -0.00079 -0.01720 AFIX 43 H7B 2 0.537900 0.870936 0.933549 11.00000 -1.20000 AFIX 0 C8B 1 0.789012 0.870377 0.888985 11.00000 0.06897 0.04940 = 0.05382 -0.01727 -0.00636 -0.03086 AFIX 43 H8B 2 0.788688 0.954293 0.911503 11.00000 -1.20000 AFIX 0 C9B 1 0.940814 0.793346 0.842301 11.00000 0.05529 0.06467 = 0.05159 -0.01429 -0.00626 -0.03635 AFIX 43 H9B 2 1.044924 0.822798 0.834127 11.00000 -1.20000 AFIX 0 C10B 1 0.933577 0.672742 0.808516 11.00000 0.03681 0.05430 = 0.04266 -0.01302 -0.00466 -0.02045 AFIX 43 H10B 2 1.036071 0.620313 0.777860 11.00000 -1.20000 AFIX 0 N3B 4 0.785111 0.625978 0.817434 11.00000 0.03334 0.03762 = 0.03649 -0.00956 -0.00394 -0.01372 REM REM Azid ligands REM N4 4 0.980432 0.309654 0.753392 11.00000 0.04001 0.03877 = 0.04537 -0.00575 -0.00479 0.00291 N3 4 0.824441 0.806892 0.522979 11.00000 0.05344 0.07886 = 0.05594 0.01521 -0.00701 -0.02387 N5 4 0.997817 0.226066 0.815938 11.00000 0.03110 0.03443 = 0.04955 -0.00729 -0.00440 -0.00846 REM REM water molecule REM O1 5 0.219462 0.850400 0.975991 11.00000 0.05585 0.06102 = 0.05525 -0.01907 0.00509 0.00095 H1 2 0.151605 0.837557 1.018366 11.00000 -1.50000 H2 2 0.166362 0.935154 0.945785 11.00000 -1.50000 REM REM wm4222_.hkl REM HKLF 4 REM SETIFI_FedpaN3_Tamb_0m_a.res in P-1 REM wR2 = 0.1085, GooF = S = 1.094, Restrained GooF = 1.094 for all data REM R1 = 0.0373 for 7610 Fo > 4sig(Fo) and 0.0736 for all 10836 data REM 315 parameters refined using 2 restraints END WGHT 0.0356 0.3316 REM Highest difference peak 0.382, deepest hole -0.651, 1-sigma level 0.059 Q1 1 0.4530 0.3992 0.5989 11.00000 0.05 0.38 Q2 1 0.6210 0.6137 0.7024 11.00000 0.05 0.37 Q3 1 0.8789 0.5498 0.6989 11.00000 0.05 0.33 Q4 1 0.7525 0.5897 0.8002 11.00000 0.05 0.32 Q5 1 0.7417 0.2738 0.5663 11.00000 0.05 0.32 ; _shelx_res_checksum 98064 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe Fe1 0.75182(2) 0.51720(2) 0.71642(2) 0.02855(5) Uani d 1 . . N N1 0.93226(16) 0.60191(16) 0.63027(8) 0.0407(3) Uani d 1 . . N N1A 0.65214(14) 0.42814(12) 0.62585(7) 0.0299(2) Uani d 1 . . N N6 1.0198(2) 0.1417(2) 0.87772(11) 0.0623(4) Uani d 1 . . C C1A 0.77883(19) 0.31328(16) 0.59070(9) 0.0361(3) Uani d 1 . . H H1A 0.902781 0.300924 0.592767 0.043 Uiso calc 1 . . C C2A 0.7342(2) 0.21435(18) 0.55229(10) 0.0432(3) Uani d 1 . . H H2A 0.825505 0.135541 0.529849 0.052 Uiso calc 1 . . C C3A 0.5487(2) 0.23478(18) 0.54770(10) 0.0436(3) Uani d 1 . . H H3A 0.514078 0.167702 0.523344 0.052 Uiso calc 1 . . C C4A 0.4174(2) 0.35459(17) 0.57936(9) 0.0378(3) Uani d 1 . . H H4A 0.292675 0.371479 0.575537 0.045 Uiso calc 1 . . C C5A 0.47400(17) 0.45148(14) 0.61767(8) 0.0288(2) Uani d 1 . . N N2A 0.33800(14) 0.57235(13) 0.64863(8) 0.0332(2) Uani d 1 . . H H21 0.224127 0.575159 0.642404 0.040(4) Uiso d 1 . . C C6A 0.34840(16) 0.71080(14) 0.66191(8) 0.0286(2) Uani d 1 . . C C7A 0.18479(19) 0.83846(16) 0.65752(10) 0.0388(3) Uani d 1 . . H H7A 0.074958 0.829053 0.645695 0.047 Uiso calc 1 . . C C8A 0.1891(2) 0.97676(17) 0.67087(11) 0.0458(3) Uani d 1 . . H H8A 0.081235 1.061619 0.669914 0.055 Uiso calc 1 . . C C9A 0.3551(2) 0.98975(16) 0.68581(10) 0.0426(3) Uani d 1 . . H H9A 0.361499 1.083335 0.693806 0.051 Uiso calc 1 . . C C10A 0.5092(2) 0.86086(15) 0.68847(9) 0.0363(3) Uani d 1 . . H H10A 0.621159 0.870158 0.697129 0.044 Uiso calc 1 . . N N3A 0.50850(14) 0.72022(12) 0.67923(7) 0.0298(2) Uani d 1 . . N N1B 0.57667(16) 0.43066(13) 0.81383(7) 0.0331(2) Uani d 1 . . C C1B 0.5491(2) 0.29847(16) 0.80710(10) 0.0400(3) Uani d 1 . . H H1B 0.628281 0.235554 0.771837 0.048 Uiso calc 1 . . C C2B 0.4115(2) 0.25227(19) 0.84919(11) 0.0474(4) Uani d 1 . . H H2B 0.396359 0.161449 0.841875 0.057 Uiso calc 1 . . C C3B 0.2952(2) 0.3441(2) 0.90305(11) 0.0500(4) Uani d 1 . . H H3B 0.198122 0.317344 0.931310 0.060 Uiso calc 1 . . C C4B 0.3250(2) 0.4747(2) 0.91413(10) 0.0442(3) Uani d 1 . . H H4B 0.251129 0.535740 0.951412 0.053 Uiso calc 1 . . C C5B 0.46853(18) 0.51505(16) 0.86852(8) 0.0331(2) Uani d 1 . . N N2B 0.49131(17) 0.64924(14) 0.88067(8) 0.0389(3) Uani d 1 . . H H22 0.403667 0.703840 0.913001 0.044(5) Uiso d 1 . . N N2 0.87538(16) 0.70541(16) 0.57544(8) 0.0385(3) Uani d 1 . . C C6B 0.64315(19) 0.69641(15) 0.86547(8) 0.0334(2) Uani d 1 . . C C7B 0.6399(2) 0.82180(18) 0.90159(10) 0.0451(3) Uani d 1 . . H H7B 0.537900 0.870936 0.933549 0.054 Uiso calc 1 . . C C8B 0.7890(3) 0.8704(2) 0.88898(12) 0.0530(4) Uani d 1 . . H H8B 0.788688 0.954293 0.911503 0.064 Uiso calc 1 . . C C9B 0.9408(3) 0.7933(2) 0.84230(11) 0.0519(4) Uani d 1 . . H H9B 1.044924 0.822798 0.834127 0.062 Uiso calc 1 . . C C10B 0.9336(2) 0.6727(2) 0.80852(10) 0.0423(3) Uani d 1 . . H H10B 1.036071 0.620313 0.777860 0.051 Uiso calc 1 . . N N3B 0.78511(16) 0.62598(14) 0.81743(7) 0.0347(2) Uani d 1 . . N N4 0.98043(19) 0.30965(15) 0.75339(9) 0.0456(3) Uani d 1 . . N N3 0.8244(2) 0.8069(2) 0.52298(11) 0.0654(5) Uani d 1 . . N N5 0.99782(16) 0.22607(14) 0.81594(8) 0.0388(3) Uani d 1 . . O O1 0.2195(2) 0.85040(17) 0.97599(9) 0.0622(4) Uani d 1 . . H H1 0.152(3) 0.838(3) 1.0184(9) 0.093 Uiso d 1 . . H H2 0.166(3) 0.9352(15) 0.9458(13) 0.093 Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Fe1 0.02457(8) 0.02777(8) 0.03363(9) -0.00780(6) -0.00253(6) -0.00701(6) N1 0.0289(5) 0.0486(7) 0.0461(7) -0.0169(5) -0.0018(5) -0.0033(6) N1A 0.0260(4) 0.0288(5) 0.0345(5) -0.0065(4) -0.0030(4) -0.0084(4) N6 0.0579(9) 0.0577(9) 0.0642(10) -0.0215(8) -0.0044(8) 0.0134(8) C1A 0.0317(6) 0.0360(6) 0.0375(7) -0.0050(5) -0.0014(5) -0.0112(5) C2A 0.0472(8) 0.0376(7) 0.0430(8) -0.0072(6) -0.0003(6) -0.0170(6) C3A 0.0552(9) 0.0391(7) 0.0445(8) -0.0212(7) -0.0039(7) -0.0149(6) C4A 0.0377(7) 0.0385(7) 0.0434(7) -0.0181(6) -0.0055(5) -0.0090(6) C5A 0.0287(5) 0.0266(5) 0.0317(6) -0.0101(4) -0.0031(4) -0.0035(4) N2A 0.0222(4) 0.0318(5) 0.0471(6) -0.0086(4) -0.0024(4) -0.0101(5) C6A 0.0248(5) 0.0269(5) 0.0318(6) -0.0061(4) -0.0009(4) -0.0044(4) C7A 0.0269(6) 0.0348(6) 0.0493(8) -0.0023(5) -0.0051(5) -0.0076(6) C8A 0.0407(7) 0.0302(6) 0.0559(9) 0.0019(6) -0.0048(7) -0.0071(6) C9A 0.0520(8) 0.0246(6) 0.0486(8) -0.0097(6) -0.0039(7) -0.0049(5) C10A 0.0389(7) 0.0287(6) 0.0429(7) -0.0133(5) -0.0043(5) -0.0044(5) N3A 0.0260(4) 0.0253(4) 0.0378(5) -0.0081(4) -0.0023(4) -0.0052(4) N1B 0.0337(5) 0.0295(5) 0.0372(6) -0.0125(4) -0.0005(4) -0.0051(4) C1B 0.0454(8) 0.0317(6) 0.0448(8) -0.0155(6) -0.0039(6) -0.0043(6) C2B 0.0535(9) 0.0408(8) 0.0542(9) -0.0266(7) -0.0085(7) 0.0015(7) C3B 0.0449(8) 0.0574(10) 0.0523(9) -0.0291(8) 0.0005(7) 0.0024(8) C4B 0.0384(7) 0.0522(9) 0.0431(8) -0.0189(7) 0.0048(6) -0.0067(7) C5B 0.0303(6) 0.0346(6) 0.0338(6) -0.0109(5) -0.0030(5) -0.0032(5) N2B 0.0360(6) 0.0383(6) 0.0448(7) -0.0131(5) 0.0071(5) -0.0163(5) N2 0.0297(5) 0.0522(7) 0.0386(6) -0.0203(5) 0.0003(4) -0.0075(5) C6B 0.0366(6) 0.0315(6) 0.0330(6) -0.0111(5) -0.0038(5) -0.0068(5) C7B 0.0543(9) 0.0404(7) 0.0453(8) -0.0172(7) -0.0008(7) -0.0165(6) C8B 0.0690(11) 0.0494(9) 0.0538(10) -0.0309(9) -0.0064(8) -0.0173(8) C9B 0.0553(10) 0.0647(11) 0.0516(9) -0.0363(9) -0.0063(7) -0.0143(8) C10B 0.0368(7) 0.0543(9) 0.0427(8) -0.0205(6) -0.0047(6) -0.0130(7) N3B 0.0333(5) 0.0376(6) 0.0365(6) -0.0137(4) -0.0039(4) -0.0096(5) N4 0.0400(6) 0.0388(6) 0.0454(7) 0.0029(5) -0.0048(5) -0.0058(5) N3 0.0534(9) 0.0789(12) 0.0559(9) -0.0239(8) -0.0070(7) 0.0152(8) N5 0.0311(5) 0.0344(6) 0.0496(7) -0.0085(4) -0.0044(5) -0.0073(5) O1 0.0559(8) 0.0610(8) 0.0552(8) 0.0009(6) 0.0051(6) -0.0191(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag N1 Fe1 N4 . . 89.86(5) ? N1 Fe1 N1A . . 93.92(5) ? N4 Fe1 N1A . . 96.72(5) ? N1 Fe1 N3B . . 95.82(5) ? N4 Fe1 N3B . . 92.31(5) ? N1A Fe1 N3B . . 166.73(4) ? N1 Fe1 N3A . . 92.72(5) ? N4 Fe1 N3A . . 176.62(5) ? N1A Fe1 N3A . . 80.94(4) ? N3B Fe1 N3A . . 89.60(4) ? N1 Fe1 N1B . . 175.48(5) ? N4 Fe1 N1B . . 88.33(5) ? N1A Fe1 N1B . . 90.41(4) ? N3B Fe1 N1B . . 80.12(4) ? N3A Fe1 N1B . . 89.25(4) ? C5A N1A C1A . . 117.71(11) ? C5A N1A Fe1 . . 123.97(8) ? C1A N1A Fe1 . . 116.25(8) ? N1A C1A C2A . . 123.49(13) ? N1A C1A H1A . . 118.3 ? C2A C1A H1A . . 118.3 ? C1A C2A C3A . . 118.27(13) ? C1A C2A H2A . . 120.9 ? C3A C2A H2A . . 120.9 ? C4A C3A C2A . . 119.43(13) ? C4A C3A H3A . . 120.3 ? C2A C3A H3A . . 120.3 ? C3A C4A C5A . . 118.95(13) ? C3A C4A H4A . . 120.5 ? C5A C4A H4A . . 120.5 ? N1A C5A N2A . . 120.37(11) ? N1A C5A C4A . . 121.97(12) ? N2A C5A C4A . . 117.64(11) ? C6A N2A C5A . . 128.64(10) ? C6A N2A H21 . . 114.1 ? C5A N2A H21 . . 113.5 ? N3A C6A N2A . . 120.69(10) ? N3A C6A C7A . . 121.94(12) ? N2A C6A C7A . . 117.36(11) ? C8A C7A C6A . . 119.12(13) ? C8A C7A H7A . . 120.4 ? C6A C7A H7A . . 120.4 ? C7A C8A C9A . . 119.60(13) ? C7A C8A H8A . . 120.2 ? C9A C8A H8A . . 120.2 ? C10A C9A C8A . . 118.04(13) ? C10A C9A H9A . . 121.0 ? C8A C9A H9A . . 121.0 ? N3A C10A C9A . . 123.91(13) ? N3A C10A H10A . . 118.0 ? C9A C10A H10A . . 118.0 ? C6A N3A C10A . . 117.26(11) ? C6A N3A Fe1 . . 123.49(8) ? C10A N3A Fe1 . . 118.17(9) ? C5B N1B C1B . . 117.27(12) ? C5B N1B Fe1 . . 123.75(9) ? C1B N1B Fe1 . . 117.56(10) ? N1B C1B C2B . . 123.75(15) ? N1B C1B H1B . . 118.1 ? C2B C1B H1B . . 118.1 ? C1B C2B C3B . . 118.39(15) ? C1B C2B H2B . . 120.8 ? C3B C2B H2B . . 120.8 ? C4B C3B C2B . . 119.22(15) ? C4B C3B H3B . . 120.4 ? C2B C3B H3B . . 120.4 ? C3B C4B C5B . . 119.13(15) ? C3B C4B H4B . . 120.4 ? C5B C4B H4B . . 120.4 ? N1B C5B N2B . . 120.80(12) ? N1B C5B C4B . . 122.09(13) ? N2B C5B C4B . . 117.09(13) ? C6B N2B C5B . . 130.43(12) ? C6B N2B H22 . . 113.9 ? C5B N2B H22 . . 114.1 ? N1 N2 N3 . . 177.99(16) yes N3B C6B N2B . . 120.69(12) ? N3B C6B C7B . . 122.07(13) ? N2B C6B C7B . . 117.23(13) ? C8B C7B C6B . . 118.95(15) ? C8B C7B H7B . . 120.5 ? C6B C7B H7B . . 120.5 ? C7B C8B C9B . . 119.40(15) ? C7B C8B H8B . . 120.3 ? C9B C8B H8B . . 120.3 ? C10B C9B C8B . . 118.37(15) ? C10B C9B H9B . . 120.8 ? C8B C9B H9B . . 120.8 ? N3B C10B C9B . . 123.44(15) ? N3B C10B H10B . . 118.3 ? C9B C10B H10B . . 118.3 ? C6B N3B C10B . . 117.62(12) ? C6B N3B Fe1 . . 122.47(9) ? C10B N3B Fe1 . . 114.90(10) ? N2 N1 Fe1 . . 122.09(9) yes N4 N5 N6 . . 178.30(17) yes N5 N4 Fe1 . . 128.32(11) yes H1 O1 H2 . . 110(3) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Fe1 N1 . 2.1397(13) ? Fe1 N4 . 2.1645(13) ? Fe1 N1A . 2.1710(11) ? Fe1 N3B . 2.1963(11) ? Fe1 N3A . 2.2061(10) ? Fe1 N1B . 2.2254(12) ? N1 N2 . 1.1958(18) yes N2 N3 . 1.153(2) yes N1A C5A . 1.3377(16) ? N1A C1A . 1.3541(16) ? N4 N5 . 1.1713(19) yes N5 N6 . 1.164(2) yes C1A C2A . 1.369(2) ? C1A H1A . 0.9300 ? C2A C3A . 1.391(2) ? C2A H2A . 0.9300 ? C3A C4A . 1.370(2) ? C3A H3A . 0.9300 ? C4A C5A . 1.4043(18) ? C4A H4A . 0.9300 ? C5A N2A . 1.3865(16) ? N2A C6A . 1.3864(16) ? N2A H21 . 0.8900 ? C6A N3A . 1.3383(15) ? C6A C7A . 1.4042(17) ? C7A C8A . 1.367(2) ? C7A H7A . 0.9300 ? C8A C9A . 1.385(2) ? C8A H8A . 0.9300 ? C9A C10A . 1.368(2) ? C9A H9A . 0.9300 ? C10A N3A . 1.3572(16) ? C10A H10A . 0.9300 ? N1B C5B . 1.3386(17) ? N1B C1B . 1.3549(17) ? C1B C2B . 1.367(2) ? C1B H1B . 0.9300 ? C2B C3B . 1.387(3) ? C2B H2B . 0.9300 ? C3B C4B . 1.369(2) ? C3B H3B . 0.9300 ? C4B C5B . 1.403(2) ? C4B H4B . 0.9300 ? C5B N2B . 1.3824(18) ? N2B C6B . 1.3802(18) ? N2B H22 . 0.8900 ? C6B N3B . 1.3350(18) ? C6B C7B . 1.4059(19) ? C7B C8B . 1.367(2) ? C7B H7B . 0.9300 ? C8B C9B . 1.387(3) ? C8B H8B . 0.9300 ? C9B C10B . 1.371(2) ? C9B H9B . 0.9300 ? C10B N3B . 1.3534(18) ? C10B H10B . 0.9300 ? O1 H1 . 0.8500(10) ? O1 H2 . 0.8500(10) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N2A H21 N1 1_455 0.89 2.21 3.1012(15) 175 yes N2B H22 O1 . 0.89 1.96 2.8479(17) 172 yes O1 H1 N6 2_667 0.8500(10) 2.060(7) 2.894(2) 167(3) yes O1 H2 N6 1_465 0.8500(10) 2.063(3) 2.911(2) 176(3) yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C5A N1A C1A C2A . . . . -4.5(2) ? Fe1 N1A C1A C2A . . . . 159.85(13) ? N1A C1A C2A C3A . . . . 1.3(2) ? C1A C2A C3A C4A . . . . 1.8(2) ? C2A C3A C4A C5A . . . . -1.7(2) ? C1A N1A C5A N2A . . . . -176.65(12) ? Fe1 N1A C5A N2A . . . . 20.36(17) ? C1A N1A C5A C4A . . . . 4.54(19) ? Fe1 N1A C5A C4A . . . . -158.45(11) ? C3A C4A C5A N1A . . . . -1.6(2) ? C3A C4A C5A N2A . . . . 179.57(14) ? N1A C5A N2A C6A . . . . 26.3(2) ? C4A C5A N2A C6A . . . . -154.82(13) ? C5A N2A C6A N3A . . . . -29.1(2) ? C5A N2A C6A C7A . . . . 151.72(14) ? N3A C6A C7A C8A . . . . 0.4(2) ? N2A C6A C7A C8A . . . . 179.51(14) ? C6A C7A C8A C9A . . . . 2.1(2) ? C7A C8A C9A C10A . . . . -1.5(2) ? C8A C9A C10A N3A . . . . -1.6(2) ? N2A C6A N3A C10A . . . . 177.64(12) ? C7A C6A N3A C10A . . . . -3.25(19) ? N2A C6A N3A Fe1 . . . . -14.53(17) ? C7A C6A N3A Fe1 . . . . 164.58(11) ? C9A C10A N3A C6A . . . . 3.9(2) ? C9A C10A N3A Fe1 . . . . -164.56(12) ? C5B N1B C1B C2B . . . . 3.9(2) ? Fe1 N1B C1B C2B . . . . -163.01(13) ? N1B C1B C2B C3B . . . . -1.2(3) ? C1B C2B C3B C4B . . . . -1.9(3) ? C2B C3B C4B C5B . . . . 2.2(3) ? C1B N1B C5B N2B . . . . 178.21(13) ? Fe1 N1B C5B N2B . . . . -15.71(18) ? C1B N1B C5B C4B . . . . -3.6(2) ? Fe1 N1B C5B C4B . . . . 162.50(11) ? C3B C4B C5B N1B . . . . 0.6(2) ? C3B C4B C5B N2B . . . . 178.86(15) ? N1B C5B N2B C6B . . . . -23.0(2) ? C4B C5B N2B C6B . . . . 158.66(15) ? C5B N2B C6B N3B . . . . 15.5(2) ? C5B N2B C6B C7B . . . . -165.32(15) ? N3B C6B C7B C8B . . . . -1.9(2) ? N2B C6B C7B C8B . . . . 179.00(15) ? C6B C7B C8B C9B . . . . -1.2(3) ? C7B C8B C9B C10B . . . . 1.7(3) ? C8B C9B C10B N3B . . . . 0.9(3) ? N2B C6B N3B C10B . . . . -176.64(13) ? C7B C6B N3B C10B . . . . 4.3(2) ? N2B C6B N3B Fe1 . . . . 29.71(18) ? C7B C6B N3B Fe1 . . . . -149.40(12) ? C9B C10B N3B C6B . . . . -3.8(2) ? C9B C10B N3B Fe1 . . . . 151.83(14) ?