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Information card for entry 1571754
Preview
| Coordinates | 1571754.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C83 H60 Cl6 |
|---|---|
| Calculated formula | C83 H60 Cl6 |
| Title of publication | Helically twisted nanoribbons <i>via</i> stereospecific annulative π-extension reaction employing [7]helicene as a molecular wrench. |
| Authors of publication | Swain, Asim; Radacki, Krzysztof; Braunschweig, Holger; Ravat, Prince |
| Journal of publication | Chemical science |
| Year of publication | 2024 |
| Journal volume | 15 |
| Journal issue | 30 |
| Pages of publication | 11737 - 11747 |
| a | 14.6922 ± 0.0004 Å |
| b | 15.4658 ± 0.0004 Å |
| c | 16.5251 ± 0.0004 Å |
| α | 114.189 ± 0.003° |
| β | 109.595 ± 0.003° |
| γ | 93.418 ± 0.002° |
| Cell volume | 3140.92 ± 0.19 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100.01 ± 0.1 K |
| Number of distinct elements | 3 |
| Space group number | 1 |
| Hermann-Mauguin space group symbol | P 1 |
| Hall space group symbol | P 1 |
| Residual factor for all reflections | 0.1143 |
| Residual factor for significantly intense reflections | 0.0936 |
| Weighted residual factors for significantly intense reflections | 0.2424 |
| Weighted residual factors for all reflections included in the refinement | 0.2691 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.052 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 293770 (current) | 2024-08-05 | cif/ Updating files of 1571753, 1571754 Original log message: Adding full bibliography for 1571753--1571754.cif. |
1571754.cif |
| 292136 | 2024-06-01 | cif/ Adding structures of 1571753, 1571754 via cif-deposit CGI script. |
1571754.cif |
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Users of the data should acknowledge the original authors of the
structural data.