#------------------------------------------------------------------------------ #$Date: 2024-07-05 17:11:09 +0300 (Fri, 05 Jul 2024) $ #$Revision: 292875 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571738.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571738 loop_ _publ_author_name 'Karmakar, Pratik' 'Finnegan, Tyler J.' 'Rostam, Darian C.' 'Taneja, Sagarika' 'U\,car, Sefa' 'Hansen, Alexandar L.' 'Moore, Curtis E.' 'Hadad, Christopher M.' 'Pratumyot, Kornkanya' 'Parquette, Jon R.' 'Badji\'c, Jovica D.' _publ_section_title ; Molecular bowls for inclusion complexation of toxic anticancer drug methotrexate ; _journal_issue 26 _journal_name_full 'Chemical Science' _journal_page_first 10155 _journal_page_last 10163 _journal_paper_doi 10.1039/D3SC05627A _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'C92 H64 N6, 6(C2 F3 O2), 3[C2H3N]' _chemical_formula_sum 'C110 H73 F17 N9 O12' _chemical_formula_weight 2035.77 _space_group_crystal_system trigonal _space_group_IT_number 159 _space_group_name_Hall 'P 3 -2c' _space_group_name_H-M_alt 'P 3 1 c' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-08-15 _audit_creation_method ; Olex2 1.5-alpha (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6813) ; _audit_update_record ; 2023-08-15 deposited with the CCDC. 2024-05-16 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 2 _cell_length_a 25.2070(12) _cell_length_b 25.2070(12) _cell_length_c 14.9840(10) _cell_measurement_reflns_used 9043 _cell_measurement_temperature 100.0 _cell_measurement_theta_max 20.826 _cell_measurement_theta_min 2.308 _cell_volume 8245.2(8) _computing_cell_refinement 'SAINT v8.40B (Bruker, 2021)' _computing_data_collection 'APEX3 v2022.10-0 (Bruker, 2022)' _computing_data_reduction 'SAINT v8.40B (Bruker, 2021)' _computing_molecular_graphics 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 100.0 _diffrn_detector 'Bruker Photon III area detector' _diffrn_detector_area_resol_mean 10.5 _diffrn_detector_type 'CMOS area detector' _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device 'Kappa Four-Circle Diffractometer' _diffrn_measurement_device_type 'Bruker Kappa Photon III MoTXS' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator 'Double Bounce Multilayer Mirrors' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_xray_symbol K-L~3~ _diffrn_reflns_av_R_equivalents 0.1244 _diffrn_reflns_av_unetI/netI 0.0702 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 25 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 41774 _diffrn_reflns_point_group_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_theta_full 20.868 _diffrn_reflns_theta_max 20.868 _diffrn_reflns_theta_min 1.866 _diffrn_source 'Micro Focus Rotating Anode' _diffrn_source_current 50.0 _diffrn_source_power 2.5 _diffrn_source_type 'Bruker TXS' _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.067 _exptl_absorpt_correction_T_max 0.0847 _exptl_absorpt_correction_T_min 0.0626 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1333 before and 0.0750 after correction. The Ratio of minimum to maximum transmission is 0.7391. The \l/2 correction factor is Not present. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 0.820 _exptl_crystal_description block _exptl_crystal_F_000 2090 _exptl_crystal_size_max 0.452 _exptl_crystal_size_mid 0.232 _exptl_crystal_size_min 0.228 _refine_diff_density_max 0.603 _refine_diff_density_min -0.389 _refine_diff_density_rms 0.093 _refine_ls_abs_structure_details ; Flack x determined using 878 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.9(6) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.396 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 334 _refine_ls_number_reflns 5758 _refine_ls_number_restraints 760 _refine_ls_restrained_S_all 1.380 _refine_ls_R_factor_all 0.2652 _refine_ls_R_factor_gt 0.1611 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3690 _refine_ls_wR_factor_ref 0.4500 _reflns_Friedel_coverage 0.983 _reflns_Friedel_fraction_full 0.987 _reflns_Friedel_fraction_max 0.987 _reflns_number_gt 2539 _reflns_number_total 5758 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d3sc05627a2.cif _cod_data_source_block Badjic_PK20230327 _cod_depositor_comments ; The following automatic conversions were performed: data item '_diffrn_radiation_probe' value 'X-ray' was changed to 'x-ray' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas Adding full bibliography for 1571738.cif. ; _cod_original_cell_volume 8245.2(10) _cod_database_code 1571738 _shelx_shelxl_version_number 2019/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Twinned data refinement Scales: 0.539(18) 0.461(18) 2. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 3. Restrained distances C6-C5 = C10-C5 = C10-C9 = C8-C9 = C8-C7 = C6-C7 = C13-C15 = C16-C15 = C17-C16 = N1-C14 = N1-C17 = C13-C14 = C20-C21 = C20-C22 = C23-C22 = C24-C23 = N2-C24 = N2-C21 = C28-C27 = C31-C30 = C31-C26 = C26-C27 = C29-C28 = C29-C30 1.39 with sigma of 0.005 C29-C32 = N2-C32 = C26-C25 = N1-C25 1.45 with sigma of 0.02 C11-C12 = C19-C18 1.1 with sigma of 0.02 C14-C25 2.5 with sigma of 0.02 C17-C25 2.5 with sigma of 0.02 C21-C32 2.5 with sigma of 0.02 C24-C32 2.5 with sigma of 0.02 C30-C32 2.5 with sigma of 0.02 C32-C28 2.5 with sigma of 0.02 C27-C25 2.5 with sigma of 0.02 C31-C25 2.5 with sigma of 0.02 F7A-C6A = F8A-C6A 1.34 with sigma of 0.02 F9A-C6A 1.33 with sigma of 0.02 O5A-C5A 1.25 with sigma of 0.02 O6A-C5A 1.24 with sigma of 0.02 C5A-C6A 1.55 with sigma of 0.02 F1A-C2A = F3A-C2A 1.34 with sigma of 0.02 F2A-C2A 1.33 with sigma of 0.02 O1A-C1A 1.25 with sigma of 0.02 O2A-C1A 1.24 with sigma of 0.02 C1A-C2A 1.55 with sigma of 0.02 F5A-C4A = F4A-C4A 1.34 with sigma of 0.02 F6A-C4A 1.33 with sigma of 0.02 O3A-C3A 1.25 with sigma of 0.02 O4A-C3A 1.24 with sigma of 0.02 C3A-C4A 1.55 with sigma of 0.02 F12A-C8A = F10A-C8A 1.34 with sigma of 0.02 F11A-C8A 1.33 with sigma of 0.02 O8A-C7A 1.25 with sigma of 0.02 O7A-C7A 1.24 with sigma of 0.02 C7A-C8A 1.55 with sigma of 0.02 F7A-F9A = F9A-F8A 2.16 with sigma of 0.04 F7A-F8A 2.15 with sigma of 0.04 F7A-C5A 2.37 with sigma of 0.04 F9A-C5A 2.42 with sigma of 0.04 F8A-C5A 2.39 with sigma of 0.04 O5A-O6A 2.25 with sigma of 0.04 O5A-C6A 2.38 with sigma of 0.04 O6A-C6A 2.35 with sigma of 0.04 F1A-F2A = F2A-F3A 2.16 with sigma of 0.04 F1A-F3A 2.15 with sigma of 0.04 F1A-C1A 2.37 with sigma of 0.04 F2A-C1A 2.42 with sigma of 0.04 F3A-C1A 2.39 with sigma of 0.04 O1A-O2A 2.25 with sigma of 0.04 O1A-C2A 2.38 with sigma of 0.04 O2A-C2A 2.35 with sigma of 0.04 F5A-F6A = F6A-F4A 2.16 with sigma of 0.04 F5A-F4A 2.15 with sigma of 0.04 F5A-C3A 2.37 with sigma of 0.04 F6A-C3A 2.42 with sigma of 0.04 F4A-C3A 2.39 with sigma of 0.04 O3A-O4A 2.25 with sigma of 0.04 O3A-C4A 2.38 with sigma of 0.04 O4A-C4A 2.35 with sigma of 0.04 F12A-F11A = F11A-F10A 2.16 with sigma of 0.04 F12A-F10A 2.15 with sigma of 0.04 F12A-C7A 2.37 with sigma of 0.04 F11A-C7A 2.42 with sigma of 0.04 F10A-C7A 2.39 with sigma of 0.04 O8A-O7A 2.25 with sigma of 0.04 O8A-C8A 2.38 with sigma of 0.04 O7A-C8A 2.35 with sigma of 0.04 C6A-F7A \\sim C6A-F9A \\sim C6A-F8A with sigma of 0.02 C5A-F7A \\sim C5A-F9A \\sim C5A-F8A with sigma of 0.04 F7A-F9A \\sim F9A-F8A \\sim F8A-F7A with sigma of 0.04 C5A-O6A \\sim C5A-O5A with sigma of 0.02 C2A-F1A \\sim C2A-F2A \\sim C2A-F3A with sigma of 0.02 C1A-F1A \\sim C1A-F2A \\sim C1A-F3A with sigma of 0.04 F1A-F2A \\sim F2A-F3A \\sim F3A-F1A with sigma of 0.04 C1A-O2A \\sim C1A-O1A with sigma of 0.02 C4A-F5A \\sim C4A-F6A \\sim C4A-F4A with sigma of 0.02 C3A-F5A \\sim C3A-F6A \\sim C3A-F4A with sigma of 0.04 F5A-F6A \\sim F6A-F4A \\sim F4A-F5A with sigma of 0.04 C3A-O4A \\sim C3A-O3A with sigma of 0.02 C8A-F12A \\sim C8A-F11A \\sim C8A-F10A with sigma of 0.02 C7A-F12A \\sim C7A-F11A \\sim C7A-F10A with sigma of 0.04 F12A-F11A \\sim F11A-F10A \\sim F10A-F12A with sigma of 0.04 C7A-O7A \\sim C7A-O8A with sigma of 0.02 4. Restrained planarity C11, C12, C13, C14, N1, C17, C16, C15, C25 with sigma of 0.005 C32, C25, C26, C27, C28, C29, C30, C31 with sigma of 0.005 C18, C19, C20, C22, C23, C24, N2, C21, C32 with sigma of 0.005 C5A, C6A, O5A, O6A with sigma of 0.1 C1A, C2A, O1A, O2A with sigma of 0.1 C3A, C4A, O3A, O4A with sigma of 0.1 C7A, C8A, O8A, O7A with sigma of 0.1 5. Uiso/Uaniso restraints and constraints F7A \\sim F9A \\sim F8A \\sim O5A \\sim O6A \\sim C5A \\sim C6A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A F1A \\sim F2A \\sim F3A \\sim O1A \\sim O2A \\sim C1A \\sim C2A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A F5A \\sim F6A \\sim F4A \\sim O3A \\sim O4A \\sim C3A \\sim C4A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A F12A \\sim F11A \\sim F10A \\sim O8A \\sim O7A \\sim C7A \\sim C8A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A Uanis(C31) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C11) = Uanis(C18) Uanis(C12) = Uanis(C19) Uanis(C13) = Uanis(C20) Uanis(C14) = Uanis(C21) Uanis(N1) = Uanis(N2) Uanis(C17) = Uanis(C24) Uanis(C16) = Uanis(C23) Uanis(C15) = Uanis(C22) Uanis(O5A) = Uanis(F7A) = Uanis(C6A) = Uanis(F9A) = Uanis(F8A) = Uanis(C5A) = Uanis(O6A) = Uanis(O1A) = Uanis(F1A) = Uanis(C2A) = Uanis(F2A) = Uanis(F3A) = Uanis(C1A) = Uanis(O2A) Uanis(C32) = Uanis(C29) = Uanis(C28) = Uanis(C27) = Uanis(C26) = Uanis(C31) = Uanis(C25) = Uanis(C30) 6. Rigid body (RIGU) restrains All non-hydrogen atoms with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 7. Others Fixed Sof: H32A(0.333333) H1A(0.333333) H1B(0.333333) H1C(0.333333) F7A(0.333333) F9A(0.333333) F8A(0.333333) O5A(0.333333) O6A(0.333333) C5A(0.333333) C6A(0.333333) F1A(0.666667) F2A(0.666667) F3A(0.333333) O1A(0.666667) O2A(0.666667) C1A(0.666667) C2A(0.666667) F5A(0.666667) F6A(0.666667) F4A(0.666667) O3A(0.666667) O4A(0.666667) C3A(0.666667) C4A(0.666667) F12A(0.333333) F11A(0.333333) F10A(0.333333) O8A(0.333333) O7A(0.333333) C7A(0.333333) C8A(0.333333) 8.a Secondary CH2 refined with riding coordinates: C32(H32A,H32B), C25(H25A,H25B) 8.b Aromatic/amide H refined with riding coordinates: C10(H10), C7(H7), C22(H22), C23(H23), C24(H24), C21(H21), C15(H15), C16(H16), C17(H17), C14(H14), C27(H27), C28(H28), C30(H30), C31(H31) 8.c Fitted hexagon refined as free rotating group: C5(C10,C9,C8,C7,C6), C20(C22,C23,C24,N2,C21), C13(C15,C16,C17,N1,C14), C26(C27,C28,C29,C30,C31) 8.d Idealised Me refined as rotating group: C4(H4A,H4B,H4C), C1(H1A,H1B,H1C) ; _smtbx_masks_special_details ; A solvent mask was calculated and 148 electrons were found in a volume of 3458\%A^3^ in 1 void per unit cell. This is consistent with the presence of 3[C2H3N] per Asymmetric Unit which account for 132 electrons per unit cell. ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL Badjic_PK20230327 in P-31c p-31c.res created by SHELXL-2019/1 at 13:31:58 on 15-Aug-2023 REM SHELXT solution in P31c: R1 0.443, Rweak 0.132, Alpha 0.072 REM 0.747 for 145 systematic absences, Orientation as input REM Flack x = -0.061 ( 1.532 ) from 948 Parsons' quotients REM Formula found by SHELXT: C52 N35 CELL 0.71073 25.207 25.207 14.984 90 90 120 ZERR 2 0.0012 0.0012 0.001 0 0 0 LATT -1 SYMM -Y,+X-Y,+Z SYMM +Y-X,-X,+Z SYMM +Y,+X,0.5+Z SYMM -Y+X,-Y,0.5+Z SYMM -X,-X+Y,0.5+Z SFAC C H F N O UNIT 220 146 34 18 24 RIGU DFIX 1.39 0.005 C6 C5 C10 C5 C10 C9 C8 C9 C8 C7 C6 C7 C13 C15 C16 C15 C17 = C16 N1 C14 N1 C17 C13 C14 C20 C21 C20 C22 C23 C22 C24 C23 N2 C24 N2 C21 C28 = C27 C31 C30 C31 C26 C26 C27 C29 C28 C29 C30 DFIX 1.45 C29 C32 N2 C32 C26 C25 N1 C25 DFIX 1.1 C11 C12 C19 C18 FLAT 0.005 C11 C12 C13 C14 N1 C17 C16 C15 C25 FLAT 0.005 C32 C25 C26 C27 C28 C29 C30 C31 FLAT 0.005 C18 C19 C20 C22 C23 C24 N2 C21 C32 DFIX 2.5 C14 C25 DFIX 2.5 C17 C25 DFIX 2.5 C21 C32 DFIX 2.5 C24 C32 DFIX 2.5 C30 C32 DFIX 2.5 C32 C28 DFIX 2.5 C27 C25 DFIX 2.5 C31 C25 EADP C11 C18 EADP C12 C19 EADP C13 C20 EADP C14 C21 EADP N1 N2 EADP C17 C24 EADP C16 C23 EADP C15 C22 DFIX 1.34 F7A C6A F8A C6A DANG 2.16 F7A F9A F9A F8A DANG 2.15 F7A F8A DANG 2.37 F7A C5A DFIX 1.33 F9A C6A DANG 2.42 F9A C5A DANG 2.39 F8A C5A DFIX 1.25 O5A C5A DANG 2.25 O5A O6A DANG 2.38 O5A C6A DFIX 1.24 O6A C5A DANG 2.35 O6A C6A DFIX 1.55 C5A C6A SADI C6A F7A C6A F9A C6A F8A SADI 0.04 C5A F7A C5A F9A C5A F8A SADI 0.04 F7A F9A F9A F8A F8A F7A SADI C5A O6A C5A O5A FLAT C5A C6A O5A O6A SIMU F7A F9A F8A O5A O6A C5A C6A DFIX 1.34 F1A C2A F3A C2A DANG 2.16 F1A F2A F2A F3A DANG 2.15 F1A F3A DANG 2.37 F1A C1A DFIX 1.33 F2A C2A DANG 2.42 F2A C1A DANG 2.39 F3A C1A DFIX 1.25 O1A C1A DANG 2.25 O1A O2A DANG 2.38 O1A C2A DFIX 1.24 O2A C1A DANG 2.35 O2A C2A DFIX 1.55 C1A C2A SADI C2A F1A C2A F2A C2A F3A SADI 0.04 C1A F1A C1A F2A C1A F3A SADI 0.04 F1A F2A F2A F3A F3A F1A SADI C1A O2A C1A O1A FLAT C1A C2A O1A O2A SIMU F1A F2A F3A O1A O2A C1A C2A EADP O5A F7A C6A F9A F8A C5A O6A O1A F1A C2A F2A F3A C1A O2A DFIX 1.34 F5A C4A F4A C4A DANG 2.16 F5A F6A F6A F4A DANG 2.15 F5A F4A DANG 2.37 F5A C3A DFIX 1.33 F6A C4A DANG 2.42 F6A C3A DANG 2.39 F4A C3A DFIX 1.25 O3A C3A DANG 2.25 O3A O4A DANG 2.38 O3A C4A DFIX 1.24 O4A C3A DANG 2.35 O4A C4A DFIX 1.55 C3A C4A SADI C4A F5A C4A F6A C4A F4A SADI 0.04 C3A F5A C3A F6A C3A F4A SADI 0.04 F5A F6A F6A F4A F4A F5A SADI C3A O4A C3A O3A FLAT C3A C4A O3A O4A SIMU F5A F6A F4A O3A O4A C3A C4A DFIX 1.34 F12A C8A F10A C8A DANG 2.16 F12A F11A F11A F10A DANG 2.15 F12A F10A DANG 2.37 F12A C7A DFIX 1.33 F11A C8A DANG 2.42 F11A C7A DANG 2.39 F10A C7A DFIX 1.25 O8A C7A DANG 2.25 O8A O7A DANG 2.38 O8A C8A DFIX 1.24 O7A C7A DANG 2.35 O7A C8A DFIX 1.55 C7A C8A SADI C8A F12A C8A F11A C8A F10A SADI 0.04 C7A F12A C7A F11A C7A F10A SADI 0.04 F12A F11A F11A F10A F10A F12A SADI C7A O7A C7A O8A FLAT C7A C8A O8A O7A SIMU F12A F11A F10A O8A O7A C7A C8A ISOR 0.01 0.02 C31 EADP C32 C29 C28 C27 C26 C31 C25 C30 L.S. 100 PLAN 10 TEMP -173.15 CONF FREE O3A H14 BOND list 4 MORE -1 BOND $H ABIN fmap 2 acta TWIN 0 1 0 1 0 0 0 0 -1 2 REM REM REM WGHT 0.200000 BASF 0.46148 FVAR 0.31761 PART 1 AFIX 66 C5 1 0.596111 0.249246 0.566950 11.00000 0.11031 0.07632 = 0.08711 0.01137 0.00350 0.04930 C10 1 0.547325 0.205756 0.516734 11.00000 0.11037 0.07644 = 0.11050 0.00563 0.00190 0.04058 AFIX 43 H10 2 0.509527 0.205529 0.516020 11.00000 -1.20000 AFIX 65 C9 1 0.553844 0.162599 0.467562 11.00000 0.11494 0.06740 = 0.11255 0.01195 0.00624 0.03458 C8 1 0.609149 0.162931 0.468604 11.00000 0.11864 0.08382 = 0.13583 -0.01922 -0.00206 0.04229 C7 1 0.657935 0.206420 0.518819 11.00000 0.10732 0.06366 = 0.09253 0.01964 0.00765 0.03431 AFIX 43 H7 2 0.695734 0.206647 0.519531 11.00000 -1.20000 AFIX 65 C6 1 0.651417 0.249578 0.567993 11.00000 0.10013 0.07045 = 0.08654 0.00862 -0.00197 0.03500 AFIX 0 C2 1 0.666667 0.333333 0.662790 10.33333 0.11833 0.11833 = 0.08996 0.00000 0.00000 0.05917 C4 1 0.543623 0.271517 0.696598 11.00000 0.13718 0.08695 = 0.11053 0.00704 0.00962 0.07417 AFIX 137 H4A 2 0.526250 0.227034 0.699863 11.00000 -1.50000 H4B 2 0.511978 0.280653 0.676866 11.00000 -1.50000 H4C 2 0.558578 0.289530 0.755664 11.00000 -1.50000 AFIX 0 C3 1 0.601358 0.300898 0.624396 11.00000 0.11277 0.08771 = 0.08746 0.00272 -0.00903 0.05301 AFIX 66 C20 1 0.402441 0.048925 0.318936 11.00000 0.17936 0.18093 = 0.26461 -0.11291 -0.03048 0.09251 C22 1 0.348926 0.043776 0.353654 11.00000 0.18687 0.21071 = 0.27110 -0.09789 -0.02095 0.11050 AFIX 43 H22 2 0.351038 0.073087 0.395497 11.00000 -1.20000 AFIX 65 C23 1 0.292320 -0.004260 0.327149 11.00000 0.19928 0.21838 = 0.32399 -0.11504 -0.03166 0.11875 AFIX 43 H23 2 0.255745 -0.007779 0.350877 11.00000 -1.20000 AFIX 65 C24 1 0.289229 -0.047147 0.265925 11.00000 0.23893 0.25344 = 0.31699 -0.13277 -0.04756 0.14142 AFIX 43 H24 2 0.250541 -0.079977 0.247810 11.00000 -1.20000 AFIX 65 N2 4 0.342744 -0.041999 0.231206 11.00000 0.22741 0.20445 = 0.30263 -0.14356 -0.05717 0.11164 C21 1 0.399350 0.006037 0.257711 11.00000 0.20184 0.20040 = 0.26877 -0.11987 -0.03536 0.10721 AFIX 43 H21 2 0.435925 0.009555 0.233982 11.00000 -1.20000 AFIX 0 C19 1 0.467630 0.093439 0.373576 11.00000 0.16019 0.17870 = 0.23140 -0.08631 -0.02361 0.08478 C18 1 0.510145 0.122469 0.409215 11.00000 0.13778 0.09330 = 0.14024 -0.01092 0.00749 0.04517 C32 1 0.336778 -0.070758 0.141372 11.00000 0.24862 0.18901 = 0.28311 -0.14747 -0.06002 0.10554 AFIX 23 H32A 2 0.302606 -0.113629 0.139080 10.33333 -1.20000 H32B 2 0.332446 -0.046680 0.092624 11.00000 -1.20000 AFIX 0 C1 1 0.666667 0.333333 0.770037 10.33333 0.09346 0.09346 = 0.08453 0.00000 0.00000 0.04673 AFIX 137 H1A 2 0.686317 0.375623 0.791838 10.33333 -1.50000 H1B 2 0.689306 0.313683 0.791838 10.33333 -1.50000 H1C 2 0.624377 0.310694 0.791838 10.33333 -1.50000 AFIX 66 C13 1 0.648557 0.047461 0.331571 11.00000 0.17936 0.18093 = 0.26461 -0.11291 -0.03048 0.09251 C15 1 0.675751 0.017819 0.373343 11.00000 0.18687 0.21071 = 0.27110 -0.09789 -0.02095 0.11050 AFIX 43 H15 2 0.697993 0.033792 0.427223 11.00000 -1.20000 AFIX 65 C16 1 0.670401 -0.035194 0.336281 11.00000 0.19928 0.21838 = 0.32399 -0.11504 -0.03166 0.11875 AFIX 43 H16 2 0.688986 -0.055453 0.364831 11.00000 -1.20000 AFIX 65 C17 1 0.637857 -0.058566 0.257447 11.00000 0.23893 0.25344 = 0.31699 -0.13277 -0.04756 0.14142 AFIX 43 H17 2 0.634201 -0.094798 0.232117 11.00000 -1.20000 AFIX 65 N1 4 0.610664 -0.028925 0.215674 11.00000 0.22741 0.20445 = 0.30263 -0.14356 -0.05717 0.11164 C14 1 0.616012 0.024089 0.252735 11.00000 0.20184 0.20040 = 0.26877 -0.11987 -0.03536 0.10721 AFIX 43 H14 2 0.597426 0.044347 0.224186 11.00000 -1.20000 AFIX 0 C12 1 0.630717 0.087484 0.380597 11.00000 0.16019 0.17870 = 0.23140 -0.08631 -0.02361 0.08478 C11 1 0.617684 0.116739 0.416439 11.00000 0.13778 0.09330 = 0.14024 -0.01092 0.00749 0.04517 C25 1 0.570186 -0.058477 0.135884 11.00000 0.24862 0.18901 = 0.28311 -0.14747 -0.06002 0.10554 AFIX 23 H25A 2 0.592713 -0.035832 0.081831 11.00000 -1.20000 H25B 2 0.562856 -0.100768 0.130498 11.00000 -1.20000 AFIX 66 C26 1 0.509456 -0.061349 0.136753 11.00000 0.24862 0.18901 = 0.28311 -0.14747 -0.06002 0.10554 C27 1 0.497144 -0.026620 0.077145 11.00000 0.24862 0.18901 = 0.28311 -0.14747 -0.06002 0.10554 AFIX 43 H27 2 0.527289 -0.001056 0.034962 11.00000 -1.20000 AFIX 65 C28 1 0.440725 -0.029297 0.079257 11.00000 0.24862 0.18901 = 0.28311 -0.14747 -0.06002 0.10554 AFIX 43 H28 2 0.432310 -0.005561 0.038517 11.00000 -1.20000 AFIX 65 C29 1 0.396618 -0.066701 0.140977 11.00000 0.24862 0.18901 = 0.28311 -0.14747 -0.06002 0.10554 C30 1 0.408930 -0.101430 0.200585 11.00000 0.24862 0.18901 = 0.28311 -0.14747 -0.06002 0.10554 AFIX 43 H30 2 0.378785 -0.126995 0.242768 11.00000 -1.20000 AFIX 65 C31 1 0.465348 -0.098755 0.198475 11.00000 0.24862 0.18901 = 0.28311 -0.14747 -0.06002 0.10554 AFIX 43 H31 2 0.473763 -0.122490 0.239214 11.00000 -1.20000 AFIX 0 PART -2 F7A 3 0.645411 0.338527 0.396845 10.33333 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 F9A 3 0.630358 0.247355 0.392340 10.33333 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 F8A 3 0.657618 0.303093 0.272607 10.33333 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 O5A 5 0.547933 0.299847 0.273847 10.33333 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 O6A 5 0.520099 0.213279 0.355585 10.33333 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 C5A 1 0.555116 0.264090 0.322116 10.33333 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 C6A 1 0.623587 0.288530 0.346315 10.33333 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 PART -1 F1A 3 0.423048 0.265140 0.370539 10.66667 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 F2A 3 0.463081 0.209092 0.408707 10.66667 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 F3A 3 0.381400 0.173964 0.323479 10.33333 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 O1A 5 0.393390 0.198523 0.554483 10.66667 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 O2A 5 0.314019 0.164253 0.449331 10.66667 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 C1A 1 0.368577 0.187422 0.477746 10.66667 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 C2A 1 0.409703 0.208090 0.394637 10.66667 0.23602 0.20713 = 0.32864 -0.01342 -0.03911 0.12078 F5A 3 0.635743 0.208339 0.094402 10.66667 0.26965 0.33250 = 0.30754 0.00877 0.04352 0.09449 F6A 3 0.569373 0.171522 0.192022 10.66667 0.30554 0.26234 = 0.29245 0.01797 0.07969 0.12377 F4A 3 0.664061 0.223107 0.228912 10.66667 0.31193 0.26935 = 0.29325 0.01297 0.05888 0.13677 O3A 5 0.579863 0.074981 0.203401 10.66667 0.28750 0.25619 = 0.13380 -0.05638 0.00134 0.09772 O4A 5 0.666825 0.104789 0.146276 10.66667 0.30710 0.23596 = 0.27164 0.02708 0.07530 0.11154 C3A 1 0.627987 0.119066 0.171585 10.66667 0.29301 0.27327 = 0.24947 -0.02117 0.04299 0.11662 C4A 1 0.625059 0.178822 0.172892 10.66667 0.30028 0.27448 = 0.29308 -0.00682 0.06318 0.12125 F12A 3 0.382599 0.136424 0.003883 10.33333 0.30717 0.27335 = 0.25762 -0.05551 0.04474 0.11971 F11A 3 0.463709 0.215313 0.055975 10.33333 0.33745 0.25422 = 0.25209 -0.03044 0.04858 0.11407 F10A 3 0.373878 0.202061 0.086757 10.33333 0.33360 0.25320 = 0.22306 -0.04120 0.05230 0.11160 O8A 5 0.424768 0.226380 -0.135754 10.33333 0.28099 0.33420 = 0.21930 -0.04149 0.07026 0.15240 O7A 5 0.385589 0.266186 -0.037022 10.33333 0.11296 0.15359 = 0.20656 -0.04939 0.06207 -0.02800 C7A 1 0.407166 0.232812 -0.059901 10.33333 0.28713 0.27396 = 0.22346 -0.04055 0.07323 0.11595 C8A 1 0.407957 0.196275 0.022560 10.33333 0.32933 0.26584 = 0.22626 -0.04490 0.05523 0.11593 HKLF 4 REM Badjic_PK20230327 in P-31c REM wR2 = 0.4500, GooF = S = 1.396, Restrained GooF = 1.380 for all data REM R1 = 0.1611 for 2539 Fo > 4sig(Fo) and 0.2652 for all 5758 data REM 334 parameters refined using 760 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 0.603, deepest hole -0.389, 1-sigma level 0.093 Q1 1 0.6667 0.3333 0.3740 10.33333 0.05 0.60 Q2 1 0.6764 0.0322 0.3544 11.00000 0.05 0.44 Q3 1 0.4694 -0.0812 0.1619 11.00000 0.05 0.35 Q4 1 0.3899 0.2182 0.5808 11.00000 0.05 0.35 Q5 1 0.5647 0.1514 0.4474 11.00000 0.05 0.32 Q6 1 0.4503 0.0825 0.3541 11.00000 0.05 0.31 Q7 1 0.3391 -0.1098 0.1871 11.00000 0.05 0.29 Q8 1 0.6057 0.0939 0.4014 11.00000 0.05 0.29 Q9 1 0.4078 0.0218 0.3084 11.00000 0.05 0.29 Q10 1 0.6597 0.0370 0.0346 11.00000 0.05 0.29 ; _shelx_res_checksum 16632 _shelx_fab_file ; 0 0 2 40.7050 41.2407 0 0 4 48.3681 -9.3312 0 0 6 -3.3662 5.9765 0 0 8 22.7910 -19.0420 0 0 10 -1.0920 -12.3872 0 0 12 0.6869 -1.9156 0 0 14 1.6683 -0.7737 1 0 0 -22.4575 0.0463 1 0 1 -2.7618 -34.6597 1 0 2 -33.5665 13.7616 1 0 3 8.3827 -9.1571 1 0 4 -14.7598 10.3978 1 0 5 1.8676 -6.8832 1 0 6 -1.8876 10.0849 1 0 7 -1.5643 -3.6586 1 0 8 4.6193 -1.4577 1 0 9 -2.1865 -1.4927 1 0 10 -0.9638 1.9811 1 0 11 -1.1422 -0.8854 1 0 12 -0.6050 0.0675 1 0 13 0.3452 -0.8158 1 0 14 -0.1000 -0.5779 1 0 15 0.7908 -1.1646 1 1 -14 1.8725 -5.9912 1 1 -12 0.0853 -0.5346 1 1 -10 7.1194 -4.3860 1 1 -8 -4.3941 -0.8213 1 1 -6 0.2885 -1.1283 1 1 -4 14.9075 -6.1705 1 1 -2 13.4876 3.7585 1 1 0 -39.2417 -11.8642 1 1 2 -7.8065 9.5457 1 1 4 -32.4699 32.7641 1 1 6 13.2329 21.9794 1 1 8 -0.0973 0.3119 1 1 10 -2.7047 -0.5709 1 1 12 2.3810 -0.0945 1 1 14 -5.1589 -0.2027 2 0 0 -58.7775 0.0172 2 0 1 -5.5512 -7.2190 2 0 2 48.8042 -16.0902 2 0 3 17.4269 42.2831 2 0 4 18.2015 -36.3140 2 0 5 -9.6981 1.6308 2 0 6 -1.8531 -17.8090 2 0 7 -2.9112 1.0168 2 0 8 -1.3587 -6.2312 2 0 9 5.7400 1.1665 2 0 10 -1.1053 -4.3229 2 0 11 1.6370 3.0535 2 0 12 -0.8575 0.8421 2 0 13 -1.1443 -0.6479 2 0 14 -4.8554 1.6074 2 1 -14 -2.4290 -4.2344 2 1 -13 -0.4627 -1.2005 2 1 -12 -0.1077 0.1426 2 1 -11 -0.0231 -2.2899 2 1 -10 0.5641 -4.8795 2 1 -9 -5.0992 -1.9252 2 1 -8 0.3864 -0.8267 2 1 -7 -10.7803 10.1252 2 1 -6 -1.7160 6.5952 2 1 -5 -28.8668 -9.8868 2 1 -4 15.5121 -4.5668 2 1 -3 -31.6168 21.4419 2 1 -2 35.2747 -25.4586 2 1 -1 -9.6422 37.0401 2 1 0 -41.2214 -12.8439 2 1 1 20.5238 36.8424 2 1 2 -0.8210 6.8844 2 1 3 54.2792 44.1545 2 1 4 -16.2407 -7.1351 2 1 5 38.2627 -0.9873 2 1 6 -3.4873 -4.5935 2 1 7 12.2695 -8.5040 2 1 8 -8.3502 4.8594 2 1 9 2.1056 3.3104 2 1 10 -0.9430 5.1386 2 1 11 -0.6288 -0.0912 2 1 12 -0.6918 -0.9343 2 1 13 -1.8749 -0.4068 2 1 14 -4.7109 2.5564 2 2 -14 2.2625 -4.1196 2 2 -12 -0.9134 -1.1284 2 2 -10 5.0999 3.8448 2 2 -8 13.6872 -9.0386 2 2 -6 -9.0022 -7.6248 2 2 -4 30.2608 1.9160 2 2 -2 27.9380 -65.8935 2 2 0 12.0572 3.5255 2 2 2 -14.1404 22.9753 2 2 4 -26.6510 -11.0221 2 2 6 -10.6120 18.9833 2 2 8 5.0252 -2.0683 2 2 10 -5.6467 -1.9731 2 2 12 -2.7707 -1.1602 2 2 14 -5.1792 -0.4842 3 0 0 -104.9935 0.0256 3 0 1 -37.2947 -20.0417 3 0 2 35.5890 52.4033 3 0 3 -47.6565 23.7154 3 0 4 27.8805 47.7868 3 0 5 13.5859 5.8208 3 0 6 9.1373 19.3124 3 0 7 -3.2263 0.6923 3 0 8 -6.1759 5.9930 3 0 9 -3.7561 1.0967 3 0 10 3.4432 -1.9168 3 0 11 -0.4529 1.8002 3 0 12 1.4745 -1.7638 3 0 13 0.3947 -0.4756 3 0 14 -4.4572 2.1110 3 1 -14 -1.6633 -3.3160 3 1 -13 1.7877 0.9960 3 1 -12 -0.1485 -1.4029 3 1 -11 -3.3128 0.9223 3 1 -10 -1.5483 -4.2141 3 1 -9 -2.8875 3.2345 3 1 -8 1.9354 -7.7379 3 1 -7 -1.1154 15.9162 3 1 -6 2.8516 1.3281 3 1 -5 -18.5517 3.1934 3 1 -4 -7.5878 22.3783 3 1 -3 46.4182 5.6575 3 1 -2 37.2943 16.9801 3 1 -1 14.4679 46.5479 3 1 0 38.2420 8.0367 3 1 1 -4.0783 42.0751 3 1 2 29.0848 -45.1879 3 1 3 -13.2524 2.6448 3 1 4 -39.7736 -11.5740 3 1 5 6.5715 4.4698 3 1 6 -1.3450 11.0279 3 1 7 1.0157 -4.4454 3 1 8 4.3065 -6.3206 3 1 9 5.3194 -0.0994 3 1 10 0.0095 4.6985 3 1 11 -1.0679 -1.0745 3 1 12 -0.7116 0.9834 3 1 13 0.7786 -0.1020 3 1 14 -4.7932 0.8865 3 2 -14 0.4396 -1.0791 3 2 -13 0.0503 0.4629 3 2 -12 -0.9383 0.7840 3 2 -11 1.2745 -0.6576 3 2 -10 2.0672 -4.8320 3 2 -9 9.0992 -4.1507 3 2 -8 -2.4272 -5.4514 3 2 -7 -8.6750 1.1335 3 2 -6 -10.7981 1.1999 3 2 -5 -13.1630 -3.1952 3 2 -4 18.0809 -10.9274 3 2 -3 33.3253 -6.9305 3 2 -2 -9.0371 -31.2280 3 2 -1 23.6942 1.6531 3 2 0 13.2320 17.7693 3 2 1 -21.7096 8.6457 3 2 2 1.9061 -18.2951 3 2 3 -27.3411 -23.2097 3 2 4 4.6724 10.0813 3 2 5 -15.5094 -2.3381 3 2 6 7.3946 4.8558 3 2 7 6.9520 2.5667 3 2 8 4.6812 2.3330 3 2 9 -6.2421 -0.2685 3 2 10 2.0114 1.1903 3 2 11 -1.6489 -0.2712 3 2 12 -0.9750 -2.6484 3 2 13 1.1338 0.2561 3 2 14 -0.1737 4.7027 3 3 -14 -0.7049 0.8918 3 3 -12 1.7066 1.0037 3 3 -10 5.4732 1.8510 3 3 -8 5.3220 0.2673 3 3 -6 -9.5469 -19.2150 3 3 -4 -27.6947 -14.4030 3 3 -2 -17.7097 67.6294 3 3 0 71.6001 11.4657 3 3 2 17.5229 -133.2120 3 3 4 6.7340 -2.9136 3 3 6 2.7811 13.2003 3 3 8 -3.1763 -2.2558 3 3 10 -0.5824 -0.9915 3 3 12 0.2433 -0.4284 3 3 14 -1.5174 3.0289 4 0 0 -100.4506 0.0115 4 0 1 46.4941 73.0257 4 0 2 40.5090 50.2757 4 0 3 16.6598 -60.5942 4 0 4 27.5745 -9.8703 4 0 5 43.1361 -6.0563 4 0 6 2.4289 -0.9850 4 0 7 0.8360 10.3055 4 0 8 2.9828 11.8308 4 0 9 0.9689 -3.4077 4 0 10 5.0927 0.9327 4 0 11 -6.2363 1.6074 4 0 12 0.1347 -0.6939 4 0 13 0.3366 0.0496 4 0 14 -4.9962 -1.3059 4 1 -14 -0.6716 0.2595 4 1 -13 -1.7510 -0.8764 4 1 -12 -0.4254 -0.0477 4 1 -11 -1.0311 3.5404 4 1 -10 0.7750 1.6753 4 1 -9 -3.6157 4.9979 4 1 -8 6.5819 1.4934 4 1 -7 -6.0392 4.7434 4 1 -6 0.5724 -10.7101 4 1 -5 -25.4011 3.4599 4 1 -4 9.3370 -16.9394 4 1 -3 61.2494 19.5457 4 1 -2 29.1178 -25.3036 4 1 -1 23.1867 25.8179 4 1 0 5.4638 23.0851 4 1 1 -18.4646 10.6853 4 1 2 27.2822 -15.8225 4 1 3 -4.7476 4.2610 4 1 4 8.1157 -0.6269 4 1 5 38.4852 28.6584 4 1 6 -3.9994 -2.0232 4 1 7 2.6853 -11.8886 4 1 8 1.6204 0.8950 4 1 9 -6.4399 3.8304 4 1 10 2.7335 0.8275 4 1 11 4.8085 2.3438 4 1 12 -0.0957 1.1444 4 1 13 -0.8028 0.4138 4 1 14 -1.0962 2.0707 4 2 -14 0.3394 -0.4296 4 2 -13 -0.3775 0.7219 4 2 -12 -1.0172 0.8379 4 2 -11 0.4480 0.2068 4 2 -10 -0.0359 -0.8711 4 2 -9 -2.6144 6.9425 4 2 -8 3.8356 2.6526 4 2 -7 -4.0094 13.4767 4 2 -6 -15.3576 3.1974 4 2 -5 11.5944 -32.8030 4 2 -4 0.0544 -11.1294 4 2 -3 12.4668 -10.3129 4 2 -2 -10.6185 -7.3132 4 2 -1 26.3331 26.2281 4 2 0 -0.7977 48.2380 4 2 1 4.9816 23.3625 4 2 2 -3.6249 -39.7429 4 2 3 20.7947 -26.2389 4 2 4 -12.9798 12.2496 4 2 5 -7.1174 -25.0446 4 2 6 -5.0666 9.9566 4 2 7 8.6717 -9.8185 4 2 8 9.5900 -3.7400 4 2 9 -10.0301 -5.8866 4 2 10 -5.5870 2.1174 4 2 11 -1.4802 -1.5901 4 2 12 -0.3501 0.2688 4 2 13 -0.0304 -0.0628 4 2 14 -2.9015 0.5718 4 3 -14 0.6323 0.5223 4 3 -13 0.1012 0.5060 4 3 -12 1.5403 -0.4616 4 3 -11 1.1205 -2.7432 4 3 -10 2.3886 0.9222 4 3 -9 -0.7866 7.3560 4 3 -8 -4.8263 -4.7377 4 3 -7 -7.1626 0.3825 4 3 -6 -2.7699 -3.2713 4 3 -5 -14.1879 -7.0967 4 3 -4 22.1684 -9.4912 4 3 -3 7.3537 10.3752 4 3 -2 2.0722 5.3786 4 3 -1 38.0922 -35.5836 4 3 0 -19.0345 46.4492 4 3 1 -43.4646 -17.5741 4 3 2 -11.3946 -15.2256 4 3 3 0.5103 2.8606 4 3 4 36.6644 2.2976 4 3 5 12.9213 -16.8066 4 3 6 14.8328 9.3312 4 3 7 -6.9315 8.3752 4 3 8 6.5432 3.9543 4 3 9 -6.5440 3.1384 4 3 10 4.9327 -3.4929 4 3 11 0.7124 -2.0677 4 3 12 0.7073 1.4409 4 3 13 -1.8621 -0.5878 4 3 14 1.0425 0.4650 4 4 -14 -1.2077 0.4080 4 4 -12 1.1615 1.7251 4 4 -10 -0.3481 3.4569 4 4 -8 -3.3180 4.2954 4 4 -6 1.4567 -4.5305 4 4 -4 14.6500 -18.2149 4 4 -2 32.9588 -6.6850 4 4 0 -19.9131 13.2708 4 4 2 -30.2613 7.8184 4 4 4 17.5358 -4.9522 4 4 6 12.6935 9.1809 4 4 8 -4.9685 0.4881 4 4 10 0.1657 -0.9245 4 4 12 0.8161 -2.2940 4 4 14 1.9491 -1.0720 5 0 0 -27.3013 -0.0507 5 0 1 46.1362 24.8269 5 0 2 -21.6640 1.2469 5 0 3 -10.5297 -13.0256 5 0 4 11.4708 5.2765 5 0 5 -0.9681 7.9062 5 0 6 8.8776 5.1781 5 0 7 -3.3303 -1.3089 5 0 8 -2.4553 -5.6427 5 0 9 8.1708 -4.0686 5 0 10 -4.5859 4.2048 5 0 11 -1.8778 0.4052 5 0 12 1.2635 1.7066 5 0 13 -1.4484 1.6693 5 0 14 -0.0762 -0.5978 5 1 -14 -0.5632 -0.6936 5 1 -13 0.5059 -0.6277 5 1 -12 -0.6976 2.1528 5 1 -11 -2.2187 0.5264 5 1 -10 -0.0651 -2.8074 5 1 -9 -5.1802 2.6049 5 1 -8 -1.7029 5.9696 5 1 -7 -9.6106 1.5534 5 1 -6 -5.1291 15.7741 5 1 -5 -8.0581 2.5131 5 1 -4 33.7886 3.2256 5 1 -3 34.2998 39.7498 5 1 -2 -0.0953 -20.7086 5 1 -1 -21.7213 -18.5986 5 1 0 3.8824 67.9991 5 1 1 0.7927 -36.8055 5 1 2 -2.3290 -4.3493 5 1 3 15.5008 14.5427 5 1 4 30.7175 -22.7009 5 1 5 -9.5909 11.9383 5 1 6 -5.0801 -17.5830 5 1 7 4.1127 -6.2726 5 1 8 5.7782 -6.5409 5 1 9 -0.9401 -6.8593 5 1 10 2.6638 1.5197 5 1 11 0.9165 -3.1030 5 1 12 1.1923 -1.5299 5 1 13 1.7988 -0.0993 5 1 14 0.0173 1.1652 5 2 -14 -0.0168 -0.3053 5 2 -13 0.7197 -0.4410 5 2 -12 1.6242 -0.8001 5 2 -11 -0.6776 1.8786 5 2 -10 0.8423 -2.3811 5 2 -9 1.6657 0.9457 5 2 -8 -5.4607 1.9863 5 2 -7 -5.9290 -8.2877 5 2 -6 -4.8975 -7.8460 5 2 -5 -13.5190 7.5867 5 2 -4 -3.1124 -8.7811 5 2 -3 15.8186 40.9233 5 2 -2 12.7345 -8.5668 5 2 -1 20.8229 -53.5595 5 2 0 10.2522 49.6402 5 2 1 -58.8749 -39.7782 5 2 2 -19.7093 -2.2623 5 2 3 -23.4576 51.1273 5 2 4 -11.4503 3.0245 5 2 5 -4.0148 0.9429 5 2 6 -15.3725 -8.2127 5 2 7 4.9227 -6.5055 5 2 8 -3.5423 -9.3331 5 2 9 -2.1606 -4.3580 5 2 10 -0.3177 2.0119 5 2 11 1.6635 4.4219 5 2 12 2.5710 0.8894 5 2 13 0.3235 0.4349 5 2 14 0.0453 -0.4777 5 3 -14 0.5090 1.1481 5 3 -13 -0.8036 -1.2556 5 3 -12 -2.0452 -1.1985 5 3 -11 -0.2516 3.1466 5 3 -10 -0.0772 0.2316 5 3 -9 -3.4751 1.8693 5 3 -8 3.4268 2.4432 5 3 -7 -13.3947 -8.4484 5 3 -6 -2.5078 -3.8259 5 3 -5 -2.1413 13.7893 5 3 -4 -17.7487 -5.6998 5 3 -3 -12.4902 -0.7571 5 3 -2 24.0183 -9.4057 5 3 -1 25.6091 -55.9469 5 3 0 -1.6959 11.3967 5 3 1 -31.5472 -29.2475 5 3 2 -19.4368 -11.0106 5 3 3 -0.7428 13.3992 5 3 4 -21.5073 -31.0554 5 3 5 17.7833 -11.8600 5 3 6 10.3891 10.1009 5 3 7 0.2147 -8.6500 5 3 8 13.5013 7.6127 5 3 9 -0.8282 -10.1525 5 3 10 -0.7940 -0.8889 5 3 11 1.3835 2.6968 5 3 12 -2.2095 1.0456 5 3 13 -0.1850 -2.0106 5 3 14 3.4286 0.2391 5 4 -14 1.6010 -0.4096 5 4 -13 -0.6955 0.7206 5 4 -12 -0.7760 -1.1912 5 4 -11 -0.0158 -0.5644 5 4 -10 -6.7376 1.5381 5 4 -9 -0.8291 -1.2459 5 4 -8 2.4439 -3.0862 5 4 -7 0.6480 -1.9513 5 4 -6 -2.4718 0.4366 5 4 -5 0.2618 8.9138 5 4 -4 -5.8799 -2.8148 5 4 -3 -21.0444 -11.0207 5 4 -2 19.9624 3.6145 5 4 -1 11.2762 -37.0249 5 4 0 -23.9204 2.1678 5 4 1 -22.2301 -23.2483 5 4 2 -14.6490 11.0129 5 4 3 6.6203 -4.1490 5 4 4 -2.9361 0.4721 5 4 5 6.7381 8.5574 5 4 6 9.2593 2.9325 5 4 7 -1.1596 6.2856 5 4 8 1.9479 -4.3484 5 4 9 0.4557 -1.0569 5 4 10 -1.1528 2.5379 5 4 11 -1.7454 -0.0619 5 4 12 -0.0859 1.0188 5 4 13 -0.3245 1.8247 5 4 14 6.9970 -0.2955 5 5 -12 -0.8134 -0.0693 5 5 -10 -2.6442 0.3064 5 5 -8 -0.7746 1.1397 5 5 -6 0.5787 5.4245 5 5 -4 5.6643 -9.1926 5 5 -2 2.6019 20.2269 5 5 0 28.1074 3.3892 5 5 2 -0.3766 -39.6963 5 5 4 -26.6729 -0.5718 5 5 6 -7.6252 -2.6233 5 5 8 4.2975 -10.2050 5 5 10 3.1683 -3.1591 5 5 12 -2.6904 -1.8843 6 0 0 21.3850 -0.0094 6 0 1 50.9608 11.2258 6 0 2 -19.6825 -3.9868 6 0 3 19.4741 29.6912 6 0 4 15.8868 -17.7402 6 0 5 4.9537 -4.9602 6 0 6 -13.7068 16.3555 6 0 7 6.2483 1.1904 6 0 8 4.6232 -3.5624 6 0 9 -2.0606 -0.4681 6 0 10 -6.1619 0.8821 6 0 11 -1.2626 -1.4879 6 0 12 2.8877 3.5607 6 0 13 2.2852 -0.0344 6 0 14 0.0161 -0.6781 6 1 -14 0.3833 0.3182 6 1 -13 0.3384 1.4103 6 1 -12 -0.3842 -1.6144 6 1 -11 2.2207 -1.0651 6 1 -10 -0.8700 3.2638 6 1 -9 -0.1566 0.1499 6 1 -8 5.4426 2.4253 6 1 -7 10.1608 -5.9429 6 1 -6 7.1216 -4.0446 6 1 -5 4.6597 -11.3385 6 1 -4 17.0369 -0.0771 6 1 -3 4.1558 41.6762 6 1 -2 10.7002 -11.4771 6 1 -1 -25.5514 -1.3974 6 1 0 12.6208 37.9970 6 1 1 -14.7739 -34.8380 6 1 2 -11.4114 -17.3956 6 1 3 3.4206 27.6589 6 1 4 14.9390 -18.0539 6 1 5 -10.8419 -19.2909 6 1 6 -10.5410 3.2597 6 1 7 -7.8128 -5.1549 6 1 8 3.1272 -7.0683 6 1 9 0.1785 -3.6006 6 1 10 -0.5050 -0.1497 6 1 11 -1.1710 -1.3894 6 1 12 -1.4786 1.2943 6 1 13 -0.1721 2.3147 6 1 14 0.5700 1.0359 6 2 -14 -0.5902 -0.8104 6 2 -13 -0.1164 0.0093 6 2 -12 -0.8424 -0.8215 6 2 -11 0.4169 -1.8848 6 2 -10 -0.9294 1.1029 6 2 -9 -2.0147 0.7462 6 2 -8 -2.1223 1.1924 6 2 -7 -1.9979 -0.7400 6 2 -6 0.6866 9.5087 6 2 -5 3.6432 0.8625 6 2 -4 -2.3527 6.5481 6 2 -3 -8.5537 -3.8384 6 2 -2 27.5855 -28.9793 6 2 -1 -10.4057 -18.0005 6 2 0 -14.9485 14.2965 6 2 1 -4.2042 -11.0451 6 2 2 19.0942 23.2103 6 2 3 10.6675 24.9693 6 2 4 -0.2225 0.1241 6 2 5 -6.7920 -18.1850 6 2 6 -1.5364 7.7783 6 2 7 -9.3296 5.5814 6 2 8 7.7510 -7.8892 6 2 9 2.0324 0.9673 6 2 10 -2.0669 0.8208 6 2 11 0.0228 -0.1414 6 2 12 -0.0164 -2.4990 6 2 13 -1.4434 -0.5612 6 2 14 -0.3934 -0.2346 6 3 -13 0.5196 0.9090 6 3 -12 -0.6907 -1.6580 6 3 -11 0.6715 -0.0965 6 3 -10 0.8436 -2.1538 6 3 -9 -2.4681 -4.3792 6 3 -8 -5.0432 -0.7252 6 3 -7 -7.8548 -4.2546 6 3 -6 -3.7438 9.5548 6 3 -5 3.2752 8.7339 6 3 -4 -0.8553 -2.3025 6 3 -3 -23.7755 -11.1428 6 3 -2 20.5500 -15.2356 6 3 -1 2.0819 -28.7405 6 3 0 -16.6141 -7.4534 6 3 1 -21.8342 -9.3796 6 3 2 28.5740 8.8954 6 3 3 4.6467 16.5545 6 3 4 13.7094 -20.6480 6 3 5 -3.9084 3.4190 6 3 6 -4.1222 0.3285 6 3 7 3.1524 -6.7482 6 3 8 -5.0006 1.9367 6 3 9 3.0418 -3.0379 6 3 10 -2.2933 0.3002 6 3 11 -0.5565 0.4338 6 3 12 -3.2351 -0.6121 6 3 13 0.4165 -0.2631 6 4 -13 -0.0207 -0.9434 6 4 -12 0.7656 0.1212 6 4 -11 1.6274 0.9504 6 4 -10 0.0773 1.6154 6 4 -9 0.0647 -5.8026 6 4 -8 -3.8225 -3.8172 6 4 -7 -2.4733 -1.7223 6 4 -6 -0.6732 1.1129 6 4 -5 10.5530 5.3398 6 4 -4 25.7091 5.6195 6 4 -3 -7.9637 -6.3266 6 4 -2 8.3749 -0.9620 6 4 -1 3.5782 10.3261 6 4 0 -17.7428 1.4007 6 4 1 -10.8386 18.2249 6 4 2 6.9650 -6.5562 6 4 3 31.5714 -2.1271 6 4 4 12.0336 -3.8680 6 4 5 4.5161 7.8650 6 4 6 1.0179 6.3352 6 4 7 3.1630 -3.0619 6 4 8 -1.7098 -1.9640 6 4 9 -0.1166 1.0627 6 4 10 0.5017 0.4258 6 4 11 1.4832 -0.9024 6 4 12 0.1457 -0.1110 6 4 13 -0.4512 -1.1617 6 5 -13 0.6568 0.9907 6 5 -12 0.4016 -0.3303 6 5 -11 1.3196 -0.1482 6 5 -10 0.9717 0.7129 6 5 -9 -1.7132 -3.2382 6 5 -8 -0.6219 4.3844 6 5 -7 -0.5130 -0.6386 6 5 -6 3.1040 0.9903 6 5 -5 -0.5436 -0.4055 6 5 -4 8.4100 -1.1005 6 5 -3 -1.3162 2.1907 6 5 -2 -33.2619 0.6265 6 5 -1 1.0638 11.1422 6 5 0 8.4308 8.3126 6 5 1 -13.3547 10.9073 6 5 2 4.5306 -2.5846 6 5 3 -3.8134 3.0819 6 5 4 -7.4400 10.6094 6 5 5 -3.4276 3.1146 6 5 6 -5.0441 -3.9033 6 5 7 -0.0629 -3.5537 6 5 8 -2.7147 -5.6399 6 5 9 -2.1930 -3.4926 6 5 10 -1.6908 0.4888 6 5 11 -1.3062 0.9678 6 5 12 0.5907 0.2212 6 5 13 0.5152 1.3796 6 6 -12 -1.8455 1.0449 6 6 -10 3.8349 -0.8516 6 6 -8 1.9829 -2.0340 6 6 -6 0.4243 -9.4919 6 6 -4 17.2850 0.8169 6 6 -2 -21.8886 -11.0019 6 6 0 -12.7296 -6.6724 6 6 2 34.0764 -2.6906 6 6 4 1.4762 -18.1175 6 6 6 -9.3622 7.8220 6 6 8 2.8420 4.0650 6 6 10 1.1660 -0.1592 6 6 12 0.9989 0.0860 7 0 0 31.7336 0.0134 7 0 1 -6.8927 19.5259 7 0 2 -15.3946 -29.8100 7 0 3 -3.3372 11.9491 7 0 4 5.2225 5.5479 7 0 5 5.6469 3.9605 7 0 6 22.5998 3.6976 7 0 7 2.5754 13.6110 7 0 8 0.7491 -6.6640 7 0 9 -5.3159 2.6592 7 0 10 -0.1480 3.4450 7 0 11 -0.2049 -2.8480 7 0 12 0.0086 -2.3586 7 0 13 0.3970 1.9283 7 0 14 -0.1403 0.7675 7 1 -14 0.0487 0.8863 7 1 -13 -0.7414 -0.0185 7 1 -12 -0.6810 0.7877 7 1 -11 -1.8088 0.6458 7 1 -10 6.0884 1.3378 7 1 -9 0.9913 0.1776 7 1 -8 -6.9896 -1.7962 7 1 -7 -10.1793 -5.0587 7 1 -6 -3.4261 5.3099 7 1 -5 0.7391 4.1449 7 1 -4 2.0279 -5.5089 7 1 -3 13.6663 -11.3799 7 1 -2 18.4243 6.1241 7 1 -1 -8.8543 16.0537 7 1 0 -15.1313 20.7084 7 1 1 -28.3598 -1.1878 7 1 2 -0.2672 -7.1554 7 1 3 -7.4085 -7.6864 7 1 4 4.8108 -5.3281 7 1 5 -5.0209 -0.6600 7 1 6 1.6229 14.0408 7 1 7 -0.4471 17.6567 7 1 8 3.3113 -2.3079 7 1 9 -2.6991 -0.5697 7 1 10 2.4715 0.2546 7 1 11 3.7532 -0.1736 7 1 12 -1.1788 -1.0901 7 1 13 2.0088 -0.4386 7 1 14 -0.8080 0.0688 7 2 -13 1.0498 1.0141 7 2 -12 0.4132 -0.2634 7 2 -11 -0.3467 2.2201 7 2 -10 -2.8362 -3.6546 7 2 -9 3.0964 0.5572 7 2 -8 -1.1186 -4.0357 7 2 -7 -2.6672 -12.1594 7 2 -6 -1.6192 6.9410 7 2 -5 10.4013 4.8241 7 2 -4 -16.0770 -2.9909 7 2 -3 12.1329 -9.5643 7 2 -2 7.5472 15.7973 7 2 -1 -11.7526 -11.3193 7 2 0 5.9539 -14.5986 7 2 1 -11.9564 -7.3342 7 2 2 14.2870 -12.4844 7 2 3 7.4691 28.4554 7 2 4 -2.1866 -0.7036 7 2 5 -5.4726 5.1651 7 2 6 -7.0567 0.1397 7 2 7 -5.7873 -4.0271 7 2 8 6.1192 -6.5016 7 2 9 -0.0422 3.6995 7 2 10 -3.1758 6.1476 7 2 11 -1.3528 -0.7273 7 2 12 -1.3992 0.9816 7 2 13 -1.2168 -1.6500 7 3 -13 -0.3581 0.5479 7 3 -12 0.8874 -1.0398 7 3 -11 1.2155 0.5516 7 3 -10 -2.5957 -2.7071 7 3 -9 1.3405 -1.7361 7 3 -8 4.7649 -2.5139 7 3 -7 -0.1724 0.4434 7 3 -6 -2.9157 4.6502 7 3 -5 12.2397 0.1890 7 3 -4 1.0677 8.3593 7 3 -3 0.9299 -0.2060 7 3 -2 0.6117 13.0418 7 3 -1 -8.4456 22.2649 7 3 0 7.1007 -4.9406 7 3 1 8.4331 3.2951 7 3 2 -1.7825 -20.6786 7 3 3 17.6507 -4.5891 7 3 4 -1.3206 -5.4423 7 3 5 -11.1568 11.3423 7 3 6 3.4900 0.8982 7 3 7 3.1191 -0.6889 7 3 8 5.5288 -1.7365 7 3 9 -1.6542 2.7781 7 3 10 -0.5091 1.1065 7 3 11 -4.3552 -1.6682 7 3 12 -1.3359 -0.1460 7 3 13 -0.1762 -1.2645 7 4 -13 -0.1312 0.8904 7 4 -12 1.0545 -0.7502 7 4 -11 2.4082 -1.1617 7 4 -10 1.5867 1.3555 7 4 -9 -1.9166 0.2160 7 4 -8 0.5262 -4.0502 7 4 -7 4.7577 7.0626 7 4 -6 3.5244 -4.7482 7 4 -5 4.8034 -8.5417 7 4 -4 6.7553 2.3691 7 4 -3 18.8619 -10.4780 7 4 -2 -21.7927 -9.0652 7 4 -1 7.7609 7.0617 7 4 0 1.6725 3.7017 7 4 1 -5.2093 8.4555 7 4 2 8.1502 -12.0954 7 4 3 -0.5290 -14.8426 7 4 4 2.5441 -1.8026 7 4 5 -3.8713 1.2755 7 4 6 2.8090 -4.7034 7 4 7 8.7980 10.0837 7 4 8 -4.6161 -3.0769 7 4 9 0.1326 0.8611 7 4 10 1.9532 -0.1439 7 4 11 -3.5671 -0.7359 7 4 12 0.2636 -0.2908 7 4 13 -0.5826 -0.3450 7 5 -13 0.4907 -0.7302 7 5 -12 -0.3367 0.3439 7 5 -11 0.0159 0.2369 7 5 -10 0.2772 -0.8103 7 5 -9 1.5562 3.1589 7 5 -8 -0.4873 0.9712 7 5 -7 9.6343 -3.2778 7 5 -6 11.1049 0.3489 7 5 -5 -0.0160 5.6085 7 5 -4 -2.3850 4.8330 7 5 -3 5.8381 7.0266 7 5 -2 -16.3553 7.1490 7 5 -1 4.0022 -3.6151 7 5 0 4.8133 -1.5312 7 5 1 4.4770 17.1929 7 5 2 18.1441 -2.9400 7 5 3 6.9702 11.0318 7 5 4 -9.5445 1.4795 7 5 5 -0.5268 -4.4678 7 5 6 -5.5846 7.8490 7 5 7 0.2226 -1.8934 7 5 8 0.5450 2.7406 7 5 9 -1.9649 0.4646 7 5 10 2.2881 -1.2967 7 5 11 -0.9944 2.6945 7 5 12 1.9697 -0.5450 7 5 13 0.3496 -1.5251 7 6 -12 -0.7047 -0.2041 7 6 -11 -0.3040 0.2309 7 6 -10 -2.9623 -2.4800 7 6 -9 1.7919 -1.2355 7 6 -8 0.1856 1.3811 7 6 -7 -2.7236 5.8628 7 6 -6 8.4493 -5.2651 7 6 -5 2.6560 9.3274 7 6 -4 -10.0678 -2.0088 7 6 -3 -3.8250 -10.0662 7 6 -2 7.0815 8.7344 7 6 -1 -5.0744 -5.1807 7 6 0 -1.9142 -6.8796 7 6 1 2.4732 -4.4310 7 6 2 5.4105 7.3135 7 6 3 -4.7828 -12.9798 7 6 4 -7.8890 -6.8128 7 6 5 -10.9298 3.6989 7 6 6 6.3616 5.7515 7 6 7 3.0844 4.6194 7 6 8 3.1944 -2.5980 7 6 9 -0.3490 0.3365 7 6 10 0.1030 -1.2495 7 6 11 0.4787 0.0509 7 6 12 0.6943 -0.1672 7 7 -12 1.7695 -1.6162 7 7 -10 -1.2022 -1.1680 7 7 -8 1.9009 -2.3574 7 7 -6 1.6149 -0.4257 7 7 -4 -9.7574 9.9569 7 7 -2 16.2500 8.2943 7 7 0 22.9656 -6.4725 7 7 2 10.7804 -6.7398 7 7 4 -3.9348 -16.1805 7 7 6 0.7052 -2.1464 7 7 8 1.2678 -2.6867 7 7 10 0.0041 -1.6587 7 7 12 0.8403 0.9134 8 0 0 8.7697 0.0118 8 0 1 -27.9657 12.0981 8 0 2 -1.4438 -13.0863 8 0 3 3.8661 -27.8318 8 0 4 -12.4996 2.6654 8 0 5 21.6997 -12.0886 8 0 6 16.0842 12.7093 8 0 7 4.3226 9.8331 8 0 8 1.2944 -3.2684 8 0 9 -6.5796 8.0093 8 0 10 1.3631 0.4229 8 0 11 2.9765 0.5613 8 0 12 1.4865 -0.0455 8 0 13 1.5319 0.8417 8 1 -13 -1.3817 3.4342 8 1 -12 -2.7406 0.7712 8 1 -11 -2.9142 -1.0343 8 1 -10 1.5079 3.7180 8 1 -9 -1.2687 0.8647 8 1 -8 -7.5894 7.4204 8 1 -7 0.7926 9.0153 8 1 -6 -4.6174 -1.5463 8 1 -5 2.5361 -0.0635 8 1 -4 -13.7407 -20.6444 8 1 -3 -7.9648 -39.5483 8 1 -2 3.6113 20.6526 8 1 -1 -9.1720 12.0488 8 1 0 15.1452 13.0296 8 1 1 0.8655 10.1040 8 1 2 -10.3326 -8.0432 8 1 3 6.8123 -23.7680 8 1 4 1.3062 -2.1871 8 1 5 11.6204 -13.0124 8 1 6 5.8746 8.0696 8 1 7 11.6026 10.5977 8 1 8 0.4843 -6.1712 8 1 9 -1.1616 0.0337 8 1 10 -0.3118 -4.7210 8 1 11 1.1224 -0.9748 8 1 12 -2.5890 -1.3876 8 1 13 3.0483 0.1996 8 2 -13 -0.1675 -1.2951 8 2 -12 0.9089 -1.7560 8 2 -11 0.8977 -1.1439 8 2 -10 -3.2717 -3.7388 8 2 -9 -0.7549 2.6515 8 2 -8 1.2446 1.1219 8 2 -7 8.4758 -2.2732 8 2 -6 -12.3087 10.3076 8 2 -5 8.9031 -2.3804 8 2 -4 0.8541 -5.0561 8 2 -3 2.7801 -9.7954 8 2 -2 -7.8780 1.6204 8 2 -1 -17.0465 11.2929 8 2 0 -3.9341 8.3281 8 2 1 9.8407 2.0416 8 2 2 -1.7568 1.9632 8 2 3 24.8925 2.4501 8 2 4 14.1282 -0.6858 8 2 5 -2.7783 5.3712 8 2 6 -8.8102 0.9525 8 2 7 -7.3691 4.6674 8 2 8 8.3132 -4.5047 8 2 9 4.0768 6.3735 8 2 10 -0.6854 0.0165 8 2 11 1.2138 -0.5172 8 2 12 1.8271 1.7301 8 2 13 -0.9671 -1.7250 8 3 -13 0.0606 -0.3667 8 3 -12 0.2736 -0.4717 8 3 -11 2.1739 0.1742 8 3 -10 -0.7976 -0.3609 8 3 -9 -2.0762 1.2471 8 3 -8 8.1262 0.6762 8 3 -7 4.1263 5.1958 8 3 -6 -5.4502 7.6644 8 3 -5 -0.5528 -0.5306 8 3 -4 -4.5622 -1.6363 8 3 -3 17.3301 -8.0021 8 3 -2 -3.8378 0.8434 8 3 -1 4.4787 8.5752 8 3 0 18.4383 8.8283 8 3 1 2.7370 5.9809 8 3 2 -10.0589 -11.9257 8 3 3 -2.1552 7.6570 8 3 4 -5.0842 -5.0631 8 3 5 1.7587 6.2652 8 3 6 -3.4986 -13.3455 8 3 7 7.2791 0.9316 8 3 8 -1.4438 2.6346 8 3 9 4.9205 0.8865 8 3 10 -1.0484 -0.4491 8 3 11 -4.0316 1.3065 8 3 12 -0.0769 0.6427 8 3 13 1.2885 0.6024 8 4 -13 0.1944 -0.0197 8 4 -12 0.7773 0.8310 8 4 -11 0.3837 -0.6024 8 4 -10 -0.1509 4.0677 8 4 -9 -0.5698 1.1574 8 4 -8 5.8421 -1.6330 8 4 -7 1.6648 4.8834 8 4 -6 -1.8674 -3.1989 8 4 -5 -2.4408 1.1612 8 4 -4 -7.6008 -0.9355 8 4 -3 4.2779 -12.4652 8 4 -2 -6.7836 -19.7886 8 4 -1 -10.3131 -1.3089 8 4 0 -19.4953 -1.4460 8 4 1 3.5600 12.1770 8 4 2 -3.5467 6.5989 8 4 3 0.2637 -3.3476 8 4 4 -15.4721 4.3731 8 4 5 2.2631 -13.6424 8 4 6 -0.4705 6.9208 8 4 7 -0.1770 5.9780 8 4 8 1.7796 3.4916 8 4 9 1.1868 5.0951 8 4 10 -0.6142 -0.1248 8 4 11 -0.5247 -1.0243 8 4 12 2.5716 0.6534 8 4 13 -1.5047 1.0284 8 5 -12 -0.0963 -0.2274 8 5 -11 -0.3477 0.3541 8 5 -10 -0.4165 2.1431 8 5 -9 -0.9280 1.3210 8 5 -8 -1.4112 -3.5167 8 5 -7 1.9354 -1.5106 8 5 -6 -4.0230 -0.7670 8 5 -5 6.8163 0.1196 8 5 -4 -7.6761 -1.3318 8 5 -3 -0.7258 -3.9304 8 5 -2 18.3971 -5.2809 8 5 -1 -5.2263 -4.0776 8 5 0 -10.1399 -10.6654 8 5 1 1.6339 6.2459 8 5 2 4.0614 8.3057 8 5 3 12.7294 -2.4900 8 5 4 -3.1230 -5.3185 8 5 5 -8.4630 -1.3393 8 5 6 -4.2314 1.9559 8 5 7 -1.1770 -0.0194 8 5 8 -0.3500 -0.1346 8 5 9 -1.0265 -0.3333 8 5 10 1.0134 -1.6221 8 5 11 0.1867 0.4969 8 5 12 0.4886 -0.8109 8 6 -12 0.8863 -0.5273 8 6 -11 -0.1248 0.7102 8 6 -10 0.3191 0.9970 8 6 -9 1.8420 -1.3292 8 6 -8 2.3482 -1.9669 8 6 -7 -0.9528 1.9981 8 6 -6 5.3648 2.5646 8 6 -5 -2.2195 0.1444 8 6 -4 -1.0558 5.6134 8 6 -3 -1.7095 -5.1138 8 6 -2 12.9630 -2.6266 8 6 -1 -6.0912 3.0715 8 6 0 -10.1808 -5.2829 8 6 1 7.2708 1.9637 8 6 2 -7.7868 10.0935 8 6 3 12.4604 -2.7031 8 6 4 -5.0331 -9.5776 8 6 5 -4.0298 5.0765 8 6 6 -0.5122 -3.7584 8 6 7 -0.3052 -0.1003 8 6 8 1.4245 -0.2908 8 6 9 0.1194 -0.6027 8 6 10 -0.3945 1.1452 8 6 11 0.6495 0.0519 8 6 12 -0.6179 0.8593 8 7 -12 1.2622 -0.8511 8 7 -11 -2.1439 0.4877 8 7 -10 3.6547 -0.4517 8 7 -9 -0.2900 -0.7186 8 7 -8 1.3733 -3.6851 8 7 -7 0.3216 -1.4529 8 7 -6 -2.3859 0.2975 8 7 -5 -0.6666 -1.3177 8 7 -4 -0.5442 1.1344 8 7 -3 8.6349 6.6338 8 7 -2 6.0091 2.3972 8 7 -1 -5.6625 -0.3023 8 7 0 8.5794 7.2591 8 7 1 -3.1724 -3.6042 8 7 2 -5.7638 -0.6861 8 7 3 2.8068 4.2110 8 7 4 0.2665 2.7494 8 7 5 1.5077 -1.3698 8 7 6 -0.9256 -1.5936 8 7 7 -3.1111 -1.0267 8 7 8 2.0092 2.0917 8 7 9 -0.4765 -1.2372 8 7 10 -0.6325 -0.5379 8 7 11 0.5006 -0.9458 8 7 12 -1.0661 0.0506 8 8 -10 2.7513 -2.3288 8 8 -8 3.1260 -2.3224 8 8 -6 2.9317 -1.1793 8 8 -4 -2.8187 -2.0250 8 8 -2 -0.8601 -4.4577 8 8 0 7.6363 0.6240 8 8 2 -6.0726 -3.9810 8 8 4 -0.5252 6.9434 8 8 6 1.2569 1.5084 8 8 8 3.0526 1.4348 8 8 10 -1.1188 3.4262 9 0 0 11.6969 0.0014 9 0 1 -0.6600 -3.3575 9 0 2 -4.2746 14.9157 9 0 3 2.8630 -16.9155 9 0 4 -0.2601 9.3662 9 0 5 22.4369 -22.6675 9 0 6 0.5973 8.6381 9 0 7 6.3501 -0.2014 9 0 8 -9.9019 -4.3406 9 0 9 0.6835 1.4182 9 0 10 3.1898 1.3975 9 0 11 7.7900 -2.5976 9 0 12 -1.8120 2.9822 9 0 13 -1.4594 -1.3877 9 1 -13 1.1668 -0.0221 9 1 -12 0.0893 -1.4125 9 1 -11 0.9472 -0.2494 9 1 -10 2.6193 2.1009 9 1 -9 -1.6687 -5.1290 9 1 -8 -0.2878 5.9960 9 1 -7 -3.1480 -3.1140 9 1 -6 2.7173 -2.1797 9 1 -5 -14.5610 0.3095 9 1 -4 5.1211 -10.7494 9 1 -3 -0.0108 1.8958 9 1 -2 -1.9325 1.3870 9 1 -1 3.5416 -1.1138 9 1 0 10.2052 10.3915 9 1 1 2.6742 -9.3176 9 1 2 -8.2522 2.2403 9 1 3 -11.9649 -4.9629 9 1 4 14.4855 -0.1959 9 1 5 7.9755 -13.4320 9 1 6 -3.9042 5.1194 9 1 7 3.7894 3.5486 9 1 8 -2.2878 -6.0973 9 1 9 -1.0526 -4.4971 9 1 10 -0.4336 0.6209 9 1 11 -1.1868 1.7114 9 1 12 0.2396 0.7579 9 1 13 -0.5146 0.2117 9 2 -13 0.5373 -0.5985 9 2 -12 -1.2243 -1.1798 9 2 -11 -0.9937 -2.1699 9 2 -10 -1.0520 -2.4493 9 2 -9 -3.1260 4.8270 9 2 -8 6.7319 -5.1203 9 2 -7 3.9365 -0.3901 9 2 -6 -5.4566 -1.3676 9 2 -5 -7.5379 -0.9380 9 2 -4 -7.2545 -6.9120 9 2 -3 8.0198 -5.8181 9 2 -2 -16.5700 6.9351 9 2 -1 11.1440 6.4511 9 2 0 12.7638 16.0271 9 2 1 -10.0079 -4.1052 9 2 2 3.0579 -25.8931 9 2 3 0.7792 3.6590 9 2 4 -0.9631 -10.4393 9 2 5 14.1424 -1.0527 9 2 6 -12.3568 -1.7071 9 2 7 -5.3065 -1.7124 9 2 8 3.0060 0.0234 9 2 9 1.9772 -2.4483 9 2 10 0.5187 0.9043 9 2 11 0.0828 -1.1798 9 2 12 -0.1293 0.9022 9 2 13 -0.7461 -1.1826 9 3 -13 0.0122 -0.4019 9 3 -12 -0.5876 -0.1064 9 3 -11 0.5474 -0.0794 9 3 -10 1.4639 1.0273 9 3 -9 -1.3086 1.0161 9 3 -8 6.5311 1.3337 9 3 -7 4.1865 -1.9469 9 3 -6 -0.8902 2.2547 9 3 -5 -4.1629 2.9238 9 3 -4 1.8726 -6.4826 9 3 -3 8.2859 -4.2873 9 3 -2 -2.1144 -6.7534 9 3 -1 11.3329 -7.6173 9 3 0 6.9465 -6.8843 9 3 1 -2.4375 0.8269 9 3 2 -2.5995 -14.2183 9 3 3 1.6843 8.9562 9 3 4 -5.9582 7.5729 9 3 5 3.4036 -13.2543 9 3 6 1.9093 -6.5599 9 3 7 -0.6936 -1.4990 9 3 8 -1.2831 -4.7836 9 3 9 2.3958 1.8904 9 3 10 0.4859 0.2553 9 3 11 -2.6679 -0.6456 9 3 12 2.8404 -1.0093 9 3 13 0.3062 0.3263 9 4 -12 -1.3308 0.6545 9 4 -11 -0.9203 0.2541 9 4 -10 -0.4528 0.8165 9 4 -9 -0.2864 2.0176 9 4 -8 -2.5696 -4.8381 9 4 -7 -3.4490 -6.2507 9 4 -6 1.1012 -1.5905 9 4 -5 2.1579 -1.8707 9 4 -4 0.6100 -2.6744 9 4 -3 6.1457 -1.8935 9 4 -2 -0.0519 1.0284 9 4 -1 4.1008 3.6909 9 4 0 -8.5515 -8.2292 9 4 1 0.5429 2.2526 9 4 2 -9.8565 10.3597 9 4 3 0.8130 0.7867 9 4 4 0.0534 7.3079 9 4 5 1.2195 -1.3444 9 4 6 2.9519 -0.0509 9 4 7 6.8485 0.4400 9 4 8 3.4045 0.6533 9 4 9 0.9615 4.4117 9 4 10 -2.2259 -0.4746 9 4 11 1.7587 -1.7354 9 4 12 1.3250 -0.1107 9 5 -12 1.5805 -0.2184 9 5 -11 -0.3976 -0.8938 9 5 -10 -0.8940 0.9152 9 5 -9 2.0467 1.0216 9 5 -8 -1.8401 2.2373 9 5 -7 1.3812 -2.7164 9 5 -6 4.2834 -2.8165 9 5 -5 -6.1623 2.1769 9 5 -4 -3.0836 0.7858 9 5 -3 -3.0036 0.0433 9 5 -2 7.3124 9.6905 9 5 -1 2.0199 -3.2114 9 5 0 -0.8661 -2.8467 9 5 1 2.8153 -0.6452 9 5 2 -7.1385 4.0452 9 5 3 8.6225 -0.2567 9 5 4 -0.9745 -3.3741 9 5 5 -2.8470 6.8525 9 5 6 -1.9871 -0.0078 9 5 7 -1.2531 -3.5075 9 5 8 -1.0092 -0.5026 9 5 9 -3.8969 -1.2494 9 5 10 -1.3715 0.1513 9 5 11 -2.2116 -1.4702 9 5 12 -0.0812 -0.4350 9 6 -12 4.0698 -3.0718 9 6 -11 0.6800 1.0298 9 6 -10 0.5597 -1.5478 9 6 -9 -1.4799 -3.4219 9 6 -8 -1.2887 2.2392 9 6 -7 1.6680 0.6514 9 6 -6 2.8571 -2.2938 9 6 -5 1.6696 -1.6683 9 6 -4 -5.5145 -3.6279 9 6 -3 0.6167 -1.9235 9 6 -2 -0.2522 12.8252 9 6 -1 -17.2080 6.4457 9 6 0 -0.2920 4.9584 9 6 1 9.8278 -1.5865 9 6 2 -16.1855 -2.4035 9 6 3 -0.3660 -1.9832 9 6 4 -2.0386 3.6455 9 6 5 -5.2840 6.5031 9 6 6 2.7736 -2.9675 9 6 7 1.0657 3.5048 9 6 8 -0.7317 -2.6636 9 6 9 4.3275 -1.7464 9 6 10 1.8890 -0.2719 9 6 11 0.3721 -0.2345 9 6 12 0.9348 -0.3782 9 7 -11 1.8602 0.6003 9 7 -10 0.1740 0.8884 9 7 -9 -2.9882 -1.2642 9 7 -8 0.7995 -1.8322 9 7 -7 -0.1281 -1.3011 9 7 -6 -0.3934 2.7395 9 7 -5 6.0659 -0.7359 9 7 -4 0.1211 -3.8996 9 7 -3 4.1202 0.0452 9 7 -2 -2.5283 -6.6781 9 7 -1 -5.5638 6.9029 9 7 0 -1.4330 10.0460 9 7 1 7.5554 0.6007 9 7 2 -1.1809 1.1645 9 7 3 -1.2523 1.3571 9 7 4 -0.2765 -0.9754 9 7 5 -2.1525 -0.1604 9 7 6 -2.2459 -0.4726 9 7 7 1.1088 0.1781 9 7 8 0.8118 0.8553 9 7 9 3.5299 -1.4580 9 7 10 1.7392 2.0532 9 7 11 -1.0839 0.2122 9 8 -11 -0.1984 1.1368 9 8 -10 1.8967 -3.3570 9 8 -9 -0.4924 1.3034 9 8 -8 -1.4026 -6.0038 9 8 -7 -0.9308 -0.7448 9 8 -6 3.7356 -1.6530 9 8 -5 0.6334 1.5089 9 8 -4 -1.0587 0.7268 9 8 -3 -0.8176 -2.8899 9 8 -2 -4.6083 -2.5097 9 8 -1 2.9825 -5.1114 9 8 0 -2.8297 3.5394 9 8 1 -6.0122 -0.4471 9 8 2 0.1182 3.4719 9 8 3 -2.2601 3.3078 9 8 4 0.6116 0.3627 9 8 5 -1.2870 1.0928 9 8 6 3.3503 0.6213 9 8 7 0.5002 -1.0214 9 8 8 0.7468 -0.1925 9 8 9 0.5180 0.7019 9 8 10 -0.4028 0.3137 9 8 11 0.2665 0.5057 9 9 -10 -0.2679 -3.0037 9 9 -8 -1.8736 -1.8956 9 9 -6 3.4702 0.1673 9 9 -4 2.8653 -1.2976 9 9 -2 4.9587 -2.0934 9 9 0 2.8374 -1.4787 9 9 2 -3.6021 -4.4340 9 9 4 3.1509 -2.3955 9 9 6 5.1192 -1.0955 9 9 8 -0.8516 -0.9623 9 9 10 -1.8264 -3.3009 10 0 0 -0.7893 0.0037 10 0 1 7.5836 -3.9493 10 0 2 2.8757 14.6251 10 0 3 0.1996 11.8841 10 0 4 8.5165 -1.9097 10 0 5 16.5258 -18.4306 10 0 6 -7.9797 15.3628 10 0 7 -0.6963 -2.4220 10 0 8 2.0240 3.6021 10 0 9 0.4008 -0.2357 10 0 10 3.9080 -0.0624 10 0 11 3.4400 3.1398 10 0 12 0.2260 0.5409 10 0 13 -0.1340 -0.7880 10 1 -13 -0.0480 1.1968 10 1 -12 -0.0922 -1.3481 10 1 -11 0.5383 0.0773 10 1 -10 -0.4457 0.2786 10 1 -9 1.0839 -3.6340 10 1 -8 0.7676 4.8360 10 1 -7 4.5906 -4.3866 10 1 -6 7.3183 -2.7795 10 1 -5 -4.5776 -8.6810 10 1 -4 14.5950 -5.6554 10 1 -3 3.2004 -14.1642 10 1 -2 1.4105 1.2219 10 1 -1 1.4608 -5.0499 10 1 0 5.0754 8.9668 10 1 1 -7.3955 10.1528 10 1 2 -0.6919 -7.6789 10 1 3 -4.9165 -0.9630 10 1 4 14.1598 1.2306 10 1 5 11.6727 -20.5974 10 1 6 -0.3816 7.4680 10 1 7 1.1274 -3.3819 10 1 8 3.8128 -0.7649 10 1 9 -3.2916 -3.8383 10 1 10 -0.7867 1.1448 10 1 11 -2.6660 3.4004 10 1 12 -0.0017 1.8806 10 1 13 1.2879 1.1698 10 2 -12 -0.3281 1.4083 10 2 -11 -0.7336 0.0038 10 2 -10 -0.3804 -0.4132 10 2 -9 -4.2673 3.0770 10 2 -8 7.4539 0.5606 10 2 -7 -3.9383 -0.7617 10 2 -6 0.8127 1.2269 10 2 -5 -1.3864 4.3308 10 2 -4 4.2603 -0.6964 10 2 -3 0.5241 -3.0851 10 2 -2 5.3925 -6.2008 10 2 -1 8.1969 6.7541 10 2 0 -1.8236 1.3344 10 2 1 -9.2087 -2.9489 10 2 2 0.4535 -5.5916 10 2 3 -3.4460 2.8805 10 2 4 2.6875 0.6343 10 2 5 5.3096 1.4579 10 2 6 1.0004 5.2732 10 2 7 -2.4943 3.5666 10 2 8 4.3251 2.2082 10 2 9 2.9264 1.9408 10 2 10 -0.3223 -0.2252 10 2 11 -1.6874 -0.9222 10 2 12 0.4430 -2.1809 10 3 -12 -0.9463 -1.7546 10 3 -11 0.1298 -0.3834 10 3 -10 -4.3723 -1.1811 10 3 -9 2.6620 -1.7919 10 3 -8 0.1452 0.8538 10 3 -7 1.3014 -7.3777 10 3 -6 1.9855 0.8755 10 3 -5 5.9250 -4.1752 10 3 -4 12.5954 -1.7434 10 3 -3 5.4826 -0.0977 10 3 -2 3.9844 -3.4646 10 3 -1 9.1819 8.0356 10 3 0 -1.4114 -8.8086 10 3 1 -13.8294 -4.8777 10 3 2 4.9347 -3.5116 10 3 3 -9.6761 5.3315 10 3 4 -0.5746 -0.3768 10 3 5 1.4424 -5.1912 10 3 6 -1.7974 0.0021 10 3 7 -0.8036 -0.0058 10 3 8 0.7093 -1.0025 10 3 9 -1.1305 1.6611 10 3 10 -3.9383 -0.6839 10 3 11 -0.5663 -1.7802 10 3 12 0.0428 -2.3896 10 4 -12 1.2104 0.7109 10 4 -11 0.9712 -1.7433 10 4 -10 -1.2227 0.4626 10 4 -9 -1.5815 -2.1135 10 4 -8 -0.7975 3.9557 10 4 -7 -4.2033 -0.1607 10 4 -6 3.9566 -1.5975 10 4 -5 -0.0532 -5.0056 10 4 -4 2.7374 -1.7464 10 4 -3 0.4314 -5.4170 10 4 -2 -2.5956 2.5096 10 4 -1 13.9183 4.1160 10 4 0 -1.1929 -3.7823 10 4 1 -0.2717 3.1058 10 4 2 1.1172 1.8443 10 4 3 3.6499 1.4029 10 4 4 6.9388 -1.9082 10 4 5 1.1266 -3.2239 10 4 6 2.9298 0.4476 10 4 7 0.5698 -1.9597 10 4 8 5.4830 -0.3776 10 4 9 0.4293 -1.1833 10 4 10 -2.3094 -1.2451 10 4 11 -0.1458 -1.4629 10 4 12 -0.5226 -1.9340 10 5 -11 0.7306 -0.1336 10 5 -10 0.0549 -0.8416 10 5 -9 -0.2614 -2.6919 10 5 -8 -0.1884 -1.3834 10 5 -7 3.5601 -2.4869 10 5 -6 -1.5311 -2.4995 10 5 -5 0.0457 -2.9916 10 5 -4 3.4722 4.4164 10 5 -3 -2.6493 -4.4822 10 5 -2 2.3337 3.2938 10 5 -1 -5.7480 -5.7980 10 5 0 -0.0134 3.9840 10 5 1 2.3061 -4.2286 10 5 2 0.4370 -0.8903 10 5 3 3.3704 1.5700 10 5 4 3.9752 -1.6863 10 5 5 -1.7294 5.5689 10 5 6 -1.2427 1.6952 10 5 7 -3.0092 -0.3098 10 5 8 -2.1107 3.4761 10 5 9 0.4125 -1.3353 10 5 10 1.2097 0.6350 10 5 11 -0.2110 1.6204 10 6 -11 0.2362 -1.5579 10 6 -10 -1.1001 0.3387 10 6 -9 -2.9738 -0.5919 10 6 -8 -0.4123 0.4045 10 6 -7 2.9090 1.0774 10 6 -6 1.0498 0.1490 10 6 -5 -1.4008 0.7316 10 6 -4 1.0169 -0.5141 10 6 -3 4.7380 0.3864 10 6 -2 -0.7557 1.2747 10 6 -1 -2.5499 -2.0048 10 6 0 -3.2515 4.2970 10 6 1 -3.7699 0.6419 10 6 2 -5.2766 -2.1791 10 6 3 0.8664 0.6860 10 6 4 -4.1678 -1.6034 10 6 5 2.4028 -1.4873 10 6 6 0.8097 -0.5036 10 6 7 -1.7016 0.8190 10 6 8 0.5333 -4.8389 10 6 9 1.4631 -0.2885 10 6 10 1.1854 1.4754 10 6 11 0.0395 0.1672 10 7 -11 2.9292 1.2674 10 7 -10 -1.7390 -1.2595 10 7 -9 2.3924 0.9628 10 7 -8 -4.1625 -5.4224 10 7 -7 -0.3566 -2.2181 10 7 -6 -2.9863 -0.1433 10 7 -5 2.7622 2.4440 10 7 -4 -1.2087 -0.4807 10 7 -3 -5.0346 -4.5972 10 7 -2 2.6947 2.4440 10 7 -1 2.5302 -0.5591 10 7 0 1.2223 -3.5793 10 7 1 -0.0063 3.6769 10 7 2 0.8625 -4.9084 10 7 3 4.2029 1.0101 10 7 4 -2.5076 -1.1122 10 7 5 1.3113 -1.2604 10 7 6 -1.8700 0.3619 10 7 7 0.3920 -2.4823 10 7 8 2.4548 -8.1484 10 7 9 1.4890 -1.0936 10 7 10 -0.3551 -0.7423 10 7 11 0.5449 -1.3384 10 8 -10 -0.6694 -0.0730 10 8 -9 0.7463 -0.2140 10 8 -8 0.6263 -2.4886 10 8 -7 -1.8110 -0.7526 10 8 -6 1.2691 -1.0030 10 8 -5 -2.2408 0.1507 10 8 -4 0.5837 1.7703 10 8 -3 -3.0794 -2.0326 10 8 -2 4.8131 0.2547 10 8 -1 4.2779 0.8626 10 8 0 -2.6444 -1.0900 10 8 1 1.1662 0.0175 10 8 2 -2.7045 -0.7383 10 8 3 4.1124 -0.2551 10 8 4 -1.2343 1.1297 10 8 5 0.2637 0.2399 10 8 6 1.3639 -0.7957 10 8 7 1.5867 -1.3798 10 8 8 0.6007 -2.8078 10 8 9 2.6531 0.5632 10 8 10 0.8631 1.2312 10 9 -9 -1.3720 -0.4720 10 9 -8 1.2159 -0.0832 10 9 -7 1.3267 0.3829 10 9 -6 0.1802 0.8712 10 9 -5 -2.0296 -2.2803 10 9 -4 0.4091 0.9483 10 9 -3 -2.4527 -1.9672 10 9 -2 -0.2505 -3.4319 10 9 -1 0.3839 -0.0725 10 9 0 0.7690 -1.5661 10 9 1 -1.9734 -1.7738 10 9 2 -6.1449 1.1952 10 9 3 0.4495 -3.9989 10 9 4 0.1923 0.1908 10 9 5 1.4764 -3.4689 10 9 6 -0.3279 -2.6414 10 9 7 0.7511 -0.7233 10 9 8 -0.1025 1.1854 10 9 9 0.6394 0.8158 10 10 -8 4.3060 1.9113 10 10 -6 0.9929 -2.0378 10 10 -4 0.2376 0.3794 10 10 -2 -5.1310 -1.2043 10 10 0 0.9528 -0.3230 10 10 2 1.2465 1.7144 10 10 4 -1.0393 0.6375 10 10 6 -1.1235 -0.1260 10 10 8 0.3622 2.7374 11 0 0 3.9148 -0.0003 11 0 1 7.5987 5.0001 11 0 2 8.7290 -1.1717 11 0 3 2.9514 -1.3359 11 0 4 21.6154 -3.9349 11 0 5 1.6713 -8.1463 11 0 6 -0.3993 8.8126 11 0 7 2.9140 -0.0254 11 0 8 6.9490 8.1280 11 0 9 6.5127 0.3412 11 0 10 5.8397 1.0006 11 0 11 1.5891 -2.7997 11 0 12 -0.3675 -0.5990 11 1 -12 2.0075 1.2241 11 1 -11 -1.3651 1.0937 11 1 -10 0.5448 -1.1784 11 1 -9 0.9387 2.4547 11 1 -8 -1.9885 -1.8270 11 1 -7 2.2652 2.5379 11 1 -6 4.0892 1.2412 11 1 -5 -1.9541 -2.3541 11 1 -4 13.1362 -6.1278 11 1 -3 -8.6320 -7.7388 11 1 -2 -2.3205 -8.1151 11 1 -1 3.0801 8.9561 11 1 0 2.9158 6.6868 11 1 1 3.3104 7.1551 11 1 2 1.5243 -0.3605 11 1 3 -2.2459 -2.3416 11 1 4 1.3246 -0.1062 11 1 5 -3.6859 -7.3813 11 1 6 -0.7322 -4.5639 11 1 7 -0.4875 -1.5246 11 1 8 -2.2764 3.5575 11 1 9 -2.8565 5.0671 11 1 10 4.4672 4.6722 11 1 11 0.1405 1.0603 11 1 12 2.3440 -3.4512 11 2 -12 -2.3187 -1.2805 11 2 -11 0.8840 -3.0240 11 2 -10 -2.5169 -1.4604 11 2 -9 -1.6743 0.1375 11 2 -8 -0.4296 1.0461 11 2 -7 -2.3735 -1.0393 11 2 -6 2.5921 6.4483 11 2 -5 0.3978 3.7258 11 2 -4 11.4919 -0.4895 11 2 -3 5.8402 4.4720 11 2 -2 2.9329 1.9483 11 2 -1 2.8727 7.6563 11 2 0 -8.0975 6.1126 11 2 1 -4.1534 -3.5505 11 2 2 4.3529 -6.1517 11 2 3 3.3502 3.8275 11 2 4 -1.2114 -5.9325 11 2 5 8.4759 -0.4904 11 2 6 5.0249 -1.5457 11 2 7 4.1501 0.9081 11 2 8 0.4772 0.0319 11 2 9 2.9286 3.7900 11 2 10 -1.4414 0.8618 11 2 11 0.3972 -1.8141 11 2 12 -1.1258 1.6345 11 3 -12 0.0906 -0.2440 11 3 -11 0.5449 1.1716 11 3 -10 -0.9196 -1.0567 11 3 -9 3.7055 -1.4387 11 3 -8 -1.5214 -3.5650 11 3 -7 0.3024 -2.8255 11 3 -6 -1.6489 -0.1295 11 3 -5 -1.9102 -0.2152 11 3 -4 7.4633 -3.5972 11 3 -3 -4.5852 -0.5124 11 3 -2 8.9746 4.9201 11 3 -1 5.2107 4.3444 11 3 0 3.0704 5.1991 11 3 1 -0.0658 1.2708 11 3 2 8.9208 2.9896 11 3 3 2.6791 6.7854 11 3 4 3.1427 1.5080 11 3 5 2.9467 -3.0073 11 3 6 0.6006 -2.3543 11 3 7 1.4305 0.8398 11 3 8 -0.5256 0.5546 11 3 9 -1.2194 -1.3773 11 3 10 -2.0639 2.2067 11 3 11 -3.7831 -0.3982 11 3 12 -1.1003 -2.7449 11 4 -11 -0.6315 -2.1902 11 4 -10 -2.3029 1.2073 11 4 -9 5.0430 -1.4483 11 4 -8 2.8538 -1.4711 11 4 -7 6.6564 -3.6610 11 4 -6 3.0553 0.2949 11 4 -5 -1.8051 -1.1630 11 4 -4 -2.7700 -1.5242 11 4 -3 -5.7296 6.4838 11 4 -2 -4.9868 -2.0537 11 4 -1 3.9928 2.5405 11 4 0 1.4633 -0.5192 11 4 1 -5.0714 -3.0724 11 4 2 2.5148 1.2502 11 4 3 1.0044 3.7092 11 4 4 1.3988 6.0375 11 4 5 -0.6137 -1.0909 11 4 6 1.7791 -1.0896 11 4 7 0.3231 -1.6364 11 4 8 1.3982 0.1556 11 4 9 0.1818 -3.0017 11 4 10 -0.0806 -0.0537 11 4 11 -0.1251 0.9865 11 5 -11 -1.9592 -1.7830 11 5 -10 1.2172 0.6652 11 5 -9 0.3442 -1.3699 11 5 -8 0.2852 -1.1517 11 5 -7 2.7340 -0.6480 11 5 -6 -1.6557 -3.1083 11 5 -5 0.6026 2.2691 11 5 -4 -0.6970 0.8617 11 5 -3 -0.4484 0.4927 11 5 -2 -5.2151 3.3172 11 5 -1 0.9991 -1.3656 11 5 0 -1.0053 1.8134 11 5 1 -3.0544 -8.9864 11 5 2 3.7000 -4.0578 11 5 3 0.6176 -4.2646 11 5 4 1.6234 2.5340 11 5 5 2.5451 0.9514 11 5 6 -0.9153 3.2146 11 5 7 2.6852 0.7100 11 5 8 -1.8045 0.7087 11 5 9 -0.8273 -0.8312 11 5 10 1.5499 -0.0885 11 5 11 -1.5931 1.9989 11 6 -10 -0.3596 1.6618 11 6 -9 1.5762 2.1476 11 6 -8 -1.0917 0.6628 11 6 -7 4.5389 -0.7217 11 6 -6 0.8667 -0.7178 11 6 -5 0.2929 -1.3007 11 6 -4 -0.0479 -1.6378 11 6 -3 -5.0698 -0.6896 11 6 -2 -4.5878 -1.0669 11 6 -1 1.1895 -1.9325 11 6 0 -2.6974 0.1560 11 6 1 -4.3144 -0.0544 11 6 2 -2.3980 0.4417 11 6 3 -0.6825 -1.4379 11 6 4 -3.7472 1.1557 11 6 5 1.0622 -3.2254 11 6 6 -0.1471 1.3042 11 6 7 0.6738 -2.5479 11 6 8 0.5346 -4.3164 11 6 9 -0.1946 0.4684 11 6 10 -1.9971 -0.7160 11 7 -10 -1.7290 -1.2196 11 7 -9 -0.8915 0.3072 11 7 -8 -6.4920 -0.1922 11 7 -7 1.0960 3.3732 11 7 -6 0.0918 2.3183 11 7 -5 -1.2580 0.2608 11 7 -4 -0.9695 -1.2736 11 7 -3 -3.0359 0.8207 11 7 -2 2.5700 0.0461 11 7 -1 -0.8311 -0.8041 11 7 0 -2.2491 -4.4895 11 7 1 -0.5348 -2.5282 11 7 2 1.2676 -2.4523 11 7 3 -0.4589 -3.9528 11 7 4 0.5169 1.3651 11 7 5 1.9375 0.5169 11 7 6 -0.4487 -1.2682 11 7 7 1.8876 -5.1589 11 7 8 0.3264 -4.7879 11 7 9 -3.5549 -1.2378 11 7 10 -0.9182 -1.1322 11 8 -9 -2.8271 -6.4539 11 8 -8 -1.0306 1.7376 11 8 -7 0.1639 -2.7683 11 8 -6 0.6773 3.1901 11 8 -5 -3.1592 -0.8571 11 8 -4 -0.4943 -1.9075 11 8 -3 2.4582 -0.0965 11 8 -2 -0.0290 -2.2789 11 8 -1 3.6011 -2.2485 11 8 0 -0.3893 -1.4067 11 8 1 -1.2272 -3.2790 11 8 2 -0.5790 -0.9613 11 8 3 -4.3925 -2.3557 11 8 4 1.4303 1.9027 11 8 5 1.5328 -0.8185 11 8 6 1.2828 -1.4629 11 8 7 2.3940 -2.3367 11 8 8 -0.4361 -1.5706 11 8 9 4.8969 0.9020 11 9 -9 -7.9030 -3.5756 11 9 -8 6.6769 -0.0358 11 9 -7 -0.4877 -0.9549 11 9 -6 1.8094 -0.0617 11 9 -5 2.7185 0.0487 11 9 -4 -1.2600 -1.0271 11 9 -3 0.3624 -2.0710 11 9 -2 -4.9225 0.3239 11 9 -1 -0.0794 -1.7372 11 9 0 0.8834 1.7187 11 9 1 -3.2421 2.4425 11 9 2 -1.6408 1.2403 11 9 3 -1.7807 -1.1602 11 9 4 0.2019 -2.3048 11 9 5 -0.4606 -1.3035 11 9 6 2.3750 0.1173 11 9 7 0.7088 -0.8239 11 9 8 0.7894 4.3708 11 9 9 5.0883 1.3311 11 10 -8 0.8533 -2.8082 11 10 -7 -0.7775 -1.4144 11 10 -6 -0.8356 -0.9903 11 10 -5 1.7860 1.3111 11 10 -4 -1.0568 1.1326 11 10 -3 0.7364 -1.7505 11 10 -2 0.0214 -0.8526 11 10 -1 1.3142 -0.6431 11 10 0 1.5428 -0.4320 11 10 1 -1.0103 -1.2759 11 10 2 -0.3707 0.7080 11 10 3 -0.3863 -1.0532 11 10 4 -2.8479 -1.0975 11 10 5 -1.3097 1.0751 11 10 6 -0.6250 1.1371 11 10 7 -1.7103 0.7748 11 10 8 -2.0715 2.6858 11 11 -6 -2.1580 -1.1753 11 11 -4 -1.4162 3.3824 11 11 -2 1.1947 -2.0888 11 11 0 2.6483 0.1380 11 11 2 -0.6558 2.3304 11 11 4 -0.3178 0.9698 11 11 6 0.0289 -0.2549 12 0 0 -8.1660 0.0030 12 0 1 9.0649 5.9962 12 0 2 -4.1954 10.6743 12 0 3 5.2024 -2.7662 12 0 4 2.3912 6.0968 12 0 5 -5.6484 -1.1232 12 0 6 -2.7612 2.0832 12 0 7 7.4272 -3.2263 12 0 8 0.0083 1.3401 12 0 9 4.5898 3.4771 12 0 10 3.3042 -1.8191 12 0 11 4.8878 0.2167 12 0 12 -0.9378 0.4279 12 1 -12 2.0598 0.3015 12 1 -11 -1.3247 0.1527 12 1 -10 1.3090 -2.1001 12 1 -9 1.7907 -0.5279 12 1 -8 -3.0839 -0.4079 12 1 -7 -1.1753 -0.0486 12 1 -6 8.5908 -0.5842 12 1 -5 1.8862 0.7525 12 1 -4 1.9523 -1.3919 12 1 -3 0.1341 -1.1786 12 1 -2 -1.3756 -5.9221 12 1 -1 -5.2192 2.0139 12 1 0 -7.2312 -0.7717 12 1 1 -1.4609 -0.4238 12 1 2 -0.7554 10.7700 12 1 3 0.6925 4.0197 12 1 4 -6.2879 10.7780 12 1 5 -7.2863 -3.6306 12 1 6 -0.5122 -0.9827 12 1 7 0.7340 -1.5429 12 1 8 -4.2934 3.9923 12 1 9 0.4173 3.6216 12 1 10 1.4042 2.9815 12 1 11 -0.7258 -1.9776 12 1 12 -2.2249 -1.0678 12 2 -12 -3.3699 -0.9816 12 2 -11 0.3350 5.5941 12 2 -10 -2.9814 2.8633 12 2 -9 -0.3858 1.0218 12 2 -8 3.5586 0.7371 12 2 -7 -2.6560 3.0896 12 2 -6 -1.8018 -0.7967 12 2 -5 1.8525 2.7852 12 2 -4 -1.6844 -1.7220 12 2 -3 2.4098 1.1215 12 2 -2 5.0760 -6.0914 12 2 -1 -1.5343 10.0469 12 2 0 -9.5109 6.8436 12 2 1 -4.6739 2.3159 12 2 2 -2.3556 7.2929 12 2 3 -5.8904 8.6271 12 2 4 -0.9851 -5.0425 12 2 5 2.4398 -0.2400 12 2 6 0.6861 -2.7805 12 2 7 2.6719 -2.3102 12 2 8 -0.3372 -0.9371 12 2 9 0.5095 -0.1480 12 2 10 -1.6632 -3.3544 12 2 11 2.2031 -1.7856 12 2 12 -4.9019 -2.0087 12 3 -11 -0.9192 1.3884 12 3 -10 -1.5630 1.3297 12 3 -9 1.1338 -0.6125 12 3 -8 1.7058 -4.0631 12 3 -7 1.4358 0.6060 12 3 -6 -1.6950 1.3675 12 3 -5 -0.3069 0.5680 12 3 -4 -3.7663 2.1227 12 3 -3 -1.3881 -6.0519 12 3 -2 -4.6778 -0.2922 12 3 -1 1.4814 -4.5003 12 3 0 1.9365 -1.0014 12 3 1 -4.0944 -5.5376 12 3 2 -1.0886 -2.9109 12 3 3 -6.8859 3.3336 12 3 4 -4.0402 0.8760 12 3 5 -3.3579 0.1382 12 3 6 -0.6805 -0.0759 12 3 7 2.2395 -1.1657 12 3 8 0.3226 0.0731 12 3 9 0.6677 -2.0121 12 3 10 -1.1227 2.4140 12 3 11 1.3465 -1.0342 12 4 -11 -1.3388 0.4481 12 4 -10 0.1361 -0.1665 12 4 -9 0.7623 -0.3930 12 4 -8 3.3668 -6.4049 12 4 -7 0.9714 -1.9423 12 4 -6 1.5916 -2.8069 12 4 -5 1.8380 -0.0010 12 4 -4 -0.5503 1.2289 12 4 -3 0.2139 0.5404 12 4 -2 -4.6108 5.3748 12 4 -1 -0.4763 1.3788 12 4 0 0.2847 3.1086 12 4 1 -4.4747 -5.4543 12 4 2 2.9597 -4.7105 12 4 3 0.7190 0.0520 12 4 4 -2.9464 -0.3695 12 4 5 -1.7692 -1.6443 12 4 6 0.7603 1.5585 12 4 7 1.0648 -0.7214 12 4 8 1.6936 -0.9560 12 4 9 -0.4609 -1.5018 12 4 10 -0.2055 0.2879 12 4 11 1.3136 -0.8666 12 5 -10 1.6141 -0.1458 12 5 -9 -0.4072 0.7751 12 5 -8 1.1627 -1.1575 12 5 -7 -1.2978 1.5990 12 5 -6 1.4525 -1.3491 12 5 -5 5.0196 2.6877 12 5 -4 1.6165 -1.7361 12 5 -3 2.7742 -5.3811 12 5 -2 2.2596 1.6075 12 5 -1 -5.7541 -1.1180 12 5 0 2.5035 -2.9628 12 5 1 -4.1014 -3.6128 12 5 2 -2.6523 -2.1692 12 5 3 0.2884 -4.0785 12 5 4 2.2683 -0.8637 12 5 5 1.6031 0.0007 12 5 6 1.9704 2.3583 12 5 7 2.1249 1.1862 12 5 8 1.4735 -0.0304 12 5 9 -1.7192 -1.1964 12 5 10 -2.0185 0.0779 12 6 -10 0.4749 -0.5036 12 6 -9 0.6264 -1.6097 12 6 -8 -3.4311 -0.2471 12 6 -7 1.1566 1.1661 12 6 -6 -1.7437 -1.4062 12 6 -5 -2.3060 -3.3201 12 6 -4 -1.1611 6.4271 12 6 -3 -1.9294 2.7017 12 6 -2 5.4879 -1.8720 12 6 -1 -0.1874 5.0144 12 6 0 -4.5476 -5.1098 12 6 1 1.9667 0.3154 12 6 2 -0.4438 2.7091 12 6 3 -1.2350 2.0085 12 6 4 -3.6058 -0.5922 12 6 5 -0.2369 2.3346 12 6 6 -1.0438 1.4310 12 6 7 1.1935 -1.2511 12 6 8 -0.0026 -2.4073 12 6 9 -1.7019 -0.8413 12 6 10 -5.0863 -0.6438 12 7 -9 -2.8231 -4.0881 12 7 -8 -0.4833 0.8042 12 7 -7 3.4930 1.1266 12 7 -6 1.9128 -0.5244 12 7 -5 -3.0466 -2.0637 12 7 -4 -1.0439 1.2262 12 7 -3 0.0540 2.9877 12 7 -2 1.8746 2.6045 12 7 -1 0.4046 -1.2501 12 7 0 -3.1981 2.1906 12 7 1 0.7447 -0.7552 12 7 2 0.9208 -2.1341 12 7 3 -0.6511 -1.9100 12 7 4 -2.4370 -0.0724 12 7 5 1.6540 -1.2006 12 7 6 0.4264 -2.6704 12 7 7 3.5494 -2.4756 12 7 8 -0.9800 0.8784 12 7 9 1.0716 -5.2001 12 8 -9 -5.0706 -4.2268 12 8 -8 3.5713 -2.0711 12 8 -7 2.5012 0.8743 12 8 -6 0.8045 2.8211 12 8 -5 2.2163 -0.6871 12 8 -4 -0.7972 0.8372 12 8 -3 0.1950 -0.5207 12 8 -2 -2.2196 -0.8188 12 8 -1 -2.2603 -4.8209 12 8 0 -0.2488 1.5961 12 8 1 -3.3292 1.8516 12 8 2 -0.0166 0.3032 12 8 3 0.1071 -0.2038 12 8 4 0.1131 -1.1330 12 8 5 1.1832 -0.9144 12 8 6 1.9507 -0.4806 12 8 7 0.8395 3.0176 12 8 8 0.9800 4.8644 12 8 9 5.9395 1.1649 12 9 -8 6.6120 -3.5230 12 9 -7 -0.9860 -0.6984 12 9 -6 0.2045 1.6646 12 9 -5 0.6492 -1.4215 12 9 -4 -0.5726 1.2565 12 9 -3 -0.6268 -1.6961 12 9 -2 0.9242 1.2632 12 9 -1 1.0444 0.0021 12 9 0 4.3112 -0.3432 12 9 1 -1.2462 2.8948 12 9 2 1.1312 -1.4637 12 9 3 1.4998 -1.0097 12 9 4 0.1498 -3.7925 12 9 5 -1.3040 -2.0913 12 9 6 -0.4620 -0.2877 12 9 7 0.1417 -0.3992 12 9 8 -0.9988 5.8008 12 10 -7 0.6322 0.0991 12 10 -6 -0.5978 -0.2589 12 10 -5 -1.6307 0.6169 12 10 -4 -0.9015 1.3970 12 10 -3 -1.4870 -0.2376 12 10 -2 0.7624 0.5095 12 10 -1 1.2595 0.2676 12 10 0 1.8530 -1.8597 12 10 1 1.4130 -0.4109 12 10 2 -1.5449 -0.3523 12 10 3 -0.0662 1.6382 12 10 4 -0.7420 -0.5941 12 10 5 0.2666 1.1864 12 10 6 0.2843 1.0474 12 10 7 -1.3583 -0.0566 12 11 -6 -0.4274 0.3363 12 11 -5 0.4074 0.7840 12 11 -4 -0.7866 -0.2506 12 11 -3 -0.2483 -0.8347 12 11 -2 -1.3903 -0.4717 12 11 -1 -0.9281 0.1473 12 11 0 1.7425 1.7236 12 11 1 1.5357 -0.8415 12 11 2 -0.6230 1.0829 12 11 3 -0.3621 -0.5676 12 11 4 0.0870 0.1344 12 11 5 1.1145 0.1349 12 11 6 0.3408 -1.1766 12 12 -4 0.0694 -0.2764 12 12 -2 1.0903 -1.0912 12 12 0 1.0125 0.8223 12 12 2 3.0544 -1.3070 12 12 4 -1.8320 -0.5781 13 0 0 -7.3621 0.0032 13 0 1 -4.6139 -0.9011 13 0 2 -0.2153 -4.7117 13 0 3 -4.0995 9.8133 13 0 4 -4.0816 4.2627 13 0 5 -5.4026 5.8594 13 0 6 0.6152 1.3867 13 0 7 1.9914 1.0365 13 0 8 1.3461 -3.5035 13 0 9 0.0656 -1.8132 13 0 10 5.0588 -2.9520 13 0 11 4.4883 -2.1918 13 0 12 -3.0908 1.7766 13 1 -11 -1.0029 -0.1960 13 1 -10 0.2081 -1.4113 13 1 -9 -1.4603 2.0096 13 1 -8 -1.7732 -0.9878 13 1 -7 -2.1391 1.1412 13 1 -6 0.8931 -1.3007 13 1 -5 1.4003 -7.4243 13 1 -4 -1.4119 3.3843 13 1 -3 2.5147 -3.7900 13 1 -2 2.4075 0.1582 13 1 -1 -7.4202 4.0176 13 1 0 -1.6673 3.1398 13 1 1 -3.9468 -2.3923 13 1 2 -2.5097 -2.6778 13 1 3 1.5107 3.5817 13 1 4 -5.1883 1.3316 13 1 5 0.0965 3.8217 13 1 6 -4.2962 -0.5481 13 1 7 -1.1600 -1.3424 13 1 8 -1.2323 -0.6903 13 1 9 0.3507 0.4884 13 1 10 2.5728 4.7194 13 1 11 1.1610 -2.8106 13 2 -11 2.6938 3.6323 13 2 -10 -0.5331 0.9396 13 2 -9 0.6939 0.8202 13 2 -8 0.4597 -1.5832 13 2 -7 -4.0622 1.0506 13 2 -6 1.2609 0.0315 13 2 -5 -2.6736 -1.3854 13 2 -4 -0.4274 2.1717 13 2 -3 -2.4847 -2.6207 13 2 -2 2.3853 -7.1296 13 2 -1 -5.8132 5.2470 13 2 0 11.9573 1.1061 13 2 1 2.5495 2.1193 13 2 2 -5.5858 2.0898 13 2 3 -1.6728 -1.5914 13 2 4 -2.4801 -4.9044 13 2 5 -2.5558 3.4820 13 2 6 -1.6441 -0.9384 13 2 7 3.1658 -2.9237 13 2 8 0.3245 -1.7255 13 2 9 -1.1927 -1.1385 13 2 10 -1.6196 -0.5222 13 2 11 -1.4190 0.3440 13 3 -11 -0.9460 -0.7995 13 3 -10 1.1367 1.9477 13 3 -9 1.9497 -0.6032 13 3 -8 -0.4263 -2.6986 13 3 -7 0.1841 1.9614 13 3 -6 2.3144 -1.1067 13 3 -5 0.8776 2.8834 13 3 -4 0.4420 -1.3954 13 3 -3 0.6686 -5.7455 13 3 -2 -7.3698 2.3640 13 3 -1 -5.2098 0.4204 13 3 0 4.4765 2.0621 13 3 1 -0.2665 1.6106 13 3 2 0.0609 2.8967 13 3 3 -3.5366 -1.9411 13 3 4 -1.7228 0.6720 13 3 5 -1.4063 1.5196 13 3 6 -0.2485 -1.8012 13 3 7 7.0751 0.6685 13 3 8 1.4838 0.2855 13 3 9 1.3009 -1.3696 13 3 10 1.3110 0.6289 13 3 11 -0.2866 -1.1173 13 4 -10 2.7022 -0.2270 13 4 -9 -2.5846 0.5526 13 4 -8 1.0235 0.2112 13 4 -7 -4.4147 1.7845 13 4 -6 1.1708 0.6990 13 4 -5 3.9521 1.4616 13 4 -4 -0.6166 0.6063 13 4 -3 5.9404 -3.4413 13 4 -2 5.7391 2.9280 13 4 -1 -2.2630 2.3539 13 4 0 0.6934 -2.8397 13 4 1 -1.0686 0.6495 13 4 2 -2.0135 0.0332 13 4 3 -2.9299 1.9709 13 4 4 1.9862 -1.6429 13 4 5 1.3055 -0.3267 13 4 6 1.0410 0.9206 13 4 7 0.3900 3.2843 13 4 8 1.0493 0.1321 13 4 9 0.2564 2.2104 13 4 10 1.0056 -0.7386 13 5 -10 5.5271 -0.4621 13 5 -9 -2.4701 -2.2231 13 5 -8 -0.5763 -0.1742 13 5 -7 -1.0687 -0.8735 13 5 -6 2.7658 -2.5258 13 5 -5 -1.6769 -2.8993 13 5 -4 0.3857 0.1133 13 5 -3 -3.0963 0.4162 13 5 -2 2.3164 2.6921 13 5 -1 0.8182 0.3070 13 5 0 0.0383 -2.2061 13 5 1 1.4787 -4.2536 13 5 2 -5.3221 3.4911 13 5 3 -1.0875 1.8530 13 5 4 2.0851 -1.1604 13 5 5 1.5504 1.2283 13 5 6 -0.4277 -0.8172 13 5 7 1.9011 -0.5403 13 5 8 -2.2192 0.9729 13 5 9 0.1191 -1.1666 13 5 10 -2.4586 -1.0755 13 6 -9 -1.0732 -1.4673 13 6 -8 -2.6428 1.4815 13 6 -7 3.9303 1.5237 13 6 -6 1.8288 -1.2083 13 6 -5 -0.7246 0.9625 13 6 -4 0.1281 1.5939 13 6 -3 -0.0474 -0.0108 13 6 -2 4.8529 2.7235 13 6 -1 -0.1736 -0.6631 13 6 0 0.8406 1.0842 13 6 1 0.9894 1.1268 13 6 2 -0.9034 2.6896 13 6 3 -0.8628 2.0727 13 6 4 -1.1637 1.9520 13 6 5 0.3119 1.1326 13 6 6 1.8183 -2.7603 13 6 7 1.7125 -1.2530 13 6 8 -0.9834 2.7758 13 6 9 0.9551 0.1853 13 7 -8 -0.4553 -0.1338 13 7 -7 -0.2111 2.0324 13 7 -6 0.0780 1.2264 13 7 -5 -0.9449 0.5955 13 7 -4 -0.8587 1.4068 13 7 -3 -0.7359 0.6449 13 7 -2 1.7684 -0.6918 13 7 -1 -1.2600 -2.8353 13 7 0 -0.4802 0.4381 13 7 1 -0.2958 0.9419 13 7 2 -1.0040 -0.0362 13 7 3 0.9216 0.7970 13 7 4 0.2589 0.2271 13 7 5 3.2218 0.2062 13 7 6 1.5791 -3.8939 13 7 7 2.6835 1.6850 13 7 8 -2.9698 2.5816 13 8 -8 2.4235 -6.5553 13 8 -7 -1.1585 3.1567 13 8 -6 0.2305 0.4971 13 8 -5 -0.0134 -1.8430 13 8 -4 1.5509 0.6841 13 8 -3 0.3179 0.3227 13 8 -2 -0.4745 -0.7586 13 8 -1 -0.8869 1.0382 13 8 0 1.2050 0.2479 13 8 1 1.3140 0.8315 13 8 2 0.7304 0.6553 13 8 3 2.4428 0.5971 13 8 4 2.4613 -1.8033 13 8 5 2.1545 -1.2039 13 8 6 0.8718 -1.4547 13 8 7 0.9947 2.1603 13 8 8 1.7989 3.7626 13 9 -7 1.0486 1.2889 13 9 -6 0.8916 0.2035 13 9 -5 -2.3293 -0.1546 13 9 -4 -1.4624 1.0342 13 9 -3 -0.7753 0.3349 13 9 -2 0.6135 0.7632 13 9 -1 1.0061 0.7099 13 9 0 1.0678 -0.3616 13 9 1 0.7798 -1.3587 13 9 2 -0.3352 -0.5386 13 9 3 -1.3568 0.3920 13 9 4 -1.8638 -1.1339 13 9 5 0.8188 0.7388 13 9 6 0.3062 -0.7857 13 9 7 1.1777 0.8679 13 10 -6 -0.9600 -0.6081 13 10 -5 -0.2450 0.4022 13 10 -4 0.1378 1.0701 13 10 -3 -0.0024 0.6814 13 10 -2 -0.2669 -0.1217 13 10 -1 -0.6665 0.4125 13 10 0 -0.4625 -0.3603 13 10 1 -0.4861 -0.6268 13 10 2 0.4309 0.0983 13 10 3 -0.2331 -0.4962 13 10 4 0.3767 -0.5325 13 10 5 0.7033 0.3507 13 10 6 -1.1191 0.6807 13 11 -4 0.0283 -0.9281 13 11 -3 0.8373 0.2002 13 11 -2 -0.6425 -0.3086 13 11 -1 0.4722 0.9626 13 11 0 -0.3704 -0.5944 13 11 1 -0.2750 0.2025 13 11 2 1.1725 -0.7606 13 11 3 -0.7632 -1.4819 13 11 4 0.6456 0.4322 13 12 -2 -0.7550 -0.5600 13 12 -1 -0.7649 0.4702 13 12 0 -0.3104 0.0902 13 12 1 0.2264 1.3741 13 12 2 5.5246 -0.3350 14 0 0 -11.9160 0.0034 14 0 1 -1.0718 5.0340 14 0 2 8.8650 4.7389 14 0 3 -1.2674 5.9404 14 0 4 8.5235 -5.5099 14 0 5 4.2048 2.5416 14 0 6 -0.4416 1.7412 14 0 7 -0.8816 -6.6844 14 0 8 4.3223 -0.5470 14 0 9 -4.1891 -3.7114 14 0 10 2.4212 0.2695 14 0 11 -0.8794 0.2670 14 1 -11 -0.0582 -0.1638 14 1 -10 0.0955 1.4235 14 1 -9 2.1953 3.5815 14 1 -8 2.1800 -1.1234 14 1 -7 0.6167 -3.6875 14 1 -6 4.3321 0.3183 14 1 -5 -2.6603 -6.2916 14 1 -4 -1.3037 5.6417 14 1 -3 4.1915 0.8259 14 1 -2 -2.2022 -6.9791 14 1 -1 0.6036 1.0403 14 1 0 0.3064 3.2468 14 1 1 -3.3264 -3.3578 14 1 2 -5.1249 3.1069 14 1 3 -2.0978 -0.1218 14 1 4 0.1713 -5.4473 14 1 5 1.4515 6.8345 14 1 6 -0.9907 0.4411 14 1 7 -5.2663 -3.6531 14 1 8 5.9828 0.9776 14 1 9 0.8926 -0.0028 14 1 10 -0.3833 0.9498 14 1 11 0.0294 -2.1668 14 2 -10 -0.2737 -1.3327 14 2 -9 0.0380 1.7519 14 2 -8 -1.1277 2.9565 14 2 -7 -2.0325 -0.7483 14 2 -6 5.1193 1.6077 14 2 -5 -2.4884 -0.8850 14 2 -4 -0.8401 4.2113 14 2 -3 -3.0296 -0.2441 14 2 -2 2.9443 -1.4644 14 2 -1 -3.6435 -2.5818 14 2 0 8.4897 5.3138 14 2 1 -0.9892 3.9980 14 2 2 1.6828 1.2511 14 2 3 1.3904 -0.8272 14 2 4 -3.7759 -4.7550 14 2 5 2.0277 1.1997 14 2 6 0.8771 0.0681 14 2 7 4.0408 -1.9463 14 2 8 1.2344 1.5403 14 2 9 -0.7617 2.1490 14 2 10 0.5241 1.3250 14 3 -10 0.1790 -0.0345 14 3 -9 1.8597 -1.3712 14 3 -8 -2.3200 0.1369 14 3 -7 -3.1385 4.0629 14 3 -6 6.1823 -0.7462 14 3 -5 -4.1511 -0.3181 14 3 -4 -3.0120 -1.5549 14 3 -3 -1.5173 -2.6206 14 3 -2 0.5104 1.1090 14 3 -1 1.8453 -0.6925 14 3 0 0.7821 -1.1407 14 3 1 -0.5421 3.4706 14 3 2 -0.8164 3.9108 14 3 3 1.5682 -0.2419 14 3 4 -3.0816 4.4974 14 3 5 2.4748 -2.4373 14 3 6 4.7661 -0.5907 14 3 7 4.0359 1.7995 14 3 8 0.1932 -0.9933 14 3 9 -0.6619 0.3928 14 3 10 0.1109 0.8712 14 4 -9 0.2527 -3.4675 14 4 -8 0.4947 2.3291 14 4 -7 -0.1107 0.4263 14 4 -6 6.3649 -2.4323 14 4 -5 -0.3367 0.4730 14 4 -4 -2.3757 -2.2300 14 4 -3 0.8456 -2.2971 14 4 -2 -1.4949 1.4144 14 4 -1 2.0835 -0.7232 14 4 0 0.5570 -0.2090 14 4 1 -0.1354 -0.6860 14 4 2 -0.4458 3.0597 14 4 3 -3.6259 -0.9604 14 4 4 0.2144 -1.4798 14 4 5 4.1219 -2.0427 14 4 6 0.0819 3.2173 14 4 7 -1.6327 1.9141 14 4 8 0.4869 0.3821 14 4 9 -0.1717 1.2462 14 5 -9 -3.0751 -7.4185 14 5 -8 -1.0577 1.5050 14 5 -7 -0.4900 -2.6346 14 5 -6 1.7369 -3.4962 14 5 -5 1.2752 2.4618 14 5 -4 -0.3292 1.2963 14 5 -3 1.9241 0.2077 14 5 -2 0.2902 6.9810 14 5 -1 0.0116 -0.3234 14 5 0 -0.0990 0.8009 14 5 1 -1.7425 1.6402 14 5 2 -3.5149 -1.1532 14 5 3 -1.0986 -1.5575 14 5 4 2.3982 1.3983 14 5 5 1.7976 -1.1300 14 5 6 1.3608 0.6700 14 5 7 -0.2713 -1.4578 14 5 8 -2.7721 -0.1806 14 5 9 -0.8125 -0.9899 14 6 -8 -0.8496 -2.1736 14 6 -7 1.5243 0.1588 14 6 -6 -0.5507 -3.2602 14 6 -5 0.4096 0.5420 14 6 -4 -1.3303 -0.3985 14 6 -3 1.6886 -2.8785 14 6 -2 -0.1425 -0.1487 14 6 -1 0.3687 -2.1051 14 6 0 0.2312 -0.6335 14 6 1 0.2146 0.5012 14 6 2 -2.1483 0.5859 14 6 3 -0.7769 1.2443 14 6 4 -1.2580 2.6449 14 6 5 -0.2232 -0.7285 14 6 6 0.7354 0.9947 14 6 7 -0.0416 0.2328 14 6 8 -0.1117 0.8770 14 7 -8 -1.9437 -0.6345 14 7 -7 0.4974 1.2399 14 7 -6 -0.5516 -0.5030 14 7 -5 -1.1773 0.9758 14 7 -4 1.6400 -0.9306 14 7 -3 1.8520 -0.2143 14 7 -2 -0.7571 0.1183 14 7 -1 -1.0310 -0.7262 14 7 0 -0.4387 0.4268 14 7 1 1.3829 -1.8404 14 7 2 0.4663 0.2981 14 7 3 0.7024 -1.6118 14 7 4 1.5490 -0.0899 14 7 5 2.3376 -3.6129 14 7 6 0.6162 -1.3082 14 7 7 -0.4932 0.9452 14 7 8 -2.1651 -0.3261 14 8 -7 -0.2640 2.5247 14 8 -6 0.4664 -1.2623 14 8 -5 -0.5693 -0.2559 14 8 -4 -1.3974 -0.8622 14 8 -3 -0.0990 -0.6457 14 8 -2 0.4864 0.6842 14 8 -1 -1.3991 -0.2247 14 8 0 0.1099 0.4933 14 8 1 0.8601 -0.1996 14 8 2 2.2319 -1.1657 14 8 3 -0.0848 -1.9002 14 8 4 -0.3157 -0.4323 14 8 5 -0.1206 -1.6431 14 8 6 -0.0411 0.1156 14 8 7 0.9436 -0.2264 14 9 -5 -0.7438 1.1698 14 9 -4 -1.2331 1.8181 14 9 -3 -0.0080 0.5342 14 9 -2 0.8119 -0.2076 14 9 -1 -0.5027 -1.0235 14 9 0 -0.2310 -0.1307 14 9 1 -0.4531 0.4370 14 9 2 -0.7380 1.0137 14 9 3 -0.6100 1.6167 14 9 4 -0.3250 -0.7156 14 9 5 -0.2980 1.1681 14 10 -4 0.9571 0.1102 14 10 -3 -0.2595 -0.9627 14 10 -2 0.9280 -0.8821 14 10 -1 0.2725 -0.0777 14 10 0 0.5161 0.2572 14 10 1 -0.1127 0.1319 14 10 2 -0.0631 -0.3617 14 10 3 2.2143 -1.4266 14 10 4 0.1736 -0.4123 14 11 -1 0.4465 -1.3214 14 11 0 -1.3217 0.3704 14 11 1 -1.0875 1.3079 15 0 0 0.7700 -0.0023 15 0 1 4.1477 -1.8649 15 0 2 3.1735 -5.8411 15 0 3 -1.4355 -8.1523 15 0 4 6.4432 -10.5488 15 0 5 0.4540 1.4870 15 0 6 4.3133 -4.6035 15 0 7 -5.2251 -2.6405 15 0 8 2.0826 -1.5766 15 0 9 -0.4239 0.0883 15 0 10 0.5250 1.0858 15 1 -10 0.0040 -0.4484 15 1 -9 -1.7494 2.3877 15 1 -8 0.3999 -1.1602 15 1 -7 0.4997 0.3571 15 1 -6 3.1045 4.8562 15 1 -5 2.6474 -2.1984 15 1 -4 3.0408 4.9667 15 1 -3 -2.9808 4.6114 15 1 -2 4.0483 -4.4419 15 1 -1 -7.8415 1.8580 15 1 0 -3.9923 4.3549 15 1 1 2.1569 1.1722 15 1 2 -0.6266 2.4894 15 1 3 5.5015 -3.7364 15 1 4 5.0428 -2.5128 15 1 5 0.7657 5.1866 15 1 6 0.9315 -0.9186 15 1 7 0.7039 -1.5071 15 1 8 -0.3885 1.1224 15 1 9 1.2845 -0.5888 15 1 10 -0.8314 1.2712 15 2 -10 -0.3104 -0.1227 15 2 -9 -0.7379 1.0089 15 2 -8 -2.9893 1.1127 15 2 -7 -0.4301 3.8865 15 2 -6 -0.6267 3.2288 15 2 -5 0.2449 -0.8178 15 2 -4 0.9307 2.6356 15 2 -3 0.4830 2.7196 15 2 -2 5.5092 -1.6484 15 2 -1 4.4368 -1.3715 15 2 0 -2.5357 1.8551 15 2 1 -2.5501 -1.1327 15 2 2 5.8272 2.2105 15 2 3 1.9645 -1.6469 15 2 4 0.0066 2.1329 15 2 5 -1.3544 -0.4060 15 2 6 2.4925 1.3559 15 2 7 3.6081 0.4060 15 2 8 -0.0231 -0.2906 15 2 9 0.3122 -1.3932 15 2 10 0.0411 0.3036 15 3 -9 1.0407 -2.9453 15 3 -8 -0.3635 0.5649 15 3 -7 -0.2232 2.9631 15 3 -6 1.5266 -0.9197 15 3 -5 -6.9309 -2.6771 15 3 -4 0.3965 3.4574 15 3 -3 -2.0730 -2.2828 15 3 -2 -2.5849 1.0787 15 3 -1 5.7615 -4.2386 15 3 0 -4.0255 0.0418 15 3 1 -1.5356 -1.6837 15 3 2 5.6930 2.4968 15 3 3 0.8400 3.7855 15 3 4 1.2422 1.1928 15 3 5 1.0880 -1.3056 15 3 6 2.1002 0.3695 15 3 7 -1.0825 -0.3955 15 3 8 -0.4109 -1.1756 15 3 9 0.5943 -1.8030 15 4 -9 -2.8482 -4.0671 15 4 -8 2.4039 -1.9006 15 4 -7 1.5173 -0.4345 15 4 -6 1.5105 -1.5446 15 4 -5 1.3205 -2.0176 15 4 -4 0.6161 2.7092 15 4 -3 0.3451 1.2922 15 4 -2 -1.0970 6.6468 15 4 -1 -3.3356 1.3012 15 4 0 1.5436 2.0272 15 4 1 0.2124 0.8055 15 4 2 -2.0717 -4.5789 15 4 3 -2.3070 -0.6174 15 4 4 0.9234 -2.5497 15 4 5 1.0387 2.4200 15 4 6 1.2553 0.0702 15 4 7 -0.9683 0.5733 15 4 8 1.2745 0.4539 15 4 9 1.2292 0.3252 15 5 -8 -2.8173 1.1642 15 5 -7 0.4695 -0.1754 15 5 -6 0.1711 0.9390 15 5 -5 -0.3088 -1.0094 15 5 -4 1.6318 -0.9729 15 5 -3 2.8937 1.0318 15 5 -2 -0.4692 0.6968 15 5 -1 -0.3470 3.1926 15 5 0 0.4057 0.2568 15 5 1 -1.1168 1.2665 15 5 2 -3.7839 -3.9037 15 5 3 -1.5106 -2.6779 15 5 4 -1.0630 0.6262 15 5 5 2.6366 1.7494 15 5 6 0.1507 -1.0042 15 5 7 0.8617 -0.6663 15 5 8 -2.6108 1.4114 15 6 -7 -3.7334 0.6910 15 6 -6 -1.0072 0.0327 15 6 -5 -0.4223 1.1710 15 6 -4 -0.3814 -2.8621 15 6 -3 1.5257 -0.2080 15 6 -2 -3.3986 -0.9175 15 6 -1 -0.3347 0.8879 15 6 0 -0.1780 -1.4054 15 6 1 1.6349 -0.6175 15 6 2 1.2461 1.2000 15 6 3 -0.3044 0.2136 15 6 4 0.2231 1.8059 15 6 5 -0.4775 0.5489 15 6 6 -0.0070 2.2355 15 6 7 -0.1264 -1.1120 15 7 -6 -1.7867 0.0346 15 7 -5 0.2780 0.2416 15 7 -4 -0.3911 -1.3160 15 7 -3 0.1116 -0.6369 15 7 -2 0.4838 -0.1210 15 7 -1 0.5005 -0.2521 15 7 0 -1.9618 -0.2257 15 7 1 -0.5132 0.1176 15 7 2 -0.2012 1.1908 15 7 3 -1.2152 0.3397 15 7 4 -0.4818 -0.7305 15 7 5 1.1281 -0.9304 15 7 6 -0.4943 0.0376 15 8 -5 -0.1538 -0.7784 15 8 -4 -2.4455 1.1513 15 8 -3 -1.3783 -0.3849 15 8 -2 0.3720 -1.0773 15 8 -1 -0.4515 0.2271 15 8 0 -0.5573 -1.0519 15 8 1 -1.3654 1.8335 15 8 2 -1.6169 0.3913 15 8 3 -1.0750 0.4747 15 8 4 -3.9018 1.4581 15 8 5 0.5070 0.3591 15 9 -4 1.4569 0.1058 15 9 -3 0.8027 -0.1219 15 9 -2 -0.2138 -2.2344 15 9 -1 1.1147 -1.2947 15 9 0 0.5589 -0.8269 15 9 1 0.0910 -0.0649 15 9 2 -2.4840 2.8880 15 9 3 0.8994 0.4640 15 9 4 0.4779 1.4222 15 10 -1 0.1728 -2.8855 15 10 0 1.1047 0.0274 15 10 1 -0.4557 -0.4109 16 0 0 -5.6187 0.0028 16 0 1 1.5742 -0.7882 16 0 2 -2.2689 -4.6075 16 0 3 -0.4653 5.1114 16 0 4 1.6453 -4.3062 16 0 5 2.3726 1.2776 16 0 6 -2.3985 -2.5557 16 0 7 -0.3693 -0.8218 16 0 8 0.3442 1.8910 16 0 9 0.0175 -0.1587 16 0 10 4.2884 2.9282 16 1 -9 1.0095 3.6613 16 1 -8 0.6363 -1.8741 16 1 -7 -2.2961 -0.9954 16 1 -6 -4.4792 -1.4793 16 1 -5 -0.2291 -7.0427 16 1 -4 3.0342 -2.1090 16 1 -3 -1.1044 6.7695 16 1 -2 -0.1216 3.2536 16 1 -1 -0.6864 1.3469 16 1 0 -3.9644 0.8917 16 1 1 2.1382 -2.0820 16 1 2 -5.3405 -3.0352 16 1 3 5.2550 -3.4919 16 1 4 -0.3624 7.4594 16 1 5 -1.8729 -0.6747 16 1 6 0.8629 3.1609 16 1 7 2.1233 4.7319 16 1 8 1.2056 -0.2348 16 1 9 -0.0810 0.7995 16 2 -9 1.1129 2.8734 16 2 -8 -0.0200 1.0540 16 2 -7 0.8907 -0.9068 16 2 -6 -1.9004 -7.0187 16 2 -5 -2.7821 -3.9741 16 2 -4 6.2568 -6.3407 16 2 -3 -1.5733 2.5616 16 2 -2 0.6618 0.3143 16 2 -1 4.7961 -0.2415 16 2 0 -0.8840 1.0642 16 2 1 3.8020 -1.9475 16 2 2 3.3479 1.5338 16 2 3 -0.4921 -1.1791 16 2 4 -1.2384 0.9261 16 2 5 -3.5413 -1.5834 16 2 6 -3.0053 2.7530 16 2 7 -0.9891 0.3346 16 2 8 -0.0477 0.6931 16 2 9 0.1625 0.1851 16 3 -8 1.0432 -2.8558 16 3 -7 1.1269 1.1763 16 3 -6 0.2484 -1.7750 16 3 -5 -1.3353 -1.8005 16 3 -4 2.5141 0.3529 16 3 -3 -2.7016 -2.4456 16 3 -2 -5.8276 -0.7662 16 3 -1 -5.6236 3.7607 16 3 0 -7.1922 0.4123 16 3 1 8.2362 1.3408 16 3 2 1.2072 1.5652 16 3 3 3.0811 -2.8114 16 3 4 3.3156 -2.2657 16 3 5 -0.5989 -0.5044 16 3 6 -0.7825 0.4715 16 3 7 -1.1533 -1.3567 16 3 8 0.5822 -0.5511 16 4 -8 -1.1444 -0.3293 16 4 -7 0.5525 1.6837 16 4 -6 -0.9617 0.0754 16 4 -5 -0.2017 -2.0412 16 4 -4 1.0492 -3.8441 16 4 -3 1.8012 -2.2407 16 4 -2 0.5294 -2.7950 16 4 -1 0.1885 -0.5810 16 4 0 -4.4338 2.3107 16 4 1 1.6892 -0.6929 16 4 2 0.8476 -2.5894 16 4 3 -2.0281 -4.2264 16 4 4 -0.5143 -1.1270 16 4 5 0.1643 1.2866 16 4 6 -1.3382 1.4614 16 4 7 1.9758 0.5827 16 4 8 1.1036 2.1587 16 5 -7 -1.5992 1.4077 16 5 -6 0.5924 0.9783 16 5 -5 -0.4487 1.1950 16 5 -4 2.1192 -1.6688 16 5 -3 1.1261 0.5380 16 5 -2 0.8365 -1.2649 16 5 -1 2.8740 -2.4214 16 5 0 -1.8819 0.9766 16 5 1 -1.1190 -0.2011 16 5 2 1.8470 -1.4558 16 5 3 1.2406 -0.1892 16 5 4 -0.1788 -1.2254 16 5 5 -0.9567 -1.6981 16 5 6 0.6312 -1.7675 16 5 7 0.3021 1.3321 16 6 -6 0.8492 0.5900 16 6 -5 0.6236 -0.2929 16 6 -4 -1.1738 0.9052 16 6 -3 -1.8487 1.7836 16 6 -2 1.6125 0.3461 16 6 -1 1.9524 -1.4212 16 6 0 -0.6038 0.2391 16 6 1 -0.8712 -2.0571 16 6 2 -0.9542 -0.1732 16 6 3 2.4081 1.9399 16 6 4 0.0367 0.1402 16 6 5 -0.3658 0.7787 16 6 6 -0.0045 0.6946 16 7 -5 0.4692 -1.2730 16 7 -4 -0.8094 -0.0295 16 7 -3 -1.6208 1.1174 16 7 -2 1.8354 -2.0724 16 7 -1 2.5369 0.8446 16 7 0 0.2042 0.1043 16 7 1 -1.1209 -0.1310 16 7 2 -0.6834 -0.2537 16 7 3 -1.5686 -1.4792 16 7 4 -1.0454 0.2462 16 7 5 0.1660 -0.5162 16 8 -3 1.6113 1.2893 16 8 -2 0.2406 -0.7564 16 8 -1 -0.2952 1.9892 16 8 0 2.7226 0.3010 16 8 1 0.0734 1.4378 16 8 2 1.8516 0.7130 16 8 3 -0.8967 1.2761 17 0 0 -1.8133 0.0027 17 0 1 -0.3184 -4.5755 17 0 2 -3.3954 -3.4213 17 0 3 -3.6828 1.0834 17 0 4 5.6868 3.3627 17 0 5 -4.9721 -1.6119 17 0 6 -1.2847 -2.0347 17 0 7 0.4742 5.0114 17 0 8 -0.7469 -0.0534 17 0 9 0.4633 1.0327 17 1 -8 0.8614 1.2607 17 1 -7 -3.0920 -0.2829 17 1 -6 -1.3247 -3.0389 17 1 -5 7.6288 -2.1587 17 1 -4 3.4289 -7.1413 17 1 -3 3.6428 4.1034 17 1 -2 -0.7458 2.8006 17 1 -1 3.0433 -4.7017 17 1 0 -0.4613 1.2664 17 1 1 -1.5007 -4.6258 17 1 2 -4.8193 -1.4086 17 1 3 -0.2716 0.4003 17 1 4 -0.7265 0.7604 17 1 5 1.5079 -1.8097 17 1 6 3.2243 -2.2811 17 1 7 0.2599 2.4854 17 1 8 -0.1012 -0.5558 17 2 -8 1.3271 -1.7073 17 2 -7 0.9104 -0.9709 17 2 -6 -3.4961 -2.0208 17 2 -5 3.3670 -0.4001 17 2 -4 6.0812 -0.2003 17 2 -3 -1.6300 -0.1340 17 2 -2 2.2659 -3.0063 17 2 -1 -1.0399 -1.8268 17 2 0 1.8676 -3.0373 17 2 1 7.1436 -3.6858 17 2 2 1.1146 5.0365 17 2 3 0.0998 -0.9296 17 2 4 4.0726 -0.4015 17 2 5 -0.0984 3.4054 17 2 6 -1.8831 -0.2041 17 2 7 0.6275 1.5796 17 2 8 -0.2920 0.7447 17 3 -7 3.2063 2.1885 17 3 -6 0.6341 2.0474 17 3 -5 1.1208 -0.2003 17 3 -4 1.2068 -2.9324 17 3 -3 -0.2134 -1.5858 17 3 -2 0.5726 -2.2864 17 3 -1 -1.3918 0.4677 17 3 0 2.7082 -0.7049 17 3 1 3.3439 -0.7158 17 3 2 2.2195 1.3665 17 3 3 0.3583 -2.7521 17 3 4 0.9987 2.1082 17 3 5 0.3151 0.8066 17 3 6 -3.2743 -0.2454 17 3 7 0.9969 -2.1534 17 4 -7 -0.2424 6.4416 17 4 -6 -1.7633 4.5516 17 4 -5 2.0792 4.1165 17 4 -4 -0.1831 -0.0266 17 4 -3 -1.2111 -2.8554 17 4 -2 2.7979 -1.8137 17 4 -1 -0.0985 -1.7750 17 4 0 2.0015 -1.5659 17 4 1 -0.5364 2.4587 17 4 2 4.6380 0.9749 17 4 3 -0.0812 -2.5028 17 4 4 -0.2596 2.4206 17 4 5 -0.5786 0.0552 17 4 6 -0.1070 -4.3182 17 4 7 6.5065 3.7794 17 5 -6 -0.4224 1.5923 17 5 -5 -1.2583 -0.6181 17 5 -4 2.3750 4.9916 17 5 -3 0.1233 0.1426 17 5 -2 2.2024 -1.0903 17 5 -1 2.3413 0.2135 17 5 0 -1.2688 -0.8796 17 5 1 -2.1182 -0.7881 17 5 2 1.0187 1.2787 17 5 3 -0.0726 2.7673 17 5 4 -1.5363 0.4037 17 5 5 1.1073 -0.5193 17 5 6 -2.7466 -0.7312 17 6 -4 -0.3647 3.2399 17 6 -3 0.5824 0.0894 17 6 -2 3.6161 -2.7695 17 6 -1 1.0656 1.0514 17 6 0 0.8954 1.0820 17 6 1 -0.9170 -0.6142 17 6 2 0.9493 -1.5678 17 6 3 -0.4051 0.4615 17 6 4 0.4405 -0.3456 17 7 -3 1.3998 1.8847 17 7 -2 3.8050 -3.5890 17 7 -1 1.6982 3.1174 17 7 0 1.4383 -0.1496 17 7 1 -2.5155 2.4230 17 7 2 1.0880 -0.1593 17 7 3 -2.1265 1.0732 18 0 0 2.6078 -0.0020 18 0 1 -5.0200 -4.2900 18 0 2 0.0912 -6.8425 18 0 3 -0.8419 2.5254 18 0 4 -1.9340 -1.5181 18 0 5 -4.4879 -2.4795 18 0 6 4.8004 -1.6050 18 0 7 1.6570 2.0361 18 0 8 -0.5371 0.9841 18 1 -8 2.3017 0.9019 18 1 -7 0.2656 -3.3912 18 1 -6 5.7302 -2.3046 18 1 -5 0.8567 -2.4041 18 1 -4 -2.2890 -1.2985 18 1 -3 -4.7579 7.6422 18 1 -2 -4.2507 -0.7736 18 1 -1 4.9067 -0.0583 18 1 0 -3.5472 -1.5453 18 1 1 1.2625 0.5730 18 1 2 -3.2754 3.5164 18 1 3 1.2874 5.0580 18 1 4 -2.7972 -0.0512 18 1 5 2.0355 -0.3024 18 1 6 5.6263 -0.8280 18 1 7 -0.1717 -1.1579 18 1 8 -0.0714 -0.2172 18 2 -7 3.3152 1.7588 18 2 -6 1.3964 1.8487 18 2 -5 4.3465 0.8622 18 2 -4 1.1727 1.4776 18 2 -3 -2.2997 -2.2345 18 2 -2 -1.1666 -0.8444 18 2 -1 -0.2538 -1.1256 18 2 0 5.7891 -3.1802 18 2 1 4.8175 0.2971 18 2 2 0.3578 0.6549 18 2 3 -1.1997 -2.5049 18 2 4 -0.3822 0.9079 18 2 5 -2.7508 3.6464 18 2 6 0.0494 1.1764 18 2 7 0.0013 -0.3166 18 3 -6 -3.3573 4.9335 18 3 -5 -2.2121 1.8639 18 3 -4 0.0231 1.8368 18 3 -3 -2.2501 -0.8972 18 3 -2 -3.3135 -4.2957 18 3 -1 -0.7090 0.8504 18 3 0 0.6506 -0.3951 18 3 1 1.0393 5.0272 18 3 2 0.8878 3.4864 18 3 3 2.2244 1.4204 18 3 4 -1.3872 2.6726 18 3 5 2.0386 0.7376 18 3 6 -4.1888 -1.5641 18 4 -5 1.3887 -0.6142 18 4 -4 2.5093 4.1924 18 4 -3 3.8939 -5.4923 18 4 -2 -1.4689 0.3964 18 4 -1 0.2017 -3.4781 18 4 0 -0.6884 -1.4859 18 4 1 -2.1090 -1.5393 18 4 2 -0.3021 0.9397 18 4 3 -0.2563 0.5084 18 4 4 -5.8787 3.4830 18 4 5 -0.0732 -3.7808 18 5 -4 4.9713 5.5729 18 5 -3 4.1504 -2.6853 18 5 -2 4.9252 -2.0657 18 5 -1 1.4786 1.6238 18 5 0 2.2573 0.3459 18 5 1 1.9383 -2.1841 18 5 2 2.1499 1.0684 18 5 3 1.9367 0.7518 18 5 4 -0.6512 -2.0139 18 6 -2 4.3922 -1.9312 18 6 -1 -0.7203 3.0015 18 6 0 3.0454 2.5681 18 6 1 -0.2050 0.6957 18 6 2 1.7805 -0.3576 19 0 0 -6.4088 -0.0007 19 0 1 -5.9244 -4.1499 19 0 2 -2.5753 -0.2186 19 0 3 2.3582 3.2026 19 0 4 -6.8043 -2.2878 19 0 5 1.0274 0.3436 19 0 6 9.0497 0.1536 19 0 7 0.5915 4.6337 19 1 -6 2.9039 1.6948 19 1 -5 -7.3968 0.7357 19 1 -4 -2.5266 3.1408 19 1 -3 -6.2773 7.8941 19 1 -2 -2.3258 -1.4241 19 1 -1 1.6842 2.7262 19 1 0 -1.4279 -2.9786 19 1 1 2.8065 2.6252 19 1 2 0.2214 -0.6845 19 1 3 6.2189 2.8121 19 1 4 -5.5968 2.4684 19 1 5 5.9451 1.8335 19 1 6 -1.1517 0.6308 19 2 -5 -2.7605 2.6016 19 2 -4 -5.3375 0.8526 19 2 -3 2.0234 0.5061 19 2 -2 -7.3767 -1.7349 19 2 -1 -0.4107 -0.2643 19 2 0 1.9474 -2.0224 19 2 1 2.5621 2.2970 19 2 2 -4.0838 -0.6149 19 2 3 -0.2617 -1.5020 19 2 4 -3.4201 11.5269 19 2 5 0.9058 1.2639 19 3 -4 -0.0359 7.6653 19 3 -3 1.2412 -2.5951 19 3 -2 -5.3980 2.0305 19 3 -1 0.4402 3.5670 19 3 0 -0.2744 -0.2803 19 3 1 1.7603 0.6734 19 3 2 -0.0449 -1.6786 19 3 3 -1.9514 -0.9096 19 3 4 -0.9418 4.7195 19 4 -3 3.9599 -5.7166 19 4 -2 -6.4649 -0.1079 19 4 -1 0.4042 2.1664 19 4 0 -2.9113 1.7781 19 4 1 2.7126 0.0658 19 4 2 1.8575 1.0552 19 4 3 0.6494 1.6947 20 0 0 -1.5675 -0.0036 20 0 1 6.3373 2.7647 20 0 2 1.3549 -4.0451 20 0 3 5.6041 2.2133 20 0 4 -7.7312 1.4859 20 0 5 6.5839 1.8044 20 0 6 2.3232 -0.3841 20 1 -5 -7.7018 0.0832 20 1 -4 -6.9378 3.4325 20 1 -3 -4.9455 2.9629 20 1 -2 -0.8762 1.1544 20 1 -1 -9.0261 6.1425 20 1 0 -3.2053 -0.9767 20 1 1 8.8240 5.7106 20 1 2 0.9284 -2.3672 20 1 3 3.4551 2.4567 20 1 4 -4.6273 6.2598 20 1 5 4.7191 5.4912 20 2 -4 -2.4760 1.9964 20 2 -3 -3.1912 -0.7591 20 2 -2 -4.0730 -1.8632 20 2 -1 -6.3943 3.4563 20 2 0 -2.3996 -1.6112 20 2 1 3.4235 2.2724 20 2 2 -1.5913 -4.4004 20 2 3 -1.2405 1.3996 20 2 4 -4.6192 5.6993 20 3 -2 -2.5930 -3.5381 20 3 -1 1.1195 3.0803 20 3 0 -4.3374 -0.4270 20 3 1 1.9290 1.0960 20 3 2 -0.3652 -0.1635 21 0 0 -2.6685 0.0011 21 0 1 9.2112 -0.2774 21 0 2 -0.6705 -4.7406 21 0 3 -0.3769 -1.5524 21 0 4 -7.8459 4.4758 21 1 -2 3.5359 1.4446 21 1 -1 -5.8926 3.9347 21 1 0 0.7872 -3.3310 21 1 1 8.8041 2.4652 21 1 2 2.6048 -5.5480 0 0 0 0.0 0.0 ; _shelx_fab_checksum 19111 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, z+1/2' 'x-y, -y, z+1/2' '-x, -x+y, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C5 C 0.5961(9) 0.2492(6) 0.5670(9) 0.090(5) Uani 1 1 d DG . . A 1 C10 C 0.5473(6) 0.2058(8) 0.5167(12) 0.102(6) Uani 1 1 d DG . . A 1 H10 H 0.509527 0.205529 0.516020 0.122 Uiso 1 1 calc R U . A 1 C9 C 0.5538(7) 0.1626(5) 0.4676(10) 0.103(6) Uani 1 1 d DG . . A 1 C8 C 0.6091(9) 0.1629(6) 0.4686(10) 0.116(8) Uani 1 1 d DG . . A 1 C7 C 0.6579(7) 0.2064(8) 0.5188(12) 0.092(5) Uani 1 1 d DG . . A 1 H7 H 0.695734 0.206647 0.519531 0.110 Uiso 1 1 calc R U . A 1 C6 C 0.6514(7) 0.2496(5) 0.5680(9) 0.089(5) Uani 1 1 d DG . . A 1 C2 C 0.666667 0.333333 0.663(2) 0.109(8) Uani 1 3 d S T P A 1 C4 C 0.5436(9) 0.2715(11) 0.6966(13) 0.103(5) Uani 1 1 d . . . A 1 H4A H 0.526250 0.227034 0.699863 0.155 Uiso 1 1 calc R U . A 1 H4B H 0.511978 0.280653 0.676866 0.155 Uiso 1 1 calc R U . A 1 H4C H 0.558578 0.289530 0.755664 0.155 Uiso 1 1 calc R U . A 1 C3 C 0.6014(9) 0.3009(11) 0.6244(12) 0.095(4) Uani 1 1 d . . . A 1 C20 C 0.4024(10) 0.0489(11) 0.3189(19) 0.207(8) Uani 1 1 d DG . . A 1 C22 C 0.3489(12) 0.0438(11) 0.3537(19) 0.218(9) Uani 1 1 d DG . . A 1 H22 H 0.351038 0.073087 0.395497 0.262 Uiso 1 1 calc R U . A 1 C23 C 0.2923(10) -0.0043(14) 0.327(2) 0.241(10) Uani 1 1 d DG . . A 1 H23 H 0.255745 -0.007779 0.350877 0.289 Uiso 1 1 calc R U . A 1 C24 C 0.2892(9) -0.0471(12) 0.266(2) 0.262(9) Uani 1 1 d DG . . A 1 H24 H 0.250541 -0.079977 0.247810 0.314 Uiso 1 1 calc R U . A 1 N2 N 0.3427(10) -0.0420(11) 0.2312(18) 0.243(8) Uani 1 1 d DG . . A 1 C21 C 0.3994(9) 0.0060(12) 0.2577(19) 0.221(9) Uani 1 1 d DG . . A 1 H21 H 0.435925 0.009555 0.233982 0.265 Uiso 1 1 calc R U . A 1 C19 C 0.4676(12) 0.0934(9) 0.3736(13) 0.190(9) Uani 1 1 d D . . A 1 C18 C 0.5101(12) 0.1225(10) 0.4092(16) 0.129(5) Uani 1 1 d D . . A 1 C32 C 0.3368(11) -0.0708(15) 0.141(2) 0.242(7) Uani 1 1 d D . . A 1 H32A H 0.302606 -0.113629 0.139080 0.290 Uiso 0.3333 1 calc R U P A 1 H32B H 0.332446 -0.046680 0.092624 0.290 Uiso 1 1 calc R U . A 1 C1 C 0.666667 0.333333 0.7700(19) 0.090(8) Uani 1 3 d S T P A 1 H1A H 0.686317 0.375623 0.791838 0.136 Uiso 0.3333 1 calc R U P A 1 H1B H 0.689306 0.313683 0.791838 0.136 Uiso 0.3333 1 calc R U P A 1 H1C H 0.624377 0.310694 0.791838 0.136 Uiso 0.3333 1 calc R U P A 1 C13 C 0.6486(12) 0.0475(10) 0.3316(17) 0.207(8) Uani 1 1 d DG . . A 1 C15 C 0.6758(11) 0.0178(13) 0.3733(15) 0.218(9) Uani 1 1 d DG . . A 1 H15 H 0.697993 0.033792 0.427223 0.262 Uiso 1 1 calc R U . A 1 C16 C 0.6704(13) -0.0352(13) 0.3363(18) 0.241(10) Uani 1 1 d DG . . A 1 H16 H 0.688986 -0.055453 0.364831 0.289 Uiso 1 1 calc R U . A 1 C17 C 0.6379(14) -0.0586(12) 0.2574(19) 0.262(9) Uani 1 1 d DG . . A 1 H17 H 0.634201 -0.094798 0.232117 0.314 Uiso 1 1 calc R U . A 1 N1 N 0.6107(11) -0.0289(11) 0.2157(15) 0.243(8) Uani 1 1 d DG . . A 1 C14 C 0.6160(11) 0.0241(10) 0.2527(16) 0.221(9) Uani 1 1 d DG . . A 1 H14 H 0.597426 0.044347 0.224186 0.265 Uiso 1 1 calc R U . A 1 C12 C 0.6307(8) 0.0875(10) 0.3806(13) 0.190(9) Uani 1 1 d D . . A 1 C11 C 0.6177(11) 0.1167(11) 0.4164(16) 0.129(5) Uani 1 1 d D . . A 1 C25 C 0.5702(10) -0.0585(9) 0.1359(11) 0.242(7) Uani 1 1 d D . . A 1 H25A H 0.592713 -0.035832 0.081831 0.290 Uiso 1 1 calc R U . A 1 H25B H 0.562856 -0.100768 0.130498 0.290 Uiso 1 1 calc R U . A 1 C26 C 0.5095(8) -0.0613(7) 0.1368(6) 0.242(7) Uani 1 1 d DG . . A 1 C27 C 0.4971(10) -0.0266(7) 0.0771(9) 0.242(7) Uani 1 1 d DG . . A 1 H27 H 0.527289 -0.001056 0.034962 0.290 Uiso 1 1 calc R U . A 1 C28 C 0.4407(11) -0.0293(9) 0.0793(15) 0.242(7) Uani 1 1 d DG . . A 1 H28 H 0.432310 -0.005561 0.038517 0.290 Uiso 1 1 calc R U . A 1 C29 C 0.3966(9) -0.0667(11) 0.1410(18) 0.242(7) Uani 1 1 d DG . . A 1 C30 C 0.4089(9) -0.1014(9) 0.2006(14) 0.242(7) Uani 1 1 d DG . . A 1 H30 H 0.378785 -0.126995 0.242768 0.290 Uiso 1 1 calc R U . A 1 C31 C 0.4653(10) -0.0988(7) 0.1985(8) 0.242(7) Uani 1 1 d DG U . A 1 H31 H 0.473763 -0.122490 0.239214 0.290 Uiso 1 1 calc R U . A 1 F7A F 0.645(3) 0.339(2) 0.397(4) 0.253(7) Uani 0.3333 1 d D U P B -2 F9A F 0.630(3) 0.247(2) 0.392(4) 0.253(7) Uani 0.3333 1 d D U P B -2 F8A F 0.658(3) 0.303(2) 0.273(4) 0.253(7) Uani 0.3333 1 d D U P B -2 O5A O 0.548(4) 0.300(4) 0.274(7) 0.253(7) Uani 0.3333 1 d D U P B -2 O6A O 0.520(3) 0.213(3) 0.356(6) 0.253(7) Uani 0.3333 1 d D U P B -2 C5A C 0.555(2) 0.264(3) 0.322(5) 0.253(7) Uani 0.3333 1 d D U P B -2 C6A C 0.624(2) 0.289(2) 0.346(3) 0.253(7) Uani 0.3333 1 d D U P B -2 F1A F 0.4230(16) 0.2651(14) 0.371(3) 0.253(7) Uani 0.6667 1 d D U P C -1 F2A F 0.4631(16) 0.2091(15) 0.409(3) 0.253(7) Uani 0.6667 1 d D U P C -1 F3A F 0.381(2) 0.174(2) 0.323(3) 0.253(7) Uani 0.3333 1 d D U P C -1 O1A O 0.3934(19) 0.1985(19) 0.554(3) 0.253(7) Uani 0.6667 1 d D U P C -1 O2A O 0.3140(17) 0.164(2) 0.449(3) 0.253(7) Uani 0.6667 1 d D U P C -1 C1A C 0.3686(17) 0.1874(16) 0.478(3) 0.253(7) Uani 0.6667 1 d D U P C -1 C2A C 0.4097(16) 0.2081(15) 0.395(3) 0.253(7) Uani 0.6667 1 d D U P C -1 F5A F 0.636(2) 0.208(2) 0.094(3) 0.328(18) Uani 0.6667 1 d D U P D -1 F6A F 0.5694(17) 0.1715(19) 0.192(3) 0.295(16) Uani 0.6667 1 d D U P D -1 F4A F 0.664(2) 0.2231(18) 0.229(3) 0.295(16) Uani 0.6667 1 d D U P D -1 O3A O 0.5799(19) 0.0750(18) 0.203(2) 0.243(16) Uani 0.6667 1 d D U P D -1 O4A O 0.667(2) 0.105(2) 0.146(4) 0.282(19) Uani 0.6667 1 d D U P D -1 C3A C 0.628(2) 0.1191(17) 0.172(3) 0.283(18) Uani 0.6667 1 d D U P D -1 C4A C 0.6251(17) 0.1788(16) 0.173(3) 0.299(15) Uani 0.6667 1 d D U P D -1 F12A F 0.383(4) 0.136(3) 0.004(4) 0.29(3) Uani 0.3333 1 d D U P E -1 F11A F 0.464(3) 0.215(4) 0.056(4) 0.30(2) Uani 0.3333 1 d D U P E -1 F10A F 0.374(3) 0.202(3) 0.087(4) 0.29(2) Uani 0.3333 1 d D U P E -1 O8A O 0.425(5) 0.226(5) -0.136(4) 0.28(3) Uani 0.3333 1 d D U P E -1 O7A O 0.386(2) 0.266(2) -0.037(4) 0.20(2) Uani 0.3333 1 d D U P E -1 C7A C 0.407(3) 0.233(3) -0.060(3) 0.27(2) Uani 0.3333 1 d D U P E -1 C8A C 0.408(3) 0.196(3) 0.023(3) 0.29(2) Uani 0.3333 1 d D U P E -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C5 0.110(11) 0.076(10) 0.087(11) 0.011(8) 0.003(10) 0.049(10) C10 0.110(12) 0.076(12) 0.111(13) 0.006(9) 0.002(10) 0.041(10) C9 0.115(11) 0.067(11) 0.113(13) 0.012(9) 0.006(10) 0.035(9) C8 0.119(11) 0.084(13) 0.136(15) -0.019(12) -0.002(12) 0.042(11) C7 0.107(12) 0.064(11) 0.093(12) 0.020(8) 0.008(10) 0.034(10) C6 0.100(11) 0.070(11) 0.087(12) 0.009(10) -0.002(11) 0.035(10) C2 0.118(11) 0.118(11) 0.090(12) 0.000 0.000 0.059(5) C4 0.137(13) 0.087(13) 0.111(11) 0.007(13) 0.010(9) 0.074(13) C3 0.113(10) 0.088(11) 0.087(9) 0.003(9) -0.009(7) 0.053(10) C20 0.179(13) 0.181(13) 0.265(16) -0.113(12) -0.030(11) 0.093(11) C22 0.187(13) 0.211(16) 0.271(18) -0.098(14) -0.021(12) 0.110(13) C23 0.199(15) 0.218(18) 0.32(2) -0.115(15) -0.032(14) 0.119(14) C24 0.239(17) 0.253(18) 0.317(17) -0.133(14) -0.048(13) 0.141(15) N2 0.227(14) 0.204(14) 0.303(14) -0.144(12) -0.057(11) 0.112(12) C21 0.202(15) 0.200(15) 0.269(16) -0.120(13) -0.035(12) 0.107(13) C19 0.160(11) 0.179(15) 0.231(17) -0.086(14) -0.024(11) 0.085(11) C18 0.138(10) 0.093(8) 0.140(10) -0.011(7) 0.007(9) 0.045(8) C32 0.249(12) 0.189(9) 0.283(10) -0.147(8) -0.060(9) 0.106(9) C1 0.093(12) 0.093(12) 0.085(12) 0.000 0.000 0.047(6) C13 0.179(13) 0.181(13) 0.265(16) -0.113(12) -0.030(11) 0.093(11) C15 0.187(13) 0.211(16) 0.271(18) -0.098(14) -0.021(12) 0.110(13) C16 0.199(15) 0.218(18) 0.32(2) -0.115(15) -0.032(14) 0.119(14) C17 0.239(17) 0.253(18) 0.317(17) -0.133(14) -0.048(13) 0.141(15) N1 0.227(14) 0.204(14) 0.303(14) -0.144(12) -0.057(11) 0.112(12) C14 0.202(15) 0.200(15) 0.269(16) -0.120(13) -0.035(12) 0.107(13) C12 0.160(11) 0.179(15) 0.231(17) -0.086(14) -0.024(11) 0.085(11) C11 0.138(10) 0.093(8) 0.140(10) -0.011(7) 0.007(9) 0.045(8) C25 0.249(12) 0.189(9) 0.283(10) -0.147(8) -0.060(9) 0.106(9) C26 0.249(12) 0.189(9) 0.283(10) -0.147(8) -0.060(9) 0.106(9) C27 0.249(12) 0.189(9) 0.283(10) -0.147(8) -0.060(9) 0.106(9) C28 0.249(12) 0.189(9) 0.283(10) -0.147(8) -0.060(9) 0.106(9) C29 0.249(12) 0.189(9) 0.283(10) -0.147(8) -0.060(9) 0.106(9) C30 0.249(12) 0.189(9) 0.283(10) -0.147(8) -0.060(9) 0.106(9) C31 0.249(12) 0.189(9) 0.283(10) -0.147(8) -0.060(9) 0.106(9) F7A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) F9A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) F8A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) O5A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) O6A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) C5A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) C6A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) F1A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) F2A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) F3A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) O1A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) O2A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) C1A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) C2A 0.236(13) 0.207(12) 0.329(15) -0.013(12) -0.039(14) 0.121(12) F5A 0.27(3) 0.33(4) 0.31(3) 0.01(2) 0.04(2) 0.09(3) F6A 0.31(3) 0.26(3) 0.29(3) 0.02(2) 0.08(2) 0.12(2) F4A 0.31(3) 0.27(3) 0.29(3) 0.01(2) 0.06(3) 0.14(3) O3A 0.29(3) 0.26(3) 0.13(2) -0.06(2) 0.00(2) 0.10(2) O4A 0.31(4) 0.24(3) 0.27(4) 0.03(3) 0.08(3) 0.11(3) C3A 0.29(3) 0.27(3) 0.25(4) -0.02(2) 0.04(3) 0.12(2) C4A 0.30(3) 0.27(3) 0.29(3) -0.01(2) 0.06(2) 0.12(2) F12A 0.31(5) 0.27(4) 0.26(5) -0.06(3) 0.04(4) 0.12(4) F11A 0.34(5) 0.25(4) 0.25(4) -0.03(4) 0.05(3) 0.11(4) F10A 0.33(5) 0.25(4) 0.22(4) -0.04(3) 0.05(3) 0.11(4) O8A 0.28(7) 0.33(7) 0.22(4) -0.04(4) 0.07(4) 0.15(6) O7A 0.11(3) 0.15(4) 0.21(4) -0.05(3) 0.06(3) -0.03(3) C7A 0.29(5) 0.27(4) 0.22(4) -0.04(3) 0.07(3) 0.12(4) C8A 0.33(5) 0.27(4) 0.23(4) -0.04(3) 0.06(3) 0.12(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -1.00 0.00 0.00 0.1140 -1.00 0.00 -1.00 0.2310 -1.00 -1.00 0.00 0.1320 -1.00 0.00 1.00 0.1750 -1.00 1.00 0.00 0.1110 0.00 0.00 1.00 0.1370 0.00 0.00 -1.00 0.2260 0.00 -1.00 -1.00 0.2530 0.00 -1.00 0.00 0.1300 0.00 1.00 0.00 0.0900 1.00 0.00 0.00 0.0870 1.00 1.00 0.00 0.0820 1.00 0.00 -1.00 0.2150 1.00 -1.00 0.00 0.0710 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C10 C5 C6 120.0 . . ? C10 C5 C3 130.5(15) . . ? C6 C5 C3 109.5(15) . . ? C5 C10 H10 120.0 . . ? C5 C10 C9 120.0 . . ? C9 C10 H10 120.0 . . ? C10 C9 C8 120.0 . . ? C18 C9 C10 123.3(17) . . ? C18 C9 C8 116.4(17) . . ? C9 C8 C11 121.4(17) . . ? C7 C8 C9 120.0 . . ? C7 C8 C11 118.6(17) . . ? C8 C7 H7 120.0 . . ? C6 C7 C8 120.0 . . ? C6 C7 H7 120.0 . . ? C5 C6 C3 112.5(15) . 2_655 ? C7 C6 C5 120.0 . . ? C7 C6 C3 127.5(15) . 2_655 ? C3 C2 C3 106.9(14) 2_655 3_665 ? C3 C2 C3 106.9(14) 2_655 . ? C3 C2 C3 106.9(14) . 3_665 ? C3 C2 C1 112.0(13) 3_665 . ? C3 C2 C1 112.0(13) 2_655 . ? C3 C2 C1 112.0(13) . . ? H4A C4 H4B 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C4 H4A 109.5 . . ? C3 C4 H4B 109.5 . . ? C3 C4 H4C 109.5 . . ? C5 C3 C2 106.3(17) . . ? C5 C3 C4 107.9(16) . . ? C6 C3 C5 110.6(19) 3_665 . ? C6 C3 C2 104.9(19) 3_665 . ? C6 C3 C4 109.7(18) 3_665 . ? C2 C3 C4 117.4(16) . . ? C22 C20 C21 120.0 . . ? C22 C20 C19 117.5(11) . . ? C21 C20 C19 120.0(12) . . ? C20 C22 H22 120.0 . . ? C20 C22 C23 120.0 . . ? C23 C22 H22 120.0 . . ? C22 C23 H23 120.0 . . ? C24 C23 C22 120.0 . . ? C24 C23 H23 120.0 . . ? C23 C24 H24 120.0 . . ? C23 C24 N2 120.0 . . ? N2 C24 H24 120.0 . . ? C24 N2 C21 120.0 . . ? C24 N2 C32 115.6(13) . . ? C21 N2 C32 119.2(14) . . ? C20 C21 H21 120.0 . . ? N2 C21 C20 120.0 . . ? N2 C21 H21 120.0 . . ? C18 C19 C20 180.0(19) . . ? C19 C18 C9 164.7(18) . . ? N2 C32 H32A 112.4 . . ? N2 C32 H32B 112.4 . . ? H32A C32 H32B 109.9 . . ? C29 C32 N2 96.9(16) . . ? C29 C32 H32A 112.4 . . ? C29 C32 H32B 112.4 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C15 C13 C14 120.0 . . ? C15 C13 C12 122.7(14) . . ? C14 C13 C12 113.1(13) . . ? C13 C15 H15 120.0 . . ? C13 C15 C16 120.0 . . ? C16 C15 H15 120.0 . . ? C15 C16 H16 120.0 . . ? C17 C16 C15 120.0 . . ? C17 C16 H16 120.0 . . ? C16 C17 H17 120.0 . . ? C16 C17 N1 120.0 . . ? N1 C17 H17 120.0 . . ? C17 N1 C25 119.1(13) . . ? C14 N1 C17 120.0 . . ? C14 N1 C25 120.6(13) . . ? C13 C14 H14 120.0 . . ? N1 C14 C13 120.0 . . ? N1 C14 H14 120.0 . . ? C11 C12 C13 180.0(4) . . ? C12 C11 C8 171.9(18) . . ? N1 C25 H25A 108.2 . . ? N1 C25 H25B 108.2 . . ? H25A C25 H25B 107.4 . . ? C26 C25 N1 116.2(13) . . ? C26 C25 H25A 108.2 . . ? C26 C25 H25B 108.2 . . ? C27 C26 C25 120.6(11) . . ? C27 C26 C31 120.0 . . ? C31 C26 C25 119.4(11) . . ? C26 C27 H27 120.0 . . ? C28 C27 C26 120.0 . . ? C28 C27 H27 120.0 . . ? C27 C28 H28 120.0 . . ? C27 C28 C29 120.0 . . ? C29 C28 H28 120.0 . . ? C28 C29 C32 119.9(15) . . ? C28 C29 C30 120.0 . . ? C30 C29 C32 120.1(15) . . ? C29 C30 H30 120.0 . . ? C31 C30 C29 120.0 . . ? C31 C30 H30 120.0 . . ? C26 C31 H31 120.0 . . ? C30 C31 C26 120.0 . . ? C30 C31 H31 120.0 . . ? O5A C5A O6A 134(5) . . ? O5A C5A C6A 113(4) . . ? O6A C5A C6A 113(4) . . ? F7A C6A F8A 108(3) . . ? F7A C6A C5A 111(3) . . ? F9A C6A F7A 107(3) . . ? F9A C6A F8A 109(3) . . ? F9A C6A C5A 111(3) . . ? F8A C6A C5A 110(3) . . ? O1A C1A C2A 119(3) . . ? O2A C1A O1A 135(4) . . ? O2A C1A C2A 106(3) . . ? F1A C2A C1A 110(2) . . ? F2A C2A F1A 108(2) . . ? F2A C2A C1A 112(2) . . ? F3A C2A F1A 104(3) . . ? F3A C2A F2A 110(3) . . ? F3A C2A C1A 112(3) . . ? O3A C3A C4A 111(3) . . ? O4A C3A O3A 114(3) . . ? O4A C3A C4A 135(3) . . ? F5A C4A F6A 100(3) . . ? F5A C4A F4A 103(3) . . ? F5A C4A C3A 116(3) . . ? F6A C4A C3A 115(2) . . ? F4A C4A F6A 105(3) . . ? F4A C4A C3A 116(2) . . ? O8A C7A C8A 122(4) . . ? O7A C7A O8A 129(4) . . ? O7A C7A C8A 109(3) . . ? F12A C8A F10A 107(3) . . ? F12A C8A C7A 111(3) . . ? F11A C8A F12A 108(3) . . ? F11A C8A F10A 108(3) . . ? F11A C8A C7A 114(3) . . ? F10A C8A C7A 108(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C5 C10 1.3900 . ? C5 C6 1.3900 . ? C5 C3 1.51(2) . ? C10 H10 0.9500 . ? C10 C9 1.3900 . ? C9 C8 1.3900 . ? C9 C18 1.37(3) . ? C8 C7 1.3900 . ? C8 C11 1.50(3) . ? C7 H7 0.9500 . ? C7 C6 1.3900 . ? C6 C3 1.50(3) 2_655 ? C2 C3 1.54(2) 3_665 ? C2 C3 1.54(2) 2_655 ? C2 C3 1.54(2) . ? C2 C1 1.61(5) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C4 C3 1.66(3) . ? C20 C22 1.3900 . ? C20 C21 1.3900 . ? C20 C19 1.67(3) . ? C22 H22 0.9500 . ? C22 C23 1.3900 . ? C23 H23 0.9500 . ? C23 C24 1.3900 . ? C24 H24 0.9500 . ? C24 N2 1.3900 . ? N2 C21 1.3900 . ? N2 C32 1.500(18) . ? C21 H21 0.9500 . ? C19 C18 1.09(2) . ? C32 H32A 0.9900 . ? C32 H32B 0.9900 . ? C32 C29 1.460(17) . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? C13 C15 1.3900 . ? C13 C14 1.3900 . ? C13 C12 1.49(3) . ? C15 H15 0.9500 . ? C15 C16 1.3900 . ? C16 H16 0.9500 . ? C16 C17 1.3900 . ? C17 H17 0.9500 . ? C17 N1 1.3900 . ? N1 C14 1.3900 . ? N1 C25 1.505(15) . ? C14 H14 0.9500 . ? C12 C11 1.09(2) . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C25 C26 1.496(17) . ? C26 C27 1.3900 . ? C26 C31 1.3900 . ? C27 H27 0.9500 . ? C27 C28 1.3900 . ? C28 H28 0.9500 . ? C28 C29 1.3900 . ? C29 C30 1.3900 . ? C30 H30 0.9500 . ? C30 C31 1.3900 . ? C31 H31 0.9500 . ? F7A C6A 1.331(19) . ? F9A C6A 1.326(19) . ? F8A C6A 1.332(19) . ? O5A C5A 1.24(2) . ? O6A C5A 1.24(2) . ? C5A C6A 1.56(3) . ? F1A C2A 1.352(19) . ? F2A C2A 1.350(19) . ? F3A C2A 1.331(19) . ? O1A C1A 1.27(2) . ? O2A C1A 1.27(2) . ? C1A C2A 1.54(3) . ? F5A C4A 1.345(19) . ? F6A C4A 1.352(19) . ? F4A C4A 1.349(19) . ? O3A C3A 1.26(2) . ? O4A C3A 1.26(2) . ? C3A C4A 1.54(2) . ? F12A C8A 1.341(19) . ? F11A C8A 1.335(19) . ? F10A C8A 1.345(19) . ? O8A C7A 1.26(2) . ? O7A C7A 1.26(2) . ? C7A C8A 1.55(3) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C10 C9 C8 0.0 . . . . ? C5 C10 C9 C18 -172.9(16) . . . . ? C10 C5 C6 C7 0.0 . . . . ? C10 C5 C6 C3 178.9(13) . . . 2_655 ? C10 C5 C3 C6 -66.6(19) . . . 3_665 ? C10 C5 C3 C2 -179.9(13) . . . . ? C10 C5 C3 C4 53.4(18) . . . . ? C10 C9 C8 C7 0.0 . . . . ? C10 C9 C8 C11 179.8(16) . . . . ? C10 C9 C18 C19 -21(7) . . . . ? C9 C8 C7 C6 0.0 . . . . ? C8 C9 C18 C19 166(6) . . . . ? C8 C7 C6 C5 0.0 . . . . ? C8 C7 C6 C3 -178.7(15) . . . 2_655 ? C6 C5 C10 C9 0.0 . . . . ? C6 C5 C3 C6 112.6(15) . . . 3_665 ? C6 C5 C3 C2 -0.7(19) . . . . ? C6 C5 C3 C4 -127.4(13) . . . . ? C3 C5 C10 C9 179.1(15) . . . . ? C3 C5 C6 C7 -179.3(12) . . . . ? C3 C5 C6 C3 -0.3(16) . . . 2_655 ? C3 C2 C3 C5 1(2) 2_655 . . . ? C3 C2 C3 C5 115.6(11) 3_665 . . . ? C3 C2 C3 C6 -115.7(15) 2_655 . . 3_665 ? C3 C2 C3 C6 -2(2) 3_665 . . 3_665 ? C3 C2 C3 C4 122(3) 2_655 . . . ? C3 C2 C3 C4 -124(3) 3_665 . . . ? C20 C22 C23 C24 0.0 . . . . ? C22 C20 C21 N2 0.0 . . . . ? C22 C23 C24 N2 0.0 . . . . ? C23 C24 N2 C21 0.0 . . . . ? C23 C24 N2 C32 -154(3) . . . . ? C24 N2 C21 C20 0.0 . . . . ? C24 N2 C32 C29 -168.4(18) . . . . ? N2 C32 C29 C28 -114.5(18) . . . . ? N2 C32 C29 C30 67(2) . . . . ? C21 C20 C22 C23 0.0 . . . . ? C21 N2 C32 C29 37(3) . . . . ? C19 C20 C22 C23 -162(2) . . . . ? C19 C20 C21 N2 162(2) . . . . ? C18 C9 C8 C7 173.4(15) . . . . ? C18 C9 C8 C11 -7(2) . . . . ? C32 N2 C21 C20 154(3) . . . . ? C32 C29 C30 C31 178.3(17) . . . . ? C1 C2 C3 C5 -121.5(10) . . . . ? C1 C2 C3 C6 121.3(14) . . . 3_665 ? C1 C2 C3 C4 -1(2) . . . . ? C13 C15 C16 C17 0.0 . . . . ? C15 C13 C14 N1 0.0 . . . . ? C15 C16 C17 N1 0.0 . . . . ? C16 C17 N1 C14 0.0 . . . . ? C16 C17 N1 C25 -174(2) . . . . ? C17 N1 C14 C13 0.0 . . . . ? C17 N1 C25 C26 131.9(16) . . . . ? N1 C25 C26 C27 111.5(18) . . . . ? N1 C25 C26 C31 -67.8(18) . . . . ? C14 C13 C15 C16 0.0 . . . . ? C14 N1 C25 C26 -42(3) . . . . ? C12 C13 C15 C16 155.3(19) . . . . ? C12 C13 C14 N1 -157.5(18) . . . . ? C11 C8 C7 C6 -179.8(16) . . . . ? C25 N1 C14 C13 174(2) . . . . ? C25 C26 C27 C28 -179.4(6) . . . . ? C25 C26 C31 C30 179.4(6) . . . . ? C26 C27 C28 C29 0.0 . . . . ? C27 C26 C31 C30 0.0 . . . . ? C27 C28 C29 C32 -178.3(17) . . . . ? C27 C28 C29 C30 0.0 . . . . ? C28 C29 C30 C31 0.0 . . . . ? C29 C30 C31 C26 0.0 . . . . ? C31 C26 C27 C28 0.0 . . . . ? O5A C5A C6A F7A 66(5) . . . . ? O5A C5A C6A F9A -175(5) . . . . ? O5A C5A C6A F8A -54(5) . . . . ? O6A C5A C6A F7A -114(5) . . . . ? O6A C5A C6A F9A 5(5) . . . . ? O6A C5A C6A F8A 126(5) . . . . ? O1A C1A C2A F1A -91(3) . . . . ? O1A C1A C2A F2A 30(4) . . . . ? O1A C1A C2A F3A 154(4) . . . . ? O2A C1A C2A F1A 86(3) . . . . ? O2A C1A C2A F2A -154(3) . . . . ? O2A C1A C2A F3A -29(3) . . . . ? O3A C3A C4A F5A -127(4) . . . . ? O3A C3A C4A F6A -11(4) . . . . ? O3A C3A C4A F4A 112(4) . . . . ? O4A C3A C4A F5A 53(5) . . . . ? O4A C3A C4A F6A 169(4) . . . . ? O4A C3A C4A F4A -68(5) . . . . ? O8A C7A C8A F12A -48(5) . . . . ? O8A C7A C8A F11A 74(5) . . . . ? O8A C7A C8A F10A -166(5) . . . . ? O7A C7A C8A F12A 130(5) . . . . ? O7A C7A C8A F11A -107(5) . . . . ? O7A C7A C8A F10A 13(5) . . . . ? loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.539(18) 2 0.461(18) loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.599 -0.585 -0.549 3458.4 147.6 '6 Acetonitrile'