#------------------------------------------------------------------------------ #$Date: 2024-05-26 01:14:09 +0300 (Sun, 26 May 2024) $ #$Revision: 292038 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571709.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571709 loop_ _publ_author_name 'Prajapati, Bibek' 'Kwenda, Tendai' 'Lis, Tadeusz' 'Chmielewski, Piotr Jan' 'Gomez Garcia, Carlos J.' 'Majewski, Marcin A.' 'St\;epie\'n, Marcin' _publ_section_title ; Difluorenoheteroles: Topological Control of \p Conjugation in Diradicaloids and Mixed-Valence Radical Ions ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC02459A _journal_year 2024 _chemical_formula_moiety 'C60 H67 N' _chemical_formula_sum 'C60 H67 N' _chemical_formula_weight 802.207 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _symmetry_Int_Tables_number 14 _audit_creation_date 2023-06-28 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-10-22 deposited with the CCDC. 2024-05-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 93.27(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.742(2) _cell_length_b 15.560(4) _cell_length_c 30.552(12) _cell_measurement_reflns_used 7900 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 100 _cell_measurement_theta_min 2.8 _cell_volume 4624(2) _computing_cell_refinement 'CrysAlisPro 1.171.42.72a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.72a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.72a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _diffrn_ambient_temperature 100.15 _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type 'HyPix-Arc 150' _diffrn_measured_fraction_theta_full 0.9979 _diffrn_measured_fraction_theta_max 0.9542 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix-Arc 150' _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0940 _diffrn_reflns_av_unetI/netI 0.0914 _diffrn_reflns_Laue_measured_fraction_full 0.9979 _diffrn_reflns_Laue_measured_fraction_max 0.9542 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_limit_l_min -37 _diffrn_reflns_number 32984 _diffrn_reflns_point_group_measured_fraction_full 0.9979 _diffrn_reflns_point_group_measured_fraction_max 0.9542 _diffrn_reflns_theta_full 67.0000 _diffrn_reflns_theta_max 74.48 _diffrn_reflns_theta_min 2.90 _exptl_absorpt_coefficient_mu 0.485 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.775 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.72a (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour green _exptl_crystal_colour_primary green _exptl_crystal_density_diffrn 1.152 _exptl_crystal_description needle _exptl_crystal_F_000 1740.737 _exptl_crystal_size_max 0.19 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.02 _refine_diff_density_max 0.5040 _refine_diff_density_min -0.4800 _refine_diff_density_rms 0.1088 _refine_ls_d_res_high 0.8001 _refine_ls_d_res_low 15.2511 _refine_ls_goodness_of_fit_ref 1.0200 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 105 _refine_ls_number_parameters 563 _refine_ls_number_reflns 9022 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.0200 _refine_ls_R_factor_all 0.1197 _refine_ls_R_factor_gt 0.0633 _refine_ls_shift/su_max -0.0005 _refine_ls_shift/su_mean 0.0001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1034P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1556 _refine_ls_wR_factor_ref 0.1911 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 11 _reflns_limit_h_min -12 _reflns_limit_k_max 19 _reflns_limit_k_min 0 _reflns_limit_l_max 37 _reflns_limit_l_min -10 _reflns_number_gt 5296 _reflns_number_total 9022 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL tw043 in P2(1)/n CELL 1.54184 9.742 15.56 30.552 90 93.27 90 ZERR 4 0.002 0.004 0.012 0 0.04 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N UNIT 240 268 4 L.S. 10 PLAN 20 SIZE 0.02 0.03 0.19 TEMP -173 CONF acta 134 BOND $H fmap 2 MORE -1 WGHT 0.1034 FVAR 1.011122 REM REM REM N1 3 1.04535 0.41075 0.56274 11.00000 0.01909 0.02709 0.02372 = -0.00149 0.00086 -0.00475 C1 1 1.18922 0.43914 0.56481 11.00000 0.01513 0.03126 0.03166 = -0.00069 0.00236 -0.00993 AFIX 23 H1a 2 1.21031 0.46370 0.53606 11.00000 -1.20000 H1b 2 1.20134 0.48529 0.58699 11.00000 -1.20000 AFIX 0 C2 1 1.29098 0.36714 0.57636 11.00000 0.02257 0.03099 0.03365 = -0.00101 0.00244 -0.00239 AFIX 23 H2a 2 1.38517 0.39125 0.57759 11.00000 -1.20000 H2b 2 1.27352 0.34540 0.60598 11.00000 -1.20000 AFIX 0 C3 1 1.28463 0.29197 0.54450 11.00000 0.03288 0.03368 0.03589 = -0.00369 -0.00270 -0.00001 AFIX 23 H3a 2 1.19269 0.26491 0.54470 11.00000 -1.20000 H3b 2 1.29672 0.31370 0.51451 11.00000 -1.20000 AFIX 0 C4 1 1.39381 0.22458 0.55578 11.00000 0.02508 0.03660 0.04245 = -0.00481 0.00247 0.00058 AFIX 137 H4a 2 1.38556 0.17765 0.53440 11.00000 -1.50000 H4b 2 1.48517 0.25071 0.55502 11.00000 -1.50000 H4c 2 1.38113 0.20191 0.58521 11.00000 -1.50000 AFIX 0 C1A 1 0.97118 0.39396 0.59882 11.00000 0.01848 0.02046 0.02863 = -0.00084 0.00154 0.00025 C2A 1 0.84175 0.35687 0.58453 11.00000 0.02235 0.02066 0.02535 = 0.00039 0.00109 -0.00100 C3A 1 0.74977 0.33073 0.61496 11.00000 0.02002 0.02380 0.02582 = -0.00068 0.00160 -0.00247 AFIX 43 H3Aa 2 0.66374 0.30594 0.60582 11.00000 -1.20000 AFIX 0 C4A 1 0.78760 0.34200 0.65959 11.00000 0.01925 0.01793 0.02804 = 0.00052 0.00022 0.00009 C5A 1 0.72015 0.31535 0.69718 11.00000 0.02176 0.02007 0.02744 = -0.00103 -0.00056 0.00073 C6A 1 0.80880 0.33656 0.73540 11.00000 0.01489 0.01936 0.02747 = -0.00212 0.00262 0.00025 C7A 1 0.79830 0.31850 0.77975 11.00000 0.02093 0.02495 0.03160 = 0.00031 0.00276 -0.00018 AFIX 43 H7A 2 0.72033 0.28900 0.78951 11.00000 -1.20000 AFIX 0 C8A 1 0.90420 0.34444 0.80971 11.00000 0.02891 0.02883 0.02473 = 0.00072 -0.00104 0.00089 AFIX 43 H8A 2 0.89836 0.33216 0.84000 11.00000 -1.20000 AFIX 0 C9A 1 1.01929 0.38859 0.79528 11.00000 0.01935 0.02608 0.03158 = -0.00309 -0.00271 0.00001 AFIX 43 H9A 2 1.09047 0.40589 0.81596 11.00000 -1.20000 AFIX 0 C10A 1 1.02988 0.40704 0.75140 11.00000 0.02104 0.02210 0.03112 = -0.00377 0.00031 -0.00136 AFIX 43 H10A 2 1.10696 0.43805 0.74206 11.00000 -1.20000 AFIX 0 C11A 1 0.92751 0.38013 0.72095 11.00000 0.02138 0.01862 0.02611 = -0.00244 0.00169 0.00108 C12A 1 0.91616 0.38232 0.67317 11.00000 0.02189 0.01720 0.02427 = -0.00145 0.00122 0.00112 C13A 1 1.00830 0.40835 0.64330 11.00000 0.01902 0.02363 0.02864 = 0.00027 -0.00033 -0.00010 AFIX 43 H13A 2 1.09307 0.43483 0.65236 11.00000 -1.20000 AFIX 0 C21A 1 0.58525 0.27146 0.69621 11.00000 0.01843 0.02308 0.02455 = -0.00025 0.00150 -0.00022 C22A 1 0.57491 0.18370 0.68484 11.00000 0.01683 0.02349 0.03091 = 0.00012 0.00403 0.00158 C23A 1 0.44589 0.14464 0.68157 11.00000 0.02438 0.01741 0.03262 = -0.00234 0.00154 0.00081 AFIX 43 H23A 2 0.44002 0.08522 0.67458 11.00000 -1.20000 AFIX 0 C24A 1 0.32477 0.18995 0.68823 11.00000 0.01742 0.02578 0.02915 = 0.00219 0.00204 -0.00080 C25A 1 0.33763 0.27607 0.69991 11.00000 0.02055 0.02264 0.03019 = 0.00004 0.00196 -0.00004 AFIX 43 H25A 2 0.25693 0.30790 0.70507 11.00000 -1.20000 AFIX 0 C26A 1 0.46494 0.31748 0.70432 11.00000 0.01735 0.02104 0.02584 = -0.00058 0.00168 -0.00047 C27A 1 0.70259 0.13007 0.67860 11.00000 0.01992 0.02141 0.04237 = -0.00219 0.00268 0.00164 AFIX 13 H27A 2 0.78169 0.17057 0.67661 11.00000 -1.20000 AFIX 0 C28A 1 0.18680 0.14569 0.68310 11.00000 0.02207 0.01912 0.04342 = -0.00168 0.00147 -0.00128 AFIX 13 H28A 2 0.20407 0.08234 0.68340 11.00000 -1.20000 AFIX 0 C29A 1 0.47182 0.41060 0.72000 11.00000 0.02145 0.02071 0.03226 = -0.00284 -0.00041 -0.00267 AFIX 13 H29A 2 0.56871 0.43084 0.71807 11.00000 -1.20000 AFIX 0 C30A 1 0.73333 0.07242 0.71867 11.00000 0.02469 0.02836 0.05904 = 0.00624 -0.00365 -0.00017 AFIX 137 H30a 2 0.65312 0.03634 0.72346 11.00000 -1.50000 H30b 2 0.81267 0.03579 0.71357 11.00000 -1.50000 H30c 2 0.75385 0.10830 0.74458 11.00000 -1.50000 AFIX 0 C31A 1 0.69245 0.07720 0.63636 11.00000 0.03339 0.03942 0.05233 = -0.01441 0.00545 0.00295 AFIX 137 H31a 2 0.77973 0.04738 0.63282 11.00000 -1.50000 H31b 2 0.61836 0.03489 0.63790 11.00000 -1.50000 H31c 2 0.67276 0.11542 0.61129 11.00000 -1.50000 AFIX 0 C32A 1 0.11146 0.16768 0.63915 11.00000 0.02721 0.04026 0.04277 = -0.00396 -0.00303 -0.00560 AFIX 137 H32a 2 0.02620 0.13429 0.63582 11.00000 -1.50000 H32b 2 0.08962 0.22916 0.63831 11.00000 -1.50000 H32c 2 0.17035 0.15365 0.61519 11.00000 -1.50000 AFIX 0 C33A 1 0.09483 0.16572 0.72057 11.00000 0.02292 0.02991 0.04769 = 0.00039 0.00442 -0.00305 AFIX 137 H33a 2 0.06888 0.22656 0.71948 11.00000 -1.50000 H33b 2 0.01185 0.13010 0.71767 11.00000 -1.50000 H33c 2 0.14470 0.15336 0.74863 11.00000 -1.50000 AFIX 0 C34A 1 0.37893 0.46978 0.69120 11.00000 0.02648 0.02228 0.03589 = 0.00032 -0.00258 -0.00262 AFIX 137 H34a 2 0.40230 0.46419 0.66056 11.00000 -1.50000 H34b 2 0.28260 0.45351 0.69390 11.00000 -1.50000 H34c 2 0.39250 0.52946 0.70074 11.00000 -1.50000 AFIX 0 C35A 1 0.43627 0.41581 0.76817 11.00000 0.02652 0.02337 0.03774 = -0.00751 -0.00268 -0.00099 AFIX 137 H35a 2 0.34298 0.39390 0.77119 11.00000 -1.50000 H35b 2 0.50177 0.38111 0.78615 11.00000 -1.50000 H35c 2 0.44135 0.47576 0.77797 11.00000 -1.50000 AFIX 0 C1B 1 0.97006 0.38595 0.52503 11.00000 0.01730 0.02174 0.02866 = -0.00081 -0.00191 -0.00279 C2B 1 0.84102 0.35195 0.53722 11.00000 0.01968 0.02368 0.02513 = 0.00137 0.00259 -0.00273 C3B 1 0.74746 0.32001 0.50549 11.00000 0.01837 0.02400 0.02762 = 0.00193 0.00063 -0.00202 AFIX 43 H3Ba 2 0.66158 0.29744 0.51327 11.00000 -1.20000 AFIX 0 C4B 1 0.78236 0.32171 0.46158 11.00000 0.01632 0.02139 0.02918 = 0.00083 0.00048 -0.00196 C5B 1 0.71096 0.28992 0.42316 11.00000 0.01857 0.02108 0.02913 = 0.00068 0.00047 -0.00155 C6B 1 0.79274 0.30823 0.38652 11.00000 0.02129 0.02048 0.02685 = -0.00096 -0.00150 0.00145 C7B 1 0.77231 0.28983 0.34185 11.00000 0.02342 0.02959 0.02566 = 0.00034 -0.00194 -0.00234 AFIX 43 H7B 2 0.69284 0.25944 0.33106 11.00000 -1.20000 AFIX 0 C8B 1 0.87085 0.31694 0.31332 11.00000 0.02821 0.03279 0.02797 = -0.00187 0.00445 0.00226 AFIX 43 H8B 2 0.85831 0.30437 0.28292 11.00000 -1.20000 AFIX 0 C9B 1 0.98638 0.36181 0.32870 11.00000 0.02470 0.02981 0.03145 = 0.00026 0.00564 0.00036 AFIX 43 H9B 2 1.05117 0.38048 0.30865 11.00000 -1.20000 AFIX 0 C10B 1 1.00918 0.38008 0.37338 11.00000 0.02345 0.02399 0.02720 = 0.00315 0.00323 0.00085 AFIX 43 H10B 2 1.08822 0.41148 0.38365 11.00000 -1.20000 AFIX 0 C11B 1 0.91487 0.35172 0.40245 11.00000 0.01953 0.01945 0.02908 = 0.00131 0.00301 0.00253 C12B 1 0.91125 0.35881 0.44970 11.00000 0.02100 0.01894 0.02603 = 0.00017 0.00049 0.00010 C13B 1 1.00575 0.39061 0.48126 11.00000 0.01990 0.02273 0.02858 = 0.00068 0.00393 -0.00217 AFIX 43 H13B 2 1.09086 0.41449 0.47359 11.00000 -1.20000 AFIX 0 C21B 1 0.57580 0.24529 0.42275 11.00000 0.02031 0.02498 0.02194 = -0.00097 0.00176 -0.00207 C22B 1 0.57108 0.15725 0.43403 11.00000 0.02047 0.02716 0.02477 = 0.00042 -0.00011 -0.00231 C23B 1 0.44248 0.11738 0.43504 11.00000 0.02000 0.02104 0.03383 = 0.00283 0.00101 -0.00447 AFIX 43 H23B 2 0.43888 0.05783 0.44175 11.00000 -1.20000 AFIX 0 C24B 1 0.32015 0.16150 0.42663 11.00000 0.01947 0.02560 0.02496 = -0.00097 0.00357 -0.00164 C25B 1 0.32715 0.24815 0.41597 11.00000 0.01864 0.02426 0.03449 = -0.00199 0.00104 0.00014 AFIX 43 H25B 2 0.24406 0.27927 0.41046 11.00000 -1.20000 AFIX 0 C26B 1 0.45308 0.29127 0.41309 11.00000 0.02045 0.02382 0.02880 = -0.00043 0.00223 -0.00108 C27B 1 0.70104 0.10608 0.44481 11.00000 0.02338 0.02802 0.03740 = 0.00390 -0.00103 0.00167 AFIX 13 H27B 2 0.78090 0.14558 0.44173 11.00000 -1.20000 AFIX 0 C28B 1 0.18304 0.11507 0.42788 11.00000 0.02221 0.02121 0.03180 = -0.00007 -0.00143 -0.00485 AFIX 13 H28B 2 0.20343 0.05229 0.43083 11.00000 -1.20000 AFIX 0 C29B 1 0.45420 0.38484 0.39953 11.00000 0.02503 0.02435 0.04319 = 0.00484 0.00153 0.00099 AFIX 13 H29B 2 0.55245 0.40208 0.39734 11.00000 -1.20000 AFIX 0 C30B 1 0.71717 0.03130 0.41335 11.00000 0.03207 0.03864 0.05953 = -0.00810 -0.00612 0.00898 AFIX 137 H30d 2 0.80158 -0.00033 0.42176 11.00000 -1.50000 H30e 2 0.63794 -0.00726 0.41459 11.00000 -1.50000 H30f 2 0.72236 0.05337 0.38344 11.00000 -1.50000 AFIX 0 C31B 1 0.70618 0.07482 0.49225 11.00000 0.03200 0.05738 0.04660 = 0.01963 -0.00176 0.00841 AFIX 137 H31d 2 0.63034 0.03465 0.49611 11.00000 -1.50000 H31e 2 0.79393 0.04569 0.49918 11.00000 -1.50000 H31f 2 0.69755 0.12406 0.51190 11.00000 -1.50000 AFIX 0 C32B 1 0.09268 0.12693 0.38581 11.00000 0.02366 0.03064 0.03634 = 0.00357 -0.00242 -0.00370 AFIX 137 H32d 2 0.01199 0.08946 0.38654 11.00000 -1.50000 H32e 2 0.06276 0.18696 0.38339 11.00000 -1.50000 H32f 2 0.14530 0.11199 0.36049 11.00000 -1.50000 AFIX 0 C33B 1 0.10479 0.14158 0.46791 11.00000 0.02596 0.03010 0.04003 = -0.00275 0.00301 -0.00192 AFIX 137 H33d 2 0.08268 0.20296 0.46605 11.00000 -1.50000 H33e 2 0.01957 0.10824 0.46854 11.00000 -1.50000 H33f 2 0.16212 0.13047 0.49471 11.00000 -1.50000 AFIX 0 C34B 1 0.38204 0.39716 0.35418 11.00000 0.02881 0.03966 0.04955 = 0.01656 0.00243 -0.00044 AFIX 137 H34d 2 0.43388 0.36733 0.33220 11.00000 -1.50000 H34e 2 0.28883 0.37345 0.35409 11.00000 -1.50000 H34f 2 0.37718 0.45860 0.34720 11.00000 -1.50000 AFIX 0 C35B 1 0.39344 0.44256 0.43405 11.00000 0.03453 0.02605 0.05873 = 0.00010 0.00614 -0.00028 AFIX 137 H35d 2 0.29674 0.42743 0.43696 11.00000 -1.50000 H35e 2 0.44471 0.43443 0.46228 11.00000 -1.50000 H35f 2 0.39995 0.50278 0.42501 11.00000 -1.50000 AFIX 0 HKLF 4 END Q1 1 1.055556 0.351852 0.564815 11 0.05 0.5 Q2 1 0.388889 0.407407 0.509259 11 0.05 0.5 Q3 1 0.25 0.12963 0.722222 11 0.05 0.42 Q4 1 0.833333 0.314815 0.388889 11 0.05 0.41 Q5 1 0.972222 0.314815 0.574074 11 0.05 0.39 Q6 1 1.166667 0.37037 0.740741 11 0.05 0.38 Q7 1 0.277778 0.407407 0.453704 11 0.05 0.36 Q8 1 1.166667 0.444444 0.75 11 0.05 0.36 REM The information below was added by Olex2. REM REM R1 = 0.0633 for 5296 Fo > 4sig(Fo) and 0.1197 for all 9022 data REM 563 parameters refined using 0 restraints REM Highest difference peak 0.5040, deepest hole -0.4800 REM Mean Shift 0.0001, Max Shift -0.0005. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1197 REM R1_gt = 0.0633 REM wR_ref = 0.1911 REM GOOF = 1.0200 REM Shift_max = -0.0005 REM Shift_mean = 0.0001 REM Reflections_all = 9022 REM Reflections_gt = 5296 REM Parameters = 563 REM Hole = -0.4800 REM Peak = 0.5040 REM Flack = n/a ; _cod_data_source_file d4sc02459a3.cif _cod_data_source_block tw043a _cod_database_code 1571709 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C27A(H27A), C28A(H28A), C29A(H29A), C27B(H27B), C28B(H28B), C29B(H29B) 2.b Secondary CH2 refined with riding coordinates: C1(H1a,H1b), C2(H2a,H2b), C3(H3a,H3b) 2.c Aromatic/amide H refined with riding coordinates: C3A(H3Aa), C7A(H7A), C8A(H8A), C9A(H9A), C10A(H10A), C13A(H13A), C23A(H23A), C25A(H25A), C3B(H3Ba), C7B(H7B), C8B(H8B), C9B(H9B), C10B(H10B), C13B(H13B), C23B(H23B), C25B(H25B) 2.d Idealised Me refined as rotating group: C4(H4a,H4b,H4c), C30A(H30a,H30b,H30c), C31A(H31a,H31b,H31c), C32A(H32a,H32b, H32c), C33A(H33a,H33b,H33c), C34A(H34a,H34b,H34c), C35A(H35a,H35b,H35c), C30B(H30d,H30e,H30f), C31B(H31d,H31e,H31f), C32B(H32d,H32e,H32f), C33B(H33d, H33e,H33f), C34B(H34d,H34e,H34f), C35B(H35d,H35e,H35f) ; _iucr_refine_fcf_details ; data_tw043a_CCDC1 _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x+1/2,y+1/2,-z+1/2 3 -x,-y,-z 4 x-1/2,-y-1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2ybc (x-z,y,z)' _symmetry_space_group_name_H-M 'P 1 21/n 1' _symmetry_space_group_name_Hall '-P 2ybc (x-z,y,z)' _symmetry_Int_Tables_number 14 _cell_length_a 9.742(2) _cell_length_b 15.560(4) _cell_length_c 30.552(12) _cell_angle_alpha 90 _cell_angle_beta 93.27(4) _cell_angle_gamma 90 _cell_volume 4624(2) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -12 0 0 18.735 -40.408 60.070 33.944 o -12 0 2 7.093 5.613 66.368 27.817 o -12 0 4 0.047 -77.308 67.019 27.282 o -12 0 6 25.413 -24.358 65.522 28.523 o -12 1 0 34.456 -31.196 58.523 35.720 o -12 1 1 9.953 -54.095 60.264 33.737 o -12 1 2 0.344 -13.217 64.480 29.473 o -12 1 3 73.728 60.811 64.352 29.227 o -12 1 4 76.165 63.733 66.576 27.305 o -12 1 5 246.390 -17.653 67.507 25.289 o -12 1 6 29.891 53.368 60.953 32.848 o -12 2 1 68.771 48.031 59.661 34.035 o -12 2 2 0.449 -7.651 59.656 34.433 o -12 2 3 0.333 54.002 62.300 31.543 o -12 2 4 1.525 42.701 58.508 35.771 o -12 2 5 85.549 -5.996 61.144 32.475 o -11 0 -9 932.529 1030.060 73.839 7.953 o -11 0 -7 90.705 94.624 36.395 86.595 o -11 0 -5 385.237 492.469 38.541 36.252 o -11 0 -3 366.804 477.175 44.174 33.183 o -11 0 -1 0.069 -19.780 83.994 17.369 o -11 0 1 1200.870 951.591 92.637 5.585 o -11 0 3 53.474 19.265 89.384 15.302 o -11 0 5 166.561 1.531 90.576 14.698 o -11 0 7 9.451 19.788 91.630 14.592 o -11 0 9 65.494 -48.768 88.707 15.532 o -11 0 11 21.251 -145.350 87.597 15.965 o -11 0 13 8.851 0.585 78.416 19.927 o -11 1 -10 11.367 0.881 22.405 243.799 o -11 1 -9 10.930 -8.204 23.106 229.289 o -11 1 -8 36.938 54.418 21.288 259.218 o -11 1 -7 13.709 25.322 22.055 250.234 o -11 1 -6 6.927 -2.274 30.117 135.068 o -11 1 -5 0.004 -14.513 31.048 127.118 o -11 1 -4 9.123 50.322 27.729 158.219 o -11 1 -3 282.441 297.104 95.577 12.233 o -11 1 -2 104.962 108.726 68.326 25.588 o -11 1 -1 542.701 121.466 94.652 11.464 o -11 1 0 125.996 108.927 48.564 48.759 o -11 1 1 3.064 -53.467 67.969 26.525 o -11 1 2 5.623 37.287 68.228 26.308 o -11 1 3 745.905 636.419 95.400 8.462 o -11 1 4 174.147 65.501 67.765 25.553 o -11 1 5 0.039 38.232 68.678 25.971 o -11 1 6 195.500 -10.197 66.596 26.543 o -11 1 7 219.096 43.295 64.623 27.528 o -11 1 8 9.872 68.397 80.142 19.052 o -11 1 9 125.924 59.885 63.083 29.925 o -11 1 10 0.848 13.861 95.861 13.335 o -11 1 11 134.496 -39.712 60.986 32.203 o -11 1 12 1.667 15.058 80.289 19.008 o -11 1 13 320.494 44.420 76.032 19.331 o -11 1 14 10.129 -31.720 68.752 25.922 o -11 2 -10 12.164 12.894 24.561 202.592 o -11 2 -9 1.096 5.449 26.459 175.017 o -11 2 -8 10.116 15.642 28.603 149.504 o -11 2 -7 36.299 52.770 29.678 136.242 o -11 2 -6 8.169 5.904 30.297 133.415 o -11 2 -5 13.594 42.114 38.014 84.464 o -11 2 -4 29.933 29.835 30.122 133.649 o -11 2 -3 75.128 56.092 53.480 42.100 o -11 2 -2 3.305 49.114 42.037 69.202 o -11 2 -1 60.093 32.223 42.648 66.365 o -11 2 0 410.303 129.239 67.395 21.828 o -11 2 1 142.323 128.833 64.851 27.795 o -11 2 2 134.063 87.584 141.550 6.070 o -11 2 3 816.987 175.461 134.366 5.584 o -11 2 4 54.434 -65.230 67.662 26.684 o -11 2 5 34.132 -40.366 68.715 25.922 o -11 2 6 7.868 21.802 69.317 25.495 o -11 2 7 5.362 63.633 103.467 11.440 o -11 2 8 84.024 19.019 64.670 29.012 o -11 2 9 245.314 62.270 81.966 17.304 o -11 2 10 2.129 26.886 85.613 16.716 o -11 2 11 36.596 -65.720 74.768 21.895 o -11 2 12 75.194 -36.053 73.073 22.834 o -11 2 13 9.397 -12.790 70.744 24.483 o -11 3 -10 138.888 185.640 36.864 75.922 o -11 3 -9 12.194 22.617 26.161 178.362 o -11 3 -8 2.121 -6.739 27.698 159.726 o -11 3 -7 0.030 133.304 525.989 0.443 o -11 3 -6 504.842 642.466 64.627 16.517 o -11 3 -5 81.244 50.273 121.343 8.292 o -11 3 -4 196.857 156.107 162.461 4.580 o -11 3 -3 1382.090 1534.490 952.169 0.132 o -11 3 -2 163.649 124.806 57.256 34.803 o -11 3 -1 0.552 15.227 40.604 74.312 o -11 3 0 244.879 174.863 75.963 19.466 o -11 3 1 0.037 25.453 41.520 71.050 o -11 3 2 157.608 192.794 87.159 15.505 o -11 3 3 212.687 44.756 101.452 11.610 o -11 3 4 162.132 9.068 64.921 28.191 o -11 3 5 8.775 83.129 65.413 28.558 o -11 3 6 6.808 23.458 65.071 28.929 o -11 3 7 319.916 2.202 66.189 25.159 o -11 3 8 161.824 -56.141 90.094 14.869 o -11 3 9 392.552 23.174 84.201 15.579 o -11 3 10 80.049 -24.458 71.096 24.098 o -11 3 11 91.330 -88.050 70.271 24.618 o -11 3 12 187.797 29.515 66.551 26.501 o -11 4 -10 636.916 628.606 54.408 16.880 o -11 4 -9 126.649 88.138 39.554 71.956 o -11 4 -8 387.041 344.500 47.530 32.717 o -11 4 -7 0.183 6.283 43.421 64.992 o -11 4 -6 168.457 151.260 47.297 48.625 o -11 4 -5 32.100 35.420 39.036 79.798 o -11 4 -4 61.245 66.815 55.367 39.427 o -11 4 -3 47.009 2.179 58.555 35.625 o -11 4 -2 8.910 41.440 40.995 72.735 o -11 4 -1 331.175 408.702 331.049 1.104 o -11 4 0 1140.120 1162.320 749.525 0.213 o -11 4 1 710.373 803.049 515.325 0.451 o -11 4 2 282.515 171.633 124.165 7.629 o -11 4 3 564.736 518.634 75.870 13.642 o -11 4 4 174.158 -44.099 75.842 20.783 o -11 4 5 115.248 40.940 77.898 19.907 o -11 4 6 100.917 40.864 78.584 19.621 o -11 4 7 26.351 -33.781 80.388 18.953 o -11 4 8 13.988 -38.697 78.706 19.779 o -11 4 9 18.111 -16.850 80.430 18.938 o -11 4 10 5.286 148.467 74.281 22.089 o -11 4 11 4.576 -25.395 62.374 31.496 o -11 4 12 117.162 -20.977 60.210 33.204 o -11 5 -10 0.358 46.572 32.192 117.946 o -11 5 -9 48.118 51.282 37.270 86.609 o -11 5 -8 264.912 262.090 42.377 48.230 o -11 5 -7 135.705 127.659 42.773 60.703 o -11 5 -6 491.566 593.986 58.323 19.279 o -11 5 -5 98.136 76.152 45.094 57.757 o -11 5 -4 83.849 87.263 128.314 7.408 o -11 5 -3 197.474 84.823 130.650 7.066 o -11 5 -2 21.996 -9.627 38.197 83.858 o -11 5 -1 266.942 333.753 271.609 1.641 o -11 5 0 16.494 28.776 39.110 79.876 o -11 5 1 12.839 57.485 39.541 77.968 o -11 5 2 207.394 198.594 105.844 10.518 o -11 5 3 856.968 1054.700 70.599 8.697 o -11 5 5 52.057 -10.460 69.356 25.407 o -11 5 6 315.963 161.282 70.127 21.630 o -11 5 7 23.798 -7.196 70.990 24.302 o -11 5 8 306.435 9.715 68.956 23.496 o -11 5 9 669.015 607.120 71.894 12.681 o -11 5 10 267.553 264.445 66.523 23.635 o -11 5 11 15.101 38.176 54.308 41.470 o -11 6 -8 477.762 371.883 41.999 31.771 o -11 6 -7 66.858 18.271 37.068 87.437 o -11 6 -6 444.725 431.141 47.489 28.320 o -11 6 -5 109.893 88.761 40.014 71.483 o -11 6 -4 0.203 0.639 47.184 55.041 o -11 6 -3 339.099 328.473 212.151 2.652 o -11 6 -2 623.487 577.676 425.160 0.663 o -11 6 -1 14.909 11.395 33.674 107.876 o -11 6 0 505.894 466.522 315.107 1.203 o -11 6 1 5.128 -24.422 35.258 98.566 o -11 6 2 56.848 -73.040 59.839 34.076 o -11 6 3 224.129 -36.705 60.669 31.265 o -11 6 4 71.791 -13.722 59.735 34.107 o -11 6 5 117.847 -35.138 59.594 33.875 o -11 6 6 1.772 -54.056 59.978 34.064 o -11 6 7 217.171 -19.579 61.594 30.498 o -11 6 8 0.550 -39.126 61.718 32.170 o -11 6 9 59.340 37.367 61.374 32.284 o -11 7 -4 4.340 11.477 35.556 96.891 o -11 7 -3 99.935 76.740 28.356 136.922 o -11 7 -2 40.401 48.976 28.707 145.168 o -11 7 -1 755.408 602.361 421.745 0.669 o -11 7 0 1.647 -34.592 50.081 48.857 o -11 7 1 67.473 29.825 50.142 48.122 o -11 7 2 5.900 11.015 51.512 46.169 o -11 7 3 8.216 -15.184 53.513 42.787 o -11 7 4 16.192 39.508 50.748 47.469 o -11 7 5 89.963 -37.187 52.471 43.895 o -11 7 6 83.371 -45.268 52.096 44.608 o -11 7 7 114.961 4.117 51.343 45.365 o -10 0 -8 746.748 809.335 52.354 13.555 o -10 0 -6 605.347 658.650 47.574 19.104 o -10 0 -4 52.600 119.038 34.706 96.930 o -10 0 -2 12.845 50.380 35.513 96.637 o -10 0 0 2845.980 3331.420 147.864 1.033 o -10 0 2 19.102 24.899 53.142 43.319 o -10 0 4 699.064 826.017 89.582 8.815 o -10 0 6 5.879 49.675 108.787 10.350 o -10 0 8 54.675 47.415 114.000 9.408 o -10 0 10 596.086 166.946 110.342 8.528 o -10 0 12 490.327 199.050 96.225 11.229 o -10 0 14 18.091 -7.757 41.978 69.479 o -10 0 16 1.067 10.282 39.328 79.218 o -10 0 18 33.826 9.390 41.683 70.244 o -10 1 -9 369.520 408.439 25.764 55.002 o -10 1 -8 167.831 199.969 23.569 136.717 o -10 1 -7 2.286 -12.122 23.653 219.024 o -10 1 -6 420.417 423.315 66.006 19.590 o -10 1 -5 1.216 -6.077 23.773 216.825 o -10 1 -4 14.642 19.144 24.353 205.654 o -10 1 -3 45.873 68.799 24.588 192.919 o -10 1 -2 303.194 370.010 27.864 64.194 o -10 1 -1 286.838 314.278 27.244 72.990 o -10 1 0 53.668 66.831 25.198 182.625 o -10 1 1 5.655 -1.482 25.221 192.591 o -10 1 2 9.319 19.319 25.806 183.529 o -10 1 3 194.881 159.688 37.603 69.129 o -10 1 4 548.069 502.790 87.016 11.551 o -10 1 5 29.638 -55.562 50.244 48.461 o -10 1 6 28.879 -60.307 76.922 20.696 o -10 1 7 24.689 54.382 58.363 35.841 o -10 1 8 91.945 67.660 57.977 35.658 o -10 1 9 40.678 6.820 58.538 35.664 o -10 1 10 583.311 355.031 100.556 9.527 o -10 1 11 360.293 187.254 73.717 19.108 o -10 1 12 519.989 154.489 74.120 17.046 o -10 1 13 278.244 100.194 73.562 20.687 o -10 1 14 3.685 -25.240 50.465 48.115 o -10 1 15 20.865 -7.610 48.761 51.493 o -10 1 16 22.490 -46.598 57.391 37.176 o -10 1 17 70.906 31.955 48.518 51.274 o -10 1 18 118.666 84.441 42.396 63.810 o -10 1 19 172.534 109.670 40.922 63.814 o -10 1 20 243.111 107.242 37.957 65.914 o -10 1 21 100.352 57.791 49.422 48.591 o -10 2 -9 176.336 234.419 25.825 113.847 o -10 2 -8 16.366 5.624 24.557 202.621 o -10 2 -7 2.251 -4.976 23.633 219.397 o -10 2 -6 118.974 108.550 28.824 125.884 o -10 2 -5 314.886 302.201 32.206 59.227 o -10 2 -4 178.444 234.249 27.826 103.030 o -10 2 -3 30.042 45.997 23.707 212.966 o -10 2 -2 335.264 393.740 34.767 47.974 o -10 2 -1 196.346 174.905 27.538 107.393 o -10 2 0 8.925 56.944 30.393 131.709 o -10 2 1 35.009 34.024 33.736 106.468 o -10 2 2 9.306 -9.721 33.988 106.043 o -10 2 3 477.214 526.248 92.361 11.005 o -10 2 4 0.036 -3.940 41.980 69.534 o -10 2 5 49.029 64.779 42.181 67.675 o -10 2 6 28.346 6.812 42.296 68.316 o -10 2 7 5.135 35.095 54.741 40.860 o -10 2 8 12.968 -22.016 58.678 35.582 o -10 2 9 131.496 123.030 56.321 36.590 o -10 2 10 71.578 2.983 47.532 53.637 o -10 2 11 33.446 -9.550 46.891 55.596 o -10 2 12 16.056 33.842 47.201 54.873 o -10 2 13 38.774 4.570 55.741 39.339 o -10 2 14 52.030 23.901 43.815 63.192 o -10 2 15 0.001 49.019 60.339 33.631 o -10 2 16 29.399 55.994 78.583 19.794 o -10 2 17 351.421 380.498 80.263 15.637 o -10 2 18 198.813 166.195 72.748 21.612 o -10 2 19 23.058 17.053 64.841 29.113 o -10 2 20 68.044 32.756 63.348 30.280 o -10 2 21 3.798 8.798 55.300 40.067 o -10 3 -9 101.365 111.469 23.889 178.120 o -10 3 -8 3.348 7.631 24.218 208.848 o -10 3 -7 36.320 45.404 22.959 225.389 o -10 3 -6 213.208 242.142 52.193 37.646 o -10 3 -5 76.641 68.928 28.822 137.783 o -10 3 -4 23.726 11.091 29.342 141.665 o -10 3 -3 576.353 660.300 126.613 6.147 o -10 3 -2 347.975 403.421 91.205 12.563 o -10 3 -1 760.966 858.557 92.379 8.027 o -10 3 0 182.997 268.910 33.415 76.807 o -10 3 1 8.931 46.335 31.849 120.222 o -10 3 2 20.493 34.134 41.741 70.063 o -10 3 3 298.343 416.846 45.342 37.404 o -10 3 4 1131.110 831.085 65.813 7.806 o -10 3 5 180.071 182.275 50.968 41.578 o -10 3 6 290.943 281.575 42.790 45.107 o -10 3 7 852.522 646.086 85.788 8.799 o -10 3 8 64.045 40.627 53.692 42.014 o -10 3 9 397.561 188.106 54.879 29.456 o -10 3 10 26.122 40.267 45.711 58.361 o -10 3 11 0.065 -12.995 46.168 57.490 o -10 3 12 0.531 -7.151 45.634 58.845 o -10 3 13 162.057 117.848 45.779 52.644 o -10 3 14 72.761 23.643 47.914 52.599 o -10 3 15 305.557 197.623 59.919 28.059 o -10 3 16 2.625 -51.501 57.599 36.935 o -10 3 17 60.133 33.951 101.724 11.810 o -10 3 18 20.485 -4.163 71.594 23.898 o -10 3 19 23.096 -7.615 65.654 28.412 o -10 3 20 94.919 -11.963 59.612 34.073 o -10 3 21 101.062 70.479 53.896 40.942 o -10 4 -9 296.001 392.018 33.495 53.930 o -10 4 -8 2.551 14.641 29.742 138.455 o -10 4 -7 506.010 693.378 67.390 15.325 o -10 4 -6 422.236 520.955 57.660 22.122 o -10 4 -5 22.107 16.711 43.035 66.010 o -10 4 -4 7.067 46.149 29.623 138.962 o -10 4 -3 163.138 124.975 31.006 101.839 o -10 4 -2 161.307 208.884 32.845 86.641 o -10 4 -1 7.397 33.948 32.113 118.503 o -10 4 0 484.833 452.776 45.827 27.209 o -10 4 1 24.862 45.701 42.449 67.599 o -10 4 2 35.727 71.629 42.031 68.422 o -10 4 3 401.349 441.062 77.631 15.582 o -10 4 4 103.079 134.622 42.577 62.818 o -10 4 5 1.209 -2.423 37.214 88.485 o -10 4 6 369.182 181.830 45.180 40.215 o -10 4 7 619.338 248.148 52.797 22.636 o -10 4 8 37.687 27.730 50.483 47.845 o -10 4 9 227.895 78.191 58.450 32.633 o -10 4 10 162.787 36.544 51.063 44.347 o -10 4 11 196.444 154.404 65.317 26.511 o -10 4 12 87.655 95.877 48.237 50.759 o -10 4 13 34.583 -9.663 47.745 53.622 o -10 4 14 11.975 6.898 46.994 55.458 o -10 4 15 7.755 35.099 57.423 37.128 o -10 4 16 42.140 76.926 55.863 38.883 o -10 4 17 2.929 75.966 53.234 43.120 o -10 4 18 3.420 74.759 51.966 45.244 o -10 4 19 3.344 57.398 63.344 30.503 o -10 4 20 259.850 183.303 63.181 26.762 o -10 4 21 121.216 60.993 54.805 39.365 o -10 5 -9 4.481 28.226 27.561 160.966 o -10 5 -8 93.069 119.769 44.484 58.631 o -10 5 -7 16.945 20.276 30.278 133.163 o -10 5 -6 33.463 4.135 28.754 147.141 o -10 5 -5 191.199 269.514 43.160 51.756 o -10 5 -4 169.021 185.865 47.282 47.836 o -10 5 -3 36.938 -10.971 41.618 70.486 o -10 5 -2 181.493 132.627 64.767 27.313 o -10 5 -1 8.235 29.691 43.148 65.731 o -10 5 0 35.092 15.162 40.779 73.308 o -10 5 1 36.258 52.551 41.345 70.916 o -10 5 2 338.783 348.048 47.919 34.559 o -10 5 3 428.022 355.963 48.630 29.816 o -10 5 4 225.301 172.179 42.040 54.998 o -10 5 5 40.868 61.026 41.446 70.346 o -10 5 6 0.776 38.947 41.764 70.174 o -10 5 7 21.735 -9.514 46.212 57.321 o -10 5 8 10.439 26.741 50.313 48.356 o -10 5 9 109.078 17.813 51.262 45.487 o -10 5 10 69.103 17.528 51.874 45.056 o -10 5 11 228.098 4.833 72.810 22.064 o -10 5 12 57.782 48.745 57.367 36.877 o -10 5 13 41.099 34.251 43.833 63.248 o -10 5 14 51.329 -69.845 54.028 41.801 o -10 5 15 25.483 -9.188 54.155 41.740 o -10 5 16 2.745 12.735 52.028 45.263 o -10 5 17 0.403 11.206 49.960 49.092 o -10 5 18 136.220 102.005 67.827 25.706 o -10 5 19 99.768 63.215 60.863 32.364 o -10 5 20 12.953 -30.525 55.914 39.185 o -10 6 -9 35.950 40.033 49.907 48.907 o -10 6 -8 9.826 9.332 51.434 46.303 o -10 6 -7 181.787 66.932 119.971 8.386 o -10 6 -6 562.691 -26.260 140.355 5.779 o -10 6 -5 14.068 13.034 37.529 86.879 o -10 6 -4 13.175 -32.131 38.742 81.598 o -10 6 -3 17.096 44.013 39.603 77.771 o -10 6 -2 580.582 609.892 67.235 14.860 o -10 6 -1 97.110 117.016 41.171 67.696 o -10 6 0 75.552 65.819 43.123 63.973 o -10 6 1 206.905 301.227 57.655 31.169 o -10 6 2 465.334 519.505 68.759 16.958 o -10 6 3 95.535 125.686 51.255 44.621 o -10 6 4 127.504 180.882 42.135 61.238 o -10 6 5 20.488 22.595 41.495 70.972 o -10 6 6 64.949 61.387 48.132 51.920 o -10 6 7 0.054 5.631 44.842 60.939 o -10 6 8 45.187 -14.365 42.422 67.727 o -10 6 9 1.017 2.933 47.019 55.427 o -10 6 10 164.799 -42.448 48.607 49.179 o -10 6 11 23.943 20.069 58.817 35.366 o -10 6 12 40.191 25.971 47.128 54.840 o -10 6 13 1.250 4.496 48.347 52.425 o -10 6 14 73.869 -57.442 72.202 23.390 o -10 6 15 27.561 93.471 71.133 24.093 o -10 6 16 546.459 589.604 78.340 12.899 o -10 7 -9 44.647 83.060 45.610 57.924 o -10 7 -8 268.534 241.326 50.932 36.979 o -10 7 -7 9.251 38.862 37.269 87.974 o -10 7 -6 35.150 36.929 33.345 108.870 o -10 7 -5 91.213 15.999 47.321 53.604 o -10 7 -4 120.400 -17.217 76.018 20.956 o -10 7 -3 164.916 118.073 60.825 31.118 o -10 7 -2 93.506 74.981 36.867 85.054 o -10 7 -1 5.983 -35.402 37.967 84.999 o -10 7 0 137.291 178.996 69.835 23.928 o -10 7 1 9.435 22.902 38.648 81.926 o -10 7 2 400.717 310.816 46.517 33.726 o -10 7 3 97.574 73.409 38.469 78.274 o -10 7 4 95.903 101.827 43.569 61.249 o -10 7 5 95.709 83.193 42.438 64.817 o -10 7 6 221.520 44.317 141.800 6.010 o -10 7 7 150.074 7.094 43.578 60.930 o -10 7 8 0.015 -40.791 40.389 75.118 o -10 7 9 335.074 115.653 139.086 6.103 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55.383 5.955 o -4 6 14 1419.040 1428.610 66.887 4.695 o -4 6 15 485.792 516.105 36.584 30.886 o -4 6 16 13.008 35.371 32.292 117.013 o -4 6 17 573.323 611.447 39.500 23.421 o -4 6 18 36.800 13.040 33.366 109.196 o -4 6 19 457.866 497.689 37.583 32.370 o -4 6 20 646.992 669.753 47.082 18.027 o -4 6 21 684.653 806.471 65.462 12.367 o -4 6 22 997.657 1034.660 54.723 8.815 o -4 6 23 37.698 76.719 44.150 61.992 o -4 6 24 1430.910 1729.420 98.738 3.522 o -4 6 25 109.923 126.873 37.357 79.655 o -4 6 26 738.009 792.448 87.802 8.866 o -4 6 27 184.764 162.227 34.030 82.024 o -4 6 28 0.172 -5.918 32.309 117.388 o -4 6 29 1.615 6.252 30.410 132.497 o -4 6 30 0.011 -8.160 28.828 147.451 o -4 6 31 1.504 6.633 26.942 168.791 o -4 6 32 602.603 719.124 40.002 20.427 o -4 6 33 130.425 209.250 48.728 46.470 o -4 7 -3 1055.590 1085.470 38.431 9.000 o -4 7 -2 261.771 265.726 28.370 79.321 o -4 7 -1 1006.690 1128.730 63.260 7.790 o -4 7 0 3458.050 4443.130 211.477 0.619 o -4 7 1 441.029 556.629 62.219 19.359 o -4 7 2 0.006 -4.762 37.833 85.615 o -4 7 3 3.277 14.927 39.905 76.926 o -4 7 4 1181.200 1093.000 98.959 5.111 o -4 7 5 305.540 315.258 32.194 59.607 o -4 7 6 150.038 152.980 25.707 135.453 o -4 7 7 1038.580 1032.570 36.493 9.559 o -4 7 8 14.992 22.454 21.446 264.550 o -4 7 9 488.649 531.406 39.212 28.891 o -4 7 10 355.827 382.510 35.641 45.512 o -4 7 11 12.662 9.550 26.962 168.236 o -4 7 12 1258.060 1400.500 58.281 5.668 o -4 7 13 888.766 914.610 52.268 10.805 o -4 7 14 98.202 109.975 31.500 111.021 o -4 7 15 160.582 195.506 34.525 81.203 o -4 7 16 161.145 170.973 34.333 83.485 o -4 7 17 46.846 67.222 34.206 102.047 o -4 7 18 957.714 1192.780 87.068 6.430 o -4 7 19 70.549 174.677 40.696 69.051 o -4 7 20 2845.630 3665.410 166.844 0.929 o -4 7 21 513.051 602.313 77.609 13.358 o -4 7 22 166.247 119.647 47.417 49.189 o -4 7 23 37.491 95.786 38.583 80.445 o -4 7 24 450.404 633.101 45.546 25.165 o -4 7 25 173.915 351.794 68.972 22.954 o -4 7 26 935.982 1093.970 54.427 9.137 o -4 7 27 12.804 80.281 32.816 112.404 o -4 7 28 777.228 956.026 48.146 12.498 o -4 7 29 229.425 262.442 31.130 77.210 o -4 7 30 5.973 4.224 27.718 159.438 o -4 7 31 114.755 171.534 26.406 137.945 o -4 7 32 94.636 104.252 33.043 102.616 o -4 8 -3 299.146 297.377 26.479 74.083 o -4 8 -2 73.473 91.487 23.688 194.925 o -4 8 -1 454.668 370.189 26.709 46.099 o -4 8 0 530.606 635.293 32.170 27.513 o -4 8 1 301.576 370.018 30.455 59.702 o -4 8 2 123.314 153.564 20.717 197.829 o -4 8 3 414.952 416.144 41.037 34.729 o -4 8 4 677.678 647.238 43.713 18.359 o -4 8 5 483.927 493.534 29.747 35.811 o -4 8 6 54.449 38.893 22.829 223.975 o -4 8 7 1795.770 1654.670 58.458 3.393 o -4 8 8 260.954 269.882 22.971 96.307 o -4 8 9 730.081 834.363 33.378 16.631 o -4 8 10 2.752 16.621 24.152 209.871 o -4 8 11 1012.320 1222.270 45.921 8.375 o -4 8 12 389.336 406.282 32.194 45.311 o -4 8 13 47.784 39.358 39.749 76.510 o -4 8 14 1213.420 1441.290 73.542 5.286 o -4 8 15 4163.590 4393.590 198.516 0.529 o -4 8 16 682.238 819.612 49.926 15.019 o -4 8 17 301.417 340.155 42.221 43.164 o -4 8 18 1704.800 1913.940 111.584 2.657 o -4 8 19 2111.980 1917.710 121.265 2.059 o -4 8 20 56.880 54.081 48.251 51.887 o -4 8 21 0.231 9.259 29.511 140.687 o -4 8 22 86.335 78.435 28.918 134.493 o -4 8 23 869.338 996.965 48.527 10.897 o -4 8 24 1273.610 1764.050 127.936 3.187 o -4 8 25 30.256 0.701 34.165 104.582 o -4 8 26 398.864 419.965 37.175 38.984 o -4 8 27 97.804 105.104 31.835 109.321 o -4 8 28 331.923 389.787 41.039 40.806 o -4 8 29 13.882 17.684 27.219 164.849 o -4 8 30 30.415 47.636 28.917 144.137 o -4 8 31 236.118 280.461 39.950 54.005 o -4 8 32 531.718 529.354 43.813 24.839 o -4 9 -3 1377.240 1472.240 106.056 3.774 o -4 9 -2 104.609 68.507 33.497 100.967 o -4 9 -1 465.479 567.171 44.297 26.476 o -4 9 0 64.784 107.993 26.398 160.420 o -4 9 1 346.506 337.503 29.919 56.819 o -4 9 2 1220.030 1214.750 71.480 5.842 o -4 9 3 448.231 472.006 29.613 39.510 o -4 9 4 1086.880 1127.690 93.676 5.641 o -4 9 5 2538.800 2859.370 238.962 0.929 o -4 9 6 612.655 526.337 37.168 24.380 o -4 9 7 10.438 21.797 24.592 201.906 o -4 9 8 192.201 192.329 26.324 112.620 o -4 9 9 837.179 823.253 56.389 11.571 o -4 9 10 121.942 138.077 24.007 163.466 o -4 9 11 1206.660 1221.250 42.134 7.015 o -4 9 12 1.038 -35.869 23.637 219.334 o -4 9 13 98.947 84.054 32.110 108.876 o -4 9 14 1850.480 2193.940 70.198 2.652 o -4 9 15 1224.450 1265.730 91.770 4.939 o -4 9 16 146.380 199.620 33.193 88.172 o -4 9 17 373.151 376.560 35.270 44.695 o -4 9 18 737.484 855.635 65.134 11.458 o -4 9 19 2161.940 2096.240 132.450 1.843 o -4 9 20 185.710 224.687 31.486 86.694 o -4 9 21 8.587 20.500 29.874 137.049 o -4 9 22 125.664 178.540 39.842 67.819 o -4 9 23 0.248 -15.857 31.151 126.282 o -4 9 24 1498.630 1702.450 94.812 3.479 o -4 9 25 135.765 99.654 33.641 94.599 o -4 9 26 334.942 435.381 42.730 37.394 o -4 9 27 73.138 98.623 34.358 97.900 o -4 9 28 271.136 344.352 80.225 16.627 o -4 9 29 29.140 9.421 28.513 149.729 o -4 9 30 274.948 379.921 42.488 43.266 o -4 9 31 21.615 46.725 27.221 163.252 o -4 10 -3 57.073 83.668 38.222 81.291 o -4 10 -2 168.591 180.197 33.633 84.560 o -4 10 -1 2469.030 2638.810 127.693 1.450 o -4 10 0 5379.920 5895.540 301.405 0.292 o -4 10 1 3075.610 3712.480 176.226 0.836 o -4 10 2 1094.580 1411.880 78.186 5.695 o -4 10 3 445.706 533.697 56.816 21.724 o -4 10 4 2390.720 2577.980 317.033 0.743 o -4 10 5 166.869 163.808 30.533 99.925 o -4 10 6 130.373 129.886 40.092 68.511 o -4 10 7 1146.310 1090.930 57.167 7.265 o -4 10 8 19.956 30.183 31.224 124.942 o -4 10 9 1444.210 1443.100 82.817 4.204 o -4 10 10 2522.430 2735.960 111.335 1.453 o -4 10 11 1494.120 1618.230 57.111 4.304 o -4 10 12 861.973 940.008 49.692 11.243 o -4 10 13 0.151 75.426 47.708 53.679 o -4 10 14 81.209 100.475 27.316 147.954 o -4 10 15 1773.800 1782.640 157.161 2.096 o -4 10 16 58.367 91.492 37.558 83.812 o -4 10 17 482.532 531.556 33.435 32.429 o -4 10 18 435.232 439.648 31.624 40.322 o -4 10 19 16.105 16.406 26.235 177.321 o -4 10 20 8.985 23.601 32.944 112.698 o -4 10 21 2.725 -16.498 37.026 89.385 o -4 10 22 32.158 36.405 23.616 215.063 o -4 10 23 68.402 45.679 29.695 133.002 o -4 10 24 0.193 22.439 39.057 80.296 o -4 10 25 38.008 12.581 36.260 92.545 o -4 10 26 387.846 410.322 38.908 38.477 o -4 10 27 171.081 147.332 31.787 94.622 o -4 10 28 27.115 30.339 34.614 101.559 o -4 10 29 3.009 -4.870 32.895 113.243 o -4 10 30 73.030 125.799 30.216 122.439 o -4 11 -3 25.603 66.258 33.775 105.897 o -4 11 -2 3531.220 4557.080 193.002 0.620 o -4 11 -1 4378.760 5642.740 232.033 0.408 o -4 11 0 1865.250 2365.170 141.713 1.908 o -4 11 1 650.255 779.189 59.552 14.111 o -4 11 2 101.042 241.534 35.631 81.510 o -4 11 3 471.435 600.391 71.256 15.498 o -4 11 4 1.773 21.764 32.061 119.127 o -4 11 5 116.619 68.479 28.845 130.342 o -4 11 6 3403.600 3618.280 365.995 0.466 o -4 11 7 2105.950 2245.910 232.972 1.180 o -4 11 8 35.970 54.094 29.520 137.644 o -4 11 9 2907.510 3210.900 204.658 0.884 o -4 11 10 90.556 87.157 30.722 119.050 o -4 11 11 556.281 540.265 37.791 26.221 o -4 11 12 830.372 895.962 96.345 7.188 o -4 11 13 661.227 707.569 53.863 15.717 o -4 11 14 720.363 668.459 51.066 15.527 o -4 11 15 1143.640 1280.990 51.187 6.905 o -4 11 16 882.402 1006.140 44.069 11.076 o -4 11 17 162.663 158.979 27.502 118.400 o -4 11 18 389.955 347.821 42.374 37.062 o -4 11 19 653.885 578.924 46.959 19.047 o -4 11 20 1480.650 1368.390 64.972 4.626 o -4 11 21 679.037 747.985 39.268 17.992 o -4 11 22 33.745 56.405 29.882 134.486 o -4 11 23 65.038 49.727 27.917 149.847 o -4 11 24 191.738 184.017 36.405 71.750 o -4 11 25 104.855 108.948 46.273 54.178 o -4 11 26 30.623 55.362 40.291 74.740 o -4 11 27 235.479 277.106 40.539 53.090 o -4 11 28 4.598 13.718 31.119 126.456 o -4 11 29 43.480 48.864 25.321 184.809 o -4 12 -3 1258.540 1566.420 208.545 1.936 o -4 12 -2 57.180 68.816 39.906 75.072 o -4 12 -1 1675.410 1875.430 167.615 2.024 o -4 12 0 1.492 16.073 39.410 78.874 o -4 12 1 1191.770 1216.810 107.056 4.562 o -4 12 2 619.682 826.132 49.669 16.263 o -4 12 3 5210.030 6641.100 625.243 0.166 o -4 12 4 1632.380 1821.880 115.245 2.784 o -4 12 5 3364.240 4526.890 159.149 0.697 o -4 12 6 6.305 8.541 93.115 14.132 o -4 12 7 167.276 155.541 95.167 13.117 o -4 12 8 1160.850 1311.810 226.508 1.829 o -4 12 9 2.745 19.230 31.694 121.901 o -4 12 10 897.590 834.498 92.532 7.304 o -4 12 11 1816.180 1974.250 120.987 2.357 o -4 12 12 3.196 -12.754 36.035 94.367 o -4 12 13 469.692 524.465 37.202 31.185 o -4 12 14 32.145 6.599 31.595 122.028 o -4 12 15 15.774 32.864 44.666 61.270 o -4 12 16 834.841 820.356 76.581 9.262 o -4 12 17 41.123 8.521 30.818 127.711 o -4 12 18 652.888 685.430 47.932 17.487 o -4 12 19 1242.470 1410.120 67.902 5.414 o -4 12 20 398.393 411.259 36.078 40.373 o -4 12 21 234.078 170.957 92.221 13.631 o -4 12 22 132.090 103.451 102.869 11.407 o -4 12 23 5.122 0.424 27.985 156.441 o -4 12 24 1.034 7.712 43.253 65.498 o -4 12 25 26.797 -13.128 38.702 81.624 o -4 12 26 2.369 5.394 31.778 121.332 o -4 12 27 0.020 -29.259 26.986 168.270 o -4 13 -3 2123.210 2490.510 388.621 0.598 o -4 13 -2 311.434 296.265 33.325 57.962 o -4 13 -1 4005.870 4710.300 615.485 0.215 o -4 13 0 1555.050 1680.940 184.931 1.994 o -4 13 1 1508.010 1777.300 291.723 1.090 o -4 13 2 367.628 447.026 75.328 16.707 o -4 13 3 143.534 117.096 28.430 122.259 o -4 13 4 183.064 162.016 28.112 109.249 o -4 13 5 288.444 287.304 37.243 53.882 o -4 13 6 6.914 6.282 26.751 171.125 o -4 13 7 466.347 464.875 31.857 36.743 o -4 13 8 324.784 332.478 31.201 57.826 o -4 13 9 2503.640 2439.030 171.213 1.287 o -4 13 10 1.632 21.819 22.842 234.530 o -4 13 11 265.586 236.351 44.826 45.232 o -4 13 12 664.832 525.979 62.091 15.422 o -4 13 13 192.947 182.533 50.580 41.649 o -4 13 14 36.844 34.913 27.941 154.199 o -4 13 15 80.707 77.878 27.378 149.881 o -4 13 16 37.720 27.761 26.557 170.686 o -4 13 17 705.229 768.111 64.126 12.568 o -4 13 18 1.338 8.370 24.486 204.328 o -4 13 19 4.956 38.191 33.392 109.626 o -4 13 20 514.571 477.146 253.315 1.833 o -4 13 21 2.326 16.719 41.390 71.508 o -4 13 22 24.535 -27.299 52.882 43.775 o -4 13 23 13.070 62.023 39.224 79.174 o -4 13 24 28.126 14.391 34.065 105.061 o -4 13 25 332.832 306.787 35.261 51.777 o -4 14 -3 77.678 326.990 167.146 4.343 o -4 14 -2 1589.500 1390.360 72.113 4.084 o -4 14 -1 608.840 648.468 43.515 20.320 o -4 14 0 465.437 437.548 36.971 34.121 o -4 14 1 70.319 58.980 34.913 96.774 o -4 14 2 253.684 376.519 41.524 46.201 o -4 14 3 1021.540 897.023 125.545 4.708 o -4 14 4 1.689 -63.748 135.708 6.654 o -4 14 5 1739.290 1740.980 728.998 0.217 o -4 14 6 699.445 929.627 96.389 7.789 o -4 14 7 398.423 481.206 98.251 10.570 o -4 14 8 1130.070 980.326 168.142 3.007 o -4 14 9 501.568 511.893 56.713 20.619 o -4 14 10 1.453 25.409 31.460 123.694 o -4 14 11 55.949 78.141 32.337 112.567 o -4 14 12 887.296 1010.440 57.478 9.789 o -4 14 13 121.645 107.339 35.734 86.118 o -4 14 14 646.515 759.743 48.332 16.691 o -4 14 15 83.454 44.995 28.683 139.875 o -4 14 16 284.128 310.771 32.991 61.077 o -4 14 17 353.084 412.005 34.093 46.284 o -4 14 18 408.644 352.710 232.680 2.197 o -4 14 19 243.782 167.232 171.306 4.105 o -4 14 20 430.860 318.367 270.753 1.635 o -4 14 21 305.294 369.725 46.104 37.507 o -4 14 22 26.369 27.897 33.109 111.005 o -4 14 23 102.772 144.135 29.453 120.998 o -4 15 -3 454.275 428.828 40.817 32.327 o -4 15 -2 239.048 202.483 53.197 36.252 o -4 15 -1 80.015 107.226 28.197 139.268 o -4 15 0 6.820 64.760 49.530 49.803 o -4 15 1 43.929 7.475 27.158 163.746 o -4 15 2 168.190 198.826 38.639 66.842 o -4 15 3 69.758 113.151 29.671 128.156 o -4 15 4 105.056 118.584 26.081 151.550 o -4 15 5 2.555 4.933 25.701 185.488 o -4 15 6 6.892 20.691 24.846 198.052 o -4 15 7 26.721 17.343 24.532 201.628 o -4 15 8 293.885 333.070 37.502 50.769 o -4 15 9 158.536 173.606 35.430 79.505 o -4 15 10 1380.040 1595.500 69.354 4.481 o -4 15 11 358.190 405.647 45.813 34.093 o -4 15 12 42.067 18.439 28.658 146.972 o -4 15 13 4.202 8.537 26.669 172.211 o -4 15 14 215.289 298.380 31.478 75.544 o -4 15 15 32.417 20.645 24.264 205.112 o -4 15 16 115.187 50.444 85.041 16.727 o -4 15 17 289.238 301.436 48.362 37.605 o -4 15 18 67.201 49.386 39.416 76.887 o -4 15 19 125.853 127.712 36.952 79.754 o -4 15 20 74.960 69.370 29.723 130.286 o -4 16 -3 468.866 462.580 49.578 25.597 o -4 16 -2 530.106 518.576 97.657 9.805 o -4 16 -1 97.710 94.294 26.238 155.476 o -4 16 0 48.807 54.811 29.900 132.963 o -4 16 1 767.117 832.094 113.970 6.239 o -4 16 2 515.608 526.565 57.688 19.731 o -4 16 3 267.376 289.462 35.729 58.812 o -4 16 4 243.096 256.575 26.584 89.967 o -4 16 5 54.141 22.950 23.744 209.754 o -4 16 6 0.018 3.793 28.115 155.021 o -4 16 7 5.831 -2.313 30.137 134.892 o -4 16 8 114.746 112.237 30.740 113.079 o -4 16 9 20.240 33.548 28.903 145.556 o -4 16 10 3.894 15.545 28.243 153.504 o -4 16 11 105.650 71.733 27.667 142.388 o -4 16 12 392.860 404.736 32.978 44.222 o -4 16 13 20.609 36.540 24.259 205.714 o -4 16 14 42.111 30.610 39.828 76.494 o -4 16 15 0.036 1.866 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21.650 256.717 o 7 14 7 30.080 8.314 34.021 105.366 o 7 14 8 20.342 16.965 23.267 224.712 o 7 14 9 55.916 23.192 22.540 231.342 o 7 14 10 114.455 85.038 21.683 208.671 o 7 15 7 13.549 18.942 19.458 321.526 o 8 0 8 2500.640 2668.770 80.143 1.606 o 8 0 10 1640.470 1657.190 54.571 3.836 o 8 0 12 6.341 61.343 25.849 181.628 o 8 0 14 983.619 977.191 51.514 9.461 o 8 0 16 75.389 83.200 51.637 44.863 o 8 0 18 1209.890 1183.290 51.556 6.778 o 8 0 20 161.562 199.713 25.201 127.671 o 8 0 22 60.621 94.227 21.550 235.863 o 8 0 24 102.332 91.926 21.848 210.608 o 8 0 26 144.310 96.839 21.868 187.173 o 8 1 8 90.600 108.829 17.925 290.901 o 8 1 9 10.292 19.802 17.663 390.353 o 8 1 10 2081.810 2289.270 52.156 2.348 o 8 1 11 1062.240 1156.240 45.568 8.245 o 8 1 12 897.057 1073.030 33.322 11.267 o 8 1 13 0.694 -14.009 19.306 328.769 o 8 1 14 0.786 -1.112 21.485 265.477 o 8 1 15 597.443 715.814 48.150 18.413 o 8 1 16 195.489 183.647 37.713 67.533 o 8 1 17 52.818 94.046 23.914 197.883 o 8 1 18 732.140 836.253 29.085 17.180 o 8 1 19 669.946 744.358 26.838 20.838 o 8 1 20 972.491 1018.240 31.797 10.710 o 8 1 21 126.884 126.345 18.117 245.151 o 8 1 22 60.203 96.726 16.580 370.336 o 8 1 23 61.264 66.912 15.245 445.521 o 8 1 24 3.154 -12.679 13.665 656.033 o 8 1 25 53.725 65.071 13.952 532.769 o 8 1 26 15.578 11.636 16.681 436.947 o 8 2 8 444.180 512.788 21.871 43.601 o 8 2 9 1331.950 1540.540 41.821 5.387 o 8 2 10 63.514 59.389 19.550 289.357 o 8 2 11 560.059 613.047 25.453 29.064 o 8 2 12 347.444 364.249 25.145 62.367 o 8 2 13 1963.730 2119.980 64.056 2.577 o 8 2 14 347.672 429.523 31.507 49.099 o 8 2 15 722.924 825.189 51.323 13.987 o 8 2 16 62.533 61.233 26.382 166.217 o 8 2 17 814.211 790.642 31.853 15.383 o 8 2 18 168.026 230.712 21.975 141.750 o 8 2 19 939.893 1100.490 37.361 10.257 o 8 2 20 22.255 6.829 20.461 290.533 o 8 2 21 108.926 178.186 18.334 234.554 o 8 2 22 203.990 227.566 19.948 139.610 o 8 2 23 153.797 196.189 18.318 192.364 o 8 2 24 79.701 80.895 15.512 396.308 o 8 2 25 8.625 27.666 16.230 461.025 o 8 2 26 50.578 15.563 16.267 436.411 o 8 3 8 964.739 1137.450 30.734 10.112 o 8 3 9 0.594 -7.659 21.234 271.779 o 8 3 10 125.178 171.386 23.627 159.238 o 8 3 11 2752.860 3201.730 85.754 1.258 o 8 3 12 147.033 231.091 25.055 128.266 o 8 3 13 161.589 186.144 36.446 74.881 o 8 3 14 237.382 254.429 36.866 61.555 o 8 3 15 77.979 113.005 46.326 54.901 o 8 3 16 305.689 361.115 39.338 45.880 o 8 3 17 351.201 444.207 27.878 52.391 o 8 3 18 1867.340 2324.000 89.052 2.378 o 8 3 19 706.529 781.285 34.202 17.786 o 8 3 20 4.111 12.072 21.174 273.029 o 8 3 21 49.188 59.022 22.540 228.000 o 8 3 22 74.005 79.004 24.953 179.191 o 8 3 23 258.739 339.891 22.598 88.549 o 8 3 24 6.637 0.682 14.152 611.145 o 8 3 25 259.163 247.175 18.772 116.872 o 8 3 26 2.157 -13.636 21.755 258.907 o 8 4 8 473.513 594.570 28.326 33.800 o 8 4 9 126.004 131.913 22.200 183.461 o 8 4 10 257.826 298.972 23.095 92.715 o 8 4 11 103.744 134.328 23.004 183.444 o 8 4 12 21.476 65.655 35.481 96.269 o 8 4 13 13.418 17.953 39.550 78.222 o 8 4 15 2181.850 2434.440 114.753 1.800 o 8 4 16 77.291 103.075 24.241 183.854 o 8 4 17 117.884 118.422 23.307 177.015 o 8 4 18 1178.630 1400.240 57.949 6.087 o 8 4 19 707.730 815.855 39.799 16.342 o 8 4 20 396.277 484.789 30.261 42.937 o 8 4 21 1.152 13.192 19.293 328.974 o 8 4 22 145.382 163.390 20.700 181.941 o 8 4 23 70.822 93.577 19.699 270.049 o 8 4 24 1289.130 1377.600 53.350 5.717 o 8 4 25 29.878 22.162 17.997 369.232 o 8 5 8 32.551 89.241 30.270 129.734 o 8 5 9 25.325 22.914 29.025 144.352 o 8 5 10 417.254 469.991 29.638 42.256 o 8 5 11 265.503 327.071 41.751 46.811 o 8 5 12 200.910 251.793 37.699 63.534 o 8 5 13 397.637 393.660 41.995 35.593 o 8 5 14 23.121 62.584 36.273 92.149 o 8 5 15 165.532 211.132 25.078 125.278 o 8 5 16 6.412 -8.930 23.173 228.110 o 8 5 17 86.773 124.078 22.773 196.423 o 8 5 18 139.133 144.114 22.036 175.684 o 8 5 19 0.191 4.001 23.065 230.335 o 8 5 20 1195.960 1384.010 84.879 5.076 o 8 5 21 249.200 258.874 25.138 93.319 o 8 5 22 198.358 233.987 32.738 79.348 o 8 5 23 253.725 257.356 24.039 96.284 o 8 5 24 2.433 8.596 19.103 335.591 o 8 5 25 13.915 23.794 20.867 279.392 o 8 6 8 12.291 14.490 30.177 134.294 o 8 6 9 68.071 64.843 48.899 50.240 o 8 6 10 0.802 9.401 44.886 60.818 o 8 6 12 78.194 73.687 37.480 83.497 o 8 6 13 37.895 38.201 27.644 157.180 o 8 6 14 79.137 109.644 23.890 186.802 o 8 6 15 186.922 202.007 24.131 125.527 o 8 6 16 77.890 114.249 21.427 224.548 o 8 6 17 6.435 15.816 19.952 307.059 o 8 6 18 5.778 16.684 19.973 306.449 o 8 6 19 205.839 197.307 30.518 89.323 o 8 6 20 113.177 82.025 41.871 65.663 o 8 6 21 1.091 12.202 38.332 83.383 o 8 6 22 13.583 53.640 24.596 199.997 o 8 6 23 23.319 24.105 19.713 310.579 o 8 6 24 301.790 315.928 30.236 63.870 o 8 7 8 208.180 251.951 50.712 39.501 o 8 7 9 14.781 -8.311 45.532 59.078 o 8 7 10 1005.510 1105.390 61.188 8.019 o 8 7 11 406.159 451.886 31.640 42.261 o 8 7 12 71.835 66.609 26.343 164.156 o 8 7 13 74.487 107.175 25.770 165.141 o 8 7 14 506.415 544.082 37.006 28.840 o 8 7 15 165.962 146.313 24.415 141.211 o 8 7 16 79.497 111.356 22.779 202.310 o 8 7 17 173.567 183.576 29.354 102.439 o 8 7 18 167.012 209.524 28.154 107.153 o 8 7 19 300.209 276.530 30.385 66.714 o 8 7 20 210.579 219.381 40.665 57.234 o 8 7 21 1085.270 923.732 139.832 3.962 o 8 7 22 72.507 49.379 12.530 606.974 o 8 7 23 19.068 23.412 16.089 465.292 o 8 8 8 954.978 1076.590 48.748 9.447 o 8 8 9 47.034 53.634 26.881 163.709 o 8 8 10 72.029 93.624 31.449 116.025 o 8 8 11 429.058 397.657 29.628 44.542 o 8 8 12 61.732 33.651 24.711 191.482 o 8 8 13 55.779 80.699 24.047 196.961 o 8 8 14 0.036 3.206 29.252 143.211 o 8 8 15 589.578 716.378 40.822 20.648 o 8 8 16 21.793 30.447 32.006 118.866 o 8 8 17 162.232 198.118 27.478 113.520 o 8 8 18 44.356 72.855 26.191 170.910 o 8 8 19 55.197 4.397 34.371 102.371 o 8 8 20 58.208 53.218 16.289 409.121 o 8 8 21 33.113 24.924 16.583 430.171 o 8 8 22 20.958 -22.918 26.858 169.388 o 8 9 8 104.564 83.361 34.174 96.525 o 8 9 9 1.444 30.337 33.134 111.481 o 8 9 10 1.301 11.713 42.072 69.219 o 8 9 11 133.488 197.429 43.173 57.799 o 8 9 12 38.168 69.938 40.684 72.913 o 8 9 13 63.578 76.433 39.019 77.966 o 8 9 14 5.527 46.700 36.714 90.643 o 8 9 15 1.805 -3.035 35.185 98.985 o 8 9 16 452.034 380.063 57.799 23.122 o 8 9 17 64.209 34.854 35.299 95.908 o 8 9 18 13.275 -6.917 20.052 304.120 o 8 9 19 1.567 3.670 17.882 383.146 o 8 9 20 42.054 10.689 16.256 445.727 o 8 10 8 4.839 12.332 30.914 128.144 o 8 10 9 83.223 41.159 31.971 114.169 o 8 10 10 53.534 29.120 35.660 94.722 o 8 10 11 6.872 -13.689 29.076 144.908 o 8 10 12 372.665 296.468 27.619 59.714 o 8 10 13 14.181 5.621 27.079 166.797 o 8 10 14 366.966 318.354 29.882 55.490 o 8 10 15 1.360 13.949 26.278 177.378 o 8 10 16 78.227 60.162 17.442 340.426 o 8 10 17 22.714 2.012 18.261 364.536 o 8 10 18 117.406 66.127 17.003 308.922 o 8 10 19 17.907 22.162 18.207 365.240 o 8 11 8 9.032 9.478 38.474 82.731 o 8 11 9 23.951 -8.776 38.034 84.550 o 8 11 10 612.572 389.909 29.778 30.748 o 8 11 11 1.968 29.007 28.674 148.807 o 8 11 12 94.960 36.090 17.755 325.991 o 8 11 13 93.825 31.578 28.510 140.863 o 8 11 14 66.766 30.608 18.535 326.299 o 8 11 15 82.167 77.748 31.099 118.192 o 8 11 16 99.407 54.264 38.889 77.144 o 8 11 17 120.785 92.335 19.540 238.289 o 8 12 8 280.896 215.468 50.344 37.680 o 8 12 9 543.689 343.312 95.513 10.606 o 8 12 10 316.219 197.428 57.582 29.643 o 8 12 11 5.144 -2.198 15.826 488.987 o 8 12 13 181.172 113.223 21.234 170.302 o 8 13 8 54.428 -7.349 26.764 167.780 o 9 0 9 73.733 99.562 50.576 46.586 o 9 0 11 153.965 181.223 44.110 54.952 o 9 0 13 5.111 0.152 33.972 106.166 o 9 0 15 26.293 16.533 33.037 111.696 o 9 0 17 326.306 371.212 35.596 48.776 o 9 0 19 6.647 0.885 26.863 169.751 o 9 0 21 29.121 25.026 22.547 237.198 o 9 0 23 64.904 54.980 24.028 198.321 o 9 1 9 27.886 56.561 34.347 102.569 o 9 1 10 126.474 162.039 42.943 59.814 o 9 1 11 6.841 21.134 32.319 117.160 o 9 1 12 414.415 442.350 31.644 41.953 o 9 1 13 27.553 18.133 22.474 239.585 o 9 1 14 102.888 114.304 22.182 199.659 o 9 1 15 54.095 65.793 21.112 254.396 o 9 1 16 78.700 93.999 22.891 204.556 o 9 1 17 112.617 142.107 24.907 156.969 o 9 1 18 13.637 15.096 20.222 298.099 o 9 1 19 9.405 -6.508 19.049 337.295 o 9 1 20 2.211 4.069 17.335 407.654 o 9 1 21 245.505 278.631 18.339 117.828 o 9 1 22 28.668 35.261 16.052 457.506 o 9 1 23 155.899 140.540 25.058 140.695 o 9 2 10 1.834 -28.720 29.123 144.480 o 9 2 11 71.577 55.834 39.217 77.314 o 9 2 12 1486.320 1537.520 50.257 4.591 o 9 2 13 55.701 80.361 22.589 221.210 o 9 2 14 33.440 20.119 21.628 257.016 o 9 2 15 0.035 13.891 20.630 287.775 o 9 2 16 28.951 48.812 20.014 295.943 o 9 2 17 33.721 36.161 18.927 330.296 o 9 2 18 7.711 11.487 19.712 314.664 o 9 2 19 3.452 4.704 18.009 377.660 o 9 2 20 443.144 499.033 33.693 35.883 o 9 2 21 40.635 42.553 17.899 361.906 o 9 2 22 23.311 37.266 15.512 492.192 o 9 2 23 52.847 43.204 23.726 207.955 o 9 3 9 47.163 3.171 40.181 75.373 o 9 3 10 95.499 88.210 40.791 69.765 o 9 3 11 1446.850 1703.330 57.981 4.305 o 9 3 12 479.866 505.717 27.500 37.051 o 9 3 13 69.034 69.108 21.977 229.486 o 9 3 14 139.735 151.690 21.765 176.437 o 9 3 15 4.265 3.027 20.061 304.368 o 9 3 16 0.169 4.617 18.918 342.353 o 9 3 17 115.148 101.387 20.815 217.284 o 9 3 18 174.105 194.274 20.616 158.197 o 9 3 19 20.793 5.726 20.521 289.172 o 9 3 20 91.950 88.837 19.015 272.352 o 9 3 21 164.202 179.582 17.863 195.861 o 9 3 22 177.121 218.823 22.147 139.157 o 9 4 9 21.665 -15.076 28.909 146.236 o 9 4 10 25.085 45.544 23.811 212.060 o 9 4 11 136.242 141.033 25.341 144.965 o 9 4 12 170.200 195.944 25.209 125.397 o 9 4 13 120.308 100.389 27.811 134.422 o 9 4 14 126.193 138.432 23.533 166.667 o 9 4 15 16.442 22.790 21.751 257.012 o 9 4 16 1.055 26.142 20.644 286.885 o 9 4 17 74.740 70.341 19.782 273.086 o 9 4 18 94.685 128.412 18.846 257.909 o 9 4 19 157.280 140.201 17.692 219.337 o 9 4 20 449.406 477.001 25.392 42.352 o 9 4 21 49.729 31.600 24.277 200.954 o 9 4 22 0.920 -14.165 23.517 221.564 o 9 5 9 362.368 307.172 26.676 61.997 o 9 5 10 42.559 54.331 22.962 222.654 o 9 5 11 474.560 525.174 34.761 32.330 o 9 5 12 178.983 198.995 24.194 128.469 o 9 5 13 4.725 -2.032 22.302 246.326 o 9 5 14 48.536 59.848 21.719 244.605 o 9 5 15 142.710 189.442 21.813 164.774 o 9 5 16 781.586 854.676 64.778 10.999 o 9 5 17 48.856 39.281 18.559 334.156 o 9 5 18 267.716 267.163 22.646 95.882 o 9 5 19 196.826 185.359 31.028 90.038 o 9 5 20 158.125 153.617 22.375 160.623 o 9 5 21 145.940 144.870 19.639 200.135 o 9 6 9 37.234 49.549 25.718 180.294 o 9 6 10 116.793 65.568 27.338 143.548 o 9 6 11 158.774 240.335 30.300 95.152 o 9 6 12 80.753 98.956 27.696 144.563 o 9 6 13 5.955 11.234 20.771 283.606 o 9 6 14 0.185 -1.463 20.050 304.828 o 9 6 15 21.418 36.972 19.350 320.810 o 9 6 16 0.003 -26.038 18.131 372.754 o 9 6 17 279.703 304.236 34.686 58.655 o 9 6 18 33.168 21.289 25.230 189.780 o 9 6 19 25.923 -0.318 17.642 389.722 o 9 6 20 37.078 44.751 18.277 349.279 o 9 7 9 34.648 50.324 24.093 205.094 o 9 7 10 27.658 21.015 28.018 154.735 o 9 7 11 15.287 29.717 26.848 168.994 o 9 7 12 216.632 219.153 27.421 97.442 o 9 7 13 9.869 18.521 33.454 109.325 o 9 7 14 252.546 306.612 66.113 23.778 o 9 7 15 0.158 9.984 29.640 139.462 o 9 7 16 390.173 396.625 94.302 11.628 o 9 7 17 183.989 139.310 35.235 79.202 o 9 7 18 24.639 -0.466 24.664 200.486 o 9 7 19 155.306 65.902 28.589 124.311 o 9 8 9 73.022 58.669 32.349 111.781 o 9 8 10 1.584 -1.588 35.469 97.402 o 9 8 11 7.772 42.267 47.361 54.535 o 9 8 12 35.462 -0.426 44.778 60.933 o 9 8 13 10.862 25.163 43.343 65.137 o 9 8 14 0.283 6.000 40.605 74.320 o 9 8 15 85.969 64.452 38.821 77.880 o 9 8 16 315.168 172.181 37.036 57.349 o 9 8 17 99.469 49.557 31.554 114.628 o 9 8 18 77.669 19.898 14.595 491.177 o 9 9 9 0.201 32.812 52.040 45.226 o 9 9 10 126.330 171.386 46.025 52.550 o 9 9 11 65.954 24.245 41.923 68.591 o 9 9 12 17.599 2.891 39.599 78.060 o 9 9 13 3.925 37.830 37.379 87.551 o 9 9 14 387.701 247.463 39.663 43.516 o 9 9 15 95.760 23.760 31.623 116.145 o 9 9 16 261.643 151.665 17.447 144.923 o 9 10 9 294.862 134.231 127.886 7.218 o 9 10 10 318.753 221.486 22.114 89.737 o 9 10 11 259.089 203.103 37.329 60.922 o 9 10 12 6.031 -10.352 31.775 121.352 o 9 10 13 1.120 10.088 16.319 459.850 o 9 10 14 251.953 154.495 20.436 131.396 o 10 0 10 335.611 385.602 38.651 43.444 o 10 0 12 10.384 32.389 31.702 121.525 o 10 0 14 26.353 48.637 29.035 143.281 o 10 0 16 336.162 386.951 41.930 39.643 o 10 0 18 9.679 -0.265 26.771 170.873 o 10 1 10 105.770 115.975 24.338 170.253 o 10 1 11 3.182 32.531 23.219 226.541 o 10 1 12 332.875 411.388 26.796 58.457 o 10 1 13 23.175 62.787 24.219 203.997 o 10 1 14 262.788 310.175 26.341 80.430 o 10 1 15 4.467 -0.541 21.623 262.042 o 10 1 16 5.341 31.861 20.025 303.969 o 10 1 17 8.202 15.568 18.325 363.621 o 10 1 18 102.790 125.173 20.282 226.383 o 10 1 19 3.038 2.780 20.936 279.512 o 10 2 10 144.958 200.809 25.012 134.417 o 10 2 11 27.850 23.727 22.872 230.945 o 10 2 12 222.576 259.952 28.528 87.252 o 10 2 13 24.686 27.263 21.055 272.138 o 10 2 14 53.684 35.075 22.596 229.194 o 10 2 15 87.263 103.528 21.713 217.534 o 10 2 16 23.362 45.336 19.925 301.025 o 10 2 17 130.736 164.539 19.196 209.806 o 10 2 18 16.996 8.224 15.526 503.940 o 10 2 19 167.204 155.781 25.181 133.268 o 10 3 10 195.743 205.245 24.486 119.835 o 10 3 11 33.859 35.099 22.332 239.673 o 10 3 12 79.265 59.448 21.622 233.871 o 10 3 13 8.771 18.692 20.477 291.155 o 10 3 14 3.161 -16.574 19.728 314.814 o 10 3 15 6.831 -8.373 18.156 371.503 o 10 3 16 1.288 -0.367 18.681 351.136 o 10 3 17 38.680 37.349 16.944 404.799 o 10 3 18 75.621 57.055 24.024 194.913 o 10 4 10 56.084 58.869 28.185 147.792 o 10 4 11 99.865 103.304 21.882 208.433 o 10 4 12 37.595 9.350 20.352 289.909 o 10 4 13 231.442 352.754 30.131 72.160 o 10 4 14 6.602 22.375 18.110 371.928 o 10 4 15 12.988 5.262 16.483 449.110 o 10 4 16 17.363 24.628 15.614 494.145 o 10 4 17 62.282 79.509 15.806 409.433 o 10 5 10 175.022 212.366 28.376 103.767 o 10 5 11 53.664 102.104 25.908 169.410 o 10 5 12 538.400 518.761 49.205 22.504 o 10 5 13 645.829 835.064 43.508 16.865 o 10 5 14 282.177 290.953 30.308 68.550 o 10 5 15 110.303 85.427 18.991 259.663 o 10 5 16 135.501 112.241 29.362 118.212 o 10 6 10 299.776 299.894 52.759 32.725 o 10 6 11 0.101 12.178 45.397 59.455 o 10 6 12 25.798 42.136 42.394 67.789 o 10 6 13 100.261 91.388 39.473 73.850 o 10 6 14 45.473 -8.695 35.742 95.188 o 10 6 15 69.255 52.543 32.566 111.005 o 10 7 10 90.996 124.916 43.995 59.849 o 10 7 11 13.268 10.732 40.055 76.298 o 10 7 12 0.961 0.654 38.937 80.827 o 10 7 13 171.956 119.617 37.520 73.687 o 10 7 14 35.823 9.219 30.643 129.434 o 10 8 10 212.939 197.759 39.139 61.458 o 10 8 11 213.231 152.349 37.212 68.737 o 10 8 12 242.425 185.754 33.465 74.083 o 11 0 11 39.065 63.362 31.330 121.888 o 11 0 13 247.100 311.294 33.081 65.701 o 11 1 11 434.191 537.182 32.845 35.772 o 11 1 12 3.326 -3.743 19.490 322.556 o 11 1 13 1.770 21.090 17.623 393.634 o 11 2 11 103.172 184.020 32.769 97.657 o 11 2 12 42.443 53.093 21.966 242.600 o 11 2 13 5.029 21.729 25.196 192.659 o 11 3 11 81.560 81.316 22.085 219.317 o 11 4 11 37.851 36.376 33.323 108.889 o ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x+1/2,y+1/2,-z+1/2 3 -x,-y,-z 4 x-1/2,-y-1/2,z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn N1 N 1.0453(2) 0.41075(14) 0.56274(7) 0.0233(5) Uani 1.000000 . C1 C 1.1892(2) 0.43914(17) 0.56481(9) 0.0260(6) Uani 1.000000 . H1a H 1.2103(2) 0.46370(17) 0.53606(9) 0.0312(7) Uiso 1.000000 R H1b H 1.2013(2) 0.48529(17) 0.58699(9) 0.0312(7) Uiso 1.000000 R C2 C 1.2910(3) 0.36714(17) 0.57636(10) 0.0290(6) Uani 1.000000 . H2a H 1.3852(3) 0.39125(17) 0.57759(10) 0.0348(8) Uiso 1.000000 R H2b H 1.2735(3) 0.34540(17) 0.60598(10) 0.0348(8) Uiso 1.000000 R C3 C 1.2846(3) 0.29197(19) 0.54450(10) 0.0343(7) Uani 1.000000 . H3a H 1.1927(3) 0.26491(19) 0.54470(10) 0.0412(8) Uiso 1.000000 R H3b H 1.2967(3) 0.31370(19) 0.51451(10) 0.0412(8) Uiso 1.000000 R C4 C 1.3938(3) 0.22458(19) 0.55578(10) 0.0347(7) Uani 1.000000 . H4a H 1.3856(13) 0.1777(6) 0.5344(4) 0.0520(10) Uiso 1.000000 GR H4b H 1.4852(3) 0.2507(4) 0.5550(6) 0.0520(10) Uiso 1.000000 GR H4c H 1.3811(12) 0.2019(9) 0.5852(3) 0.0520(10) Uiso 1.000000 GR C1A C 0.9712(2) 0.39396(16) 0.59882(9) 0.0225(6) Uani 1.000000 . C2A C 0.8417(3) 0.35687(16) 0.58453(9) 0.0228(6) Uani 1.000000 . C3A C 0.7498(3) 0.33073(16) 0.61496(8) 0.0232(6) Uani 1.000000 . H3Aa H 0.6637(3) 0.30594(16) 0.60582(8) 0.0278(7) Uiso 1.000000 R C4A C 0.7876(2) 0.34200(16) 0.65959(9) 0.0218(6) Uani 1.000000 . C5A C 0.7201(2) 0.31535(16) 0.69718(9) 0.0232(6) Uani 1.000000 . C6A C 0.8088(2) 0.33656(16) 0.73540(8) 0.0205(5) Uani 1.000000 . C7A C 0.7983(3) 0.31850(17) 0.77975(9) 0.0258(6) Uani 1.000000 . H7A H 0.7203(3) 0.28900(17) 0.78951(9) 0.0309(7) Uiso 1.000000 R C8A C 0.9042(3) 0.34444(17) 0.80971(9) 0.0276(6) Uani 1.000000 . H8A H 0.8984(3) 0.33216(17) 0.84000(9) 0.0331(7) Uiso 1.000000 R C9A C 1.0193(3) 0.38859(17) 0.79528(9) 0.0258(6) Uani 1.000000 . H9A H 1.0905(3) 0.40589(17) 0.81596(9) 0.0310(7) Uiso 1.000000 R C10A C 1.0299(3) 0.40704(16) 0.75140(9) 0.0248(6) Uani 1.000000 . H10A H 1.1070(3) 0.43805(16) 0.74206(9) 0.0298(7) Uiso 1.000000 R C11A C 0.9275(2) 0.38013(16) 0.72095(8) 0.0220(6) Uani 1.000000 . C12A C 0.9162(2) 0.38232(15) 0.67317(8) 0.0211(5) Uani 1.000000 . C13A C 1.0083(3) 0.40835(17) 0.64330(8) 0.0238(6) Uani 1.000000 . H13A H 1.0931(3) 0.43483(17) 0.65236(8) 0.0286(7) Uiso 1.000000 R C21A C 0.5852(2) 0.27146(16) 0.69621(8) 0.0220(6) Uani 1.000000 . C22A C 0.5749(2) 0.18370(17) 0.68484(9) 0.0236(6) Uani 1.000000 . C23A C 0.4459(2) 0.14464(16) 0.68157(9) 0.0248(6) Uani 1.000000 . H23A H 0.4400(2) 0.08522(16) 0.67458(9) 0.0298(7) Uiso 1.000000 R C24A C 0.3248(2) 0.18995(17) 0.68823(9) 0.0241(6) Uani 1.000000 . C25A C 0.3376(3) 0.27607(17) 0.69991(9) 0.0244(6) Uani 1.000000 . H25A H 0.2569(3) 0.30790(17) 0.70507(9) 0.0293(7) Uiso 1.000000 R C26A C 0.4649(2) 0.31748(16) 0.70432(8) 0.0214(5) Uani 1.000000 . C27A C 0.7026(3) 0.13007(17) 0.67860(10) 0.0279(6) Uani 1.000000 . H27A H 0.7817(3) 0.17057(17) 0.67661(10) 0.0334(8) Uiso 1.000000 R C28A C 0.1868(3) 0.14569(17) 0.68310(10) 0.0282(6) Uani 1.000000 . H28A H 0.2041(3) 0.08234(17) 0.68340(10) 0.0339(7) Uiso 1.000000 R C29A C 0.4718(3) 0.41060(16) 0.72000(9) 0.0249(6) Uani 1.000000 . H29A H 0.5687(3) 0.43084(16) 0.71807(9) 0.0299(7) Uiso 1.000000 R C30A C 0.7333(3) 0.07242(19) 0.71867(11) 0.0376(8) Uani 1.000000 . H30a H 0.6531(8) 0.0363(9) 0.7235(4) 0.0564(11) Uiso 1.000000 GR H30b H 0.8127(13) 0.0358(9) 0.7136(3) 0.0564(11) Uiso 1.000000 GR H30c H 0.754(2) 0.10830(18) 0.74458(16) 0.0564(11) Uiso 1.000000 GR C31A C 0.6924(3) 0.0772(2) 0.63636(11) 0.0416(8) Uani 1.000000 . H31a H 0.7797(8) 0.0474(11) 0.6328(4) 0.0624(12) Uiso 1.000000 GR H31b H 0.6184(15) 0.0349(9) 0.6379(3) 0.0624(12) Uiso 1.000000 GR H31c H 0.673(2) 0.1154(3) 0.61129(13) 0.0624(12) Uiso 1.000000 GR C32A C 0.1115(3) 0.1677(2) 0.63915(10) 0.0369(7) Uani 1.000000 . H32a H 0.0262(11) 0.1343(10) 0.6358(3) 0.0554(11) Uiso 1.000000 GR H32b H 0.0896(18) 0.2292(3) 0.6383(3) 0.0554(11) Uiso 1.000000 GR H32c H 0.1704(9) 0.1537(12) 0.61519(10) 0.0554(11) Uiso 1.000000 GR C33A C 0.0948(3) 0.16572(18) 0.72057(10) 0.0334(7) Uani 1.000000 . H33a H 0.0689(16) 0.2266(3) 0.7195(4) 0.0501(10) Uiso 1.000000 GR H33b H 0.0118(9) 0.1301(9) 0.7177(4) 0.0501(10) Uiso 1.000000 GR H33c H 0.1447(7) 0.1534(11) 0.74863(10) 0.0501(10) Uiso 1.000000 GR C34A C 0.3789(3) 0.46978(17) 0.69120(9) 0.0284(6) Uani 1.000000 . H34a H 0.4023(13) 0.4642(9) 0.66056(12) 0.0426(9) Uiso 1.000000 GR H34b H 0.2826(3) 0.4535(8) 0.6939(5) 0.0426(9) Uiso 1.000000 GR H34c H 0.3925(14) 0.5295(2) 0.7007(4) 0.0426(9) Uiso 1.000000 GR C35A C 0.4363(3) 0.41581(17) 0.76817(9) 0.0294(6) Uani 1.000000 . H35a H 0.3430(8) 0.3939(11) 0.77119(13) 0.0441(10) Uiso 1.000000 GR H35b H 0.5018(12) 0.3811(9) 0.78615(12) 0.0441(10) Uiso 1.000000 GR H35c H 0.4413(18) 0.4758(2) 0.77797(19) 0.0441(10) Uiso 1.000000 GR C1B C 0.9701(2) 0.38595(16) 0.52503(8) 0.0227(6) Uani 1.000000 . C2B C 0.8410(2) 0.35195(16) 0.53722(8) 0.0228(6) Uani 1.000000 . C3B C 0.7475(2) 0.32001(16) 0.50549(9) 0.0234(6) Uani 1.000000 . H3Ba H 0.6616(2) 0.29744(16) 0.51327(9) 0.0280(7) Uiso 1.000000 R C4B C 0.7824(2) 0.32171(16) 0.46158(9) 0.0223(6) Uani 1.000000 . C5B C 0.7110(2) 0.28992(16) 0.42316(9) 0.0230(6) Uani 1.000000 . C6B C 0.7927(2) 0.30823(16) 0.38652(9) 0.0230(6) Uani 1.000000 . C7B C 0.7723(3) 0.28983(17) 0.34185(8) 0.0264(6) Uani 1.000000 . H7B H 0.6928(3) 0.25944(17) 0.33106(8) 0.0316(7) Uiso 1.000000 R C8B C 0.8709(3) 0.31694(18) 0.31332(9) 0.0295(6) Uani 1.000000 . H8B H 0.8583(3) 0.30437(18) 0.28292(9) 0.0355(8) Uiso 1.000000 R C9B C 0.9864(3) 0.36181(18) 0.32870(9) 0.0285(6) Uani 1.000000 . H9B H 1.0512(3) 0.38048(18) 0.30865(9) 0.0342(7) Uiso 1.000000 R C10B C 1.0092(3) 0.38008(17) 0.37338(9) 0.0248(6) Uani 1.000000 . H10B H 1.0882(3) 0.41148(17) 0.38365(9) 0.0298(7) Uiso 1.000000 R C11B C 0.9149(2) 0.35172(16) 0.40245(9) 0.0226(6) Uani 1.000000 . C12B C 0.9113(2) 0.35881(16) 0.44970(8) 0.0220(6) Uani 1.000000 . C13B C 1.0057(3) 0.39061(16) 0.48126(9) 0.0236(6) Uani 1.000000 . H13B H 1.0909(3) 0.41449(16) 0.47359(9) 0.0284(7) Uiso 1.000000 R C21B C 0.5758(2) 0.24529(16) 0.42275(8) 0.0224(6) Uani 1.000000 . C22B C 0.5711(2) 0.15725(17) 0.43403(8) 0.0242(6) Uani 1.000000 . C23B C 0.4425(2) 0.11738(17) 0.43504(9) 0.0250(6) Uani 1.000000 . H23B H 0.4389(2) 0.05783(17) 0.44175(9) 0.0300(7) Uiso 1.000000 R C24B C 0.3202(2) 0.16150(17) 0.42663(8) 0.0233(6) Uani 1.000000 . C25B C 0.3271(3) 0.24815(16) 0.41597(9) 0.0258(6) Uani 1.000000 . H25B H 0.2441(3) 0.27927(16) 0.41046(9) 0.0310(7) Uiso 1.000000 R C26B C 0.4531(2) 0.29127(16) 0.41309(9) 0.0243(6) Uani 1.000000 . C27B C 0.7010(3) 0.10608(18) 0.44481(9) 0.0297(6) Uani 1.000000 . H27B H 0.7809(3) 0.14558(18) 0.44173(9) 0.0356(8) Uiso 1.000000 R C28B C 0.1830(3) 0.11507(17) 0.42788(9) 0.0252(6) Uani 1.000000 . H28B H 0.2034(3) 0.05229(17) 0.43083(9) 0.0302(7) Uiso 1.000000 R C29B C 0.4542(3) 0.38484(17) 0.39953(10) 0.0309(7) Uani 1.000000 . H29B H 0.5525(3) 0.40208(17) 0.39734(10) 0.0370(8) Uiso 1.000000 R C30B C 0.7172(3) 0.0313(2) 0.41335(11) 0.0437(8) Uani 1.000000 . H30d H 0.8016(12) -0.0003(8) 0.4218(4) 0.0656(13) Uiso 1.000000 GR H30e H 0.6379(11) -0.0073(7) 0.4146(5) 0.0656(13) Uiso 1.000000 GR H30f H 0.722(2) 0.0534(2) 0.38344(15) 0.0656(13) Uiso 1.000000 GR C31B C 0.7062(3) 0.0748(2) 0.49225(11) 0.0455(9) Uani 1.000000 . H31d H 0.6303(14) 0.0346(11) 0.4961(2) 0.0682(13) Uiso 1.000000 GR H31e H 0.7939(10) 0.0457(12) 0.4992(2) 0.0682(13) Uiso 1.000000 GR H31f H 0.698(2) 0.1241(3) 0.51190(12) 0.0682(13) Uiso 1.000000 GR C32B C 0.0927(3) 0.12693(18) 0.38581(9) 0.0304(7) Uani 1.000000 . H32d H 0.0120(10) 0.0895(9) 0.3865(3) 0.0456(10) Uiso 1.000000 GR H32e H 0.0628(15) 0.1870(3) 0.3834(3) 0.0456(10) Uiso 1.000000 GR H32f H 0.1453(6) 0.1120(11) 0.36049(10) 0.0456(10) Uiso 1.000000 GR C33B C 0.1048(3) 0.14158(18) 0.46791(10) 0.0320(7) Uani 1.000000 . H33d H 0.0827(17) 0.2030(3) 0.4660(3) 0.0480(10) Uiso 1.000000 GR H33e H 0.0196(10) 0.1082(9) 0.4685(3) 0.0480(10) Uiso 1.000000 GR H33f H 0.1621(8) 0.1305(11) 0.49471(10) 0.0480(10) Uiso 1.000000 GR C34B C 0.3820(3) 0.3972(2) 0.35418(10) 0.0393(8) Uani 1.000000 . H34d H 0.4339(12) 0.3673(11) 0.33220(14) 0.0590(12) Uiso 1.000000 GR H34e H 0.2888(8) 0.3734(12) 0.3541(2) 0.0590(12) Uiso 1.000000 GR H34f H 0.3772(18) 0.4586(2) 0.3472(3) 0.0590(12) Uiso 1.000000 GR C35B C 0.3934(3) 0.44256(19) 0.43405(11) 0.0396(8) Uani 1.000000 . H35d H 0.2967(7) 0.4274(9) 0.4370(5) 0.0595(11) Uiso 1.000000 GR H35e H 0.4447(14) 0.4344(10) 0.46228(19) 0.0595(11) Uiso 1.000000 GR H35f H 0.4000(19) 0.5028(2) 0.4250(3) 0.0595(11) Uiso 1.000000 GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 N1 0.0191(11) 0.0271(12) 0.0237(12) -0.0048(9) 0.0009(8) -0.0015(9) C1 0.0151(12) 0.0313(15) 0.0317(16) -0.0099(11) 0.0024(10) -0.0007(12) C2 0.0226(14) 0.0310(15) 0.0336(16) -0.0024(12) 0.0024(11) -0.0010(12) C3 0.0329(16) 0.0337(16) 0.0359(17) -0.0000(13) -0.0027(12) -0.0037(13) C4 0.0251(14) 0.0366(16) 0.0425(18) 0.0006(13) 0.0025(12) -0.0048(14) C1A 0.0185(13) 0.0205(13) 0.0286(15) 0.0003(11) 0.0015(10) -0.0008(11) C2A 0.0224(13) 0.0207(13) 0.0254(14) -0.0010(11) 0.0011(10) 0.0004(11) C3A 0.0200(13) 0.0238(13) 0.0258(14) -0.0025(11) 0.0016(10) -0.0007(11) C4A 0.0193(12) 0.0179(12) 0.0280(15) 0.0001(11) 0.0002(10) 0.0005(10) C5A 0.0218(13) 0.0201(13) 0.0274(15) 0.0007(11) -0.0006(10) -0.0010(11) C6A 0.0149(12) 0.0194(12) 0.0275(14) 0.0003(10) 0.0026(10) -0.0021(10) C7A 0.0209(13) 0.0249(14) 0.0316(15) -0.0002(11) 0.0028(11) 0.0003(11) C8A 0.0289(14) 0.0288(15) 0.0247(15) 0.0009(12) -0.0010(11) 0.0007(11) C9A 0.0194(13) 0.0261(14) 0.0316(15) 0.0000(11) -0.0027(10) -0.0031(12) C10A 0.0210(13) 0.0221(13) 0.0311(15) -0.0014(11) 0.0003(11) -0.0038(11) C11A 0.0214(13) 0.0186(12) 0.0261(14) 0.0011(11) 0.0017(10) -0.0024(10) C12A 0.0219(13) 0.0172(12) 0.0243(14) 0.0011(11) 0.0012(10) -0.0015(10) C13A 0.0190(13) 0.0236(13) 0.0286(15) -0.0001(11) -0.0003(10) 0.0003(11) C21A 0.0184(13) 0.0231(13) 0.0245(14) -0.0002(11) 0.0015(10) -0.0003(11) C22A 0.0168(12) 0.0235(14) 0.0309(15) 0.0016(11) 0.0040(10) 0.0001(11) C23A 0.0244(13) 0.0174(13) 0.0326(16) 0.0008(11) 0.0015(11) -0.0023(11) C24A 0.0174(12) 0.0258(14) 0.0291(15) -0.0008(11) 0.0020(10) 0.0022(11) C25A 0.0205(13) 0.0226(13) 0.0302(15) -0.0000(11) 0.0020(10) 0.0000(11) C26A 0.0173(12) 0.0210(13) 0.0258(14) -0.0005(11) 0.0017(10) -0.0006(11) C27A 0.0199(13) 0.0214(13) 0.0424(18) 0.0016(11) 0.0027(11) -0.0022(12) C28A 0.0221(13) 0.0191(13) 0.0434(18) -0.0013(11) 0.0015(11) -0.0017(12) C29A 0.0215(13) 0.0207(13) 0.0323(15) -0.0027(11) -0.0004(11) -0.0028(11) C30A 0.0247(15) 0.0284(15) 0.059(2) -0.0002(13) -0.0036(13) 0.0062(14) C31A 0.0334(17) 0.0394(18) 0.052(2) 0.0030(14) 0.0055(14) -0.0144(15) C32A 0.0272(15) 0.0403(17) 0.0428(18) -0.0056(14) -0.0030(13) -0.0040(14) C33A 0.0229(14) 0.0299(15) 0.0477(19) -0.0030(13) 0.0044(12) 0.0004(13) C34A 0.0265(14) 0.0223(13) 0.0359(16) -0.0026(12) -0.0026(11) 0.0003(12) C35A 0.0265(14) 0.0234(14) 0.0377(17) -0.0010(12) -0.0027(12) -0.0075(12) C1B 0.0173(12) 0.0217(13) 0.0287(15) -0.0028(11) -0.0019(10) -0.0008(11) C2B 0.0197(13) 0.0237(13) 0.0251(14) -0.0027(11) 0.0026(10) 0.0014(11) C3B 0.0184(13) 0.0240(13) 0.0276(15) -0.0020(11) 0.0006(10) 0.0019(11) C4B 0.0163(12) 0.0214(13) 0.0292(15) -0.0020(11) 0.0005(10) 0.0008(11) C5B 0.0186(13) 0.0211(13) 0.0291(15) -0.0015(11) 0.0005(10) 0.0007(11) C6B 0.0213(13) 0.0205(13) 0.0268(14) 0.0015(11) -0.0015(10) -0.0010(11) C7B 0.0234(14) 0.0296(15) 0.0257(15) -0.0023(12) -0.0019(11) 0.0003(11) C8B 0.0282(14) 0.0328(15) 0.0280(15) 0.0023(12) 0.0044(11) -0.0019(12) C9B 0.0247(14) 0.0298(15) 0.0314(16) 0.0004(12) 0.0056(11) 0.0003(12) C10B 0.0235(13) 0.0240(13) 0.0272(15) 0.0008(11) 0.0032(10) 0.0031(11) C11B 0.0195(13) 0.0195(13) 0.0291(15) 0.0025(11) 0.0030(10) 0.0013(11) C12B 0.0210(13) 0.0189(12) 0.0260(14) 0.0001(10) 0.0005(10) 0.0002(11) C13B 0.0199(13) 0.0227(13) 0.0286(15) -0.0022(11) 0.0039(10) 0.0007(11) C21B 0.0203(13) 0.0250(13) 0.0219(13) -0.0021(11) 0.0018(10) -0.0010(10) C22B 0.0205(13) 0.0272(14) 0.0248(14) -0.0023(11) -0.0001(10) 0.0004(11) C23B 0.0200(13) 0.0210(13) 0.0338(16) -0.0045(11) 0.0010(11) 0.0028(11) C24B 0.0195(13) 0.0256(14) 0.0250(14) -0.0016(11) 0.0036(10) -0.0010(11) C25B 0.0186(13) 0.0243(14) 0.0345(16) 0.0001(11) 0.0010(11) -0.0020(11) C26B 0.0205(13) 0.0238(14) 0.0288(15) -0.0011(11) 0.0022(10) -0.0004(11) C27B 0.0234(14) 0.0280(14) 0.0374(17) 0.0017(12) -0.0010(11) 0.0039(12) C28B 0.0222(13) 0.0212(13) 0.0318(15) -0.0048(11) -0.0014(11) -0.0001(11) C29B 0.0250(14) 0.0243(14) 0.0432(18) 0.0010(12) 0.0015(12) 0.0048(13) C30B 0.0321(16) 0.0386(18) 0.060(2) 0.0090(14) -0.0061(14) -0.0081(16) C31B 0.0320(17) 0.057(2) 0.047(2) 0.0084(16) -0.0018(14) 0.0196(17) C32B 0.0237(14) 0.0306(15) 0.0363(17) -0.0037(12) -0.0024(12) 0.0036(12) C33B 0.0260(14) 0.0301(15) 0.0400(18) -0.0019(13) 0.0030(12) -0.0028(13) C34B 0.0288(15) 0.0397(18) 0.050(2) -0.0004(14) 0.0024(13) 0.0166(15) C35B 0.0345(17) 0.0260(15) 0.059(2) -0.0003(13) 0.0061(14) 0.0001(14) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source C 0.01920 0.00962 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.03256 0.01839 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.52900 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code 0 0 2 87.6133 16.3792 6 0 0 2 111.955 12.7781 14 0 0 3 13.5486 23.7211 6 0 0 3 2.44414 16.9226 14 0 0 4 1423.42 89.0883 6 0 0 4 1288.71 85.519 14 0 0 5 -2.40604 39.6881 6 0 0 -5 6.54603 18.502 5 0 0 5 2.67639 27.0332 14 0 0 -6 8870.56 551.156 5 0 0 6 9050.79 552.257 14 0 0 6 9333.17 554.055 6 0 0 7 18.2767 34.363 14 0 0 -7 15.2019 24.3403 5 0 0 7 -30.4354 52.2878 6 0 0 -8 72576.9 4439.94 5 0 0 8 71792.2 4440.86 14 0 0 8 72863.6 4441.92 6 0 0 9 -6.79834 37.696 14 0 0 -9 -21.4211 29.2919 5 0 0 9 -14.1416 62.3336 6 0 0 -10 5924.78 366.4 5 0 0 10 5871.67 367.839 14 0 0 10 6178.03 372.835 6 0 0 11 5.55343 65.8817 6 0 0 -11 4.30842 31.8395 5 0 0 11 8.74676 39.4348 14 0 0 -12 51.945 33.0742 5 0 0 12 44.9903 38.9933 14 0 0 -13 6.46239 33.979 5 0 0 13 13.4161 39.2777 14 0 0 -14 2157.11 137.088 21 0 0 14 2442.26 157.016 6 0 0 14 2263.13 142.655 14 0 0 -15 4.30641 19.8571 21 0 0 15 4.09069 39.5125 14 0 0 15 -9.21773 75.3011 6 0 0 16 2264.25 165.511 6 0 0 17 -17.2158 82.7515 6 0 0 18 448.149 49.9114 14 0 0 18 563.07 92.5299 6 0 0 19 31.4024 42.0822 14 0 0 19 -36.678 87.7075 6 0 0 20 814.965 70.4501 14 0 0 20 1027.32 111.038 6 0 0 21 32.1463 94.5577 6 0 0 21 -19.671 48.089 14 0 0 22 1.9819 103.655 6 0 0 22 43.6245 46.4064 14 0 0 23 -144.718 97.2561 6 0 0 23 -16.5844 46.8008 14 0 0 24 879.647 119.102 6 0 0 24 897.74 76.9417 14 0 0 25 5.18689 98.9846 6 0 0 25 -50.791 49.9243 14 0 0 26 1155.27 113.645 6 0 0 26 641.116 90.9204 22 0 0 27 -70.0124 93.4432 6 0 0 27 60.5923 66.4417 22 0 0 28 372.06 65.9091 22 0 0 29 18.0756 93.4778 6 0 0 29 -26.4892 51.7479 22 0 0 30 -10.6368 87.8949 6 0 0 31 -36.7117 89.1173 6 0 0 31 20.6072 44.2613 22 0 0 32 135.036 83.8785 6 0 0 33 -27.0031 79.0628 6 0 0 34 158.308 72.0896 6 0 0 35 -34.7609 63.2243 6 0 0 36 233.84 58.2092 6 0 0 -37 -13.8042 33.6875 15 0 -1 -1 10160.7 626.101 2 0 1 1 11662.5 626.36 2 0 -1 1 10374.3 625.4 19 0 1 -1 9579.27 625.457 11 0 1 1 12746.6 626.875 8 0 -1 -1 9299.02 625.715 6 0 -1 -2 197.059 35.1771 2 0 1 2 219.034 32.431 2 0 -1 -2 135.908 22.4378 6 0 1 2 163.003 21.6658 6 0 -1 2 170.821 12.7566 19 0 1 -2 180.896 12.6479 11 0 1 2 207.375 32.0636 8 0 -1 3 -0.26416 14.9238 14 0 -1 3 -9.22291 25.3333 5 0 1 3 -4.05337 29.8756 6 0 -1 3 14.6948 14.0265 19 0 1 3 12.7864 33.1158 8 0 1 3 -2.14026 34.3621 2 0 1 4 54315 3306.93 14 0 -1 4 60013.4 3306.64 14 0 -1 4 50880.4 3306.55 5 0 -1 -4 50816.8 3306.06 10 0 1 4 61512.3 3307.49 6 0 -1 4 59816.7 3306.7 19 0 -1 5 2671.3 166.286 19 0 -1 5 2508.21 165.101 14 0 1 5 2560.83 167.48 14 0 1 5 2803.85 170.742 6 0 1 -5 2696.8 163.457 20 0 -1 6 8346.19 532.984 19 0 1 -6 8752.58 530.928 20 0 -1 6 8549.95 532.068 14 0 1 6 8569.59 532.991 14 0 1 6 8699.61 535.172 6 0 1 -7 261.815 20.7805 20 0 1 7 274.016 41.8886 14 0 -1 7 253.069 34.6017 14 0 -1 7 259.795 46.9557 19 0 1 7 281.793 61.6783 6 0 1 -8 805.669 50.3444 20 0 -1 8 959.943 71.1872 6 0 -1 8 894.97 59.3446 14 0 -1 9 1224.99 89.3454 6 0 1 9 1236.51 96.8705 6 0 -1 9 995.792 76.6406 14 0 1 9 1102.42 80.1149 14 0 -1 10 2612.02 164.705 6 0 1 10 2584.59 169.009 6 0 1 10 2440.44 157.58 14 0 -1 10 2356.42 155.8 14 0 1 11 12.3919 73.0489 6 0 -1 -11 12.3859 27.1355 5 0 -1 11 -40.4786 66.8201 6 0 -1 11 -5.25468 35.7521 14 0 1 11 2.88926 42.0537 14 0 -1 -12 1228.17 74.9448 21 0 1 12 1362.63 86.343 14 0 -1 12 1354.61 83.4335 14 0 -1 -13 64.5956 15.5698 21 0 -1 -13 90.0415 27.486 5 0 -1 13 92.396 37.8111 14 0 1 13 69.3091 42.3255 14 0 1 -14 3179.13 192.806 21 0 -1 14 2958.41 196.024 14 0 1 14 2875.55 197.04 14 0 -1 14 3309.58 207.051 6 0 1 14 3380.22 209.55 6 0 1 -15 2021.29 126.495 21 0 1 15 2179.13 151.092 6 0 -1 15 2121.66 147.54 6 0 -1 15 1931.82 131.403 14 0 1 15 1960.88 132.871 14 0 1 -16 77.1727 23.229 21 0 -1 16 78.5737 75.6349 6 0 1 16 98.2526 82.3022 6 0 -1 17 1591.91 126.367 6 0 1 17 1576.33 128.001 6 0 1 -17 1482.02 96.2769 21 0 1 18 35.365 40.8298 14 0 -1 18 17.957 42.0564 14 0 1 18 87.1747 88.7224 6 0 -1 18 21.8139 81.37 6 0 1 19 727.153 102.782 6 0 -1 19 719.448 62.9526 14 0 1 19 658.675 62.5003 14 0 -1 19 853.369 99.5881 6 0 -1 20 687.684 63.1669 14 0 1 20 670.846 63.2589 14 0 1 20 831.135 100.93 6 0 -1 20 779.551 104.249 6 0 1 21 -38.1537 45.8968 14 0 -1 21 61.129 44.3586 14 0 1 21 -13.7374 89.1763 6 0 -1 21 -63.9907 96.1748 6 0 1 22 1210.11 91.6518 14 0 -1 22 1154.87 90.0284 14 0 -1 22 1242.36 130.204 6 0 1 22 1387.2 123.659 6 0 -1 23 307.73 54.2493 14 0 1 23 464.149 57.9233 14 0 1 23 376.685 94.5001 6 0 -1 23 489.645 110.418 6 0 1 24 656.932 81.1149 22 0 1 24 706.068 68.6419 14 0 1 24 743.278 106.018 6 0 -1 24 794.482 117.855 6 0 1 25 2.4755 65.7071 22 0 1 25 -0.48865 47.8828 14 0 1 25 50.5617 94.4837 6 0 -1 25 8.87416 104.584 6 0 1 26 26.7277 58.5515 22 0 1 26 -5.99859 48.3218 14 0 -1 26 36.4333 98.5215 6 0 1 26 2.00828 89.5819 6 0 1 27 309.774 57.7194 22 0 -1 27 134.889 72.5651 22 0 1 27 222.999 52.7835 14 0 -1 27 252.237 101.671 6 0 1 27 264.015 95.7543 6 0 1 28 52.5067 49.7644 22 0 -1 28 13.7468 68.1028 22 0 -1 29 4.66552 64.7401 22 0 -1 29 2.07302 95.4416 6 0 1 29 -38.4034 91.6702 6 0 -1 30 56.3354 93.3222 6 0 1 30 -48.4779 90.5048 6 0 -1 31 70.8365 49.8648 22 0 -1 31 158.086 90.7351 6 0 1 31 153.419 86.5642 6 0 -1 32 2.5834 43.8642 22 0 1 32 85.5746 83.9118 6 0 -1 32 147.595 85.1515 6 0 -1 33 25.314 38.6565 22 0 1 33 60.9289 78.0812 6 0 -1 33 7.01153 77.2485 6 0 -1 34 -14.2752 34.794 22 0 1 34 -63.5948 68.9275 6 0 -1 34 -41.2236 73.2728 6 0 1 35 -22.409 61.7855 6 0 -1 35 -25.2981 63.7759 6 0 -1 36 188.402 58.0241 6 0 1 -37 55.2588 35.2492 15 0 -1 -37 61.778 32.8114 15 0 2 0 48275.4 2919.05 2 0 2 0 47339.6 2918.45 1 0 -2 1 8262.82 531.844 19 0 2 1 9234.15 533.468 2 0 2 1 9598.17 534.352 8 0 -2 2 225.727 19.7948 19 0 2 2 270.8 47.712 8 0 2 2 167.932 13.8754 21 0 2 2 290.388 53.2808 2 0 2 3 1311.95 83.0325 8 0 2 3 1041.69 71.3495 6 0 2 -3 1105.78 65.8368 11 0 2 3 948.227 62.5648 22 0 -2 3 1122.25 64.6502 19 0 2 3 1521.02 85.2155 2 0 2 3 735.039 65.826 3 0 2 4 624.154 62.6447 8 0 2 4 519.131 49.835 6 0 2 -4 468.584 35.8954 11 0 2 4 378.806 33.3993 22 0 2 4 670.569 66.4857 2 0 -2 4 526.603 35.6364 19 0 2 5 77454.8 4274.82 8 0 2 5 63811.2 4273.4 6 0 2 -5 69534.7 4272.45 11 0 -2 5 68661.9 4272.74 19 0 2 5 76319.1 4274.52 2 0 -2 6 327.008 34.5469 19 0 -2 6 329.952 33.4283 14 0 2 6 325.362 48.358 14 0 2 6 468.968 66.8942 2 0 2 6 286.236 22.5828 20 0 2 -6 328.175 27.2343 20 0 2 6 319.973 54.078 6 0 2 6 341.977 61.1925 8 0 -2 7 616.77 44.1647 14 0 2 7 503.619 55.7763 14 0 -2 7 603.564 47.3015 19 0 2 7 558.078 64.4306 6 0 2 7 458.406 32.6889 20 0 2 -7 577.555 36.769 20 0 2 8 11558.8 737.462 14 0 -2 8 12171.5 736.112 14 0 -2 8 12444.1 736.936 19 0 2 8 11927.4 739.211 6 0 2 -8 11869.5 734.968 20 0 2 9 1130.39 86.0539 14 0 -2 9 1218.86 79.7785 14 0 -2 9 1213.56 86.7588 19 0 2 9 1261.46 95.6194 6 0 2 -9 1132.14 73.822 20 0 -2 10 3907.24 221.333 14 0 2 10 3348.71 222.774 14 0 -2 10 3583.21 225.629 19 0 2 -10 3445.54 218.189 20 0 2 10 3696.73 230.143 6 0 -2 11 967.076 68.5656 14 0 2 11 812.631 73.3258 14 0 2 11 954.904 91.6775 6 0 -2 11 1003.2 82.9509 6 0 2 12 174.838 45.715 14 0 -2 12 180.053 37.8519 14 0 2 13 3897.54 252.092 14 0 -2 13 3929.1 250.437 14 0 2 13 4166.04 259.554 6 0 -2 13 4244.04 257.687 6 0 -2 14 1185.73 85.8694 14 0 2 14 1137.83 88.8629 14 0 2 14 1425.54 107.685 6 0 -2 14 1409.8 108.071 6 0 2 -15 3854.86 236.688 21 0 2 15 4046.56 249.932 6 0 -2 15 4104.77 250.97 6 0 2 15 3637.97 240.723 14 0 -2 15 3702.57 239.072 14 0 2 -16 12.2097 24.7465 21 0 -2 16 37.1698 75.8286 6 0 2 16 73.8734 75.2152 6 0 2 -17 181.23 29.2451 21 0 -2 17 296.654 79.7623 6 0 2 17 183.168 77.999 6 0 -2 17 206.613 41.119 14 0 2 17 183.043 45.3479 14 0 2 -18 509.169 42.902 21 0 2 18 552.017 56.0961 14 0 -2 18 540.632 53.252 14 0 -2 18 623.953 92.2777 6 0 2 18 586.417 88.1065 6 0 -2 19 848.507 67.9005 14 0 2 19 731.784 68.907 14 0 2 19 939.141 100.073 6 0 -2 19 868.084 103.216 6 0 2 20 -11.4778 82.1935 6 0 -2 20 -101.99 89.8812 6 0 -2 20 49.1421 42.784 14 0 2 20 54.778 43.4818 14 0 -2 21 3301.44 198.677 6 0 2 21 3235.4 191.772 6 0 2 21 2686.41 173.61 14 0 2 22 44.1767 58.9034 22 0 2 22 2.56012 87.8374 6 0 -2 22 114.405 99.1246 6 0 2 22 46.9867 46.7676 14 0 2 23 3864.12 234.244 22 0 2 23 3785.82 245.983 6 0 -2 23 3939.38 252.919 6 0 2 23 3248.78 229.863 14 0 2 24 644.688 71.0863 22 0 2 24 840.69 105.434 6 0 2 24 739.303 71.3671 14 0 -2 24 962.25 118.37 6 0 2 25 808.797 79.8532 22 0 2 25 1026.25 81.6179 14 0 2 25 996.277 111.403 6 0 -2 25 1082.3 124.481 6 0 2 26 1916.78 141.767 14 0 2 26 2353.98 165.491 6 0 -2 26 2415.15 178.909 6 0 2 27 98.1982 50.5775 14 0 2 28 66.7723 48.6817 14 0 -2 28 85.701 68.5345 22 0 -2 29 207.838 70.8529 22 0 2 29 357.758 91.412 6 0 -2 29 331.35 102.021 6 0 -2 30 52.6448 93.191 6 0 2 30 210.311 86.318 6 0 2 31 757.823 92.985 6 0 -2 31 647.97 98.9064 6 0 -2 32 123.971 49.2972 22 0 2 32 272.402 82.5763 6 0 -2 32 163.374 87.0813 6 0 -2 33 -42.0925 41.6055 22 0 2 33 13.5174 73.6134 6 0 -2 33 -49.4747 78.5493 6 0 -2 34 49.7928 36.079 22 0 -2 34 33.4782 71.9041 6 0 -2 35 65.0935 31.8797 22 0 -2 35 143.71 64.9541 6 0 -2 36 0.41284 25.9201 22 0 -2 36 75.3944 55.5765 6 0 2 -37 1185.68 44.0902 15 0 2 37 -2.28054 32.9735 17 0 3 1 15193.6 790.722 2 0 3 -1 12583.5 787.679 15 0 3 1 12505.9 787.633 17 0 3 1 14852.4 791.403 8 0 -3 1 13121.8 788.308 19 0 -3 2 358.067 34.551 19 0 3 2 589.674 65.2814 2 0 3 2 439.325 29.9022 17 0 3 2 429.3 29.4 21 0 3 2 661.414 75.9717 8 0 3 3 712.651 48.6848 3 0 3 3 1048.91 88.5675 2 0 3 3 779.132 46.2721 18 0 3 3 1031.94 86.0671 8 0 -3 3 745.93 50.2265 19 0 3 3 650.489 46.171 21 0 -3 4 2096.37 116.384 19 0 3 4 1703.9 113.612 18 0 3 4 2424.3 135.949 8 0 3 4 2118.33 117.914 3 0 3 4 2694.32 139.514 2 0 3 5 3714.04 205.197 6 0 3 5 4666.26 215.908 2 0 -3 5 3933.01 201.039 19 0 3 -5 3478.04 201.869 11 0 3 5 3126.24 198.622 18 0 3 5 2875.87 199.152 22 0 3 5 4351.88 213.958 8 0 3 6 2772.96 169.114 2 0 -3 6 2550.84 155.08 19 0 3 -6 2457.81 155.487 11 0 3 6 2565.17 161.651 6 0 3 6 2355.35 153.104 22 0 3 6 2889.6 169.41 8 0 3 7 3126.53 179.233 2 0 3 7 2922.97 175.868 8 0 3 -7 2604.41 163.869 11 0 3 7 2778.84 171.837 6 0 3 7 2738.83 162.934 22 0 3 7 2311.74 161.599 20 0 3 -7 2854.94 163.069 20 0 -3 7 2861.84 164.685 19 0 3 8 1196.75 80.183 14 0 3 -8 1282.28 69.4017 11 0 3 8 1384.06 85.7593 6 0 3 8 1202.35 69.4678 22 0 3 -8 1313.26 67.4417 20 0 3 8 1076.84 63.8135 20 0 -3 8 1397.19 73.3498 19 0 3 9 6745.06 396.947 14 0 3 -9 6982.76 393.374 11 0 3 9 7369.05 398.83 6 0 3 9 5377.54 394.414 22 0 3 -9 7248.86 392.986 20 0 3 9 5885.79 391.879 20 0 -3 9 7118.79 395.351 19 0 3 10 2363.05 149.72 14 0 3 10 2392.83 153.824 6 0 3 -10 2286.57 142.165 11 0 3 -10 2411.57 141.045 20 0 -3 10 2298.78 147.438 19 0 3 11 210.739 49.8808 14 0 3 -11 205.694 32.4739 11 0 -3 11 183.083 52.1924 19 0 3 -11 180.321 24.5068 20 0 3 11 161.1 40.9811 22 0 3 -12 1400.44 87.3692 20 0 3 12 1131.33 94.6855 22 0 3 -12 1452.33 90.6277 11 0 -3 12 1546.18 103.355 19 0 3 12 1237.67 98.3009 14 0 3 13 299.061 69.8973 6 0 3 13 284.645 50.2525 14 0 3 13 339.146 47.0554 22 0 3 -13 311.353 36.1827 11 0 -3 13 359.238 64.9299 6 0 3 14 6970.78 436.567 14 0 3 14 6097.6 435.553 22 0 3 -14 7182.56 433.551 11 0 3 14 7754.51 440.977 6 0 -3 14 7951.54 440.757 6 0 3 15 6286.81 406.018 22 0 3 -15 6774.02 403.902 21 0 -3 15 6990.64 412.158 6 0 3 15 6703.96 411.98 6 0 3 15 6071.88 406.646 14 0 -3 16 69.1813 78.7963 6 0 3 16 57.3202 45.4836 22 0 3 -16 124.421 29.3807 21 0 3 16 122.063 69.3022 6 0 3 -17 2781.18 179.597 21 0 3 17 2945.87 183.905 22 0 -3 17 3312.22 198.99 6 0 3 17 2984.99 194.654 6 0 3 17 2663.49 183.973 14 0 3 18 28.5933 47.7504 22 0 3 18 -13.7935 74.5549 6 0 -3 18 59.0407 81.7831 6 0 3 18 55.7742 45.3582 14 0 3 -19 1888.42 124.302 21 0 3 19 2124.69 147.665 6 0 -3 19 2091.03 152.216 6 0 3 19 1910.58 131.199 14 0 3 -20 516.725 45.2127 21 0 3 20 465.033 58.18 14 0 -3 20 523.494 99.0635 6 0 3 20 495.641 86.8742 6 0 3 21 184.651 49.2778 14 0 3 21 233.001 82.1026 6 0 -3 21 202.843 93.3929 6 0 3 22 4006.11 271.393 14 0 -3 22 4678.13 288.593 6 0 3 22 4710.4 284.177 6 0 3 23 541.968 62.3794 14 0 -3 23 596.616 110.479 6 0 3 23 573.797 97.6731 6 0 3 24 357.448 57.0011 14 0 3 24 329.746 92.2163 6 0 -3 24 337.996 109.255 6 0 3 25 3808.67 262.188 14 0 -3 25 4644.29 284.548 6 0 3 25 4540.61 277.393 6 0 3 26 1440.11 111.94 14 0 -3 26 1722.16 152.351 6 0 3 26 1649.58 137.673 6 0 3 27 1231.76 95.2354 14 0 -3 28 315.266 113.179 6 0 3 28 282.531 92.5089 6 0 3 28 262.074 50.7863 14 0 -3 29 -3.30392 99.6615 6 0 3 29 -27.9638 84.8345 6 0 3 29 14.8723 47.619 14 0 -3 29 25.7079 66.4017 22 0 3 30 50.1938 83.7713 6 0 -3 30 44.4518 100.085 6 0 -3 31 232.483 92.0923 6 0 3 31 240.107 81.4414 6 0 -3 31 57.8183 61.278 22 0 -3 32 152.141 85.0837 6 0 -3 32 75.6209 50.7929 22 0 -3 33 424.338 81.4301 6 0 -3 33 178.24 48.4003 22 0 -3 34 18.5874 70.2373 6 0 -3 34 33.7692 37.7738 22 0 -3 35 284.748 64.4765 6 0 -3 35 91.2256 34.5136 22 0 -3 36 48.7151 27.8912 22 0 3 36 0.93812 27.5995 17 0 3 -37 66.1723 31.9863 15 0 4 0 196858 11881.3 1 0 4 0 198421 11882.5 2 0 4 0 190304 11881.1 16 0 4 1 5847.14 426.104 2 0 -4 1 5129.3 422.12 19 0 4 1 5474.65 427.682 8 0 4 -1 8793.2 422.768 1 0 4 -1 6824.39 424.657 2 0 4 -1 6465.99 421.203 15 0 4 1 8018.97 421.508 21 0 4 2 224.302 81.5935 8 0 -4 2 93.381 27.1098 19 0 4 2 240.108 67.3185 2 0 4 2 105.033 18.4752 21 0 4 2 110.521 15.7833 17 0 4 3 1139.99 70.3384 17 0 4 3 1030.9 69.9953 21 0 -4 3 1128.05 73.2903 19 0 -4 4 38.0836 27.395 19 0 4 4 4.08809 82.6186 8 0 4 4 52.3712 15.8922 21 0 4 4 137.807 89.8268 2 0 4 4 55.2731 22.4115 3 0 4 5 48.3332 83.2839 2 0 -4 5 17.5958 27.9412 19 0 4 5 65.84 81.2599 8 0 4 5 37.1362 34.2326 3 0 -4 6 397.593 37.1944 19 0 4 6 361.048 83.7901 8 0 4 6 352.854 25.239 18 0 4 7 10.2548 22.2494 22 0 4 7 115.607 71.3983 2 0 4 7 118.494 54.2177 6 0 4 -7 115.762 27.9785 20 0 4 7 87.0765 20.5525 20 0 -4 7 96.0047 30.4307 19 0 4 7 76.9334 76.319 8 0 4 7 101.853 12.1142 18 0 4 8 119.49 21.9732 22 0 4 8 184.109 20.7824 20 0 4 -8 189.785 40.3902 11 0 4 8 188.643 74.8601 2 0 4 8 193.994 54.7221 6 0 4 8 177.188 15.2196 18 0 -4 8 139.735 34.7404 19 0 4 8 197.102 73.0851 8 0 4 -8 175.697 28.5616 20 0 -4 9 1101.56 70.148 19 0 4 9 974.959 79.1985 14 0 4 9 947.812 59.0634 18 0 4 -9 973.05 68.9637 11 0 4 9 896.971 60.2875 20 0 4 9 726.813 62.5987 22 0 4 -9 1094.21 64.403 20 0 4 9 1245.47 92.6107 8 0 4 9 1185.91 84.2174 6 0 4 -10 866.652 58.3382 11 0 4 10 803.568 71.1631 14 0 4 -10 862.358 53.0951 20 0 4 10 697.942 48.2917 20 0 4 10 631.198 52.1135 22 0 -4 10 876.598 61.4381 19 0 4 11 3885.36 238.754 6 0 4 11 3875.47 235.877 14 0 4 -11 3559.86 230.918 11 0 -4 11 3905.53 234.126 19 0 4 -11 3912.66 229.792 20 0 4 11 3440.56 229.824 22 0 4 -12 53.9999 24.3863 20 0 4 12 72.8508 50.3121 14 0 4 -12 50.9574 34.3892 11 0 -4 12 48.2764 49.2536 19 0 4 12 63.0509 62.7545 6 0 4 12 63.4796 27.0274 22 0 4 13 2065.08 143.791 14 0 4 -13 2069.21 137.693 11 0 -4 13 2131.36 146.187 19 0 4 -13 2162.23 135.852 20 0 4 13 2225.23 137.306 22 0 4 13 2394.13 150.782 6 0 4 -14 1547.7 104.564 21 0 4 14 1642.45 104.451 22 0 -4 14 1573.54 116.938 19 0 4 14 1519.21 111.338 14 0 4 14 1733.76 121.78 6 0 -4 15 1519.63 113.67 6 0 4 15 1388.96 115.522 6 0 4 -15 1387.23 94.5209 21 0 4 15 1497.14 95.8109 22 0 4 16 34.7053 70.6622 6 0 4 16 103.9 48.3739 14 0 -4 16 80.332 70.2523 6 0 4 17 -34.1845 72.3093 6 0 4 17 70.1686 46.9159 14 0 -4 17 -36.9558 77.7414 6 0 4 -18 1690.65 112.122 21 0 4 18 1863.21 134.364 6 0 4 18 1548.35 118.016 14 0 -4 19 26.7894 87.6396 6 0 4 19 37.9367 77.8485 6 0 4 19 20.9001 47.4466 14 0 4 -19 37.3427 32.5167 21 0 4 -20 1779.33 120.696 21 0 4 20 2015.6 145.932 6 0 -4 20 1966.61 150.691 6 0 4 20 1804.95 126.739 14 0 4 21 600.185 88.6181 6 0 -4 21 511.073 99.2444 6 0 4 -21 549.706 49.6271 21 0 4 21 443.316 60.8289 14 0 -4 22 40.8734 96.124 6 0 4 22 184.999 88.1087 6 0 4 -22 44.7442 38.5833 21 0 4 23 1790.93 134.318 14 0 -4 23 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410.507 30.3113 17 2 3 0 105.588 38.3338 18 2 3 0 93.1092 38.6111 17 2 3 0 127.014 50.2943 16 2 -3 0 295.989 40.7957 7 2 3 0 37.3685 76.3678 13 2 3 0 139.865 42.1729 1 2 3 0 170.072 39.1555 3 2 3 0 180.188 42.8036 4 2 3 0 149.062 44.8189 8 2 3 1 717.54 52.4083 17 2 -3 1 697.683 46.97 17 2 3 1 664.292 51.6129 18 2 3 1 754.706 67.3892 16 2 -3 1 682.521 51.6021 7 2 3 1 716.213 53.0009 12 2 3 1 499.862 86.0417 13 2 -3 1 696.182 49.9513 19 2 -3 1 836.908 51.3984 22 2 3 1 724.976 59.9107 4 2 3 1 569.876 53.2283 3 2 3 1 864.806 57.539 8 2 -3 2 258.13 41.3799 22 2 3 2 290.263 35.3346 17 2 3 2 264.001 31.9799 18 2 3 2 286.324 53.5856 16 2 3 2 303.151 23.0943 14 2 3 2 274.608 33.0743 12 2 -3 2 258.507 31.5557 19 2 -3 2 318.579 31.8382 7 2 3 2 363.882 55.4484 3 2 -3 3 2154.25 125.544 19 2 3 3 2104.28 135.79 16 2 3 3 2005.3 123.503 14 2 3 3 2043.91 127.053 17 2 3 3 1854.08 124.881 12 2 -3 3 1970.1 126.476 4 2 3 3 2177.66 131.698 3 2 -3 3 1765.61 129.802 22 2 -3 4 1810.22 107.095 19 2 3 4 1701.71 120.425 16 2 3 4 1786.71 105.747 14 2 -3 4 1794.08 107.638 4 2 3 4 1710.29 109.135 17 2 3 4 1522.5 105.901 12 2 3 5 818.88 56.6363 14 2 3 5 696.692 79.3096 13 2 3 5 835.744 64.4262 22 2 -3 5 811.893 58.468 19 2 -3 5 835.269 59.4608 4 2 3 6 25.6878 27.8078 14 2 3 6 -15.0259 57.4044 13 2 3 6 17.7571 37.9313 22 2 3 6 -34.446 41.5589 6 2 -3 6 7.28855 32.1871 19 2 -3 6 -18.8441 34.461 4 2 3 7 541.875 45.0439 14 2 3 7 559.373 56.9669 6 2 3 7 470.014 47.854 22 2 -3 7 533.155 48.0034 19 2 -3 7 655.529 49.9731 4 2 3 8 949.861 76.2681 6 2 3 8 948.537 66.8308 14 2 3 8 930.705 67.7992 22 2 -3 8 1062.29 63.4914 9 2 -3 8 923.202 71.0328 19 2 3 9 104.842 52.5402 6 2 -3 9 149.946 43.3322 19 2 3 9 30.1575 34.8499 22 2 3 9 167.122 34.7945 14 2 -3 9 158.067 24.1772 9 2 3 10 211.385 56.4913 6 2 3 10 152.239 37.6645 22 2 -3 10 240.11 50.6293 19 2 3 10 223.368 35.4562 14 2 -3 10 269.064 26.8475 9 2 3 11 282.869 45.01 22 2 -3 11 335.895 58.5041 19 2 -3 11 428.331 33.4889 9 2 3 11 479.922 43.6617 14 2 -3 12 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4 2033.71 108.533 19 -2 4 4 2152.74 141.708 8 2 4 -4 1622.31 113.13 9 2 4 -4 1766.51 113.025 15 2 -4 -4 1423.21 107.763 15 2 4 -4 1309.57 134.187 13 2 4 -4 1790.5 117.183 11 2 4 -4 1681.42 115.532 1 2 4 -4 1831.15 109.339 7 -2 4 4 1975.26 137.205 2 2 4 -4 1678.94 108.943 2 -2 4 3 3768.78 226.93 2 2 4 -3 4154.36 214.912 2 2 4 -3 3273.37 219.141 11 2 4 -3 2913.34 215.936 1 2 4 -3 3510.72 215.309 18 2 -4 -3 2963.42 213.137 16 2 4 -3 3454.04 216.647 15 2 4 -3 3369.16 228.41 13 -2 -4 3 3677.42 213.005 19 2 4 -3 3393.6 213.375 7 -2 4 3 4770.7 237.338 8 -2 -4 2 139.538 22.3725 19 2 4 -2 64.5562 30.222 18 2 -4 -2 110.502 26.7481 16 2 4 -2 165.432 41.3661 15 2 4 -2 132.988 78.9675 13 2 4 -2 126.434 41.2647 1 -2 4 2 241.588 69.5453 2 2 4 -2 112.759 41.5853 2 -2 4 2 174.632 80.938 8 2 4 -2 92.2127 56.6977 11 2 4 -1 6028.82 404.136 18 2 4 -1 6569.96 405.678 16 2 4 -1 6230.66 403.861 17 2 4 -1 6564.38 403.76 4 2 4 -1 7503.54 404.722 2 -2 4 1 6598.24 409.655 2 2 4 -1 6259.71 412.263 13 2 -4 -1 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3976.97 240.319 16 2 4 3 3472.83 233.066 14 2 4 3 3790.1 233.383 12 2 4 3 4658.53 246.017 13 2 -4 3 3965.54 233.24 7 2 -4 3 3745.9 233.959 19 2 4 3 4120.72 238.502 8 2 4 3 3698.94 234.392 17 2 4 3 3598.61 233.56 18 2 4 4 635.642 50.3598 14 2 4 4 693.213 87.7292 13 2 4 4 711.636 49.5299 12 2 4 4 632.478 50.8733 18 2 4 4 695.3 54.5653 17 2 -4 4 746.489 53.1996 19 2 4 4 575.206 64.4802 3 2 -4 4 770.951 49.4163 7 2 4 5 342.206 30.6069 12 2 -4 5 340.506 36.8383 19 2 4 5 306.029 32.1101 18 2 4 5 334.403 37.0743 17 2 -4 5 382.398 37.1961 4 2 4 5 317.631 34.7696 14 2 -4 6 -0.09811 28.6493 4 2 4 6 47.5215 71.5045 13 2 4 6 18.1441 20.3362 12 2 4 6 24.2019 29.9314 14 2 -4 6 21.8369 30.1121 19 2 4 6 -21.1471 33.1973 17 2 4 7 2103.8 125.367 14 2 4 7 1819.14 122.15 12 2 -4 7 2056.49 124.137 4 2 -4 7 2050.84 126.182 19 2 4 8 148.127 33.9829 14 2 4 8 136.499 49.4807 6 2 4 8 120.752 19.468 12 2 4 8 47.5586 39.4451 22 2 -4 8 114.409 37.2726 19 2 -4 8 145.757 33.2308 4 2 4 9 753.898 58.9137 14 2 -4 9 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3 -7 2296.69 152.639 11 -3 -3 7 2566.51 153.921 6 -3 3 7 3170.21 179.209 2 3 3 -6 273.432 36.8775 18 3 -3 -6 246.572 22.6731 18 3 -3 -6 261.647 35.9469 15 3 3 -6 277.751 44.6838 15 3 3 -6 271.235 73.5091 13 -3 3 6 349.873 84.2183 8 -3 3 6 407.922 104.642 2 3 -3 -6 220.346 21.2819 1 3 -3 -6 218.025 36.8252 12 3 3 -6 254.031 50.1845 11 -3 -3 6 272.535 45.5672 6 -3 -3 5 17.5917 36.5935 6 3 3 -5 -7.52914 34.3283 7 -3 3 5 -38.751 81.5727 8 3 3 -5 3.60036 42.4608 15 3 -3 -5 27.568 31.7676 15 3 3 -5 -25.9946 69.2419 13 3 3 -5 8.25286 26.4375 9 -3 3 5 -13.0345 83.0763 2 3 -3 -5 11.8114 32.8553 12 3 3 -5 -3.68363 44.1596 12 3 3 -5 3.44977 44.7534 11 3 3 -5 12.7676 32.1483 18 3 -3 -5 -7.56879 16.9484 18 3 3 -4 771.587 68.8209 11 3 3 -4 831.412 65.6251 1 -3 -3 4 786.474 54.4375 19 3 3 -4 860.563 61.9579 18 3 3 -4 886.616 62.5587 7 -3 -3 4 889.637 60.9906 6 3 3 -4 905.377 70.6844 15 3 3 -4 750.888 86.42 13 3 3 -4 901.25 68.7782 12 -3 3 4 1068.7 97.3067 2 3 3 -4 727.556 62.512 3 -3 3 4 1112.75 102.496 8 3 3 -4 937.345 59.7543 9 -3 3 3 1192.48 95.8255 2 3 3 -3 914.163 70.9278 3 3 3 -3 1020.15 77.5744 11 3 3 -3 826.58 96.6264 5 3 3 -3 1122.96 75.2925 1 -3 -3 3 963.692 64.015 19 3 -3 -3 1068.16 67.7904 19 3 3 -3 1068.1 70.6561 18 3 -3 -3 881.971 71.7419 16 3 3 -3 1129.59 79.4099 15 3 3 -3 1186.63 77.1967 12 3 3 -3 891.664 92.1103 13 -3 -3 3 1100.79 68.0388 6 3 3 -3 1156.67 72.4195 7 -3 3 3 1362.97 107.792 8 3 3 -3 1106.63 70.2309 9 -3 3 2 -32.6671 61.2516 2 3 3 -2 65.22 36 1 3 3 -2 83.8981 40.6065 12 3 3 -2 53.2436 46.6588 11 3 3 -2 6.10627 69.5766 5 3 3 -2 46.1625 31.9529 18 3 -3 -2 33.082 40.1672 16 3 -3 -2 34.6034 37.9933 7 3 3 -2 55.4988 32.3423 7 -3 3 2 54.4008 80.1835 8 3 3 -2 53.3376 63.4773 13 3 -3 -2 15.3812 23.0399 19 -3 -3 2 21.5816 9.66118 19 3 3 -2 51.5808 32.5568 3 3 3 -2 66.1506 39.5747 9 3 3 -1 2008.19 123.036 11 3 3 -1 1225.39 132.955 5 -3 -3 1 1905.8 111.454 19 3 -3 -1 1768.86 113.725 19 3 3 -1 1963.78 116.309 18 3 3 -1 1892.33 123.109 16 3 3 -1 1969.38 117.333 17 3 -3 -1 1890.89 119.571 16 -3 -3 1 1610.81 112.021 6 3 -3 -1 1755.69 118.358 7 3 3 -1 2200.16 128.689 13 3 3 -1 1829.72 118.637 12 3 3 -1 1680.1 115.937 3 3 3 -1 1439.75 120.113 4 -3 3 1 1822.37 127.839 2 -3 3 1 1898.19 133.723 8 3 3 -1 1945.72 125.656 9 -3 -3 0 58.4575 16.4792 6 3 3 0 166.634 33.9835 17 3 -3 0 139.297 35.184 7 3 3 0 153.289 30.6497 18 3 3 0 158.896 57.9525 9 3 -3 1 1629.14 98.1538 17 3 3 1 1768.92 101.174 18 3 3 1 1729.94 102.288 17 3 -3 1 1726.73 108.472 16 3 3 1 1837.3 114.455 16 3 -3 1 1718.34 102.041 7 -3 -3 -1 1435.34 96.0288 6 3 3 1 1324.47 115.58 13 3 3 1 1782.73 102.938 12 3 -3 1 1790.64 99.1102 19 3 -3 1 1438.32 100.24 22 3 3 1 1986.46 109.36 3 -3 -3 -1 1127.22 97.8051 2 3 3 1 1929.09 104.468 4 3 3 2 2702.32 176.381 18 3 3 2 3089.71 177.624 17 3 -3 2 2753.86 174.76 17 3 3 2 2944.1 185.577 16 3 -3 2 2786.35 176.784 7 3 3 2 2428.11 183.99 13 3 -3 2 2828.57 175.338 19 3 3 2 2714.02 177.009 12 3 3 2 3173.55 179.321 4 3 -3 2 2764.35 176.079 22 3 -3 3 9.1556 32.0308 22 3 3 3 49.5347 31.5815 12 3 3 3 93.8994 59.6256 13 3 -3 3 50.5457 25.3772 19 3 -3 3 56.7082 24.355 17 3 3 3 64.028 34.7315 17 3 3 3 80.1025 61.4405 16 3 3 3 74.531 48.0024 4 3 -3 4 36.621 35.7259 22 3 3 4 5.2763 30.8854 12 3 3 4 40.0858 61.4152 13 3 -3 4 6.03566 38.9275 4 3 -3 4 14.3412 27.7646 19 3 3 4 9.08205 61.5515 16 3 3 4 4.15371 37.9887 17 3 3 5 146.034 61.4405 13 3 -3 5 95.1106 31.0677 19 3 -3 5 69.9051 39.5401 22 3 -3 5 76.52 38.0427 4 3 3 5 104.419 37.597 17 3 3 6 674.659 78.2158 13 3 3 6 746.639 59.8779 17 3 -3 6 879.939 63.0135 22 3 -3 6 658.812 57.1102 19 3 -3 6 702.399 58.1909 4 3 3 7 2556.04 154.305 17 3 3 7 2365.27 153.532 6 3 3 7 2316.74 150.282 14 3 3 7 3246.34 165.009 13 3 -3 7 3102.54 157.178 22 3 3 7 1823.91 157.315 22 3 -3 7 2230.17 154.032 19 3 -3 7 2337.83 153.242 4 3 3 8 51.3102 24.3755 14 3 3 8 159.464 63.2552 13 3 -3 8 84.9427 52.303 22 3 3 8 47.2302 45.2677 22 3 3 8 71.4843 39.391 6 3 -3 8 23.0439 39.895 19 3 -3 8 7.67148 38.3722 4 3 3 9 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52.4675 11 3 4 -5 284.523 30.7058 9 3 -4 -5 218.398 21.604 18 3 4 -5 284.393 38.4829 18 3 4 -4 14.9804 32.6667 18 3 -4 -4 22.7751 30.1194 16 3 4 -4 29.037 45.1197 15 3 4 -4 23.0646 72.4519 13 3 4 -4 53.0044 26.5011 9 3 4 -4 43.6332 51.8216 11 -3 4 4 39.3918 84.3941 8 3 4 -4 30.5232 31.241 7 3 4 -4 11.308 30.3971 8 -3 -4 4 23.5896 16.8453 19 3 -4 -3 354.252 42.4103 16 3 4 -3 383.761 40.8898 7 -3 4 3 549.27 100.307 8 3 4 -3 435.929 78.3421 13 3 4 -3 389.93 41.4488 18 3 4 -3 372.065 58.8564 11 3 4 -3 466.951 46.0383 9 -3 -4 3 411.761 29.7202 19 3 -4 -3 355.778 36.1104 19 3 4 -2 220.76 50.5947 16 3 -4 -2 206.934 39.7337 16 3 4 -2 247.698 34.1432 7 -3 4 2 321.5 88.89 8 3 4 -2 209.257 75.9265 13 3 4 -2 186.136 34.4019 18 3 4 -2 225.677 56.6456 11 3 4 -2 231.369 43.5456 12 3 4 -2 137.903 51.5592 9 -3 -4 2 235.808 21.2448 19 3 -4 -2 203.999 29.0401 19 3 -4 -1 426.791 37.6553 19 -3 -4 1 491.375 33.2803 19 3 4 -1 490.135 44.0719 18 3 4 -1 441.626 43.9226 17 3 4 -1 474.556 57.7526 16 3 -4 -1 395.246 48.7275 16 -3 4 1 567.908 82.6264 8 3 4 -1 502.82 83.7468 13 3 4 -1 482.285 48.6815 12 3 4 -1 452.841 63.1575 11 3 4 -1 419.475 63.8895 9 3 4 -1 350.311 49.5585 4 3 4 0 725.519 55.2084 18 3 4 0 761.146 55.638 17 3 4 0 749.111 70.4214 16 3 -4 0 775.598 58.4653 7 3 4 0 776.031 59.1432 12 3 4 0 941.89 90.297 13 3 -4 0 711.472 51.9426 19 3 -4 0 604.914 52.9278 22 3 4 0 767.736 59.6066 4 3 4 1 277.115 36.167 18 3 -4 1 292.73 24.6396 17 3 4 1 261.047 36.504 17 3 4 1 287.648 57.7061 16 3 -4 1 298.297 38.8533 7 3 4 1 294.081 79.5131 13 3 -4 1 291.854 32.0933 19 3 4 1 267.299 40.1777 12 3 4 1 379.827 42.5729 4 3 -4 1 215.939 30.7225 22 3 4 2 2744.83 171.51 18 3 -4 2 2687.53 168.609 17 3 4 2 2863.45 171.627 17 3 -4 2 2827.75 171.248 7 3 4 2 2884.34 171.609 12 3 4 2 2630.43 185.192 13 3 4 2 2729.43 179.793 16 3 -4 2 2681.95 170.24 19 3 4 2 3086.24 173.491 4 3 -4 2 2348.01 170.102 22 3 -4 3 2064.7 132.743 17 3 4 3 2194.85 136.265 17 3 4 3 2052.66 134.976 18 3 -4 3 2179.89 135.354 7 3 4 3 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3 -4 8 8.01244 34.5298 4 3 4 9 -6.51405 66.4718 13 3 4 9 -2.49065 24.6776 14 3 -4 9 26.361 52.7924 22 3 4 9 -1.50005 37.0281 17 3 -4 9 -26.2026 40.3916 19 3 -4 10 4792.48 235.371 22 3 4 10 4476.25 231.812 22 3 -4 10 3149.17 230.836 19 3 4 10 3260.08 226.833 14 3 4 11 56.1856 46.2969 22 3 4 11 27.2726 28.406 14 3 -4 12 103.842 39.4935 4 3 4 12 48.6041 48.7711 6 3 4 12 138.048 31.3553 14 3 4 13 292.85 55.1876 6 3 -4 13 326.243 62.6488 19 3 -4 13 259.47 43.4982 4 3 4 13 184.2 38.3956 14 3 -4 13 285.565 63.5401 22 3 4 14 25.6634 54.3171 6 3 4 14 1.23373 44.6826 22 3 -4 14 2.62277 62.399 22 3 -4 14 -11.0947 39.3162 4 3 4 14 -56.3098 33.8534 14 3 4 15 16.9362 45.731 22 3 -4 15 31.1127 62.6442 22 3 -4 15 36.1091 62.6175 6 3 4 15 18.4155 57.7794 6 3 4 16 14.1772 49.1746 22 3 -4 16 -56.9515 64.9104 22 3 -4 16 29.3007 65.0456 6 3 4 16 -0.31143 34.5217 14 3 4 16 -23.632 59.4464 6 3 4 17 275.998 55.5595 22 3 -4 17 458.533 74.138 22 3 -4 17 434.469 81.3405 6 3 4 17 340.267 42.3106 14 3 4 17 385.214 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4670.67 278.686 13 3 5 5 4179.18 265.403 12 3 -5 5 4408.23 265.554 7 3 -5 5 4500.64 267.782 22 3 5 5 4209.47 266.239 18 3 5 5 4312.07 267.281 17 3 -5 5 4070.31 266.214 19 3 5 6 173.041 35.719 17 3 5 6 264.512 81.6679 13 3 -5 6 213.302 45.7346 22 3 -5 6 179.181 33.8647 19 3 5 6 141.139 30.9813 18 3 -5 6 211.706 30.5219 7 3 -5 7 296.929 31.9315 7 3 -5 7 233.575 53.2144 22 3 5 7 299.207 42.8155 17 3 5 7 249.201 32.6569 18 3 -5 7 237.24 37.981 19 3 -5 8 348.126 57.4952 22 3 -5 8 371.564 43.2832 19 3 5 8 382.976 37.9426 18 3 5 8 387.078 46.5631 17 3 -5 9 77.9122 52.7307 22 3 5 9 71.8697 27.3641 18 3 -5 9 53.827 39.4868 19 3 5 9 27.7466 38.2084 17 3 5 10 18.8179 27.0295 18 3 -5 10 -15.9922 52.9282 22 3 5 11 23.0488 28.0608 18 3 5 12 4674.74 299.8 17 3 -5 12 4053.53 301.362 19 3 5 13 795.799 67.9306 17 3 -5 13 663.021 77.0635 19 3 -5 14 292.348 65.8538 19 3 -5 14 402.429 70.0883 22 3 -5 15 52.188 67.0584 22 3 -5 16 60.6199 68.3571 6 3 -5 16 42.8984 70.4443 22 3 -5 17 -38.644 71.4916 6 3 -5 17 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7895.79 451.304 8 4 5 -5 7309.18 433.945 9 4 5 -5 6854.2 435.012 3 4 5 -4 635.925 52.1545 7 -4 5 4 831.491 108.668 8 4 5 -4 703.887 49.4218 9 4 5 -4 610.108 66.5439 16 4 -5 -4 502.839 45.6857 19 4 5 -4 624.214 57.7765 1 -4 5 4 741.101 99.406 2 4 5 -4 523.33 52.2191 3 -4 5 3 208.907 82.8988 2 -4 5 3 252.146 93.9871 8 4 5 -3 198.95 35.0599 7 4 5 -3 203.658 37.6503 18 4 -5 -3 162.56 27.8573 19 4 5 -3 199.833 55.8572 16 4 5 -3 163.898 32.0483 9 4 5 -3 134.248 34.6978 3 -4 5 2 399.007 79.9978 2 4 5 -2 342.941 42.6303 18 4 5 -2 338.18 62.7788 16 4 5 -2 361.512 40.2864 7 -4 5 2 397.707 103.537 8 4 -5 -2 296.542 33.7896 19 4 5 -2 407.919 54.3743 3 4 5 -2 389.477 44.1168 9 -4 5 1 142.309 71.667 2 4 5 -1 118.254 35.2194 18 4 5 -1 135.467 63.1046 16 4 5 -1 149.525 36.6748 7 -4 5 1 76.0901 93.082 8 4 5 -1 140.194 83.8631 13 4 -5 -1 145.325 27.8457 19 4 5 -1 176.532 43.8162 12 4 5 -1 160.95 49.991 9 4 5 -1 132.868 59.8743 3 -4 5 0 507.693 76.2782 2 4 5 0 481.64 47.4114 18 -4 5 0 547.226 90.4951 8 4 5 0 454.59 88.2723 13 4 5 0 494.544 51.5895 12 4 5 0 439.864 62.5739 3 4 5 0 478.131 53.0218 4 4 -5 0 458.634 39.6984 19 4 5 0 496.446 69.7522 9 4 5 0 415.987 67.4119 16 4 5 0 443.752 44.9743 17 4 5 1 1471.91 134.348 13 4 5 1 1519.04 109.953 12 4 5 1 1655.89 108.382 18 4 -5 1 1627.46 105.844 19 -4 5 -1 1640.02 123.016 2 4 5 1 1497.71 116.051 3 4 5 1 1828.69 111.602 4 4 5 1 1679.81 109.014 17 4 5 1 1745.1 123.656 16 4 5 2 3178.78 199.156 16 4 -5 2 3106.86 189.196 7 4 5 2 2886.1 189.226 12 4 5 2 3181.48 205.687 13 4 5 2 3157.06 189.087 17 4 5 2 3147.44 188.612 18 4 -5 2 2909.9 186.895 19 -4 5 -2 3384.8 198.706 2 4 5 2 3515.28 190.392 4 4 -5 3 670.145 50.7063 19 4 5 3 653.126 82.4655 16 4 -5 3 673.057 55.3901 7 4 5 3 664.34 92.6438 13 4 5 3 643.958 55.568 12 4 5 3 668.289 55.2356 18 4 -5 3 608.967 52.3354 22 4 5 3 671.392 60.4833 4 4 -5 4 56.717 30.6347 19 4 5 4 141.04 69.4607 16 4 -5 4 85.8272 36.1965 7 4 5 4 120.234 83.3383 13 4 5 4 79.2298 32.3296 18 4 5 4 69.9685 35.3091 12 4 -5 4 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4 5 26 438.682 60.4394 9 4 5 26 183.169 74.3402 4 4 5 27 16.8358 62.1763 4 4 5 27 -34.5601 47.6471 17 4 -5 27 43.8175 47.9178 22 4 5 28 40.6564 59.235 4 4 5 28 94.6133 45.3276 17 4 -5 28 209.512 47.6024 22 4 5 29 312.552 44.9632 17 4 -5 29 290.157 46.7035 22 4 5 30 6.18529 48.7604 4 4 5 30 -55.703 36.3285 17 4 -5 30 13.17 41.5816 22 4 5 31 181.451 34.6599 17 4 -5 31 250.983 44.4533 22 4 5 32 5.22436 35.7261 4 4 5 32 25.634 28.1697 17 4 -5 32 8.37441 37.9826 22 4 5 33 -3.6457 20.8048 17 4 6 -33 213.935 49.8192 15 -4 6 32 746.773 52.1165 14 4 6 -32 715.92 65.9804 15 -4 6 31 14.8228 41.0463 14 4 6 -31 -14.7304 57.1204 15 4 6 -31 15.621 48.9157 1 4 6 -30 -18.3499 60.5334 15 -4 6 30 -0.82987 44.0686 14 4 6 -30 -8.61372 52.4624 1 -4 6 29 9.95034 45.7798 14 4 6 -29 -2.0239 65.7547 15 4 6 -29 9.17635 55.3766 1 -4 6 28 -30.6884 48.0592 14 4 6 -28 47.7936 68.3189 15 4 6 -28 -22.8399 60.9434 1 -4 6 27 147.405 52.5014 14 4 6 -27 168.79 65.7631 15 4 6 -27 186.006 65.6413 1 4 6 -26 810.191 89.768 1 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664.153 55.4175 7 -4 6 1 854.467 93.6571 2 4 6 -1 828.46 76.9019 3 4 -6 -1 655.487 52.4724 19 4 6 -1 718.487 74.5222 16 4 6 0 1928.99 128.7 3 -4 6 0 1931.77 136.499 2 4 -6 0 1696.81 114.71 19 4 6 0 1827.89 129.841 16 -4 6 -1 65.5741 73.8036 2 4 6 1 50.1788 53.9741 3 4 6 1 -19.3117 42.571 4 4 -6 1 33.4372 30.3654 19 4 6 1 47.873 63.9946 16 4 -6 2 27.1299 30.5046 19 -4 6 -2 -44.2055 69.0718 2 4 6 2 33.2781 41.8977 4 4 -6 3 223.162 35.1264 19 4 6 3 299.035 46.1238 4 -4 6 -3 340.323 71.621 2 4 6 4 123.3 45.5073 4 4 -6 5 41.7841 30.5471 22 4 6 5 31.9499 36.5246 17 4 6 5 142.306 46.5499 4 4 6 6 1264.95 94.1662 4 4 6 6 1259.23 86.8159 17 4 -6 6 1215.92 85.2606 22 4 -6 7 2550.05 171.188 19 4 6 7 2718.42 172.337 17 4 -6 7 2578.04 170.941 22 4 6 7 3074.28 175.734 4 4 6 8 86.959 58.2758 4 4 -6 8 25.9049 38.3806 19 4 6 8 25.5957 31.4937 18 4 6 8 27.3079 42.1688 17 4 -6 9 2259.24 159.729 19 4 6 9 2610.71 159.619 17 4 6 9 2385.71 157.059 18 4 -6 9 2479.91 159.054 22 4 6 9 2591.52 164.838 4 4 -6 10 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76.5339 81.5951 6 4 6 22 80.5817 54.0074 17 4 -6 22 107.04 54.6691 22 4 -6 23 45.2789 82.979 6 4 6 23 27.7689 51.5821 17 4 6 23 -4.37612 72.9424 9 4 -6 23 63.2329 52.3417 22 4 -6 24 65.9166 84.9228 6 4 6 24 54.3807 48.3844 17 4 -6 24 53.7239 50.7547 22 4 6 25 18.9311 63.5867 9 4 -6 25 54.443 85.6971 6 -4 6 -25 74.4342 32.8572 21 4 6 25 53.3018 67.4427 4 4 6 26 53.8369 57.2523 9 4 -6 26 134.291 81.3945 6 4 -6 26 36.0259 47.9718 22 4 6 26 23.3366 64.2242 4 4 6 26 24.9055 44.3203 17 4 -6 27 322.05 49.9246 22 4 6 27 164.453 64.5331 4 4 6 27 174.442 47.7604 9 4 6 27 353.07 47.2395 17 4 6 28 219.703 41.356 17 4 -6 28 196.634 45.7578 22 4 6 29 52.2074 51.7339 4 4 6 29 83.5816 36.462 17 4 -6 29 67.3246 39.9953 22 4 6 30 197.637 34.524 17 4 -6 30 226.275 40.2571 22 4 6 31 9.59496 39.6128 4 4 -6 31 3.32428 38.6126 22 4 6 31 28.6836 26.6556 17 4 -6 32 49.3074 35.4816 22 4 6 32 46.1643 22.7551 17 -4 7 32 106.586 33.7824 14 -4 7 31 192.638 40.539 14 4 7 -31 183.801 53.2034 15 4 7 -31 133.067 49.3706 1 -4 7 30 15.5601 41.6367 14 4 7 -30 0.54109 55.5294 15 4 7 -30 -6.56789 53.9079 1 -4 7 29 269.191 48.2853 14 4 7 -29 319.995 63.7206 15 4 7 -29 202.147 56.6137 1 -4 7 28 946.329 79.7618 14 4 7 -28 1030.04 91.3899 15 4 7 -28 963.198 85.8154 1 -4 7 27 86.4373 51.2826 14 4 7 -27 130.935 65.5412 15 4 7 -27 32.0362 60.2623 1 -4 7 26 1048.85 91.5119 14 4 7 -26 1161.66 101.053 15 4 7 -26 1149.81 97.304 1 4 7 -25 359.671 70.5162 1 -4 7 24 617.993 76.3932 14 4 7 -24 635.966 84.6676 15 4 7 -24 687.016 81.5608 1 -4 7 23 73.5975 65.2908 14 4 7 -23 77.4173 69.5792 15 4 7 -23 144.953 70.4448 1 4 7 -22 118.199 70.7922 15 -4 7 22 126.204 66.5247 14 -4 7 21 527.488 79.4598 14 4 7 -21 686.181 80.9064 15 4 7 -20 3911.99 228.722 1 4 7 -20 3570.83 226.444 15 4 7 -19 161.123 68.5894 15 -4 7 19 129.049 74.1124 14 4 7 -19 241.293 73.9182 1 4 7 -18 1351.58 103.986 1 4 7 -18 1238.29 101.984 15 -4 7 18 992.711 109.579 14 4 7 -17 -15.807 65.5632 1 4 7 -17 55.7232 79.714 11 -4 7 17 127.984 77.9053 14 4 7 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1372.7 127.557 8 4 7 2 234.758 40.6921 18 -4 7 -2 350.623 80.1046 2 4 7 2 278.87 46.6935 4 -4 7 -3 1252.47 108.424 2 4 7 3 1125.89 81.6813 4 4 7 3 1171.53 78.7932 17 4 -7 3 1025.81 76.0076 19 4 7 3 1021.39 78.446 18 4 7 4 84.7892 42.5055 4 4 7 4 34.4303 35.7588 17 4 -7 4 5.08679 32.0805 19 4 7 4 38.8018 34.252 18 -4 7 -4 -76.9221 80.0344 2 4 7 5 342.593 41.422 18 4 7 5 413.4 44.6188 17 4 -7 5 359.659 42.861 19 -4 7 -5 487.118 82.7929 2 4 7 5 378.08 50.3869 4 4 7 6 961.523 72.3139 18 4 7 6 993.9 73.858 17 4 7 6 1092.52 79.8236 4 4 -7 6 976.922 72.8309 19 4 7 7 90.2633 50.6479 4 4 7 7 125.924 40.3013 17 4 7 7 79.947 33.6228 18 4 -7 7 81.9498 37.8214 19 4 7 8 12.1671 55.1722 4 4 7 8 -21.0873 33.5415 18 4 -7 8 -7.40073 40.225 19 4 7 8 25.4893 38.5631 17 4 -7 9 734.813 70.0631 19 4 7 9 883.435 80.572 4 4 7 9 865.66 65.3053 18 4 7 9 850.598 69.123 17 4 -7 9 911.442 67.8147 22 4 -7 10 818.067 74.0372 19 4 7 10 887.838 66.4604 18 4 7 10 860.844 70.9496 17 4 -7 10 883.431 70.8051 22 4 7 10 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257.598 72.551 4 4 7 24 758.052 87.6057 4 4 7 24 641.84 93.382 9 4 -7 25 248.456 49.0653 22 -4 7 -25 176.63 36.4382 21 4 -7 25 147.966 82.6016 6 4 7 25 195.269 44.4407 17 4 7 25 157.834 65.8696 9 4 7 25 129.216 65.5219 4 4 7 26 676.559 54.9793 17 4 -7 26 584.907 57.548 22 -4 7 -26 539.009 47.8041 21 4 7 27 -38.596 55.4903 4 4 7 27 48.6439 43.6097 9 4 7 27 55.5909 39.2495 17 4 -7 27 -42.7062 41.4774 22 -4 7 -27 30.3373 29.5011 21 4 7 28 11.2909 52.2244 4 4 7 28 39.2717 32.8297 9 4 7 28 43.5785 33.8377 17 4 -7 28 16.8366 38.5121 22 4 7 29 8.14947 29.6341 17 4 7 29 23.8062 47.0056 4 4 -7 29 2.99051 36.5999 22 4 7 30 -1.47958 27.7507 17 4 -7 30 28.6816 37.1775 22 4 7 30 12.136 40.3042 4 4 -7 31 26.1725 34.6021 22 -4 8 32 541.206 44.7944 14 -4 8 31 286.741 40.8449 14 4 8 -30 53.3291 46.5123 1 -4 8 30 44.8927 38.2961 14 4 8 -29 13.5482 52.164 1 -4 8 29 34.5915 41.7336 14 4 8 -29 1.56701 53.4835 15 4 8 -28 350.702 65.0156 1 -4 8 28 353.415 53.0831 14 4 8 -28 483.616 65.3975 15 4 8 -27 78.6017 58.7106 1 -4 8 27 79.6528 50.2478 14 4 8 -27 172.538 62.2864 15 4 8 -26 418.968 66.9099 1 -4 8 26 381.098 62.3081 14 4 8 -26 485.088 68.7921 15 4 8 -25 -13.2922 59.4624 1 4 8 -25 37.4959 64.3737 15 -4 8 25 -18.8156 58.1774 14 4 8 -24 1803.55 130.8 1 4 8 -23 1014.96 83.6631 1 -4 8 23 942.457 84.8201 14 4 8 -23 1097.6 89.6619 15 4 8 -22 100.7 62.076 1 4 8 -22 108.194 48.6618 3 4 8 -22 64.604 66.0664 15 -4 8 22 36.3154 65.4944 14 4 8 -21 26.4017 63.6461 1 4 8 -21 -1.03988 48.9399 3 -4 8 21 -18.603 67.9798 14 4 8 -21 33.9637 67.7715 15 -4 8 20 16.0552 69.8335 14 4 8 -20 94.4533 69.698 15 4 8 -19 1838.58 142.208 3 -4 8 19 2086.54 153.844 14 4 8 -18 2136.15 142.093 1 -4 8 18 1676.39 148.514 14 4 8 -18 1981.04 143.42 15 4 8 -17 375.235 69.7614 1 -4 8 17 328.458 84.9859 14 4 8 -17 328.18 72.0292 15 4 8 -16 799.814 85.0379 1 -4 8 16 773.347 97.5474 14 4 8 -16 911.918 84.3847 15 4 8 -15 4691.07 290.633 15 -4 8 15 4021.52 294.504 14 4 8 -15 4683.5 288.809 1 -4 8 14 1579.07 146.969 2 4 8 -14 1546.86 113.788 1 4 8 -14 1521.23 114.651 15 -4 8 14 1179.11 125.666 14 -4 8 13 -41.1201 104.209 2 4 8 -13 75.007 65.4201 1 4 8 -13 55.1433 59.7883 15 4 8 -12 348.593 57.9192 3 -4 8 12 387.895 101.602 8 -4 8 12 547.388 111.093 2 4 8 -12 431.804 68.7981 1 4 8 -12 421.608 65.1271 15 4 8 -11 1366.91 99.3822 1 4 -8 -11 1163.3 86.9957 19 -4 8 11 1279.75 146.629 2 4 8 -11 1208.46 93.035 3 -4 8 11 1263.19 131.032 8 4 8 -10 78.2408 54.0349 1 -4 8 10 -56.7388 120.411 2 -4 8 10 6.85648 108.297 8 4 -8 -10 -11.4978 36.2972 19 4 8 -10 35.2243 51.0069 3 4 8 -9 867.342 76.9466 1 -4 8 9 995.548 140.81 2 4 8 -9 857.676 80.7497 16 -4 8 9 960.776 126.569 8 4 -8 -9 783.607 64.6307 19 4 8 -9 831.536 73.6848 3 -4 8 8 239.43 135.593 2 4 8 -8 333.119 54.447 1 4 8 -8 230.631 58.6894 16 -4 8 8 239.917 117.155 8 4 -8 -8 263.9 38.8529 19 4 8 -8 279.873 50.2698 3 4 8 -7 1709.58 121.226 1 4 8 -7 1733.13 124.891 16 4 8 -7 1663.85 118.693 3 4 -8 -7 1665.24 114.101 19 -4 8 6 42.1301 147.663 2 4 8 -6 75.2989 58.6003 16 4 -8 -6 63.9655 33.1221 19 -4 8 6 -88.0199 114.59 8 4 8 -6 29.2362 44.2419 3 -4 8 5 571.919 137.93 2 4 8 -5 489.622 69.8383 16 4 -8 -5 458.839 45.2947 19 -4 8 5 661.355 125.992 8 4 8 -5 523.903 56.4432 3 -4 8 4 833.752 125.986 2 4 8 -4 694.954 77.1072 16 4 -8 -4 600.675 52.0178 19 -4 8 4 806.156 132.66 8 4 8 -4 625.543 61.5149 3 -4 8 3 545.935 117.165 2 4 8 -3 384.3 65.5595 16 4 -8 -3 406.818 41.7704 19 4 8 -3 393.038 49.4171 3 -4 8 3 632.319 124.383 8 -4 8 2 81.5245 115.804 8 -4 8 2 138.015 109.111 2 4 8 -2 131.461 64.8989 16 4 8 -2 214.413 45.0951 9 4 -8 -2 149.164 33.497 19 4 8 -2 135.742 47.1329 3 -4 8 1 464.6 129.081 8 -4 8 1 422.224 102.891 2 4 8 -1 337.689 70.3473 16 4 8 -1 512.648 64.8555 9 4 -8 -1 270.146 40.8949 19 4 8 -1 373.894 75.4431 3 -4 8 0 731.756 131.224 8 -4 8 0 750.134 105.294 2 4 8 0 599.809 77.5091 16 4 8 0 752.062 75.3536 9 4 -8 0 551.532 52.3293 19 4 8 0 657.694 81.2771 3 -4 8 -1 495.135 117.842 8 -4 8 -1 450.522 100.726 2 4 8 1 377.713 72.1791 16 4 8 1 304.479 70.2845 9 4 8 1 357.568 69.8346 3 4 -8 1 372.799 41.8465 19 4 8 2 74.7053 39.0723 18 4 -8 2 99.414 34.5045 19 -4 8 -2 180.796 106.899 8 -4 8 -2 47.9234 90.3634 2 4 8 3 272.083 43.9314 18 4 -8 3 293.624 39.8578 19 -4 8 -3 325.524 104.484 8 -4 8 -3 415.292 89.3449 2 -4 8 -4 1942.15 147.107 2 4 8 4 1923.52 121.452 4 4 8 4 1817.28 119.075 17 4 -8 4 1707.31 118.777 19 4 8 4 1755.08 120.353 18 4 8 5 224.85 45.1283 4 4 8 5 235.277 38.8587 17 -4 8 -5 226.613 84.845 2 4 -8 5 183.223 38.384 19 4 8 5 175.901 38.523 18 4 8 6 287.978 44.8756 17 4 8 6 335.234 49.9342 4 4 8 6 273.182 41.0785 18 4 -8 6 239.567 42.0848 19 -4 8 -6 430.694 85.3345 2 4 8 7 203.616 40.1686 17 4 8 7 309.79 51.0754 4 4 -8 7 208.116 42.8481 19 4 8 7 195.189 37.1487 18 4 8 8 88.8774 51.3483 4 4 8 8 32.8257 36.1623 17 4 8 8 -16.1663 33.6541 18 4 -8 8 1.26259 41.5789 19 4 8 9 -39.8563 54.4165 4 4 8 9 24.5908 40.3039 17 4 -8 9 -9.65157 44.8662 19 4 8 10 153.55 58.68 4 4 8 10 265.52 44.123 17 4 -8 10 201.502 50.4377 19 4 8 11 2116.36 136.693 17 4 -8 11 1850.45 140.687 19 4 8 11 2200.42 143.879 4 4 8 12 1554.65 105.244 17 4 -8 12 1339.05 112.407 19 4 8 12 1671.9 115.725 4 4 -8 12 1471.71 105.568 22 4 8 13 31.7166 43.3091 17 4 8 13 50.2786 62.9428 4 4 -8 13 55.8685 60.6749 19 4 -8 13 40.6862 45.7746 22 4 8 14 269.331 48.5539 17 4 8 14 297.379 69.2432 4 4 -8 14 273.654 51.9886 22 4 -8 14 268.747 70.9243 19 4 8 15 694.903 79.8654 4 4 8 15 661.219 61.1069 17 4 -8 15 544.728 85.2226 19 4 -8 15 583.059 64.0191 22 4 8 16 26.439 44.0239 17 4 -8 16 0.51099 50.9136 22 4 8 16 -60.3976 67.1338 4 4 -8 17 556.021 63.721 22 4 8 17 520.152 78.3572 4 4 8 17 591.429 61.0839 17 4 -8 17 599.191 81.6581 6 4 8 18 195.385 50.8387 17 4 -8 18 240.949 52.9351 22 4 8 19 152.169 48.6163 17 4 -8 19 150.954 50.3672 22 4 8 20 1575.42 126.596 4 4 -8 20 1476.18 117.007 22 4 8 20 1909.41 118.016 17 4 -8 20 1739.78 138.79 6 4 -8 21 113.67 83.5433 6 4 8 21 69.6413 67.5078 4 4 8 21 94.6262 44.0332 17 -4 8 -21 79.8322 40.2645 21 4 -8 21 24.6712 47.879 22 4 -8 22 140.857 82.9997 6 4 8 22 22.1769 66.9052 4 4 8 23 131.098 66.347 4 4 8 23 164.555 43.863 17 4 -8 23 310.518 82.1539 6 4 -8 24 22.2525 43.2437 22 -4 8 -24 4.15702 34.525 21 4 -8 24 72.5907 78.5554 6 4 8 24 -19.2062 62.188 4 4 8 24 31.8282 38.5581 17 4 8 24 -54.0266 69.8101 9 4 -8 25 198.079 44.784 22 -4 8 -25 194.612 36.0837 21 4 -8 25 313.881 80.1298 6 4 8 25 278.351 40.593 17 4 8 25 81.2123 64.9551 9 4 8 25 68.028 59.0684 4 4 8 26 584.107 48.1915 17 4 8 26 175.403 67.6095 9 4 -8 26 631.435 53.3558 22 -4 8 -26 552.323 46.2993 21 4 8 26 110.113 64.4948 4 4 8 27 558.094 43.7978 17 4 8 27 67.0928 49.992 9 4 -8 27 523.31 46.832 22 -4 8 -27 497.91 41.3224 21 4 8 27 96.496 57.0934 4 4 -8 28 111.211 36.3958 22 -4 8 -28 81.7782 28.5711 21 4 8 28 19.5905 45.2999 4 4 8 28 -1.8713 32.1187 9 4 8 28 83.6256 29.3412 17 -4 8 -29 143.335 56.8462 2 4 8 29 62.843 40.3737 4 4 -8 29 198.401 36.2288 22 4 8 29 23.8987 25.0072 9 4 -8 30 -8.693 32.4568 22 4 -8 31 39.4636 29.9727 22 -4 9 31 47.7715 27.831 14 -4 9 30 388.427 43.4392 14 -4 9 29 26.7392 38.6042 14 4 9 -29 -10.0733 44.4659 1 -4 9 28 405.317 48.6847 14 4 9 -28 241.274 54.1771 1 -4 9 27 90.7083 46.9348 14 4 9 -27 112.255 52.9638 1 -4 9 26 424.938 59.2586 14 4 9 -26 467.002 64.6584 1 -4 9 25 130.037 55.2468 14 4 9 -25 59.0487 59.5556 15 4 9 -25 115.543 65.1246 1 -4 9 24 1568.94 125.562 14 4 9 -24 1692.69 127.197 15 4 9 -24 1932.32 129.515 1 4 9 -23 -55.9235 63.6081 15 4 9 -23 -19.9378 44.4764 3 4 9 -23 30.1563 65.4821 1 4 9 -22 178.941 51.6274 3 4 9 -22 187.873 66.2991 1 -4 9 21 -49.2388 67.397 14 4 9 -21 57.5968 66.5474 15 4 9 -21 31.6937 50.782 3 4 9 -21 39.0755 64.7884 1 -4 9 20 173.521 70.1199 14 4 9 -20 240.54 68.7334 15 4 9 -20 160.247 54.0369 3 4 9 -20 316.252 69.2285 1 -4 9 19 1985.52 163.457 14 4 9 -19 2407.09 160.622 15 4 9 -19 1990.23 153.574 3 -4 9 18 825.026 99.2474 14 4 9 -18 911.67 89.8088 15 -4 9 17 389.373 87.3021 14 4 9 -17 380.786 71.5254 15 4 9 -17 390.531 61.0075 3 4 9 -17 377.485 75.8766 1 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4 9 -9 860.346 73.7528 3 -4 9 8 221.209 134.307 2 4 9 -8 154.178 64.0517 16 -4 9 8 168.219 122.768 8 4 -9 -8 215.996 39.9642 19 4 9 -8 190.086 50.7078 3 -4 9 7 -126.622 144.967 2 4 9 -7 17.8454 64.0383 16 -4 9 7 14.3018 121.252 8 4 -9 -7 36.0929 35.6962 19 4 9 -7 59.3547 47.7988 3 4 9 -6 597.682 77.8816 16 4 -9 -6 527.608 49.7225 19 4 9 -6 471.193 60.4043 3 -4 9 6 664.389 129.298 8 4 9 -5 2636.7 178.389 16 4 -9 -5 2467.58 167.164 19 4 9 -5 2581.21 171.551 3 -4 9 5 3800.1 236.69 2 -4 9 5 3405.12 217.895 8 4 9 -4 1247.42 96.0595 16 -4 9 4 1456.81 155.237 8 4 9 -4 922.67 83.7653 3 -4 9 4 1400.02 159.02 2 4 -9 -4 1070.91 77.7216 19 -4 9 3 656.79 133.411 2 4 -9 -3 472.663 46.8844 19 4 9 -3 482.961 75.1692 16 4 9 -3 455.052 53.546 3 -4 9 3 483.996 135.986 8 4 9 -2 1081.33 102.519 16 -4 9 2 1398.89 152.029 8 4 -9 -2 1114.07 83.4025 19 -4 9 2 1394.21 148.75 2 4 9 -2 1375.05 101.084 3 -4 9 1 472.09 118.819 2 4 9 -1 377.172 80.5363 3 4 9 -1 367.902 62.7671 9 -4 9 1 259.003 134.267 8 4 -9 -1 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4 -10 -1 3199.71 220.275 19 -4 10 1 4186.62 264.017 2 4 10 -1 3882.52 233.937 3 -4 10 1 3970.05 267.962 8 4 -10 0 5519.24 365.161 19 -4 10 0 6672.45 394.97 2 4 10 0 5873.37 371.98 3 4 -10 1 2450.71 169.779 19 4 10 1 2524.48 180.303 9 4 10 1 2774.47 180.536 3 -4 10 -1 3105.21 212.673 2 4 -10 2 155.629 42.9251 19 -4 10 -2 201.558 116.786 2 4 10 2 180.989 73.9196 9 -4 10 -2 286.792 146.349 8 4 -10 3 45.7749 40.5194 19 -4 10 -3 110.676 107.129 2 -4 10 -3 186.435 135.102 8 4 -10 4 320.452 46.6071 19 -4 10 -4 362.034 108.34 2 -4 10 -4 362.598 135.685 8 -4 10 -5 2594.99 189.223 8 -4 10 -5 2396.1 171.29 2 -4 10 -6 1756.97 154.734 8 -4 10 -6 1801.68 140.828 2 -4 10 -7 2296.26 160.283 2 4 -10 7 1814.21 128.347 19 4 -10 8 -0.99338 45.3958 19 -4 10 -8 -46.5163 98.5925 2 4 -10 9 288.819 54.4556 19 -4 10 -9 433.861 100.079 2 -4 10 -10 3683.7 214.108 2 4 -10 10 2693.38 190.912 19 -4 10 -11 32.9428 91.1253 2 4 -10 11 61.454 53.7167 19 -4 10 -12 -66.6949 90.0973 2 4 -10 12 75.084 58.8092 19 -4 10 -13 223.997 43.6248 20 -4 10 -13 294.319 92.8948 2 4 -10 13 211.813 65.8014 19 -4 10 -14 519.123 52.3956 20 4 -10 14 536.118 78.811 19 4 -10 15 2086.4 154.125 19 4 -10 16 525.473 85.4944 19 4 10 16 554.714 69.327 4 -4 10 -16 773.142 101.721 2 4 10 17 670.932 74.4353 4 4 -10 17 746.194 88.3838 6 -4 10 -17 815.843 106.648 2 -4 10 -18 2175.42 150.174 21 4 -10 18 2442.84 165.377 6 4 10 18 2127.74 155.718 4 -4 10 -19 297.649 91.9688 2 4 -10 19 293.321 80.005 6 4 10 19 206.369 59.0418 4 -4 10 -20 385.244 90.8527 2 4 10 20 282.675 60.4467 4 4 -10 20 288.047 84.9892 6 4 -10 21 46.7066 79.7432 6 4 10 21 42.4925 54.1101 4 -4 10 -21 76.9313 37.8829 21 -4 10 -21 57.4739 83.6372 2 4 -10 22 94.2594 77.6967 6 4 10 22 57.339 51.6684 4 -4 10 -22 20.3921 37.4804 21 -4 10 -22 30.2328 78.6655 2 -4 10 -23 77.0996 36.6903 21 4 -10 23 49.5604 71.5516 6 4 10 23 36.9622 48.7572 4 4 10 23 77.2809 70.7162 9 -4 10 -23 145.236 76.0571 2 -4 10 -24 -11.5074 33.8049 21 4 -10 24 9.25741 70.1031 6 4 10 24 -25.7184 63.4974 9 4 10 24 -12.19 45.1715 4 -4 10 -24 -21.3629 70.0197 2 -4 10 -25 48.2679 33.2895 21 4 10 25 2.4866 55.7511 9 4 10 25 -13.8816 42.3049 4 -4 10 -25 62.2485 65.8772 2 -4 10 -26 296.118 35.3576 21 -4 10 -26 221.593 63.4174 2 4 10 27 2.59179 32.6887 9 4 10 28 6.69249 24.3904 9 -4 11 29 49.9584 25.8879 14 -4 11 28 14.0255 31.8161 14 -4 11 27 283.31 41.4464 14 -4 11 26 56.6014 41.1935 14 -4 11 25 111.387 47.3089 14 4 11 -24 178.177 52.989 1 -4 11 24 196.914 52.2916 14 4 11 -23 54.9103 54.2508 1 4 11 -23 6.39739 42.1872 3 -4 11 23 105.042 55.3965 14 4 11 -22 30.8615 56.8229 1 -4 11 22 65.2131 59.7808 14 4 11 -22 73.4084 45.5558 3 4 11 -21 715.31 74.757 1 -4 11 21 708.666 77.9539 14 4 -11 -21 821.29 60.0906 19 4 11 -20 1474.03 115.864 1 -4 11 20 1417.4 119.041 14 4 11 -20 1304.37 110.721 3 4 11 -19 556.445 63.9203 3 4 11 -19 632.258 72.722 1 4 11 -18 328.037 58.4033 3 4 11 -18 384.396 64.6009 1 4 -11 -17 184.959 43.4885 19 4 11 -17 151.017 63.1769 1 4 11 -17 193.071 55.5489 3 -4 11 17 69.2682 78.6872 14 4 11 -16 992.063 91.7334 1 -4 11 16 911.593 108.336 14 4 11 -16 1092 87.4914 3 4 -11 -16 1054.91 79.5749 19 4 11 -15 1194.04 104.713 1 -4 11 15 1315.13 121.478 14 4 11 -15 1306.14 102.179 3 4 -11 -15 1391.38 95.1809 19 -4 11 14 632.667 94.9849 14 4 -11 -14 703.196 62.4962 19 -4 11 13 654.772 103.392 14 4 -11 -13 747.232 65.0668 19 -4 11 12 1060.42 132.126 8 4 -11 -12 863.415 71.9626 19 4 -11 -11 560.647 55.7552 19 4 11 -11 534.273 68.2402 3 -4 11 11 538.389 118.222 8 -4 11 11 583.372 127.123 2 4 -11 -10 98.2605 41.333 19 4 11 -10 53.836 53.5408 3 -4 11 10 201.937 119.304 8 -4 11 10 28.7497 118.73 2 4 -11 -9 2914.01 194.68 19 -4 11 9 3721.23 241.463 8 -4 11 9 3643.02 245.502 2 4 11 -9 3000.58 198.912 3 4 -11 -8 36.6637 39.7593 19 4 11 -8 44.6681 52.9246 3 -4 11 8 109.647 133.869 8 -4 11 8 91.7415 138.066 2 4 -11 -7 2117.83 136.92 19 -4 11 7 2912.43 202.051 2 4 11 -7 1780.32 140.927 3 -4 11 7 2635.94 199.806 8 4 -11 -6 3267.29 206.01 19 -4 11 6 4056.79 257.756 8 -4 11 6 4698.72 267.794 2 4 11 -6 2895.76 207.479 3 4 -11 -5 131.727 40.5865 19 4 11 -5 7.27739 47.1613 3 -4 11 5 13.0563 137.837 8 -4 11 5 85.4642 157.056 2 4 -11 -4 -26.577 39.6226 19 4 11 -4 43.1417 69.2471 3 -4 11 4 30.4974 142.084 8 -4 11 4 168.336 167.408 2 4 -11 -3 456.122 54.2856 19 4 11 -3 853.606 96.7335 3 -4 11 3 706.439 151.826 8 -4 11 3 599.196 170.91 2 4 -11 -2 254.835 44.1976 19 4 11 -2 282.105 79.9822 3 -4 11 2 243.615 156.065 8 -4 11 2 120.821 150.359 2 4 -11 -1 728.993 65.5447 19 4 11 -1 784.604 88.2649 3 -4 11 1 899.491 157.294 2 -4 11 1 1035.93 166.422 8 4 -11 0 2003.07 146.329 19 -4 11 0 2658.83 202.949 2 4 11 0 2472.79 159.779 3 -4 11 0 2711.51 210.252 8 -4 11 -1 5688.31 331.082 2 -4 11 -1 5851.92 340.081 8 -4 11 -2 4838.41 288.058 8 -4 11 -2 4488.23 270.852 2 4 -11 3 47.0544 42.3851 19 -4 11 -3 35.8241 120.696 2 4 11 3 143.75 76.1608 9 -4 11 -3 29.3781 156.286 8 4 -11 4 85.0426 42.4918 19 -4 11 -4 130.984 116.441 2 4 -11 5 215.191 47.6153 19 -4 11 -5 506.866 117.881 2 -4 11 -5 455.282 150.647 8 4 -11 6 1327.65 102.709 19 -4 11 -6 1642.84 148.581 2 -4 11 -7 318.277 113.994 2 4 -11 7 372.974 53.7523 19 -4 11 -7 420.076 136.65 8 4 -11 8 1565.8 121.335 19 -4 11 -8 2018.61 159.708 2 -4 11 -9 660.82 115.604 2 4 -11 9 447.123 62.6915 19 -4 11 -9 854.919 134.067 8 4 -11 10 597.852 67.4072 19 4 -11 11 917.616 79.8457 19 -4 11 -11 775.305 69.7411 20 4 -11 12 1268.03 99.7589 19 -4 11 -12 1175.5 87.9622 20 -4 11 -13 19.9677 39.3838 20 4 -11 13 101.608 64.8437 19 -4 11 -13 169.06 98.6829 2 -4 11 -14 333.94 43.5145 20 4 -11 14 347.314 74.583 19 -4 11 -14 297.108 49.3768 21 4 -11 15 100.835 71.3071 19 -4 11 -15 181.61 100.033 2 -4 11 -15 56.2939 40.2743 21 -4 11 -16 433.757 100.434 2 -4 11 -16 283.436 44.6878 21 4 -11 17 -11.3165 71.2589 6 -4 11 -17 7.53712 93.3665 2 4 -11 18 83.8472 72.5506 6 -4 11 -18 33.2492 89.0851 2 -4 11 -19 -63.5758 87.6889 2 4 -11 19 112.078 74.1885 6 -4 11 -19 81.2554 40.2414 21 -4 11 -20 87.0785 84.3537 2 -4 11 -20 98.4755 39.7712 21 4 -11 20 38.5543 78.2523 6 4 -11 21 10.158 74.8672 6 4 11 21 44.7295 74.6311 9 -4 11 -21 -44.7446 78.0226 2 -4 11 -21 19.8886 37.5854 21 4 -11 22 5.4084 70.2285 6 4 11 22 -1.24935 69.9517 9 -4 11 -22 111.343 75.1108 2 -4 11 -22 38.8799 35.9745 21 4 -11 23 -11.6861 65.556 6 -4 11 -23 -6.93593 34.2706 21 -4 11 -23 111.847 70.3825 2 4 11 23 62.4003 62.2744 9 -4 11 -24 27.7004 33.5613 21 -4 11 -24 -47.6511 63.6461 2 4 11 24 22.985 60.5507 9 -4 11 -25 69.3545 32.7841 21 -4 11 -25 67.9981 58.9493 2 4 11 25 12.7368 44.4196 9 4 11 26 4.93319 33.9923 9 -4 11 -26 150.253 68.0375 8 4 11 27 10.3904 25.8308 9 -4 11 -27 363.893 61.905 8 -4 12 27 -29.9142 27.5901 14 -4 12 26 5.51517 32.4894 14 -4 12 25 -13.4219 39.5688 14 -4 12 24 7.88444 44.2212 14 -4 12 23 -8.12957 47.8863 14 4 12 -23 6.81387 35.681 3 -4 12 22 214.648 54.7095 14 4 12 -22 4.30287 38.9833 3 -4 12 21 264.758 59.7051 14 4 12 -21 76.1869 44.2639 3 4 -12 -20 425.969 44.5556 19 -4 12 20 407.956 65.7548 14 4 -12 -19 1492.74 91.5625 19 -4 12 19 1366.27 106.47 14 4 -12 -18 774.719 60.3651 19 -4 12 18 675.385 82.4164 14 4 12 -18 592.197 69.8056 3 4 12 -17 10.0677 52.8108 3 4 -12 -17 7.70418 39.2605 19 4 12 -16 838.724 78.2951 3 4 12 -15 56.7636 55.0043 3 -4 12 15 -0.90024 81.926 14 4 12 -14 -24.8523 55.364 3 4 -12 -14 29.4479 39.7738 19 4 12 -13 460.032 66.0485 3 4 -12 -13 556.005 53.6653 19 -4 12 13 597.595 93.3344 14 4 -12 -12 -15.4591 40.7364 19 -4 12 12 -0.99488 87.6687 14 -4 12 12 -180.68 120.157 2 4 12 -12 60.1012 55.5288 3 -4 12 11 2344.31 176.056 8 -4 12 11 2199.27 177.528 2 4 12 -11 1823.05 134.415 3 4 -12 -11 1863.54 128.27 19 -4 12 10 751.697 67.4573 20 4 -12 -10 940.904 70.1667 19 -4 12 9 37.2928 41.3069 20 4 -12 -9 -23.5192 40.993 19 -4 12 9 96.326 122.374 8 4 -12 -8 1197 90.2788 19 -4 12 8 1660.16 158.139 8 4 -12 -7 113.164 42.0946 19 -4 12 7 307.76 136.526 8 4 -12 -6 -35.0942 41.7361 19 -4 12 6 155.305 139.581 8 -4 12 5 4767.91 296.73 2 4 12 -5 4586.89 259.437 3 -4 12 5 4537.77 294.164 8 4 -12 -4 1592.68 117.424 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5 8 -29 36.567 45.5987 1 5 8 -28 49.6476 57.6187 16 -5 8 28 8.17546 41.3896 14 5 8 -28 -22.0541 48.0653 1 -5 8 27 266.754 48.348 14 5 8 -27 174.599 53.7185 1 -5 8 26 52.1121 48.9426 14 5 8 -26 10.9707 54.71 1 -5 8 25 43.4373 53.1755 14 5 8 -25 0.47441 56.578 1 -5 8 24 124.542 57.986 14 5 8 -24 136.909 58.7124 1 -5 8 23 12.3127 60.7546 14 5 8 -23 -76.3646 59.7687 1 5 8 -22 1708.72 126.091 1 5 8 -21 141.941 61.3654 1 -5 8 21 193.966 67.9165 14 -5 8 20 195.421 68.4271 14 5 8 -20 277.431 48.4096 3 -5 8 19 574.36 85.2458 14 5 8 -19 648.715 65.5015 3 -5 8 18 120.015 76.8197 14 -5 8 17 -12.6112 79.4447 14 5 8 -16 260.798 53.2461 3 -5 8 16 218.44 83.2551 14 5 8 -16 248.125 68.4143 1 5 8 -15 439.959 61.2612 3 -5 8 15 494.609 87.7997 14 5 8 -15 576.296 71.8361 1 5 8 -14 104.005 51.8156 3 -5 8 14 135.626 83.251 14 5 8 -14 207.661 64.149 1 -5 8 14 119.247 106.719 2 -5 8 13 461.164 111.108 2 5 8 -13 384.43 67.1202 1 5 8 -13 388.149 57.4411 3 5 8 -13 351.476 78.0403 16 -5 8 12 182.195 105.862 2 5 8 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5 -8 4 830.532 69.8138 19 -5 8 -4 1180.52 130.387 8 5 8 4 1159.57 97.9242 9 -5 8 -4 1007 113.168 2 5 8 4 900.216 73.9306 18 5 -8 5 895.41 77.9317 19 -5 8 -5 1382.62 129.297 8 5 8 5 1165.16 105.973 9 -5 8 -5 1219.64 120.021 2 5 8 5 1100.71 86.6533 4 5 8 5 1088.94 80.0828 18 5 8 6 1096.69 79.0577 17 -5 8 -6 1143.15 116.398 2 5 8 6 973.369 83.4205 4 5 -8 6 905.114 77.6126 19 5 8 6 1190.86 106.735 9 5 8 6 979.145 77.5252 18 -5 8 -7 92.1173 89.6482 2 5 8 7 4.56864 54.2954 4 5 8 7 -36.5722 84.9009 9 5 8 7 15.4671 44.8607 17 5 8 7 52.2227 40.388 18 5 -8 7 49.0052 44.5573 19 -5 8 -8 17.2641 85.1391 2 5 8 8 -41.9892 54.3252 4 5 8 8 55.065 85.9661 9 5 8 8 36.473 45.5932 17 5 8 8 32.7064 38.6218 18 5 -8 8 58.4268 47.5409 19 5 8 9 2162.29 142.72 4 5 -8 9 1783.49 141.559 19 5 8 9 2184.94 139.745 17 -5 8 -9 2296.35 162.691 2 5 8 9 2108.24 137.758 18 -5 8 -10 304.814 93.7135 2 5 8 10 350.776 59.5643 4 5 8 10 276.834 51.3637 17 5 8 10 351.445 44.6787 18 5 -8 10 263.253 59.7892 19 -5 8 -11 39.9464 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47.9379 17 -5 8 -23 8.22604 32.9501 21 5 -8 23 13.446 42.4898 22 5 8 23 -8.34796 52.5985 4 5 8 23 12.2378 51.7832 9 5 8 23 16.3627 40.9175 17 -5 8 -24 181.994 33.9722 21 5 -8 24 243.109 48.413 22 5 8 24 132.509 52.1374 4 5 8 24 134.816 47.7587 9 5 8 24 238.269 40.5145 17 5 -8 25 18.3257 42.3493 22 -5 8 -25 30.6594 29.0338 21 5 8 25 2.81189 34.1057 17 5 8 25 8.06489 36.182 9 5 8 25 -21.8711 47.171 4 -5 8 -26 326.604 34.2845 21 -5 8 -26 404.317 70.2535 2 5 8 26 463.869 37.6792 17 5 8 26 112.854 35.8094 9 5 8 26 162.758 48.1113 4 -5 8 -27 290.049 29.4533 21 -5 8 -27 205.798 59.7783 2 5 8 27 254.095 32.0567 17 5 8 27 42.1159 31.1587 9 5 8 27 102.686 44.5525 4 5 8 28 9.2007 24.2302 9 5 8 28 17.1707 24.4674 17 -5 9 30 57.0072 27.259 14 -5 9 29 95.4536 34.0789 14 -5 9 28 83.6189 37.5321 14 -5 9 27 50.8152 41.9998 14 5 9 -27 7.13484 47.608 1 -5 9 26 358.826 51.5933 14 5 9 -26 248.812 55.1594 1 5 9 -25 136.082 61.6505 16 -5 9 25 154.327 52.0512 14 5 9 -25 3.05851 54.4064 1 5 9 -24 303.632 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925.575 74.4841 17 6 -5 22 894.151 78.9912 22 6 5 22 694.545 79.7547 4 6 5 22 775.802 67.2809 9 6 5 23 -3.15637 56.3077 4 6 5 23 45.7179 36.9444 9 6 -5 23 49.7842 56.2158 22 6 5 23 45.4869 45.4558 17 6 5 24 -21.4665 54.2289 4 6 5 24 -8.05451 34.8479 9 6 -5 24 33.2422 55.3255 22 6 5 24 -38.7421 44.2518 17 6 5 25 91.668 42.5955 17 6 5 25 60.9446 32.3876 9 6 5 25 56.8277 51.9882 4 6 5 26 18.0144 48.9774 4 6 5 26 68.4212 37.7691 17 6 5 27 68.989 45.6626 4 6 5 27 159.545 36.7112 17 6 5 28 36.183 41.909 4 6 5 28 83.9812 32.8137 17 6 5 29 275.183 33.7201 17 6 5 30 283.258 25.9796 17 6 6 -31 244.925 51.6917 16 6 6 -30 192.91 54.653 16 -6 6 30 170.254 30.1598 14 6 6 -29 140.925 62.0019 16 -6 6 29 207.204 37.1411 14 6 6 -28 98.2747 64.7439 16 -6 6 28 157.238 38.8472 14 6 6 -27 319.784 72.4912 16 -6 6 27 353.799 45.7884 14 6 6 -27 204.263 53.9725 1 -6 6 26 103.641 45.6877 14 6 6 -26 138.731 53.4979 1 -6 6 25 216.269 50.7933 14 6 6 -25 220.277 57.223 1 -6 6 24 51.9771 53.1328 14 6 6 -24 -7.09582 57.1082 1 6 -6 -23 52.0058 72.1366 5 -6 6 23 -37.6972 55.7805 14 6 6 -23 -21.2469 59.319 1 6 -6 -22 -68.8953 75.3084 5 6 6 -22 309.358 60.3579 1 6 -6 -21 24.3089 74.5942 5 -6 6 21 25.6749 61.4149 14 6 6 -21 -65.6012 60.2957 1 -6 6 20 291.955 66.4986 14 6 6 -20 308.198 63.8453 1 6 6 -20 316.053 84.9839 11 -6 6 19 2690.14 151.023 14 6 6 -19 3052.21 159.142 11 6 6 -19 2926.39 148.27 1 6 6 -18 73.6043 83.2258 11 -6 6 18 112.24 66.4214 14 -6 6 17 -27.8953 68.6808 14 6 6 -17 98.3077 83.8097 11 -6 6 16 78.1012 72.9746 14 6 -6 -16 76.9959 82.1237 5 6 6 -16 26.4663 62.741 1 6 6 -16 129.395 84.7827 11 -6 6 15 282.775 77.631 14 6 -6 -15 236.014 77.9846 10 6 6 -15 243.89 87.2459 11 6 6 -15 192.399 70.3851 3 6 6 -15 284.922 65.5441 1 6 6 -14 13.4017 61.5839 1 -6 6 14 12.6972 76.1491 14 6 -6 -14 25.6419 73.9017 10 6 6 -14 52.1386 87.1924 11 6 6 -14 -70.9456 68.549 3 6 6 -14 -21.3475 74.9222 16 6 6 -13 81.1619 61.0562 1 -6 6 13 35.1717 75.028 14 6 6 -13 70.2195 86.7537 11 6 -6 -13 96.2323 69.3956 10 6 6 -13 102.943 69.261 3 6 6 -13 91.8369 74.2803 16 -6 6 12 1893.57 142.225 14 6 -6 -12 1996.52 135.413 10 6 6 -12 1897.05 145.943 11 6 6 -12 2032.93 143.583 16 -6 6 12 2009.93 154.098 2 6 -6 -11 776.37 86.4883 10 6 6 -11 792.795 104.069 11 -6 6 11 932.431 111.52 2 6 6 -11 691.405 87.313 3 6 6 -11 881.022 94.954 16 6 6 -11 1055.94 133.119 13 -6 6 10 123.329 99.7052 2 6 6 -10 44.7932 117.85 13 6 6 -10 72.2941 64.0194 3 6 6 -10 -35.1475 87.847 11 6 -6 -10 75.7547 50.4999 12 6 6 -10 25.667 75.4172 16 6 -6 -10 -14.3186 67.0436 10 6 6 -9 102.912 119.922 13 6 6 -9 34.6273 65.062 3 6 6 -9 72.7304 88.4762 11 6 -6 -9 104.218 51.1181 12 -6 6 9 123.073 104.487 2 6 6 -9 16.4022 74.908 16 6 6 -8 386.257 121.108 13 6 6 -8 188.796 67.8757 3 6 -6 -8 242.569 54.4305 12 -6 6 8 391.64 113.994 2 6 6 -8 250.725 82.3859 16 6 6 -7 1258.37 114.361 3 -6 6 7 1812.95 152.129 2 6 6 -7 1630.71 128.126 16 6 6 -7 1943.45 157.505 13 6 -6 -7 1412.19 108.335 12 6 6 -6 14.0559 118.701 13 6 -6 -6 -1.5546 49.806 12 -6 6 6 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18 6 6 7 244.29 64.8765 4 6 6 7 257.295 52.02 17 6 6 7 221.867 58.0013 9 6 6 8 457.993 67.2142 9 6 6 8 415.079 52.8153 18 6 6 8 388.001 69.0486 4 6 6 8 371.981 56.2545 17 -6 6 -8 483.7 86.1523 2 6 6 9 133.295 61.2521 9 6 6 9 64.1243 43.7003 18 6 6 9 108.748 63.8164 4 6 6 9 111.323 51.2129 17 -6 6 -9 23.707 80.7008 2 6 6 10 694.773 82.6219 9 6 6 10 790.605 77.5293 4 6 -6 10 470.964 69.4618 22 6 6 10 691.45 63.2291 18 6 6 10 701.007 67.6925 17 6 6 11 446.516 74.731 9 6 6 11 518.342 55.8055 18 6 6 11 526.073 63.6591 17 6 6 11 464.253 71.6129 4 6 -6 11 408.819 63.6939 22 6 6 12 207.547 68.9948 9 6 6 12 243.22 46.1692 18 6 6 12 151.841 65.4983 4 6 6 12 219.541 56.0354 17 6 -6 12 276.208 56.7247 22 6 6 13 -5.83892 65.6768 9 6 6 13 21.7854 43.5205 18 6 6 13 36.4727 62.9069 4 6 6 13 28.1373 50.2434 17 6 -6 13 -18.6801 55.1391 22 6 6 14 52.5002 65.1106 9 6 6 14 22.7102 43.7319 18 6 6 14 58.7314 62.9293 4 6 6 14 96.1224 52.1237 17 6 -6 14 108.136 56.7985 22 6 6 15 9.06051 41.8909 18 6 6 15 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6 6 25 91.5205 33.7004 9 6 6 26 55.2307 29.4958 9 6 6 26 52.7474 46.9194 4 6 6 26 161.899 36.5052 17 6 6 27 63.4828 42.7638 4 6 6 27 33.2453 32.462 17 6 6 28 252.9 33.6393 17 6 6 29 -1.68621 23.1185 17 6 7 -30 230.728 54.4598 16 -6 7 30 267.357 31.1198 14 6 7 -29 65.5264 54.6419 16 -6 7 29 41.254 33.5886 14 6 7 -28 103.672 59.9905 16 -6 7 28 99.443 36.8666 14 6 7 -27 47.1923 63.1093 16 -6 7 27 31.3178 39.4901 14 6 7 -26 60.0339 66.7926 16 -6 7 26 73.3276 44.2161 14 6 7 -25 416.83 77.6298 16 6 7 -25 347.246 60.0905 1 -6 7 25 434.628 55.4112 14 6 7 -24 433.79 78.7071 16 -6 7 24 527.264 62.5925 14 6 7 -24 432.514 65.326 1 6 -7 -23 -3.1266 68.6819 5 6 7 -23 217.592 74.5265 16 6 7 -23 145.445 59.6394 1 -6 7 23 175.626 58.1878 14 6 -7 -22 53.3399 71.6715 5 6 7 -22 140.321 59.5225 1 -6 7 22 57.2345 59.5574 14 6 -7 -21 -119.795 72.5541 5 6 7 -21 353.53 62.7976 1 -6 7 20 -11.2795 63.456 14 6 7 -20 8.70527 78.5609 16 6 -7 -20 -44.2986 72.5372 5 6 7 -20 9.25437 60.7419 1 -6 7 19 707.438 78.1244 14 6 7 -19 751.802 90.4329 16 6 7 -19 765.857 74.5376 1 -6 7 18 197.844 70.365 14 6 -7 -18 -0.66012 78.9773 5 6 7 -18 208.202 62.2552 1 6 7 -18 198.427 80.1907 16 6 7 -17 224.098 80.8078 16 6 -7 -17 4.78679 79.8349 5 -6 7 17 245.141 76.3013 14 6 7 -16 61.1801 78.9124 16 -6 7 16 -25.0906 77.8119 14 6 7 -15 -11.171 74.2675 3 -6 7 15 9.76979 78.8308 14 6 7 -15 -32.8661 63.6231 1 6 7 -15 115.012 75.1282 16 6 7 -14 140.229 63.6304 1 -6 7 14 293.843 80.1205 14 6 7 -14 270.8 77.5896 3 6 -7 -14 298.276 74.436 10 6 7 -14 201.99 76.7864 16 6 -7 -13 771.594 86.1572 10 -6 7 13 1008.57 114.303 2 6 7 -13 625.633 90.4978 3 -6 7 13 769.952 97.3075 14 6 7 -13 739.041 91.5565 16 -6 7 12 367.611 101.587 2 6 -7 -12 238.241 69.9806 10 6 7 -12 207.014 79.9819 16 6 7 -12 197.801 76.1685 3 -6 7 11 222.334 98.6251 2 6 -7 -11 271.055 70.5341 10 6 7 -11 185.392 77.1703 16 6 7 -11 242.915 73.5971 3 6 7 -10 3293.19 213.568 16 -6 7 10 3664.37 231.607 2 -6 7 9 299.054 114.809 2 -6 7 9 283.589 91.3347 8 6 7 -9 207.377 81.9167 16 6 7 -9 156.323 70.0043 3 -6 7 8 446.076 127.543 2 6 7 -8 306.907 72.5498 3 -6 7 8 521.953 102.801 8 6 7 -8 389.064 82.5109 16 -6 7 7 313.03 127.524 2 6 7 -7 255.06 69.8235 3 6 -7 -7 244.352 52.7464 12 6 7 -7 277.191 79.5388 16 -6 7 7 294.064 101.683 8 6 -7 -6 927.575 84.8031 12 6 7 -6 1020.39 105.414 16 -6 7 6 1238.33 131.262 8 6 7 -5 -9.73191 126.307 13 -6 7 5 26.9397 107.132 8 6 -7 -5 -42.3138 49.204 12 6 7 -5 -39.5453 80.4277 16 -6 7 5 6.66667 142.268 2 6 7 -4 244.23 127.765 13 -6 7 4 267.968 110.562 8 6 7 -4 144.495 42.5468 9 6 -7 -4 229.01 50.7524 12 6 7 -4 181.005 81.7283 16 -6 7 4 232.781 134.225 2 -6 7 3 134.083 113.021 8 6 7 -3 246.056 124.597 13 6 7 -3 158.316 43.7325 9 6 -7 -3 156.107 51.0579 12 -6 7 3 250.184 125.292 2 6 7 -3 191.192 80.9255 16 6 7 -2 80.9059 76.9759 16 6 7 -2 87.0987 47.0699 7 -6 7 2 269.219 116.554 8 6 7 -2 148.7 125.807 13 6 7 -2 24.2244 48.8097 18 6 -7 -2 24.2373 50.5161 12 6 7 -2 72.9881 40.9278 9 -6 7 2 92.5187 113.321 2 6 7 -1 73.1217 47.1087 7 -6 7 1 105.388 121.047 8 6 7 -1 338.535 124.414 13 6 7 -1 82.2117 84.987 16 6 7 -1 49.7365 40.8514 9 6 7 -1 62.8251 49.8916 18 -6 7 1 13.3241 111.955 2 6 7 0 509.38 56.5699 7 -6 7 0 568.597 122.77 8 6 7 0 444.001 126.844 13 6 7 0 446.024 91.8493 16 6 7 0 575.254 56.7936 9 6 7 0 497.495 57.8649 18 -6 7 0 584.984 113.589 2 -6 7 -1 122.029 115.54 8 6 7 1 94.8729 44.7292 7 6 7 1 179.553 122.934 13 6 7 1 253.942 87.9869 16 6 7 1 75.8025 46.2277 9 6 7 1 66.7159 46.3956 18 -6 7 -1 134.852 101.045 2 6 7 2 194.361 121.775 13 6 7 2 97.3361 47.5605 9 -6 7 -2 124.811 120.761 8 6 7 2 166.45 48.4847 7 6 7 2 186.555 48.1916 18 -6 7 -2 98.4607 97.6346 2 6 7 3 319.859 52.1721 9 6 7 3 399.188 52.9779 7 -6 7 -3 404.299 127.827 8 6 7 3 342.72 50.9452 18 -6 7 -3 366.652 104.421 2 6 7 4 33.3339 48.0122 9 6 7 4 10.8842 47.6547 7 -6 7 -4 49.9135 118.4 8 6 7 4 9.62719 41.8795 18 -6 7 -4 70.0353 90.264 2 6 7 5 27.8938 52.5298 9 -6 7 -5 110.239 109.632 8 -6 7 -5 -22.4831 84.2342 2 6 7 5 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69.3153 16 7 -2 -6 36.5892 79.2162 10 7 2 -6 -8.20782 84.9088 13 7 -2 -6 65.6916 94.2099 13 7 2 -6 16.5901 64.7797 12 7 -2 -6 124.293 62.0086 12 7 2 -6 72.8975 65.4812 11 7 2 -6 113.564 98.7148 5 7 -2 -6 23.0352 34.0955 18 7 2 -6 49.1285 41.9444 18 7 -2 -6 47.151 76.4138 5 7 -2 -5 1025.68 113.63 13 7 2 -5 792.683 80.6895 12 7 -2 -5 802.649 80.1686 12 7 2 -5 869.409 98.0016 13 7 -2 -5 603.237 71.4872 11 7 -2 -5 742.27 91.237 10 7 2 -5 652.323 80.6655 11 7 -2 -5 848.004 91.8011 5 7 2 -5 874.115 110.185 5 7 2 -5 788.93 95.9566 16 7 -2 -5 770.237 87.9057 16 7 -2 -5 755.429 62.1529 18 7 2 -5 749.546 68.0153 18 7 2 -4 3768.09 246.619 7 7 2 -4 4076.85 255.88 13 7 2 -4 3986.57 249.007 12 7 -2 -4 3892.06 248.257 12 7 -2 -4 4215.83 252.31 10 7 2 -4 3331.52 246.392 11 7 -2 -4 3379.41 242.624 11 7 -2 -4 3924.23 250.839 5 7 2 -4 3947.48 259.841 5 7 2 -4 3954.93 254.599 16 7 -2 -4 3637.85 251.213 16 7 -2 -4 3681.78 241.029 18 7 2 -4 3974.21 242.837 18 7 2 -3 1253.28 98.4465 7 7 2 -3 1198.36 100.472 12 7 -2 -3 1110.32 97.0666 12 7 2 -3 1264.4 111.115 13 7 2 -3 1058.69 99.4873 11 7 -2 -3 1298.42 107.002 10 7 -2 -3 1226.59 105.927 5 7 2 -3 1220.49 121.363 5 7 -2 -3 1220.98 86.4212 18 7 2 -3 1243.19 89.3318 18 7 2 -3 1191.22 113.65 16 7 -2 -3 1032.97 105.3 16 7 2 -2 21.9971 42.4009 18 7 -2 -2 81.0322 37.623 18 7 -2 -2 96.6164 74.7376 16 7 2 -2 123.167 80.829 16 7 2 -2 43.8843 57.7604 7 7 2 -2 97.9123 80.2039 13 7 -2 -2 49.4699 55.7265 12 7 2 -2 26.687 84.4795 10 7 2 -2 91.8436 64.7724 11 7 2 -2 58.3141 62.4529 12 7 2 -2 108.687 89.8528 5 7 -2 -2 82.6218 72.416 10 7 -2 -2 74.2775 68.9329 5 7 2 -1 61.7505 80.4969 16 7 -2 -1 45.4889 72.1119 16 7 -2 -1 -0.57399 59.3143 7 7 2 -1 76.3688 58.7817 7 7 2 -1 198.034 75.7162 13 7 -2 -1 52.7112 57.3563 12 7 2 -1 68.354 65.5012 11 7 2 -1 48.2908 60.0828 12 7 2 -1 147.051 86.0825 10 7 -2 -1 166.192 69.6288 5 7 2 -1 73.5469 91.9766 5 7 2 -1 16.8444 45.2777 18 7 -2 -1 45.9471 39.5843 18 7 -2 -1 74.5803 68.6067 10 7 -2 0 1490.39 114.533 7 7 2 0 1618.09 112.587 7 7 2 0 1506.59 113.798 12 7 2 0 1616.24 124.544 13 7 -2 0 1516.69 120.837 10 7 -2 0 1484.03 114.724 12 7 2 0 1653.52 129.862 10 7 -2 0 1497.96 118.269 5 7 2 0 1523.57 133.182 5 7 -2 0 1512.62 104.829 18 7 2 0 1463.69 106.885 18 7 2 0 1382.31 129.284 16 7 -2 1 195.861 61.2367 7 7 2 1 186.337 56.6041 7 7 2 1 151.226 74.7805 13 7 -2 1 178.021 59.4781 12 7 2 1 208.035 81.0866 10 7 2 1 220.573 60.5456 12 7 -2 1 212.477 67.2164 5 7 -2 1 117.937 41.6396 18 7 2 1 158.182 46.7588 18 7 2 1 127.597 88.4787 16 7 2 2 128.169 78.3511 13 7 -2 2 119.907 55.6635 12 7 2 2 67.0232 78.0017 10 7 2 2 88.406 60.3535 12 7 -2 2 143.725 66.5152 5 7 -2 2 23.0535 42.8783 18 7 2 2 97.3504 44.4101 18 7 -2 2 65.8174 57.8103 7 7 2 2 68.3983 56.6198 7 7 -2 3 656.328 71.1632 7 7 2 3 671.809 70.7684 7 7 2 3 584.64 71.8838 12 7 2 3 694.641 88.7616 13 7 2 3 646.003 62.8095 17 7 2 3 688.532 88.2807 10 7 -2 3 633.948 73.4616 12 7 2 3 583.788 62.1084 18 7 2 3 560.15 66.2365 9 7 -2 4 4721.74 327.175 7 7 2 4 5158.16 328.356 7 7 2 4 5008.1 328.967 12 7 2 4 5619.77 334.687 13 7 2 4 5669.93 327.143 17 7 -2 4 5020.38 324.41 17 7 2 4 5506.61 333.47 10 7 2 4 5219.36 326.432 18 7 2 4 5201.38 326.663 9 7 -2 5 2501.72 175.299 7 7 2 5 2645.25 176.015 7 7 2 5 2767.28 185.739 13 7 2 5 2780.69 173.907 17 7 -2 5 2675.96 171.286 17 7 2 5 2445.81 175.794 12 7 2 5 2768.05 183.814 10 7 2 5 2545.63 172.802 18 7 2 5 2771.9 173.732 9 7 2 6 65.8165 57.6029 7 7 -2 6 62.5221 52.2144 7 7 2 6 90.254 77.5199 13 7 -2 6 -6.13869 96.0935 13 7 2 6 78.9129 46.8636 17 7 -2 6 57.6366 39.0484 17 7 2 6 43.7743 55.1731 12 7 2 6 14.5538 48.7838 18 7 2 6 113.95 50.1468 9 7 2 7 3396.58 224.867 13 7 2 7 3496.94 213.729 9 7 2 7 3072.42 215.423 12 7 -2 7 3276.54 215.597 7 7 2 7 3154.91 216.782 7 7 2 7 3117.35 212.505 18 7 -2 7 3201.94 210.946 17 7 2 7 3234.58 213.858 17 7 -2 8 718.297 96.4363 13 7 2 8 636.273 87.832 13 7 2 8 499.115 59.8482 9 7 2 8 422.842 63.2441 12 7 2 8 505.058 57.5098 18 7 -2 8 506.733 53.0324 17 7 2 8 535.284 61.5373 17 7 -2 8 422.215 62.5907 7 7 2 9 22.0048 47.7208 18 7 -2 9 50.2994 54.3534 7 7 -2 9 -20.0228 82.758 13 7 2 9 85.0474 82.6781 13 7 -2 9 40.8958 42.6565 17 7 2 9 68.9799 52.8779 17 7 2 9 8.49195 53.1989 12 7 2 9 -13.5137 68.6313 4 7 2 9 13.2779 49.3694 9 7 2 10 -19.4261 48.5 18 7 -2 10 32.9809 52.0915 7 7 2 10 -57.4481 87.6106 13 7 -2 10 123.923 78.2159 13 7 2 10 50.293 48.8102 17 7 -2 10 57.1965 42.3741 17 7 2 10 -11.7296 52.9899 12 7 2 10 24.3686 49.652 9 7 2 10 -53.523 71.7994 4 7 -2 11 843.755 79.2378 7 7 -2 11 1190.37 99.671 13 7 2 11 916.8 77.0501 9 7 2 11 878.825 91.7028 4 7 2 11 964.909 78.6955 17 7 -2 11 917.076 73.0684 17 7 2 11 778.978 77.5778 18 7 2 11 818.896 78.6389 12 7 2 12 1661.7 130.499 12 7 2 12 2024.07 129.955 9 7 2 12 1976.83 140.852 4 7 -2 12 1902.6 127.879 17 7 2 12 1893.12 131.414 17 7 2 12 1906.61 131.29 18 7 -2 12 1911.31 131.169 7 7 2 13 210.801 48.9238 18 7 -2 13 208.597 46.5139 17 7 2 13 268.788 53.2565 17 7 2 13 212.595 50.5565 9 7 2 13 163.69 71.3761 4 7 -2 13 170.539 53.5467 7 7 2 14 13.8878 48.1378 18 7 -2 14 74.2225 44.6171 17 7 2 14 62.3517 52.0504 17 7 2 14 89.2981 47.0743 9 7 2 14 139.713 70.1196 4 7 -2 14 103.777 51.0767 7 7 2 15 1941.03 128.777 9 7 -2 15 1921.31 129.349 17 7 2 15 1923.08 132.894 17 7 2 15 1828.42 131.032 18 7 -2 15 1855.67 130.992 7 7 2 16 748.462 65.8449 9 7 -2 16 737.564 66.8868 17 7 2 16 676.984 70.537 17 7 2 16 749.438 66.22 18 7 -2 16 596.241 68.0911 7 7 2 17 84.2489 48.3832 18 7 -2 17 60.2341 47.7443 17 7 2 17 71.7059 52.471 17 7 2 17 56.1484 45.2945 9 7 2 17 91.9437 68.3122 4 7 -2 17 19.6377 48.6588 7 7 -2 18 221.83 50.0681 17 7 2 18 293.852 54.9087 17 7 2 18 321.855 52.8972 18 7 2 18 270.383 70.9899 4 7 2 19 81.7455 49.0729 17 7 2 19 62.9935 65.7661 4 7 2 19 92.3996 44.6364 18 7 2 20 413.576 49.3097 9 7 2 20 460.169 68.8961 4 7 -2 20 404.023 52.9019 7 7 -2 21 63.0645 42.0649 17 7 2 21 58.4163 47.1836 17 7 2 21 22.6694 42.0566 18 7 2 21 70.8028 62.1702 4 7 -2 21 46.5639 42.1772 7 7 -2 22 106.059 41.211 17 7 2 22 151.776 46.5083 17 7 2 22 165.834 40.5344 18 7 2 22 201.306 61.4033 4 7 -2 22 140.148 41.6044 7 7 2 23 -23.1058 36.6883 18 7 -2 23 34.8217 36.1882 17 7 2 23 43.9401 42.9006 17 7 2 23 -71.9683 56.3805 4 7 2 24 -64.1069 34.381 18 7 2 24 -14.5777 41.0447 17 7 2 24 20.3748 52.3225 4 7 2 25 133.454 39.4956 17 7 2 25 154.509 33.1448 18 7 2 26 124.31 36.6615 17 7 2 26 127.196 28.8649 18 7 2 27 -35.8054 32.4394 7 7 2 27 -26.2353 32.7692 17 7 -2 27 -23.8966 28.2502 18 7 2 28 15.1372 27.537 7 7 -2 28 -8.49147 22.9995 18 7 2 28 30.9171 27.5785 17 7 2 29 -21.2026 23.1088 17 7 3 -31 42.3257 49.5546 16 7 -3 -30 -14.9089 38.9263 11 7 3 -30 377.566 58.7821 16 7 -3 -29 -17.4708 45.3049 11 7 3 -29 157.511 59.8804 16 7 -3 -28 27.2331 49.0859 11 7 3 -28 -14.4156 57.7241 11 7 3 -28 134.691 63.9321 16 7 -3 -27 4.73269 54.3769 11 7 3 -27 26.3232 60.6655 11 7 -3 -26 -13.9666 59.98 11 7 3 -26 116.632 63.6733 11 7 3 -26 201.818 73.1827 16 7 -3 -25 82.559 83.8325 5 7 3 -25 216.064 70.2111 11 7 -3 -24 168.271 84.8286 5 7 3 -24 280.768 73.4451 11 7 3 -24 272.724 80.5047 16 7 -3 -23 132.507 87.6818 5 7 3 -23 142.696 74.0642 11 7 3 -23 152.84 80.5789 16 7 3 -22 141.391 74.468 11 7 -3 -22 189.884 87.5655 5 7 -3 -21 104.311 92.2266 5 7 3 -21 30.8123 79.4114 16 7 -3 -20 1010.62 124.239 5 7 3 -20 1213.69 108.48 11 7 3 -20 1201.21 112.595 16 7 -3 -19 1095.93 123.725 5 7 3 -19 1262.26 109.912 11 7 3 -19 1322.09 117.327 16 7 3 -18 912.271 98.5215 11 7 3 -18 1000.66 102.544 16 7 3 -17 629.777 81.7222 11 7 3 -17 643.206 91.5112 16 7 3 -17 367.207 109.512 13 7 -3 -16 462.64 96.2487 5 7 3 -16 553.972 77.4427 11 7 3 -16 456.863 85.146 16 7 3 -16 282.234 113.504 13 7 -3 -15 255.808 89.1009 5 7 3 -15 229.024 71.7764 11 7 3 -15 264.449 83.6677 16 7 3 -15 17.7916 109.001 13 7 -3 -14 29.206 87.7948 5 7 3 -14 9.48171 79.7657 16 7 3 -14 73.0911 104.426 13 7 -3 -14 -27.5705 85.6982 13 7 3 -14 18.1083 71.1874 11 7 -3 -14 7.57534 91.7342 10 7 3 -13 211.867 107.148 13 7 -3 -13 318.835 89.0265 13 7 3 -13 303.589 75.9734 11 7 -3 -13 300.416 92.0221 10 7 3 -13 245.049 81.8063 16 7 -3 -13 261.512 90.083 5 7 -3 -12 1043.96 110.065 5 7 3 -12 1162.98 136.638 5 7 -3 -12 1118.43 114.29 10 7 3 -12 1021.21 100.214 11 7 3 -12 1166.23 106.896 16 7 -3 -12 997.194 113.852 13 7 -3 -12 1044.38 94.9905 12 7 3 -12 1022.38 124.193 13 7 3 -11 192.952 106.897 13 7 -3 -11 82.4184 89.0104 13 7 3 -11 97.1352 73.8434 11 7 -3 -11 162.634 89.5346 10 7 -3 -11 176.12 65.315 12 7 3 -11 154.617 116.43 5 7 3 -11 138.618 82.7942 16 7 -3 -11 248.928 86.2752 5 7 -3 -10 1365.58 115.535 5 7 3 -10 1053.65 140.631 5 7 -3 -10 1421.46 120.579 10 7 3 -10 1200.31 107.825 11 7 3 -10 1123.33 115.844 16 7 -3 -10 1218.94 103.154 16 7 -3 -10 881.088 122.406 13 7 -3 -10 1263.3 103.089 12 7 3 -10 1202.92 141.156 13 7 -3 -9 121.161 84.875 10 7 3 -9 155.899 110.127 13 7 -3 -9 61.5045 95.8963 13 7 -3 -9 100.481 62.9805 12 7 3 -9 107.643 73.0765 11 7 3 -9 104.468 112.543 5 7 3 -9 154.077 82.1676 16 7 -3 -9 133.025 67.4475 16 7 -3 -9 129.669 80.6332 5 7 -3 -8 163.891 79.7105 10 7 -3 -8 211.823 99.93 13 7 3 -8 107.762 109.646 13 7 -3 -8 168.09 62.3639 12 7 3 -8 181.426 73.5707 11 7 3 -8 73.5004 109.904 5 7 -3 -8 130.396 81.5568 5 7 3 -8 156.828 81.8289 16 7 -3 -8 100.046 65.8279 16 7 3 -7 135.284 82.5723 16 7 -3 -7 117.266 69.2916 16 7 -3 -7 180.289 78.0061 10 7 3 -7 295.286 105.751 13 7 -3 -7 161.917 60.3434 12 7 3 -7 109.138 72.3761 11 7 3 -7 184.73 108.788 5 7 -3 -7 172.229 78.8793 5 7 3 -7 160.343 49.5884 18 7 3 -6 399.286 83.6041 16 7 -3 -6 284.846 71.9885 16 7 -3 -6 395.067 81.2937 10 7 3 -6 411.272 105.875 13 7 3 -6 348.93 68.8938 12 7 3 -6 336.439 74.2811 11 7 -3 -6 365.79 66.6625 12 7 3 -6 350.926 109.973 5 7 -3 -6 385.492 81.3201 5 7 3 -6 405.166 53.2794 18 7 -3 -5 218.897 71.3917 16 7 3 -5 194.798 79.9096 16 7 -3 -5 198.559 73.064 10 7 3 -5 114.963 99.1739 13 7 3 -5 226.377 64.0859 12 7 3 -5 149.321 72.3871 11 7 -3 -5 149.072 63.3807 12 7 3 -5 213.603 103.744 5 7 3 -5 202.487 47.1896 18 7 -3 -5 252.147 78.3068 5 7 3 -4 306.589 49.1753 18 7 -3 -4 300.288 73.2756 16 7 3 -4 300.876 88.7866 16 7 3 -4 312.839 62.2811 7 7 3 -4 370.235 96.5483 13 7 -3 -4 261.497 63.4383 12 7 3 -4 357.111 67.7527 12 7 3 -4 265.874 73.8468 11 7 -3 -4 353.846 75.714 10 7 -3 -4 296.597 78.6574 5 7 3 -3 793.938 77.8708 7 7 3 -3 760.05 81.1264 12 7 3 -3 850.104 110.575 13 7 -3 -3 697.37 77.2848 12 7 -3 -3 737.695 89.3479 10 7 3 -3 618.792 85.8777 11 7 -3 -3 759.314 88.0789 5 7 -3 -3 794.852 61.0307 18 7 3 -3 775.157 66.8654 18 7 -3 -3 688.759 85.0876 16 7 3 -3 780.56 96.8334 16 7 3 -2 99.1982 58.3287 7 7 3 -2 163.002 93.3374 13 7 3 -2 196.623 82.6541 16 7 -3 -2 75.3066 59.3943 12 7 3 -2 61.8532 61.3486 12 7 3 -2 54.7003 46.0303 18 7 -3 -2 107.715 36.8176 18 7 -3 -2 173.909 71.1042 5 7 3 -1 311.928 61.4309 7 7 3 -1 315.505 93.5904 13 7 3 -1 222.704 87.4579 16 7 -3 -1 241.991 58.2414 12 7 3 -1 221.711 60.0824 12 7 3 -1 307.075 49.1494 18 7 -3 -1 256.88 40.2354 18 7 -3 -1 176.468 71.1912 5 7 -3 0 59.3197 57.7094 7 7 3 0 77.9204 55.3433 7 7 3 0 77.7641 91.0051 13 7 3 0 82.2144 85.361 16 7 -3 0 102.725 56.1693 12 7 3 0 1.22175 59.2201 12 7 3 0 54.198 46.1196 18 7 -3 0 56.692 37.3424 18 7 -3 0 85.1381 65.7876 5 7 -3 1 72.8713 37.9974 18 7 3 1 65.6434 45.5007 18 7 3 1 -29.3719 89.9165 16 7 -3 1 83.2425 58.5276 7 7 3 1 84.8293 54.0233 7 7 3 1 142.339 90.2387 13 7 -3 1 121.567 56.2439 12 7 3 1 114.572 59.1458 12 7 -3 1 62.6163 64.125 5 7 3 1 84.8774 50.8887 9 7 -3 2 712.278 76.5224 7 7 3 2 777.016 76.0861 7 7 3 2 756.256 78.1643 12 7 3 2 958.71 108.07 13 7 -3 2 644.269 77.7623 12 7 -3 2 616.126 79.3466 5 7 3 2 791.276 68.8582 18 7 3 2 890.607 71.3533 9 7 -3 3 65.3321 56.365 7 7 3 3 98.4975 58.1843 7 7 3 3 136.347 91.4029 13 7 3 3 57.1467 48.0768 17 7 3 3 113.139 58.0347 12 7 3 3 58.866 47.3152 18 7 3 3 76.4443 50.4455 9 7 -3 4 186.786 57.8378 7 7 3 4 172.548 58.9069 7 7 3 4 280.314 94.7202 13 7 3 4 194.704 49.0501 17 7 3 4 227.01 57.6718 12 7 3 4 180.685 49.9931 18 7 3 4 157.13 50.7375 9 7 3 5 260.07 59.3769 7 7 -3 5 312.964 60.3782 7 7 3 5 392.506 100.305 13 7 3 5 352.694 55.3259 17 7 3 5 320.468 59.6846 12 7 3 5 259.15 52.0493 18 7 3 5 348.496 54.864 9 7 3 6 -2.84494 58.3542 7 7 -3 6 -63.9814 52.1983 7 7 3 6 22.6517 94.6749 13 7 3 6 51.6269 50.6967 17 7 3 6 9.27532 54.7203 12 7 3 6 48.9716 48.2253 18 7 3 6 3.80058 49.1463 9 7 3 7 1704.87 131.146 12 7 3 7 2000.01 157.218 13 7 3 7 2030.52 129.085 9 7 3 7 1848.67 128.406 18 7 3 7 1997.98 129.703 17 7 -3 7 1694.81 129.388 7 7 -3 8 129.15 51.7191 7 7 3 8 243.353 99.3517 13 7 3 8 120.043 51.364 17 7 3 8 123.689 54.5181 12 7 3 8 142.184 48.1099 18 7 3 8 143.545 50.298 9 7 3 9 521.215 61.2986 18 7 -3 9 444.68 60.8723 7 7 3 9 585.052 100.682 13 7 3 9 467.352 62.9336 17 7 3 9 475.011 62.4226 12 7 3 9 546.27 78.3366 4 7 3 9 555.335 59.3507 9 7 3 10 394.507 55.5478 18 7 -3 10 360.742 57.7214 7 7 3 10 373.105 58.4238 17 7 3 10 350.122 58.3053 12 7 3 10 376.654 56.0064 9 7 3 10 434.775 76.7139 4 7 3 11 725.393 70.8551 9 7 3 11 796.617 89.2533 4 7 3 11 759.842 72.8404 18 7 -3 11 744.082 66.3801 17 7 3 11 858.195 75.4929 17 7 -3 11 772.65 74.4467 7 7 3 12 866.086 75.1275 9 7 3 12 810.64 92.2898 4 7 3 12 878.094 75.1736 18 7 3 12 952.372 77.5145 17 7 -3 12 830.043 70.4795 17 7 -3 12 946.054 78.1614 7 7 3 13 121.422 49.325 18 7 -3 13 98.3934 41.3449 17 7 3 13 111.427 54.1078 17 7 3 13 144.736 48.2383 9 7 3 13 195.737 71.5642 4 7 -3 13 100.276 50.2008 7 7 -3 14 172.802 43.0239 17 7 3 14 161.269 52.8501 17 7 3 14 170.807 50.7161 9 7 3 14 206.942 47.6309 18 7 -3 14 215.055 52.1502 7 7 3 15 661.107 65.5575 9 7 3 15 684.375 65.984 18 7 -3 15 651.771 61.3356 17 7 3 15 759.937 69.7853 17 7 -3 15 725.491 67.1645 7 7 3 16 489.033 57.22 9 7 3 16 537.675 78.1893 4 7 3 16 525.69 59.7111 18 7 -3 16 474.141 53.9319 17 7 3 16 583.233 63.1934 17 7 -3 16 440.923 59.0781 7 7 3 17 1612.86 104.197 9 7 3 17 1462.72 117.729 4 7 3 17 1516.28 105.791 18 7 -3 17 1359.08 103.19 17 7 3 17 1572.87 109.27 17 7 -3 17 1326.38 104.693 7 7 3 18 1793.05 116.364 18 7 -3 18 1527.28 113.566 17 7 3 18 1728.23 119.387 17 7 3 18 1631.23 126.444 4 7 3 19 21.9769 66.0551 4 7 3 19 76.5779 43.2062 9 7 3 20 1206.33 101.953 4 7 3 20 1288.27 89.7875 18 7 3 20 1141.44 86.9476 9 7 3 21 1329.7 105.044 4 7 3 21 1308.85 93.9461 18 7 3 21 1354.11 97.3321 17 7 3 21 1285.35 92.6844 9 7 3 22 113.937 38.5322 18 7 3 22 129.08 45.4269 17 7 3 22 106.686 60.5925 4 7 3 23 42.0735 34.7159 18 7 3 23 -47.9679 42.1587 17 7 3 23 -1.79094 56.5915 4 7 3 24 358.67 40.946 18 7 3 24 450.446 50.0345 17 7 3 24 337.896 58.8524 4 7 3 25 1182.09 74.7533 17 7 3 25 696.659 79.2318 4 7 3 26 50.3559 36.1084 17 7 3 27 5.87266 31.3445 17 7 3 27 -3.32124 32.4 7 7 3 28 2.4707 27.9591 7 7 -3 28 61.5368 22.9343 18 7 3 28 57.5498 27.2494 17 7 3 29 235.429 25.2027 17 7 4 -31 195.587 49.0021 16 7 -4 -30 25.3471 36.0345 11 7 4 -30 24.3671 53.6546 16 7 -4 -29 -40.644 42.3707 11 7 4 -29 468.045 64.2155 16 7 -4 -28 4.71003 49.3828 11 7 4 -28 149.014 62.9538 16 7 -4 -27 27.5277 52.3205 11 7 4 -27 126.804 66.3622 16 7 4 -26 56.694 66.6002 11 7 4 -26 133.891 70.6586 16 7 4 -25 123.478 68.7166 11 7 4 -25 79.3403 73.1163 16 7 -4 -24 119.691 82.6426 5 7 4 -24 260.769 72.6854 11 7 4 -24 211.855 77.9904 16 7 -4 -23 1.24686 79.4536 5 7 4 -23 41.7876 72.8694 11 7 4 -23 72.5564 76.9455 16 7 4 -22 10.9429 73.6406 11 7 -4 -22 -44.1292 86.9803 5 7 -4 -21 13.1942 89.6618 5 7 -4 -20 234.394 88.0325 5 7 4 -20 50.4449 80.8268 16 7 -4 -19 120.492 88.203 5 7 4 -19 90.4275 80.4043 11 7 4 -19 135.186 83.1306 16 7 -4 -18 87.0272 87.7114 5 7 4 -18 80.3473 82.5566 16 7 4 -18 179.139 79.9718 11 7 4 -17 10.1185 78.2526 16 7 4 -17 -33.6252 78.3657 11 7 4 -16 6.01823 81.7806 16 7 4 -16 -39.6005 80.3834 11 7 4 -16 -86.7688 110.669 13 7 -4 -15 92.2819 88.0928 10 7 4 -15 25.3016 80.1405 11 7 4 -15 -125.895 111.907 13 7 4 -15 98.8103 78.73 16 7 -4 -15 -27.3843 85.2386 5 7 -4 -14 359.049 90.1654 10 7 4 -14 296.348 82.52 11 7 4 -14 160.444 116.368 13 7 -4 -14 135.406 84.2163 13 7 4 -14 304.706 84.4751 16 7 -4 -14 174.923 88.3225 5 7 -4 -13 -12.3479 88.4991 10 7 4 -13 131.901 81.3074 11 7 4 -13 102.511 114.642 13 7 -4 -13 74.7818 84.0484 13 7 4 -13 -3.87284 80.1419 16 7 -4 -13 38.4272 85.992 5 7 -4 -12 -21.3538 88.317 10 7 -4 -12 86.6504 61.0987 12 7 4 -12 -7.63335 81.3973 11 7 4 -12 81.2955 113.078 13 7 -4 -12 8.37129 87.4429 13 7 4 -12 66.754 80.2104 16 7 -4 -12 98.7472 84.5633 5 7 -4 -11 150.204 84.0674 10 7 -4 -11 74.4534 61.9788 12 7 4 -11 -16.2005 78.2859 11 7 -4 -11 41.881 90.8708 13 7 4 -11 8.98749 108.324 13 7 4 -11 13.9228 86.5907 16 7 -4 -11 126.403 82.6842 5 7 -4 -10 -55.4449 83.4038 10 7 -4 -10 24.388 61.4149 12 7 4 -10 -12.7386 78.8729 11 7 4 -10 -0.99202 108.545 13 7 -4 -10 17.8602 97.0867 13 7 4 -10 8.95537 84.874 16 7 -4 -10 -61.8845 83.6438 5 7 -4 -9 134.892 79.0978 10 7 4 -9 68.5755 78.4697 11 7 -4 -9 87.5397 59.3567 12 7 4 -9 266.371 106.403 13 7 4 -9 138.456 88.4701 16 7 -4 -9 111.591 82.2789 5 7 -4 -8 154.009 77.7581 10 7 4 -8 233.259 107.768 13 7 4 -8 138.676 79.4444 11 7 -4 -8 116.696 60.2139 12 7 -4 -8 242.103 85.1276 5 7 4 -8 138.448 90.3607 16 7 -4 -7 1436.47 118.448 5 7 4 -7 1250.13 115.671 11 7 -4 -7 1238.34 114.544 10 7 4 -7 1362.73 125.523 16 7 -4 -7 1220.36 104.144 12 7 4 -7 1539.54 143.275 13 7 -4 -6 182.475 76.9611 10 7 4 -6 121.953 116.192 13 7 4 -6 100.046 84.908 16 7 4 -6 194.201 78.5815 11 7 -4 -6 186.264 60.6976 12 7 4 -6 209.84 50.0254 18 7 -4 -6 195.748 83.0011 5 7 -4 -5 164.292 75.0654 10 7 4 -5 272.815 118.002 13 7 -4 -5 263.74 80.426 5 7 4 -5 207.938 80.2632 11 7 -4 -5 94.246 61.0121 12 7 4 -5 204.178 47.3687 18 7 4 -5 165.317 87.7526 16 7 4 -4 403.615 89.3784 16 7 4 -4 595.34 125.35 13 7 4 -4 374.604 63.1166 7 7 -4 -4 393.541 65.1161 12 7 4 -4 419.614 68.4984 12 7 4 -4 393.702 55.8798 18 7 -4 -4 440.742 83.1884 5 7 4 -3 483.429 97.5292 16 7 4 -3 474.421 121.474 13 7 4 -3 562.327 67.2334 7 7 -4 -3 437.073 65.6682 12 7 4 -3 410.193 70.8132 12 7 4 -3 430.434 58.0003 18 7 -4 -3 543.731 82.9577 5 7 4 -2 120.959 82.1781 16 7 4 -2 74.7838 58.17 7 7 4 -2 -22.2322 110.708 13 7 -4 -2 56.6956 58.0606 12 7 4 -2 -34.3277 59.5883 12 7 4 -2 -3.34799 48.3923 18 7 -4 -2 111.531 71.927 5 7 4 -1 1895.35 131.469 7 7 4 -1 1797.16 133.971 12 7 -4 -1 1791.34 132.327 12 7 -4 -1 1848.29 138.053 5 7 -4 -1 1783.76 122.55 18 7 4 -1 1887.11 127.255 18 7 4 -1 1854.74 148.238 16 7 4 0 393.511 92.6093 16 7 4 0 358.713 60.7048 7 7 4 0 381.93 114.278 13 7 -4 0 436.201 66.2278 12 7 4 0 278.038 64.8853 12 7 -4 0 525.872 74.087 5 7 -4 0 323.94 44.6213 18 7 4 0 347.939 54.132 18 7 4 0 346.57 57.2777 9 7 4 1 -34.4002 91.3434 16 7 4 1 139.467 53.6811 7 7 4 1 0.98812 110.546 13 7 4 1 55.2929 48.4045 18 7 -4 1 54.42 38.9265 18 7 4 1 32.9015 59.4318 12 7 -4 1 -1.24263 61.0629 12 7 -4 1 118.775 66.6317 5 7 4 1 22.6158 50.1761 9 7 -4 2 382.805 63.9493 7 7 4 2 422.11 62.6572 7 7 4 2 667.85 118.908 13 7 4 2 460.72 54.2304 18 7 4 2 459.51 64.0842 12 7 -4 2 418.055 70.2541 5 7 4 2 438.822 58.1631 9 7 4 3 629.889 68.2469 7 7 -4 3 513.727 67.7073 7 7 4 3 586.531 69.1396 12 7 4 3 655.933 119.01 13 7 4 3 642.802 62.8228 18 7 -4 3 510.921 71.4321 5 7 4 3 546.649 61.9685 9 7 -4 4 3.41678 56.5002 7 7 4 4 -5.57535 55.9074 7 7 4 4 -38.4575 108.672 13 7 4 4 -37.4383 47.3791 18 7 4 4 -44.225 55.6613 12 7 4 4 11.6628 49.9681 17 7 4 4 71.6407 51.6318 9 7 4 5 278.403 59.7474 7 7 -4 5 312.403 59.5756 7 7 4 5 374.662 108.818 13 7 4 5 330.235 53.5804 18 7 4 5 292.589 58.6138 12 7 4 5 301.96 55.6242 17 7 4 5 351.77 55.4472 9 7 -4 6 2500.32 168.966 7 7 4 6 2364.18 170.611 7 7 4 6 2301.67 168.759 12 7 4 6 2613.15 190.95 13 7 4 6 2415.96 168.112 18 7 4 6 2929.47 170.236 17 7 4 6 2717.82 167.717 9 7 -4 7 27.3904 53.3844 7 7 4 7 121.726 95.6331 13 7 4 7 81.5037 50.6975 18 7 4 7 87.894 52.1697 12 7 4 7 99.7432 48.9852 9 7 4 7 22.0788 50.5382 17 7 4 8 107.543 96.2737 13 7 4 8 188.815 52.4825 17 7 4 8 211.751 50.3281 18 7 4 8 172.104 50.6229 9 7 -4 8 110.354 52.7948 7 7 4 9 109.907 50.3096 9 7 -4 9 75.3168 50.6924 7 7 4 9 163.078 96.6905 13 7 4 9 109.86 47.4436 18 7 4 9 134.81 71.1351 4 -7 4 -9 93.7764 72.9664 2 7 4 9 121.157 52.812 17 -7 4 -10 2017.15 169.044 2 7 4 10 2356.72 157.725 18 7 4 10 2561.91 158.722 17 7 4 10 2391.44 165.485 4 7 -4 10 2388.46 157.111 7 7 4 10 2290.07 157.166 9 7 4 11 312.533 55.7356 17 7 4 11 269.737 53.7998 18 7 4 11 304.669 74.2884 4 7 -4 11 201.65 51.4111 7 7 4 11 299.409 54.2624 9 7 4 12 574.278 62.6539 18 7 4 12 624.368 67.3518 17 7 4 12 545.437 81.4751 4 7 4 12 644.753 64.8281 9 7 -4 12 590.79 62.2124 7 7 4 13 15.5039 48.4981 18 7 -4 13 120.626 46.9731 7 7 4 13 34.5631 48.2715 9 7 4 13 38.3819 55.4966 17 7 4 14 0.59146 47.0328 18 7 4 14 43.1207 48.7149 9 7 4 14 60.3683 54.3097 17 7 4 15 1003.14 82.9708 18 7 4 15 1156.48 87.5145 17 7 4 15 983.888 82.2156 9 7 4 15 952.929 97.0249 4 7 4 16 609.469 61.2373 18 7 4 16 630.368 68.4505 17 7 4 16 597.901 80.3345 4 7 4 16 615.829 61.9809 9 7 4 17 61.0671 44.8499 18 7 4 17 -15.5805 69.2901 4 7 4 17 28.3171 49.689 17 7 4 18 256.755 71.0007 4 7 4 18 268.883 52.614 17 7 4 19 321.766 48.4318 9 7 4 19 268.415 69.2008 4 7 4 20 915.437 76.5201 17 7 4 20 905.577 69.8205 18 7 4 20 889.773 85.9905 4 7 4 20 795.403 69.9329 9 7 4 21 -16.2412 37.9545 18 7 4 21 25.2229 60.8529 4 7 4 21 17.9073 39.5556 9 7 4 21 17.6831 45.667 17 7 4 22 75.2115 35.0813 18 7 4 22 14.5041 59.8678 4 7 4 22 51.718 46.641 17 7 4 22 63.1033 36.6261 9 7 4 23 54.1448 55.6115 4 7 4 23 -12.3666 43.0607 17 7 4 23 4.06739 35.3141 9 7 4 24 50.7834 52.2598 4 7 4 24 20.1733 41.8413 17 7 4 25 185.602 49.6462 4 7 4 25 276.045 40.7271 17 -7 4 -25 97.9396 54.6547 2 7 4 26 -15.4288 32.575 17 7 4 27 72.1369 29.9032 17 7 4 27 74.1758 32.194 7 7 4 28 -19.9172 27.3884 7 7 -4 28 42.5589 22.6351 18 7 4 28 14.6691 26.9223 17 7 5 -30 61.6922 54.147 16 7 5 -29 223.474 59.4918 16 7 -5 -29 6.35449 38.6997 11 7 5 -28 12.7516 62.3719 16 7 -5 -28 -30.5168 45.3115 11 7 5 -27 63.9772 67.1412 16 7 -5 -27 -44.0506 50.9375 11 7 5 -26 80.9292 69.5985 16 7 5 -25 168.121 73.6342 16 7 5 -24 68.8172 76.8087 16 7 -5 -24 8.07697 73.9775 5 7 -5 -23 -19.644 76.6465 5 7 5 -23 130.132 78.6045 16 7 5 -23 72.3004 77.2797 11 7 5 -22 428.695 82.198 16 7 5 -22 318.685 80.4713 11 7 -5 -21 28.3812 83.7424 5 7 5 -21 207.246 79.6767 11 7 -5 -20 147.938 84.611 5 7 5 -19 1162.41 100.336 16 7 -5 -19 494.601 102.035 5 7 -5 -18 57.2035 83.7658 5 7 5 -18 84.1058 81.8051 16 7 5 -18 127.695 84.2425 11 7 -5 -17 116.245 83.3941 5 7 5 -17 195.204 84.6549 11 7 5 -17 66.8944 83.742 16 7 5 -16 188.519 86.2675 11 7 5 -16 181.03 84.7155 16 7 5 -15 701.82 95.7412 11 7 -5 -15 396.605 93.5336 10 7 5 -15 656.04 91.1221 16 7 -5 -14 70.6699 87.1846 10 7 5 -14 147.864 85.4991 11 7 5 -14 228.951 119.422 13 7 5 -14 144.332 82.7806 16 7 -5 -13 581.298 91.2702 10 7 5 -13 665.093 93.075 11 7 5 -13 671.44 126.586 13 -7 5 13 380.815 76.4524 14 7 -5 -13 384.795 90.9127 5 7 5 -13 495.492 91.2258 16 7 -5 -12 644.907 94.2464 10 7 -5 -12 491.192 69.24 12 7 5 -12 679.45 94.5393 11 7 5 -12 632.283 128.907 13 -7 5 12 597.805 78.9239 14 7 -5 -12 454.217 93.668 5 7 5 -12 620.476 94.7852 16 7 -5 -11 6.12427 82.0528 10 7 5 -11 181.482 123.556 13 7 -5 -11 31.924 100.727 13 -7 5 11 9.23818 68.0846 14 7 -5 -11 30.7897 58.3186 12 7 5 -11 105.536 88.3439 11 7 -5 -11 137.443 84.4192 5 7 5 -11 25.0389 87.0434 16 7 -5 -10 1303.38 107.787 12 7 5 -10 1537.61 153.99 13 7 -5 -10 1510.61 120.863 10 7 5 -10 1368.31 124.212 11 7 -5 -10 1378.79 124.45 5 -7 5 10 1296.02 115.419 14 7 5 -10 1320.03 128.807 16 7 5 -9 287.455 88.8576 11 7 -5 -9 274.065 62.343 12 7 5 -9 307.519 122.616 13 7 -5 -9 214.072 78.5352 10 7 5 -9 342.204 99.1629 16 7 -5 -9 197.092 87.5022 5 7 5 -8 3644.49 233.917 13 7 -5 -8 2936.07 201.712 12 7 -5 -8 3043.99 213.019 5 7 5 -8 3382.2 217.366 16 7 5 -8 2974.5 212.598 11 7 -5 -8 2853.77 208.978 10 7 -5 -7 -89.1356 75.6776 10 7 5 -7 12.0644 87.7855 16 7 5 -7 120.211 118.772 13 7 -5 -7 29.9425 58.2814 12 7 5 -6 70.7849 80.8587 16 7 5 -6 63.9478 118.244 13 7 -5 -6 -61.7113 57.6052 12 7 5 -5 687.209 71.0897 18 7 5 -5 792.984 99.1895 16 7 -5 -5 714.237 77.0767 12 7 5 -5 806.666 126.304 13 7 5 -4 719.82 103.663 16 7 5 -4 714.826 121.606 13 7 5 -4 742.163 68.4069 18 7 -5 -4 574.906 73.0413 12 7 5 -3 1983.94 136.315 7 7 5 -3 1882.81 155.175 16 7 5 -3 2228.74 172.055 13 7 5 -3 2025.97 134.587 18 7 -5 -3 1769.73 136.967 12 7 5 -2 34.1572 57.2221 7 7 5 -2 33.4897 108.5 13 7 5 -2 -27.3503 92.5592 16 7 5 -2 44.9412 48.7889 18 7 -5 -2 80.9846 55.8972 12 7 5 -1 219.234 57.0304 7 7 5 -1 159.483 108.624 13 7 5 -1 137.415 92.4922 16 7 5 -1 123.543 50.2769 9 7 5 -1 111.874 49.1343 18 7 -5 -1 64.4353 58.8142 12 7 5 -1 88.2417 60.9183 12 7 5 0 -3.40279 54.5444 7 7 5 0 152.343 107.203 13 7 5 0 75.7196 89.3793 16 7 5 0 4.33852 49.5628 9 7 5 0 -19.8738 48.5704 18 7 -5 0 49.3335 56.4787 12 7 5 0 25.8179 58.4571 12 7 5 1 44.7566 52.6948 7 7 5 1 99.9032 107.555 13 7 5 1 106.252 92.8646 16 7 5 1 4.78539 51.1122 9 7 5 1 56.7642 49.2879 18 7 -5 1 19.694 35.8533 18 7 5 1 5.44363 57.0805 12 7 5 2 26.838 55.2673 12 7 5 2 -56.9641 110.413 13 7 5 2 -11.8909 52.4761 7 7 5 2 27.1363 48.9409 9 7 -5 2 31.2131 66.1744 5 7 5 2 -19.3078 50.4823 18 7 -5 3 1531.66 137.813 5 7 5 3 2146.46 136.086 7 7 5 3 2241.88 167.448 13 7 5 3 1802.18 135.199 12 7 5 3 1906.33 133.993 18 -7 5 -3 1885.53 152.664 2 7 5 3 2151.23 133.108 9 7 5 4 82.1169 55.093 7 7 5 4 119.826 106.545 13 7 5 4 51.174 49.7722 18 7 5 4 -38.0754 54.5904 12 7 5 4 8.30157 49.2461 9 -7 5 -4 152.171 86.5146 2 7 -5 5 168.989 56.039 7 7 5 5 287.965 59.3838 7 7 5 5 239.378 110.508 13 7 5 5 295.248 52.5712 17 7 5 5 239.994 51.9223 18 7 5 5 234.522 54.3637 9 -7 5 -5 351.84 85.9763 2 7 5 6 41.2693 55.1003 7 7 -5 6 62.6898 53.6143 7 7 5 6 39.3899 109.832 13 7 5 6 33.2266 50.897 17 7 5 6 13.6564 47.0675 18 7 5 6 -20.7726 50.5515 9 -7 5 -6 33.4051 77.6917 2 7 5 7 20.1555 55.9912 7 7 -5 7 44.0798 53.2363 7 7 5 7 -3.84681 108.503 13 7 5 7 69.9531 55.0159 17 7 5 7 35.7787 47.781 18 7 5 7 18.1364 50.8956 9 -7 5 -7 -26.7783 79.3695 2 7 -5 8 136.22 54.4017 7 7 5 8 208.762 108.674 13 7 5 8 219.275 54.0789 9 -7 5 -8 128.107 80.3307 2 7 5 8 201.815 50.1818 18 7 5 8 193.321 54.7126 17 7 5 9 876.825 76.4853 18 7 5 9 978.714 79.9017 17 7 5 9 871.339 77.3685 9 7 -5 9 956.828 78.0623 7 7 5 9 652.942 90.6044 4 -7 5 -9 713.339 98.7244 2 -7 5 -10 1558.81 136.215 2 7 5 10 1888.67 121.042 9 7 5 10 1459.38 131.14 4 7 5 10 1803.84 121.754 17 7 5 10 1654.97 120.992 18 7 5 11 875.319 75.2029 9 7 5 11 805.996 90.4041 4 -7 5 -11 683.333 97.5033 2 7 5 11 829.911 74.8428 18 7 5 11 803.244 74.1228 17 7 5 12 675.422 67.3963 9 7 5 12 569.109 63.4078 18 7 5 12 697.277 68.1828 17 7 5 13 69.2272 50.2908 9 7 5 13 86.1625 54.0522 17 7 5 13 70.6088 48.5259 18 7 5 14 300.487 54.2325 9 7 5 14 371.34 72.8795 4 7 5 14 335.239 59.2186 17 7 5 14 234.079 52.224 18 7 5 15 134.927 49.3338 9 7 5 15 201.344 71.0605 4 7 5 15 185.959 54.6615 17 7 5 15 152.691 46.0067 18 7 5 16 198.716 70.6178 4 7 5 16 324.263 57.8084 17 7 5 16 269.207 50.8986 18 7 5 17 1868.63 124.532 17 7 5 17 1566.03 130.109 4 7 5 18 848.449 70.4573 9 7 5 18 806.063 86.5566 4 7 5 19 207.65 45.6347 9 7 5 19 217.059 67.6128 4 7 5 19 221.357 53.9303 17 7 5 19 264.456 42.8595 18 7 5 20 110.905 62.5007 4 7 5 20 85.585 49.1248 17 7 5 20 118.433 41.6459 9 7 5 21 62.0011 59.9394 4 7 5 21 43.0255 44.7989 17 7 5 21 75.272 39.3327 9 7 5 22 161.982 58.0451 4 -7 5 -22 85.9027 66.6024 2 7 5 22 145.685 45.1331 17 7 5 22 124.816 38.6509 9 7 5 23 129.136 54.5026 4 -7 5 -23 48.9042 61.9886 2 7 5 23 52.194 41.557 17 7 5 23 116.358 34.8492 9 7 5 24 35.7691 37.5593 17 7 5 24 99.3943 50.5745 4 -7 5 -24 -20.0851 55.839 2 -7 5 -24 -32.0779 23.4231 21 7 5 25 17.6766 34.7525 17 7 5 26 503.287 46.2124 17 7 5 27 133.558 30.3508 17 7 5 27 126.475 30.3779 7 7 6 -29 43.0799 56.726 16 7 -6 -28 -14.5275 41.4274 11 7 6 -28 1.76872 61.621 16 7 6 -27 224.856 68.8395 16 -7 6 26 54.9103 33.4481 14 7 6 -26 17.4178 70.9259 16 -7 6 25 57.206 37.3494 14 7 6 -25 24.6463 72.2744 16 -7 6 24 30.8246 39.727 14 7 6 -24 26.5423 72.4974 16 7 -6 -24 -8.60188 66.275 5 -7 6 23 27.2083 44.5821 14 7 6 -23 18.0022 75.9032 16 7 -6 -23 -33.4999 78.7821 5 -7 6 22 109.326 48.5044 14 7 6 -22 43.3235 80.0923 16 7 -6 -22 44.1112 77.8885 5 -7 6 21 -11.9092 52.1519 14 7 6 -21 108.266 78.7371 16 7 -6 -21 6.20163 77.0676 5 -7 6 20 219.643 56.4731 14 7 -6 -20 22.351 81.1138 5 7 -6 -19 94.8967 80.7789 5 7 6 -18 196.549 81.314 16 7 -6 -18 54.3412 81.5723 5 -7 6 17 320.062 64.9566 14 7 6 -17 329.807 84.8335 16 -7 6 16 312.525 67.5029 14 7 -6 -16 86.2709 83.4172 10 7 -6 -16 111.878 84.4066 5 7 6 -16 336.465 86.7271 16 7 -6 -15 5.43794 81.4277 10 -7 6 15 62.1202 66.3422 14 7 -6 -15 -24.288 83.4691 5 7 6 -15 -21.6868 86.946 16 7 6 -14 158.213 86.8849 16 -7 6 14 104.415 71.2103 14 7 -6 -14 78.821 84.068 10 7 6 -13 867.124 98.4372 16 -7 6 13 693.396 86.7998 14 7 -6 -13 804.527 95.2886 10 7 -6 -12 -48.5189 97.2957 13 -7 6 12 47.513 73.8095 14 7 6 -12 4.39733 88.4831 16 7 -6 -12 12.373 82.446 10 7 6 -11 2196.64 169.657 13 7 -6 -11 1760.54 132.34 10 -7 6 11 1704.82 129.299 14 7 6 -11 1767.56 142.899 16 7 6 -10 968.228 145.37 13 7 -6 -10 982.289 85.1153 12 7 -6 -10 920.451 100.843 10 -7 6 10 825.65 100.963 14 7 6 -10 1065.85 119.495 16 7 -6 -9 539.196 70.255 12 7 -6 -9 540.808 85.3223 10 7 6 -9 699.964 136.003 13 7 6 -9 638.824 102.661 16 7 -6 -8 446.255 65.3177 12 7 -6 -8 418.816 82.7313 10 7 6 -8 615.794 135.019 13 7 6 -8 472.647 94.9305 16 7 -6 -7 279.822 63.0667 12 7 6 -7 384.96 133.994 13 7 6 -7 335.385 88.2808 16 7 -6 -6 220.253 60.8058 12 7 6 -6 234.101 131.877 13 7 6 -6 137.203 85.98 16 7 -6 -5 367.62 64.8344 12 7 6 -5 424.6 95.9349 16 7 6 -5 566.66 134.543 13 7 6 -4 1968.05 149.1 16 7 -6 -4 1620.17 127.894 12 7 6 -4 2019.69 174.989 13 7 6 -3 114.158 126.593 13 7 6 -3 47.1625 53.1773 18 7 -6 -3 74.2138 56.669 12 7 6 -3 113.932 92.4056 16 7 6 -3 59.6489 53.6699 7 7 6 -2 -1.14402 53.3561 7 7 6 -2 -38.2048 123.46 13 7 6 -2 2.50707 49.2766 18 7 -6 -2 -72.4666 55.4091 12 -7 6 2 62.1016 125.938 2 7 6 -2 34.6529 91.3232 16 7 6 -1 1302.88 127.339 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9 2 21 62.2927 29.7983 18 9 -2 21 36.725 30.3144 18 9 2 21 28.8635 35.9987 7 9 2 22 20.9949 24.5682 18 9 -2 22 56.4871 26.9641 18 9 2 22 38.5677 32.5482 7 9 -2 23 44.1714 24.2573 18 9 3 -25 557.513 58.8078 16 9 -3 -25 20.0317 44.0873 11 9 3 -24 12.7336 62.528 16 9 -3 -24 -15.8736 45.8221 11 9 3 -23 51.8721 67.3929 16 9 -3 -23 84.0178 51.3114 11 9 3 -22 15.5566 72.4789 16 9 -3 -22 36.4826 49.0167 11 9 -3 -21 141.703 88.375 5 9 3 -21 307.886 78.358 16 9 -3 -21 63.6249 51.1156 11 9 -3 -20 94.5571 89.0438 5 9 3 -20 188.496 80.3946 16 9 -3 -20 25.6998 53.3535 11 9 -3 -19 546.118 100.224 5 9 -3 -19 369.714 66.6394 11 9 -3 -18 212.98 98.1108 5 9 3 -18 292.848 89.2391 16 9 -3 -18 218.289 59.0218 11 9 3 -18 398.019 80.1517 11 9 -3 -17 551.434 101.631 5 9 3 -17 517.908 92.4777 16 9 -3 -17 365.927 63.7781 11 9 3 -17 500.916 84.2871 11 9 -3 -16 40.3066 96.6005 5 9 -3 -16 -17.0702 57.6147 11 9 3 -16 31.4058 79.0139 11 9 3 -16 83.729 87.1366 16 9 -3 -15 245.772 95.7216 5 9 3 -15 198.68 89.5954 16 9 3 -15 19.1276 111.359 13 9 -3 -15 72.2515 88.3778 13 9 -3 -15 179.357 59.8819 11 9 3 -15 369.648 81.5398 11 9 -3 -14 182.023 98.3684 5 9 3 -14 125.87 117.219 13 9 -3 -14 143.327 86.2249 13 9 -3 -14 69.3251 57.711 11 9 3 -14 148.53 80.5333 11 9 -3 -13 217.773 100.045 5 9 -3 -13 93.3791 79.8839 13 9 -3 -13 69.3139 56.8045 11 9 3 -13 162.567 79.7582 11 9 -3 -12 430.958 64.5957 11 9 -3 -12 850.556 113.249 5 9 3 -11 3.40321 94.3144 16 9 3 -11 -58.0435 121.146 13 9 -3 -11 4.36172 104.837 5 9 3 -10 22.4698 90.2228 16 9 -3 -10 32.1023 101.706 5 9 -3 -10 64.1172 90.1509 13 9 3 -10 6.64926 115.128 13 9 -3 -9 104.329 98.6757 5 9 3 -9 100.493 97.4021 16 9 -3 -9 102.851 70.4332 12 9 -3 -9 21.0567 97.4145 13 9 3 -9 198.662 116.847 13 9 -3 -8 243.088 98.6883 5 9 3 -8 287.896 96.122 16 9 -3 -8 277.275 72.9474 12 9 -3 -8 249.078 102.903 10 9 -3 -8 413.063 109.399 13 9 3 -8 21.2407 117.889 13 9 -3 -7 612.373 107.229 5 9 3 -7 706.697 107.627 16 9 -3 -7 604.424 111.384 10 9 -3 -7 776.006 89.4138 12 9 -3 -7 907.587 121.699 13 9 3 -7 540.256 125.434 13 9 -3 -6 1095.92 120.34 5 9 3 -6 1104.66 124.815 16 9 -3 -6 1267.66 127.847 10 9 -3 -6 1145.24 103.787 12 9 3 -6 811.436 138.332 13 9 -3 -6 1331.76 136.088 13 9 -3 -5 298.17 96.7644 5 9 3 -5 450.851 106.301 16 9 -3 -5 466.769 76.6765 12 9 -3 -5 373.444 105.615 10 9 3 -5 475.296 120.129 13 9 -3 -5 595.604 113.565 13 9 -3 -4 2269.34 181.95 13 9 -3 -4 2280.72 160.625 12 9 3 -4 2129.64 188.52 13 9 3 -4 2082.27 173.044 16 9 -3 -4 1722.93 170.597 5 9 -3 -4 2264.54 176.571 10 9 3 -4 2502.38 152.393 18 9 -3 -3 98.0495 93.2667 5 9 -3 -3 166.655 102.086 10 9 -3 -3 120.886 71.1868 12 9 3 -3 120.354 121.079 13 9 -3 -3 152.635 105.247 13 9 3 -3 110.985 53.057 18 9 -3 -2 1360.06 129.01 10 9 3 -2 1298.69 98.937 18 9 -3 -2 1569.07 138.063 13 9 -3 -2 1214.1 111.845 12 9 3 -2 1376.44 110.211 12 9 3 -2 1330.41 147.721 13 9 3 -1 66.6416 71.3453 12 9 -3 -1 149.493 96.5612 10 9 -3 -1 72.7185 70.4679 12 9 3 -1 39.0037 54.4491 18 9 3 -1 21.6628 120.467 13 9 -3 -1 86.6855 102.453 13 9 3 0 188.21 69.0556 12 9 -3 0 105.15 69.2324 12 9 -3 0 75.4008 42.7618 18 9 3 0 49.8168 49.7122 18 9 -3 0 65.5819 90.009 10 9 3 0 187.883 119.741 13 9 -3 0 39.4405 101.442 13 9 3 1 107.233 113.504 13 9 -3 1 124.82 101.596 13 9 3 1 49.5222 66.9927 7 9 3 1 40.7993 66.6002 12 9 -3 1 77.7197 70.3345 12 9 -3 1 -21.2681 90.1132 10 9 -3 1 32.6967 44.2656 18 9 3 1 -0.66591 52.5503 18 9 3 2 304.941 116.274 13 9 -3 2 115.832 100.301 13 9 3 2 287.65 70.9611 7 9 3 2 233.364 68.6572 12 9 -3 2 166.872 70.196 12 9 -3 2 317.461 90.7147 10 9 3 2 224.824 55.4553 18 9 -3 2 203.809 47.8638 18 9 3 3 35.3555 105.742 13 9 -3 3 68.1881 98.7683 13 9 3 3 -42.7046 68.6405 7 9 -3 3 -1.54676 70.736 12 9 3 3 30.6199 64.851 12 9 -3 3 32.715 85.1303 10 9 3 3 -15.2608 52.1441 18 9 -3 3 -13.0623 45.9933 18 9 -3 4 1179.64 120.918 13 9 3 4 1011.19 94.6832 12 9 -3 4 999.045 96.6169 12 9 3 4 859.77 127.232 13 9 -3 4 964.754 81.7455 18 9 3 4 1049.76 87.5486 18 9 3 4 1176.45 96.9715 7 9 3 5 32.9201 54.3999 18 9 -3 5 19.0023 45.1664 18 9 -3 5 93.2715 66.7376 12 9 3 5 103.278 62.6637 12 9 3 5 15.6033 103.404 13 9 -3 5 -47.7255 94.2029 13 9 3 6 7.96833 53.9037 18 9 -3 6 13.2996 47.0073 18 9 -3 6 58.5992 65.2486 12 9 3 6 32.1926 101.808 13 9 -3 6 79.0148 93.9005 13 9 -3 7 279.037 69.4871 12 9 3 7 293.985 56.2671 18 9 -3 7 232.959 49.5995 18 9 3 8 45.2719 53.0392 18 9 -3 9 15.5531 55.5734 7 9 3 9 -10.2712 60.9981 7 9 -3 10 -3.66863 65.0863 13 9 -3 10 132.242 56.0886 7 9 3 10 131.209 59.2699 7 9 -3 11 1739.18 119.764 18 9 3 11 1934.08 122.847 18 9 -3 11 1654.16 123 7 9 3 11 1810.65 125.862 7 9 -3 11 1500.06 126.11 12 9 -3 12 541.461 57.5121 18 9 3 12 564.507 60.5694 18 9 -3 12 485.082 63.2988 7 9 3 12 524.073 67.2228 7 9 -3 12 429.421 67.5397 12 9 3 13 65.2813 46.8756 18 9 -3 13 76.2431 44.4973 18 9 -3 13 73.7673 50.5959 7 9 3 13 56.0687 56.0971 7 9 -3 13 81.2719 56.5967 12 9 3 14 201.752 47.3252 18 9 -3 14 148.192 45.45 18 9 -3 14 159.056 48.8671 7 9 3 14 130.767 54.9349 7 9 -3 14 107.184 54.3213 12 9 3 15 -9.87514 42.0278 18 9 -3 15 23.4449 42.2989 18 9 -3 15 -33.0526 45.3562 7 9 3 15 3.00858 50.9618 7 9 -3 15 35.1746 51.2345 12 9 3 16 -23.8418 40.5691 18 9 -3 16 35.1717 40.56 18 9 -3 16 6.97697 41.3447 7 9 3 16 -13.6167 48.8704 7 9 -3 16 17.576 46.941 12 9 3 17 121.821 40.0428 18 9 -3 17 95.3728 39.0615 18 9 3 17 134.292 47.1385 7 9 -3 17 62.63 45.6952 12 9 3 18 218.873 39.3487 18 9 -3 18 196.402 40.1071 18 9 3 18 208.699 46.4768 7 9 -3 18 154.208 43.8334 12 9 3 19 0.68378 33.9544 18 9 -3 19 29.5956 34.9137 18 9 3 19 -15.9818 41.3769 7 9 3 20 96.3822 30.7371 18 9 -3 20 99.7694 32.9712 18 9 3 20 72.9233 38.7038 7 9 3 21 186.899 27.4987 18 9 -3 21 196.567 32.2607 18 9 3 21 153.945 37.4053 7 9 -3 22 203.374 29.5571 18 9 3 22 247.476 35.2266 7 9 4 -25 255.854 56.5911 16 9 -4 -24 -36.7906 41.6611 11 9 4 -24 32.5789 60.3843 16 9 -4 -23 58.9364 46.2118 11 9 4 -23 449.88 70.439 16 9 -4 -22 84.0489 75.7771 5 9 -4 -22 32.926 45.2351 11 9 4 -22 -16.5579 71.7297 16 9 -4 -21 169.394 48.0747 11 9 -4 -20 127.951 86.0269 5 9 -4 -20 137.814 51.7184 11 9 4 -20 305.386 81.6331 16 9 -4 -19 204.129 90.4759 5 9 -4 -19 82.9854 54.3056 11 9 -4 -18 99.1644 86.6034 5 9 -4 -18 55.5451 53.2824 11 9 4 -18 267.519 87.577 16 9 -4 -17 209.517 56.0731 11 9 -4 -16 79.0932 92.7226 5 9 -4 -16 141.073 56.2038 11 9 4 -16 311.833 90.4718 16 9 -4 -15 -39.1965 95.8865 5 9 4 -15 121.8 93.3867 16 9 -4 -15 -81.0918 54.8575 11 9 -4 -14 55.0618 102.395 5 9 4 -14 -81.0092 94.4376 16 9 -4 -14 22.4032 54.1128 11 9 -4 -14 84.6254 74.6055 13 9 -4 -13 182.516 98.2379 5 9 -4 -13 110.477 54.4811 11 9 -4 -13 244.916 78.3952 13 9 4 -13 80.0986 119.797 13 9 -4 -12 5.63094 98.6875 5 9 -4 -12 -85.7222 72.6716 13 9 -4 -11 869.668 111.894 5 9 -4 -11 764.103 112.783 10 9 -4 -10 -47.7403 93.5578 5 9 -4 -9 54.5777 92.4333 5 9 4 -9 25.2048 97.1031 16 9 4 -9 160.938 127.618 13 9 -4 -9 83.7815 67.7668 12 9 -4 -8 75.4741 87.4536 5 9 4 -8 63.7906 96.7681 16 9 4 -8 35.028 127.331 13 9 -4 -8 -102.013 101.403 13 9 -4 -8 -32.115 68.7918 12 9 -4 -7 330.33 92.8652 5 9 4 -7 432.926 100.961 16 9 4 -7 284.947 129.548 13 9 -4 -7 364.623 106.926 13 9 -4 -7 437.68 78.1807 12 9 -4 -6 154.802 88.344 5 9 4 -6 127.883 97.4579 16 9 4 -6 214.358 125.01 13 9 -4 -6 475.205 105.578 13 9 -4 -6 196.779 70.5874 12 9 -4 -5 32.4545 85.0328 5 9 4 -5 107.178 100.851 16 9 4 -5 106.105 121.036 13 9 -4 -5 121.906 102.728 13 9 -4 -5 74.1092 71.3002 12 9 -4 -5 93.8374 96.3396 10 9 -4 -4 397.333 90.9321 5 9 4 -4 453.156 101.729 16 9 -4 -4 549.085 103.267 10 9 -4 -4 553.848 80.6368 12 9 4 -4 497.698 126.823 13 9 -4 -4 355.748 108.496 13 9 4 -3 335.155 124.691 13 9 -4 -3 394.031 108.446 13 9 -4 -3 371.027 77.5749 12 9 -4 -3 279.851 87.1938 5 9 -4 -3 551.394 101.267 10 9 4 -3 455.887 62.6193 18 9 4 -2 665.978 127.866 13 9 -4 -2 319.822 105.658 13 9 -4 -2 346.865 75.7765 12 9 -4 -2 438.989 98.287 10 9 4 -2 445.594 62.5465 18 9 -4 -2 146.437 83.8701 5 9 4 -1 755.453 75.2809 18 9 -4 -1 784.13 102.92 10 9 4 -1 978.377 134.442 13 9 -4 -1 780.494 88.1862 12 9 -4 -1 556.404 114.647 13 9 -4 0 324.005 73.3015 12 9 4 0 300.557 57.9724 18 9 -4 0 247.011 92.0265 10 9 4 0 236.591 120.83 13 9 -4 0 323.033 103.801 13 9 4 1 118.263 116.624 13 9 -4 1 -21.5266 99.3064 13 9 4 1 38.9358 64.5804 7 9 -4 1 39.8136 68.3091 12 9 -4 1 17.7413 84.6464 10 9 4 1 19.0616 53.3672 18 9 -4 2 262.719 70.9945 12 9 4 2 314.31 56.879 18 9 4 2 333.349 119.468 13 9 -4 2 267.355 102.522 13 9 -4 3 563.53 81.7517 12 9 4 3 508.918 74.8234 12 9 -4 3 605.897 58.9699 18 9 4 3 672.831 68.5436 18 9 4 3 564.011 121.121 13 9 -4 3 470.258 105.559 13 9 -4 4 371.416 71.7654 12 9 4 4 421.592 60.7042 18 9 -4 4 327.882 49.343 18 9 4 4 450.927 115.96 13 9 -4 4 312.773 99.2386 13 9 -4 5 41.7463 64.5965 12 9 4 5 -0.6561 52.3354 18 9 -4 5 14.2719 90.8765 13 9 4 6 282.86 56.655 18 9 -4 6 330.734 68.3009 12 9 -4 7 350.064 77.1311 10 9 4 7 421.188 70.663 7 9 -4 8 129.735 72.0893 10 9 4 8 254.298 64.3249 7 9 -4 9 -29.6817 44.8829 18 9 -4 9 -17.2645 68.635 10 9 -4 9 -9.3896 81.5418 13 9 4 9 0.62221 59.1687 7 9 -4 10 30.2017 59.025 12 9 -4 10 51.6866 78.4698 13 9 4 10 62.1084 50.942 18 9 -4 10 36.3382 42.4659 18 9 4 10 55.1099 57.9239 7 9 4 11 192.146 49.4204 18 9 -4 11 126.263 44.5575 18 9 4 11 113.072 58.2096 7 9 -4 11 125.082 59.6034 12 9 4 12 222.19 48.601 18 9 -4 12 209.191 45.0288 18 9 4 12 199.957 58.0458 7 9 -4 12 142.83 58.5156 12 9 4 13 114.444 45.168 18 9 -4 13 142.594 43.4319 18 9 4 13 138.979 53.6269 7 9 -4 13 -6.25286 55.9569 12 9 4 14 167.865 45.552 18 9 -4 14 115.9 42.6875 18 9 4 14 147.956 52.8717 7 9 -4 14 128.975 54.309 12 9 4 15 61.7942 41.7649 18 9 -4 15 25.3956 39.7515 18 9 4 15 10.9922 48.872 7 9 -4 15 -12.9494 50.1688 12 9 4 16 1.70612 38.8132 18 9 -4 16 44.3382 37.4998 18 9 4 16 51.4162 47.1983 7 9 -4 16 9.76318 48.7433 12 9 4 17 55.3547 36.7177 18 9 -4 17 124.465 37.739 18 9 4 17 59.8616 45.0108 7 9 -4 17 35.8668 44.3996 12 9 4 18 154.593 34.796 18 9 -4 18 118.584 36.6593 18 9 4 18 152.609 42.6335 7 9 -4 18 80.5448 41.7609 12 9 4 19 165.766 32.5176 18 9 -4 19 136.17 34.317 18 9 4 19 163.843 41.5014 7 9 -4 19 84.1076 38.3231 12 9 -4 20 494.686 44.3604 18 9 4 20 481.467 42.1422 18 9 4 20 487.301 49.2375 7 9 -4 21 53.8791 26.7898 18 9 4 21 4.23731 34.86 7 9 -4 22 -14.4822 24.0439 18 9 5 -25 269.489 52.8132 16 9 5 -24 232.112 62.1922 16 9 -5 -23 1.75176 37.436 11 9 5 -23 256.815 65.9065 16 9 -5 -22 22.1193 41.0953 11 9 5 -22 -22.2931 72.0603 16 9 -5 -21 148.427 74.8978 5 9 -5 -21 4.08705 44.367 11 9 5 -21 39.7767 74.5514 16 9 -5 -20 -73.2793 79.7265 5 9 -5 -20 -4.7937 46.9595 11 9 5 -20 91.7514 79.8288 16 9 -5 -19 -17.8033 80.1308 5 9 -5 -19 84.6728 49.4834 11 9 -5 -18 32.994 78.7727 5 9 -5 -18 57.9913 48.7742 11 9 5 -18 -65.9117 85.3339 16 9 -5 -17 39.6229 85.5734 5 9 -5 -17 40.1093 50.5445 11 9 5 -17 201.105 85.8492 16 9 -5 -16 80.2478 95.194 5 9 -5 -16 18.9471 50.9505 11 9 5 -16 114.27 88.6559 16 9 -5 -15 91.7624 94.2957 5 9 5 -15 251.789 93.0059 16 9 5 -14 36.3685 92.6363 16 9 -5 -14 -7.96692 90.6184 5 9 -5 -14 -23.8243 69.8504 13 9 5 -13 112.611 95.3254 16 9 -5 -13 1.44834 89.3984 5 9 -5 -13 10.4938 66.1113 13 9 5 -12 261.878 94.3525 16 9 -5 -12 140.68 91.5313 5 9 -5 -12 59.1314 81.0008 13 9 -5 -11 53.9808 87.9376 5 9 -5 -11 100.787 94.5154 10 9 -5 -11 -42.339 91.4741 13 9 -5 -10 71.83 88.976 5 9 -5 -10 256.582 95.052 10 9 -5 -10 34.2912 95.6178 13 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1A N1 C1 124.5(2) . . ? C1B N1 C1 125.4(2) . . ? C1B N1 C1A 109.6(2) . . ? H1a C1 N1 108.91(14) . . ? H1b C1 N1 108.91(14) . . ? H1b C1 H1a 107.7 . . ? C2 C1 N1 113.3(2) . . ? C2 C1 H1a 108.91(15) . . ? C2 C1 H1b 108.91(14) . . ? H2a C2 C1 108.63(13) . . ? H2b C2 C1 108.63(15) . . ? H2b C2 H2a 107.6 . . ? C3 C2 C1 114.5(2) . . ? C3 C2 H2a 108.63(15) . . ? C3 C2 H2b 108.63(16) . . ? H3a C3 C2 109.09(15) . . ? H3b C3 C2 109.09(16) . . ? H3b C3 H3a 107.8 . . ? C4 C3 C2 112.5(2) . . ? C4 C3 H3a 109.09(16) . . ? C4 C3 H3b 109.09(17) . . ? H4a C4 C3 109.5 . . ? H4b C4 C3 109.5 . . ? H4b C4 H4a 109.5 . . ? H4c C4 C3 109.5 . . ? H4c C4 H4a 109.5 . . ? H4c C4 H4b 109.5 . . ? C2A C1A N1 109.0(2) . . ? C13A C1A N1 128.8(2) . . ? C13A C1A C2A 122.2(2) . . ? C3A C2A C1A 120.3(2) . . ? C2B C2A C1A 106.3(2) . . ? C2B C2A C3A 133.4(2) . . ? H3Aa C3A C2A 120.97(14) . . ? C4A C3A C2A 118.1(2) . . ? C4A C3A H3Aa 120.97(15) . . ? C5A C4A C3A 130.0(2) . . ? C12A C4A C3A 120.7(2) . . ? C12A C4A C5A 109.3(2) . . ? C6A C5A C4A 107.7(2) . . ? C21A C5A C4A 124.8(2) . . ? C21A C5A C6A 127.5(2) . . ? C7A C6A C5A 131.6(2) . . ? C11A C6A C5A 108.3(2) . . ? C11A C6A C7A 120.1(2) . . ? H7A C7A C6A 120.47(14) . . ? C8A C7A C6A 119.1(2) . . ? C8A C7A H7A 120.47(17) . . ? H8A C8A C7A 119.77(17) . . ? C9A C8A C7A 120.5(3) . . ? C9A C8A H8A 119.77(15) . . ? H9A C9A C8A 119.65(15) . . ? C10A C9A C8A 120.7(2) . . ? C10A C9A H9A 119.65(15) . . ? H10A C10A C9A 120.10(15) . . ? C11A C10A C9A 119.8(2) . . ? C11A C10A H10A 120.10(16) . . ? C10A C11A C6A 119.9(2) . . ? C12A C11A C6A 107.7(2) . . ? C12A C11A C10A 132.4(2) . . ? C11A C12A C4A 107.0(2) . . ? C13A C12A C4A 121.7(2) . . ? C13A C12A C11A 130.9(2) . . ? C12A C13A C1A 116.9(2) . . ? H13A C13A C1A 121.53(15) . . ? H13A C13A C12A 121.53(14) . . ? C22A C21A C5A 120.2(2) . . ? C26A C21A C5A 120.6(2) . . ? C26A C21A C22A 119.2(2) . . ? C23A C22A C21A 119.4(2) . . ? C27A C22A C21A 121.0(2) . . ? C27A C22A C23A 119.5(2) . . ? H23A C23A C22A 118.86(15) . . ? C24A C23A C22A 122.3(2) . . ? C24A C23A H23A 118.86(14) . . ? C25A C24A C23A 117.3(2) . . ? C28A C24A C23A 120.5(2) . . ? C28A C24A C25A 122.2(2) . . ? H25A C25A C24A 118.81(15) . . ? C26A C25A C24A 122.4(2) . . ? C26A C25A H25A 118.81(15) . . ? C25A C26A C21A 119.5(2) . . ? C29A C26A C21A 121.1(2) . . ? C29A C26A C25A 119.4(2) . . ? H27A C27A C22A 107.51(14) . . ? C30A C27A C22A 110.2(2) . . ? C30A C27A H27A 107.51(14) . . ? C31A C27A C22A 112.8(2) . . ? C31A C27A H27A 107.51(16) . . ? C31A C27A C30A 111.1(2) . . ? H28A C28A C24A 107.47(14) . . ? C32A C28A C24A 111.6(2) . . ? C32A C28A H28A 107.47(15) . . ? C33A C28A C24A 112.7(2) . . ? C33A C28A H28A 107.47(15) . . ? C33A C28A C32A 109.9(2) . . ? H29A C29A C26A 107.78(13) . . ? C34A C29A C26A 112.1(2) . . ? C34A C29A H29A 107.78(14) . . ? C35A C29A C26A 110.1(2) . . ? C35A C29A H29A 107.78(13) . . ? C35A C29A C34A 111.1(2) . . ? H30a C30A C27A 109.5 . . ? H30b C30A C27A 109.5 . . ? H30b C30A H30a 109.5 . . ? H30c C30A C27A 109.5 . . ? H30c C30A H30a 109.5 . . ? H30c C30A H30b 109.5 . . ? H31a C31A C27A 109.5 . . ? H31b C31A C27A 109.5 . . ? H31b C31A H31a 109.5 . . ? H31c C31A C27A 109.5 . . ? H31c C31A H31a 109.5 . . ? H31c C31A H31b 109.5 . . ? H32a C32A C28A 109.5 . . ? H32b C32A C28A 109.5 . . ? H32b C32A H32a 109.5 . . ? H32c C32A C28A 109.5 . . ? H32c C32A H32a 109.5 . . ? H32c C32A H32b 109.5 . . ? H33a C33A C28A 109.5 . . ? H33b C33A C28A 109.5 . . ? H33b C33A H33a 109.5 . . ? H33c C33A C28A 109.5 . . ? H33c C33A H33a 109.5 . . ? H33c C33A H33b 109.5 . . ? H34a C34A C29A 109.5 . . ? H34b C34A C29A 109.5 . . ? H34b C34A H34a 109.5 . . ? H34c C34A C29A 109.5 . . ? H34c C34A H34a 109.5 . . ? H34c C34A H34b 109.5 . . ? H35a C35A C29A 109.5 . . ? H35b C35A C29A 109.5 . . ? H35b C35A H35a 109.5 . . ? H35c C35A C29A 109.5 . . ? H35c C35A H35a 109.5 . . ? H35c C35A H35b 109.5 . . ? C2B C1B N1 108.5(2) . . ? C13B C1B N1 129.1(2) . . ? C13B C1B C2B 122.4(2) . . ? C1B C2B C2A 106.6(2) . . ? C3B C2B C2A 133.2(2) . . ? C3B C2B C1B 120.2(2) . . ? H3Ba C3B C2B 120.75(15) . . ? C4B C3B C2B 118.5(2) . . ? C4B C3B H3Ba 120.75(14) . . ? C5B C4B C3B 130.6(2) . . ? C12B C4B C3B 120.6(2) . . ? C12B C4B C5B 108.9(2) . . ? C6B C5B C4B 107.9(2) . . ? C21B C5B C4B 124.2(2) . . ? C21B C5B C6B 127.9(2) . . ? C7B C6B C5B 131.7(2) . . ? C11B C6B C5B 108.4(2) . . ? C11B C6B C7B 119.9(2) . . ? H7B C7B C6B 120.58(15) . . ? C8B C7B C6B 118.8(2) . . ? C8B C7B H7B 120.58(15) . . ? H8B C8B C7B 119.52(15) . . ? C9B C8B C7B 121.0(3) . . ? C9B C8B H8B 119.52(17) . . ? H9B C9B C8B 119.52(17) . . ? C10B C9B C8B 121.0(3) . . ? C10B C9B H9B 119.52(16) . . ? H10B C10B C9B 120.46(16) . . ? C11B C10B C9B 119.1(2) . . ? C11B C10B H10B 120.46(15) . . ? C10B C11B C6B 120.1(2) . . ? C12B C11B C6B 107.9(2) . . ? C12B C11B C10B 131.9(2) . . ? C11B C12B C4B 106.9(2) . . ? C13B C12B C4B 121.3(2) . . ? C13B C12B C11B 131.8(2) . . ? C12B C13B C1B 117.0(2) . . ? H13B C13B C1B 121.50(14) . . ? H13B C13B C12B 121.50(16) . . ? C22B C21B C5B 119.4(2) . . ? C26B C21B C5B 120.3(2) . . ? C26B C21B C22B 120.2(2) . . ? C23B C22B C21B 118.5(2) . . ? C27B C22B C21B 121.6(2) . . ? C27B C22B C23B 120.0(2) . . ? H23B C23B C22B 118.76(15) . . ? C24B C23B C22B 122.5(2) . . ? C24B C23B H23B 118.76(15) . . ? C25B C24B C23B 118.1(2) . . ? C28B C24B C23B 120.5(2) . . ? C28B C24B C25B 121.4(2) . . ? H25B C25B C24B 118.91(15) . . ? C26B C25B C24B 122.2(2) . . ? C26B C25B H25B 118.91(15) . . ? C25B C26B C21B 118.5(2) . . ? C29B C26B C21B 121.7(2) . . ? C29B C26B C25B 119.7(2) . . ? H27B C27B C22B 107.54(14) . . ? C30B C27B C22B 112.3(2) . . ? C30B C27B H27B 107.54(16) . . ? C31B C27B C22B 110.8(2) . . ? C31B C27B H27B 107.54(16) . . ? C31B C27B C30B 110.9(3) . . ? H28B C28B C24B 107.22(14) . . ? C32B C28B C24B 112.7(2) . . ? C32B C28B H28B 107.22(14) . . ? C33B C28B C24B 111.7(2) . . ? C33B C28B H28B 107.22(15) . . ? C33B C28B C32B 110.5(2) . . ? H29B C29B C26B 107.34(14) . . ? C34B C29B C26B 111.0(2) . . ? C34B C29B H29B 107.34(15) . . ? C35B C29B C26B 111.5(2) . . ? C35B C29B H29B 107.34(15) . . ? C35B C29B C34B 112.0(2) . . ? H30d C30B C27B 109.5 . . ? H30e C30B C27B 109.5 . . ? H30e C30B H30d 109.5 . . ? H30f C30B C27B 109.5 . . ? H30f C30B H30d 109.5 . . ? H30f C30B H30e 109.5 . . ? H31d C31B C27B 109.5 . . ? H31e C31B C27B 109.5 . . ? H31e C31B H31d 109.5 . . ? H31f C31B C27B 109.5 . . ? H31f C31B H31d 109.5 . . ? H31f C31B H31e 109.5 . . ? H32d C32B C28B 109.5 . . ? H32e C32B C28B 109.5 . . ? H32e C32B H32d 109.5 . . ? H32f C32B C28B 109.5 . . ? H32f C32B H32d 109.5 . . ? H32f C32B H32e 109.5 . . ? H33d C33B C28B 109.5 . . ? H33e C33B C28B 109.5 . . ? H33e C33B H33d 109.5 . . ? H33f C33B C28B 109.5 . . ? H33f C33B H33d 109.5 . . ? H33f C33B H33e 109.5 . . ? H34d C34B C29B 109.5 . . ? H34e C34B C29B 109.5 . . ? H34e C34B H34d 109.5 . . ? H34f C34B C29B 109.5 . . ? H34f C34B H34d 109.5 . . ? H34f C34B H34e 109.5 . . ? H35d C35B C29B 109.5 . . ? H35e C35B C29B 109.5 . . ? H35e C35B H35d 109.5 . . ? H35f C35B C29B 109.5 . . ? H35f C35B H35d 109.5 . . ? H35f C35B H35e 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C1 1.468(3) . ? N1 C1A 1.377(3) . ? N1 C1B 1.385(3) . ? C1 H1a 0.9900 . ? C1 H1b 0.9900 . ? C1 C2 1.524(4) . ? C2 H2a 0.9900 . ? C2 H2b 0.9900 . ? C2 C3 1.521(4) . ? C3 H3a 0.9900 . ? C3 H3b 0.9900 . ? C3 C4 1.519(4) . ? C4 H4a 0.9800 . ? C4 H4b 0.9800 . ? C4 H4c 0.9800 . ? C1A C2A 1.432(3) . ? C1A C13A 1.404(4) . ? C2A C3A 1.388(4) . ? C2A C2B 1.447(4) . ? C3A H3Aa 0.9500 . ? C3A C4A 1.403(4) . ? C4A C5A 1.417(4) . ? C4A C12A 1.440(3) . ? C5A C6A 1.450(3) . ? C5A C21A 1.480(3) . ? C6A C7A 1.393(4) . ? C6A C11A 1.432(3) . ? C7A H7A 0.9500 . ? C7A C8A 1.399(3) . ? C8A H8A 0.9500 . ? C8A C9A 1.407(4) . ? C9A H9A 0.9500 . ? C9A C10A 1.381(4) . ? C10A H10A 0.9500 . ? C10A C11A 1.389(3) . ? C11A C12A 1.458(4) . ? C12A C13A 1.377(4) . ? C13A H13A 0.9500 . ? C21A C22A 1.411(4) . ? C21A C26A 1.407(3) . ? C22A C23A 1.395(3) . ? C22A C27A 1.519(4) . ? C23A H23A 0.9500 . ? C23A C24A 1.399(3) . ? C24A C25A 1.391(4) . ? C24A C28A 1.510(3) . ? C25A H25A 0.9500 . ? C25A C26A 1.397(3) . ? C26A C29A 1.526(3) . ? C27A H27A 1.0000 . ? C27A C30A 1.533(4) . ? C27A C31A 1.529(4) . ? C28A H28A 1.0000 . ? C28A C32A 1.532(4) . ? C28A C33A 1.526(4) . ? C29A H29A 1.0000 . ? C29A C34A 1.533(3) . ? C29A C35A 1.533(4) . ? C30A H30a 0.9800 . ? C30A H30b 0.9800 . ? C30A H30c 0.9800 . ? C31A H31a 0.9800 . ? C31A H31b 0.9800 . ? C31A H31c 0.9800 . ? C32A H32a 0.9800 . ? C32A H32b 0.9800 . ? C32A H32c 0.9800 . ? C33A H33a 0.9800 . ? C33A H33b 0.9800 . ? C33A H33c 0.9800 . ? C34A H34a 0.9800 . ? C34A H34b 0.9800 . ? C34A H34c 0.9800 . ? C35A H35a 0.9800 . ? C35A H35b 0.9800 . ? C35A H35c 0.9800 . ? C1B C2B 1.433(3) . ? C1B C13B 1.403(4) . ? C2B C3B 1.384(3) . ? C3B H3Ba 0.9500 . ? C3B C4B 1.403(4) . ? C4B C5B 1.419(3) . ? C4B C12B 1.447(3) . ? C5B C6B 1.439(4) . ? C5B C21B 1.488(3) . ? C6B C7B 1.398(4) . ? C6B C11B 1.430(3) . ? C7B H7B 0.9500 . ? C7B C8B 1.398(4) . ? C8B H8B 0.9500 . ? C8B C9B 1.384(4) . ? C9B H9B 0.9500 . ? C9B C10B 1.400(4) . ? C10B H10B 0.9500 . ? C10B C11B 1.386(4) . ? C11B C12B 1.450(4) . ? C12B C13B 1.386(3) . ? C13B H13B 0.9500 . ? C21B C22B 1.414(4) . ? C21B C26B 1.410(3) . ? C22B C23B 1.400(3) . ? C22B C27B 1.516(3) . ? C23B H23B 0.9500 . ? C23B C24B 1.387(3) . ? C24B C25B 1.390(4) . ? C24B C28B 1.521(3) . ? C25B H25B 0.9500 . ? C25B C26B 1.406(4) . ? C26B C29B 1.514(4) . ? C27B H27B 1.0000 . ? C27B C30B 1.523(4) . ? C27B C31B 1.527(4) . ? C28B H28B 1.0000 . ? C28B C32B 1.527(3) . ? C28B C33B 1.534(4) . ? C29B H29B 1.0000 . ? C29B C34B 1.529(4) . ? C29B C35B 1.530(4) . ? C30B H30d 0.9800 . ? C30B H30e 0.9800 . ? C30B H30f 0.9800 . ? C31B H31d 0.9800 . ? C31B H31e 0.9800 . ? C31B H31f 0.9800 . ? C32B H32d 0.9800 . ? C32B H32e 0.9800 . ? C32B H32f 0.9800 . ? C33B H33d 0.9800 . ? C33B H33e 0.9800 . ? C33B H33f 0.9800 . ? C34B H34d 0.9800 . ? C34B H34e 0.9800 . ? C34B H34f 0.9800 . ? C35B H35d 0.9800 . ? C35B H35e 0.9800 . ? C35B H35f 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C1 C2 C3 59.3(3) . . . . ? N1 C1A C2A C3A 177.4(2) . . . . ? N1 C1A C2A C2B -0.0(2) . . . . ? N1 C1A C13A C12A -177.5(3) . . . . ? N1 C1B C2B C2A -0.3(2) . . . . ? N1 C1B C2B C3B -178.1(2) . . . . ? N1 C1B C13B C12B 178.4(3) . . . . ? C1 C2 C3 C4 176.4(2) . . . . ? C1A C2A C3A C4A 0.1(3) . . . . ? C1A C2A C2B C1B 0.2(2) . . . . ? C1A C2A C2B C3B 177.58(19) . . . . ? C1A C13A C12A C4A 0.1(3) . . . . ? C1A C13A C12A C11A 173.5(2) . . . . ? C2A C3A C4A C5A -174.3(2) . . . . ? C2A C3A C4A C12A 2.1(3) . . . . ? C2A C2B C1B C13B 179.51(19) . . . . ? C2A C2B C3B C4B -177.0(3) . . . . ? C3A C4A C5A C6A 175.0(3) . . . . ? C3A C4A C5A C21A -3.3(3) . . . . ? C3A C4A C12A C11A -177.1(3) . . . . ? C3A C4A C12A C13A -2.3(3) . . . . ? C4A C5A C6A C7A -174.0(2) . . . . ? C4A C5A C6A C11A 2.8(2) . . . . ? C4A C5A C21A C22A 75.9(3) . . . . ? C4A C5A C21A C26A -100.8(3) . . . . ? C4A C12A C11A C6A 1.7(2) . . . . ? C4A C12A C11A C10A 177.9(2) . . . . ? C5A C6A C7A C8A 177.3(3) . . . . ? C5A C6A C11A C10A -179.5(2) . . . . ? C5A C6A C11A C12A -2.8(2) . . . . ? C5A C21A C22A C23A -176.2(2) . . . . ? C5A C21A C22A C27A 7.2(3) . . . . ? C5A C21A C26A C25A 175.1(2) . . . . ? C5A C21A C26A C29A -7.9(3) . . . . ? C6A C7A C8A C9A 0.4(3) . . . . ? C6A C11A C10A C9A 2.6(3) . . . . ? C6A C11A C12A C13A -172.4(2) . . . . ? C7A C8A C9A C10A -0.0(3) . . . . ? C8A C9A C10A C11A -1.5(3) . . . . ? C9A C10A C11A C12A -173.1(2) . . . . ? C10A C11A C12A C13A 3.8(4) . . . . ? C21A C22A C23A C24A 1.5(3) . . . . ? C21A C22A C27A C30A 103.2(3) . . . . ? C21A C22A C27A C31A -132.0(3) . . . . ? C21A C26A C25A C24A 0.8(3) . . . . ? C21A C26A C29A C34A 127.3(3) . . . . ? C21A C26A C29A C35A -108.5(3) . . . . ? C22A C23A C24A C25A -2.2(3) . . . . ? C22A C23A C24A C28A 178.3(3) . . . . ? C23A C24A C25A C26A 1.0(3) . . . . ? C23A C24A C28A C32A -101.8(3) . . . . ? C23A C24A C28A C33A 134.0(3) . . . . ? C24A C25A C26A C29A -176.2(3) . . . . ? C25A C26A C29A C34A -55.7(3) . . . . ? C25A C26A C29A C35A 68.5(3) . . . . ? C1B C2B C3B C4B 0.1(3) . . . . ? C1B C13B C12B C4B -0.6(3) . . . . ? C1B C13B C12B C11B -178.6(2) . . . . ? C2B C3B C4B C5B 176.4(2) . . . . ? C2B C3B C4B C12B -2.1(3) . . . . ? C3B C4B C5B C6B -179.8(3) . . . . ? C3B C4B C5B C21B -0.3(3) . . . . ? C3B C4B C12B C11B -179.1(2) . . . . ? C3B C4B C12B C13B 2.5(3) . . . . ? C4B C5B C6B C7B 178.7(2) . . . . ? C4B C5B C6B C11B -0.2(2) . . . . ? C4B C5B C21B C22B -80.5(3) . . . . ? C4B C5B C21B C26B 96.7(3) . . . . ? C4B C12B C11B C6B -2.1(2) . . . . ? C4B C12B C11B C10B 176.33(19) . . . . ? C5B C6B C7B C8B 179.3(3) . . . . ? C5B C6B C11B C10B -177.2(2) . . . . ? C5B C6B C11B C12B 1.4(2) . . . . ? C5B C21B C22B C23B 177.6(2) . . . . ? C5B C21B C22B C27B -2.5(3) . . . . ? C5B C21B C26B C25B -175.7(2) . . . . ? C5B C21B C26B C29B 4.7(3) . . . . ? C6B C7B C8B C9B -0.5(3) . . . . ? C6B C11B C10B C9B -3.1(3) . . . . ? C6B C11B C12B C13B 176.0(2) . . . . ? C7B C8B C9B C10B 1.1(3) . . . . ? C8B C9B C10B C11B 0.7(3) . . . . ? C9B C10B C11B C12B 178.6(2) . . . . ? C10B C11B C12B C13B -5.5(4) . . . . ? C21B C22B C23B C24B -1.9(3) . . . . ? C21B C22B C27B C30B -119.0(3) . . . . ? C21B C22B C27B C31B 116.4(3) . . . . ? C21B C26B C25B C24B -2.1(3) . . . . ? C21B C26B C29B C34B 120.7(3) . . . . ? C21B C26B C29B C35B -113.6(3) . . . . ? C22B C23B C24B C25B 1.3(3) . . . . ? C22B C23B C24B C28B 179.7(3) . . . . ? C23B C24B C25B C26B 0.7(3) . . . . ? C23B C24B C28B C32B -126.1(3) . . . . ? C23B C24B C28B C33B 108.9(3) . . . . ? C24B C25B C26B C29B 177.5(3) . . . . ? C25B C26B C29B C34B -58.9(3) . . . . ? C25B C26B C29B C35B 66.8(3) . . . . ?