#------------------------------------------------------------------------------ #$Date: 2024-07-05 17:10:15 +0300 (Fri, 05 Jul 2024) $ #$Revision: 292873 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/17/1571703.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1571703 loop_ _publ_author_name 'Zhou, Lei' 'Li, Kailei' 'Chang, Yuanyuan' 'Yao, Yuan' 'Peng, Yuqi' 'Li, Ming' 'He, Rongxing' _publ_section_title ; High-efficiency color-tunable ultralong room-temperature phosphorescence from organic--inorganic metal halides via synergistic inter/intramolecular interactions ; _journal_issue 26 _journal_name_full 'Chemical Science' _journal_page_first 10046 _journal_page_last 10055 _journal_paper_doi 10.1039/D4SC01630K _journal_volume 15 _journal_year 2024 _chemical_formula_moiety 'Cl6 Sn, 2(C8 H10 N O)' _chemical_formula_sum 'C16 H20 Cl6 N2 O2 Sn' _chemical_formula_weight 603.73 _chemical_name_common A2SnCl6 _chemical_name_systematic A2SnCl6 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2022-06-01 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6226) ; _audit_update_record ; 2023-12-26 deposited with the CCDC. 2024-05-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 108.353(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 9.3919(6) _cell_length_b 11.4149(7) _cell_length_c 11.0818(6) _cell_measurement_reflns_used 9867 _cell_measurement_temperature 296.15 _cell_measurement_theta_max 28.33 _cell_measurement_theta_min 2.28 _cell_volume 1127.62(12) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2014/7 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296.15 _diffrn_measured_fraction_theta_full 0.964 _diffrn_measured_fraction_theta_max 0.964 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0364 _diffrn_reflns_av_unetI/netI 0.0179 _diffrn_reflns_Laue_measured_fraction_full 0.964 _diffrn_reflns_Laue_measured_fraction_max 0.964 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 19440 _diffrn_reflns_point_group_measured_fraction_full 0.964 _diffrn_reflns_point_group_measured_fraction_max 0.964 _diffrn_reflns_theta_full 24.992 _diffrn_reflns_theta_max 24.992 _diffrn_reflns_theta_min 2.899 _diffrn_source_current 1.0 _diffrn_source_power 0.05 _diffrn_source_voltage 50.0 _exptl_absorpt_coefficient_mu 1.859 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.5571 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1456 before and 0.0586 after correction. The Ratio of minimum to maximum transmission is 0.7471. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.778 _exptl_crystal_description block _exptl_crystal_F_000 596 _refine_diff_density_max 0.453 _refine_diff_density_min -0.486 _refine_diff_density_rms 0.069 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.254 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 126 _refine_ls_number_reflns 1914 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.254 _refine_ls_R_factor_all 0.0328 _refine_ls_R_factor_gt 0.0278 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0179P)^2^+1.6781P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0678 _refine_ls_wR_factor_ref 0.0700 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1717 _reflns_number_total 1914 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; aaa.res created by SHELXL-2014/7 TITL aaa_a.res in P2(1)/c REM Old TITL AAA in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.137, Rweak 0.028, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C16 N2 O2 Cl6 Sn CELL 0.71073 9.3919 11.4149 11.0818 90 108.353 90 ZERR 2 0.0006 0.0007 0.0006 0 0.002 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cl N O Sn UNIT 32 40 12 4 4 2 L.S. 10 0 0 PLAN 4 TEMP 23 CONF list 4 MORE -1 BOND $H fmap 2 53 acta OMIT -3 50 OMIT 1 0 0 OMIT 0 1 1 OMIT -1 1 3 REM REM REM WGHT 0.017900 1.678100 FVAR 0.84477 SN01 6 0.000000 0.500000 0.000000 10.50000 0.03837 0.03229 = 0.02886 -0.00195 0.00700 -0.00430 CL02 3 0.026625 0.589508 0.204825 11.00000 0.07816 0.04366 = 0.03249 -0.00664 0.01201 0.00097 CL03 3 0.028504 0.691762 -0.085047 11.00000 0.10820 0.03793 = 0.05165 0.00168 0.03309 -0.01287 CL04 3 0.265402 0.467977 0.061772 11.00000 0.04036 0.10126 = 0.07243 -0.02072 0.00437 0.00549 O005 5 0.146368 0.528785 0.566249 11.00000 0.04677 0.07776 = 0.07201 -0.02374 0.00706 0.01173 N006 4 0.116144 0.358738 0.398195 11.00000 0.04169 0.04593 = 0.04407 -0.00207 0.00531 -0.00377 AFIX 137 H00A 2 0.093416 0.352518 0.314189 11.00000 -1.20000 H00B 2 0.084460 0.427599 0.417473 11.00000 -1.20000 H00C 2 0.071622 0.301313 0.427162 11.00000 -1.20000 AFIX 0 C007 1 0.352027 0.411274 0.568982 11.00000 0.03739 0.03644 = 0.03868 0.00568 0.01000 -0.00226 C008 1 0.506387 0.393772 0.621457 11.00000 0.03942 0.05122 = 0.04814 0.00765 0.00623 -0.00223 AFIX 43 H008 2 0.558467 0.432531 0.696132 11.00000 -1.20000 AFIX 0 C009 1 0.279392 0.350129 0.457200 11.00000 0.03914 0.03571 = 0.04119 0.00787 0.00940 -0.00139 C00A 1 0.355067 0.278218 0.401206 11.00000 0.05565 0.04711 = 0.05858 -0.00950 0.01587 0.00096 AFIX 43 H00D 2 0.304257 0.238879 0.326570 11.00000 -1.20000 AFIX 0 C00B 1 0.271140 0.496174 0.626185 11.00000 0.03836 0.04891 = 0.04910 -0.00195 0.01258 -0.00613 C00C 1 0.508115 0.263762 0.455726 11.00000 0.05860 0.05267 = 0.08108 -0.00496 0.03076 0.00997 AFIX 43 H00E 2 0.560366 0.214852 0.417343 11.00000 -1.20000 AFIX 0 C00D 1 0.582803 0.320835 0.565452 11.00000 0.04020 0.05406 = 0.06955 0.01126 0.01319 0.00830 AFIX 43 H00F 2 0.685589 0.310234 0.602237 11.00000 -1.20000 AFIX 0 C00E 1 0.345414 0.545218 0.755269 11.00000 0.06070 0.08806 = 0.05815 -0.02490 0.01616 -0.00359 AFIX 137 H00G 2 0.431462 0.590221 0.754467 11.00000 -1.50000 H00H 2 0.376523 0.482327 0.815355 11.00000 -1.50000 H00I 2 0.276135 0.594722 0.779194 11.00000 -1.50000 AFIX 0 HKLF 4 REM aaa_a.res in P2(1)/c REM R1 = 0.0278 for 1717 Fo > 4sig(Fo) and 0.0328 for all 1914 data REM 126 parameters refined using 0 restraints END WGHT 0.0179 1.6781 REM Highest difference peak 0.453, deepest hole -0.486, 1-sigma level 0.069 Q1 1 0.2365 0.4178 0.1214 11.00000 0.05 0.45 Q2 1 0.0990 0.6815 -0.0159 11.00000 0.05 0.41 Q3 1 -0.0634 0.6767 -0.0811 11.00000 0.05 0.31 Q4 1 0.1353 0.5596 0.2372 11.00000 0.05 0.29 REM The information below was added by Olex2. REM REM R1 = 0.0278 for 1717 Fo > 4sig(Fo) and 0.0328 for all 23492 data REM 126 parameters refined using n/a restraints REM Highest difference peak 0.45, deepest hole -0.49 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0328 REM R1_gt = 0.0278 REM wR_ref = 0.0700 REM GOOF = 1.254 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 23492 REM Reflections_gt = 1717 REM Parameters = 126 REM Hole = -0.49 REM Peak = 0.45 REM Flack = n/a ; _cod_data_source_file d4sc01630k2.cif _cod_data_source_block aaa _cod_depositor_comments 'Adding full bibliography for 1571699--1571704.cif.' _cod_database_code 1571703 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H,H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C008(H008), C00A(H00D), C00C(H00E), C00D(H00F) 2.b Idealised Me refined as rotating group: N006(H00A,H00B,H00C), C00E(H00G,H00H,H00I) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Sn01 Sn 0.0000 0.5000 0.0000 0.03400(13) Uani 1 2 d S . P . . Cl02 Cl 0.02663(13) 0.58951(9) 0.20482(8) 0.0527(3) Uani 1 1 d . . . . . Cl03 Cl 0.02850(15) 0.69176(9) -0.08505(10) 0.0641(3) Uani 1 1 d . . . . . Cl04 Cl 0.26540(12) 0.46798(13) 0.06177(12) 0.0745(4) Uani 1 1 d . . . . . O005 O 0.1464(3) 0.5288(3) 0.5662(3) 0.0682(9) Uani 1 1 d . . . . . N006 N 0.1161(3) 0.3587(3) 0.3982(3) 0.0458(8) Uani 1 1 d . . . . . H00A H 0.0934 0.3525 0.3142 0.055 Uiso 1 1 calc R U . . . H00B H 0.0845 0.4276 0.4175 0.055 Uiso 1 1 calc R U . . . H00C H 0.0716 0.3013 0.4272 0.055 Uiso 1 1 calc R U . . . C007 C 0.3520(4) 0.4113(3) 0.5690(3) 0.0380(8) Uani 1 1 d . . . . . C008 C 0.5064(4) 0.3938(4) 0.6215(4) 0.0480(9) Uani 1 1 d . . . . . H008 H 0.5585 0.4325 0.6961 0.058 Uiso 1 1 calc R U . . . C009 C 0.2794(4) 0.3501(3) 0.4572(3) 0.0394(8) Uani 1 1 d . . . . . C00A C 0.3551(5) 0.2782(4) 0.4012(4) 0.0543(10) Uani 1 1 d . . . . . H00D H 0.3043 0.2389 0.3266 0.065 Uiso 1 1 calc R U . . . C00B C 0.2711(4) 0.4962(3) 0.6262(4) 0.0457(9) Uani 1 1 d . . . . . C00C C 0.5081(5) 0.2638(4) 0.4557(5) 0.0621(12) Uani 1 1 d . . . . . H00E H 0.5604 0.2149 0.4173 0.074 Uiso 1 1 calc R U . . . C00D C 0.5828(5) 0.3208(4) 0.5655(4) 0.0556(11) Uani 1 1 d . . . . . H00F H 0.6856 0.3102 0.6022 0.067 Uiso 1 1 calc R U . . . C00E C 0.3454(5) 0.5452(5) 0.7553(4) 0.0696(13) Uani 1 1 d . . . . . H00G H 0.4315 0.5902 0.7545 0.104 Uiso 1 1 calc R U . . . H00H H 0.3765 0.4823 0.8154 0.104 Uiso 1 1 calc R U . . . H00I H 0.2761 0.5947 0.7792 0.104 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sn01 0.0384(2) 0.0323(2) 0.02886(19) -0.00195(14) 0.00700(13) -0.00430(15) Cl02 0.0782(7) 0.0437(5) 0.0325(5) -0.0066(4) 0.0120(5) 0.0010(5) Cl03 0.1082(10) 0.0379(5) 0.0517(6) 0.0017(4) 0.0331(6) -0.0129(6) Cl04 0.0404(6) 0.1013(10) 0.0724(8) -0.0207(7) 0.0044(5) 0.0055(6) O005 0.0468(18) 0.078(2) 0.072(2) -0.0237(17) 0.0071(15) 0.0117(16) N006 0.0417(18) 0.0459(18) 0.0441(18) -0.0021(14) 0.0053(14) -0.0038(14) C007 0.037(2) 0.0364(19) 0.0387(19) 0.0057(15) 0.0100(16) -0.0023(15) C008 0.039(2) 0.051(2) 0.048(2) 0.0076(19) 0.0062(18) -0.0022(18) C009 0.039(2) 0.0357(19) 0.041(2) 0.0079(16) 0.0094(16) -0.0014(16) C00A 0.056(3) 0.047(2) 0.059(3) -0.009(2) 0.016(2) 0.001(2) C00B 0.038(2) 0.049(2) 0.049(2) -0.0020(19) 0.0126(17) -0.0061(19) C00C 0.059(3) 0.053(3) 0.081(3) -0.005(2) 0.031(2) 0.010(2) C00D 0.040(2) 0.054(3) 0.070(3) 0.011(2) 0.013(2) 0.0083(19) C00E 0.061(3) 0.088(3) 0.058(3) -0.025(3) 0.016(2) -0.004(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 1 0 0 118.29 6.9 -1 0 0 102.29 6.7 -5 0 0 881.61 35.3 -5 0 0 884.31 48.4 -5 0 0 929.91 50.19 5 0 0 968.5 47.6 5 0 0 944.31 42.2 5 0 0 864.01 51.19 -6 0 0 1993.8 64.69 -6 0 0 2153.88 81.69 6 0 0 2025.8 66.09 6 0 0 1933.21 64.89 6 0 0 2087.59 80.39 6 0 0 1952 82.59 -6 0 0 1947.81 83.09 -6 0 0 2026.3 85.49 6 0 0 1895.01 84.49 7 0 0 2634.94 98.19 -7 0 0 2554.34 96.59 7 0 0 2571.04 80.99 7 0 0 2185.68 100.59 -7 0 0 2542.35 104.79 -7 0 0 2509.45 78.99 -7 0 0 2269.57 97.89 7 0 0 2451.35 80.19 7 0 0 2428.86 98.69 8 0 0 2628.74 86.89 -8 0 0 2506.05 100.59 8 0 0 2604.34 103.89 8 0 0 2531.25 106.19 9 0 0 74.39 24.9 9 0 0 104.29 35.6 9 0 0 57.99 16.6 10 0 0 74.69 30.4 10 0 0 53.09 17.4 -10 0 0 28.1 17.4 10 0 0 43.1 24.4 -11 0 0 238.48 38.1 11 0 0 272.27 34.3 11 0 0 308.27 43.5 1 -1 0 769.32 20.7 -1 -1 0 779.82 22.4 -1 -1 0 636.74 19.5 1 -1 0 788.52 24.6 -1 1 0 758.42 21.1 1 1 0 775.62 25.2 1 1 0 772.52 23.5 -1 1 0 715.53 26.2 -2 -1 0 275.97 15.7 2 -1 0 231.58 18.9 2 -1 0 233.88 18.4 -2 -1 0 263.77 18 -2 -1 0 232.78 20.3 2 -1 0 185.98 19.3 2 -1 0 279.47 12.9 -2 -1 0 224.28 12.1 2 -1 0 235.78 12.3 -2 1 0 216.38 17.3 2 1 0 266.97 17 2 1 0 252.27 13.4 -2 1 0 234.48 11.9 2 1 0 267.17 16.7 -2 1 0 193.78 16.6 2 1 0 211.48 19.1 -3 -1 0 1708.13 59.99 -3 -1 0 1734.83 57.39 3 -1 0 1635.64 56.09 3 -1 0 1656.53 47.3 -3 -1 0 1621.84 46.4 3 -1 0 1669.03 47.8 -3 -1 0 1652.13 53.69 3 -1 0 1629.04 59.79 3 -1 0 1658.63 56.49 -3 1 0 1546.25 58.49 3 1 0 1580.74 55.99 -3 1 0 1610.04 56.09 3 1 0 1652.93 57.89 -3 1 0 1596.54 56.09 -3 1 0 1665.93 46.9 3 1 0 1695.73 47.1 3 1 0 1663.53 55.49 4 -1 0 40 13.8 4 -1 0 74.19 11 -4 -1 0 57.69 16.2 -4 -1 0 53.39 18.7 4 -1 0 64.49 17.7 4 -1 0 56.19 10.4 -4 -1 0 62.69 9.6 -4 -1 0 40.9 10.9 4 -1 0 54.59 15.8 -4 1 0 45.6 14.3 4 1 0 58.79 15.4 4 1 0 55.89 10.1 -4 1 0 54.19 9.1 4 1 0 51.49 13.8 -4 1 0 51.29 16 4 1 0 87.19 21.2 -4 1 0 44.5 14.4 5 -1 0 686.13 45.4 -5 -1 0 796.62 47.7 -5 -1 0 775.92 32.6 5 -1 0 807.62 44.5 5 -1 0 826.82 46.1 5 -1 0 735.03 33.1 -5 -1 0 754.82 44.6 5 -1 0 783.02 33.4 -5 -1 0 796.12 47.7 -5 1 0 794.72 32.6 -5 1 0 728.53 42.8 5 1 0 754.12 44.5 -5 1 0 795.72 45.1 5 1 0 816.52 43 5 1 0 716.63 46.2 5 1 0 796.02 33.2 -5 1 0 817.22 46.7 6 -1 0 370.16 35.5 6 -1 0 313.07 36.2 6 -1 0 321.57 24 -6 -1 0 333.07 22.3 6 -1 0 345.07 24.5 -6 -1 0 340.57 37.5 -6 -1 0 371.66 31.9 -6 -1 0 329.07 35 6 -1 0 364.96 35.7 -6 1 0 319.87 33.3 6 1 0 338.37 25.2 -6 1 0 310.67 21.9 -6 1 0 309.47 33.4 6 1 0 322.67 34.5 -6 1 0 355.36 37.6 6 1 0 370.86 32.8 6 1 0 303.67 38.8 -7 -1 0 384.06 27.2 -7 -1 0 499.35 38.5 7 -1 0 451.25 41.9 7 -1 0 391.76 44 7 -1 0 353.66 44.4 7 -1 0 341.27 27 -7 -1 0 401.56 43.7 7 -1 0 407.26 29.5 -7 -1 0 356.16 43.9 -7 1 0 390.26 26.5 7 1 0 302.27 41.6 -7 1 0 417.86 42.8 7 1 0 443.46 40.5 7 1 0 387.76 28.4 7 1 0 407.76 41.9 -7 1 0 359.76 42.2 -7 1 0 416.36 43 -8 -1 0 81.19 20 8 -1 0 97.49 28.8 8 -1 0 99.09 30.7 8 -1 0 65.69 16.9 8 1 0 82.49 23.5 8 1 0 105.09 30.6 8 1 0 86.29 17.6 -8 1 0 69.29 22.4 9 -1 0 -13.1 17.7 9 -1 0 3.2 24.7 9 -1 0 -8.4 11.3 9 1 0 -14 13.1 9 1 0 4.1 19 9 1 0 -5.4 13.3 10 -1 0 4.1 19.3 -10 -1 0 20.3 14.4 10 -1 0 31.3 15.9 10 -1 0 31.6 25.9 10 1 0 30 15.5 -10 1 0 2.4 16.9 10 1 0 20.4 18.9 10 1 0 32.7 23.7 11 -1 0 -23.4 12.8 -11 -1 0 -8.2 13 11 -1 0 42 29.3 11 1 0 -10.6 12.2 -11 1 0 -12.6 16.7 11 1 0 31 24.8 -2 -2 0 153.88 10.5 2 -2 0 109.59 14.2 -2 -2 0 104.79 16.3 -2 -2 0 135.69 10.2 2 -2 0 137.59 9.5 -2 -2 0 160.48 13.5 2 -2 0 139.59 9.6 2 -2 0 93.69 15.2 -2 2 0 108.19 17.2 -2 2 0 104.89 12.8 -2 2 0 128.19 9 2 2 0 124.09 10.1 2 2 0 111.29 15.4 2 2 0 141.19 11.6 3 -2 0 3964.3 108.09 3 -2 0 3932.51 108.89 3 -2 0 3900.31 97.49 -3 -2 0 4042.9 96.69 -3 2 0 4102.69 116.29 3 2 0 3629.74 104.89 3 2 0 3909.61 106.49 -3 2 0 3896.91 99.29 -3 2 0 3864.71 113.69 3 2 0 3912.51 110.69 4 -2 0 4425.56 125.39 4 -2 0 4241.48 110.09 -4 -2 0 4205.68 108.99 4 -2 0 4130.39 128.89 -4 -2 0 4667.13 119.49 4 -2 0 4500.15 124.69 -4 -2 0 4437.16 124.19 -4 -2 0 4348.06 129.59 4 -2 0 4454.55 111.19 4 2 0 4293.67 126.29 4 2 0 4167.08 122.39 4 2 0 4398.36 122.19 4 2 0 4436.86 109.89 -4 2 0 4252.97 129.09 -4 2 0 4168.98 109.39 -4 2 0 4239.68 122.89 5 -2 0 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252.07 31.3 9 3 -2 218.08 61.89 -9 3 2 179.78 39.9 9 3 -2 195.48 30.8 8 -3 -2 17.4 20.8 -8 -3 2 -6.6 10.4 8 -3 -2 12.3 22 8 -3 -2 19.1 13.1 -8 3 2 8.5 24.4 8 3 -2 -7.1 18.2 8 3 -2 6.2 14.3 7 -3 -2 459.85 27.3 -7 -3 2 513.65 32.9 7 -3 -2 385.96 42.1 7 -3 -2 493.05 46.5 -7 -3 2 460.35 47.6 -7 -3 2 524.45 38.1 -7 -3 2 498.75 45.8 7 -3 -2 474.55 40.2 7 -3 -2 519.35 33.5 7 3 -2 467.85 38.6 7 3 -2 470.25 40.3 -7 3 2 468.25 41.9 7 3 -2 379.56 43.4 -7 3 2 454.25 29.7 -7 3 2 492.25 52.99 -6 -3 2 180.08 33.8 6 -3 -2 158.58 24.9 6 -3 -2 165.28 15.3 -6 -3 2 137.29 26.9 -6 -3 2 179.08 22 -6 -3 2 138.69 18.4 6 -3 -2 179.18 30.8 6 -3 -2 137.49 18.7 6 -3 -2 137.09 26.6 -6 3 2 151.78 16.7 6 3 -2 129.79 23.5 -6 3 2 129.29 24.6 6 3 -2 153.78 22.4 -6 3 2 141.79 29.3 6 3 -2 127.49 25.5 -5 -3 2 2082.89 72.79 -5 -3 2 2006.4 62.79 5 -3 -2 2003.2 68.79 5 -3 -2 2107.79 90.79 5 -3 -2 1939.21 60.79 5 -3 -2 2000.3 62.99 5 -3 -2 1760.12 78.39 -5 -3 2 1975.3 75.39 -5 -3 2 2067.69 78.99 5 3 -2 1995.6 73.99 -5 3 2 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571.94 26.9 -2 3 2 589.94 20.9 -2 3 2 593.14 23.4 2 3 -2 571.44 25.9 2 3 -2 559.54 19.7 0 -3 2 2.3 5.6 0 -3 -2 -1.1 7.5 0 -3 2 1.8 3.8 0 -3 -2 9.8 4.9 0 -3 2 1.9 3.2 0 -3 -2 13 2.7 0 -3 -2 2.3 3.7 0 -3 2 6.4 3 0 -3 -2 6.3 3.3 0 -3 2 5.9 3 0 -3 2 5.8 3.2 0 3 2 6.8 1.3 0 3 2 2.2 6.3 0 3 2 2.4 3.8 0 3 -2 11.1 4 0 3 -2 14.1 4.1 0 3 -2 6.1 2.9 0 3 -2 4.2 6.1 -1 -3 -2 1492.75 51.99 -1 -3 -2 1490.25 46 1 -3 2 1410.26 46.4 1 -3 2 1373.56 40.3 1 -3 2 1395.96 41.1 1 -3 2 1396.46 52.09 -1 -3 -2 1415.76 43.5 -1 3 -2 1429.96 45.5 1 3 2 1450.85 41.7 1 3 2 1441.46 49.7 -1 3 -2 1433.86 41.8 -1 3 -2 1392.96 41.3 -1 3 -2 1430.76 41.3 1 3 2 1418.26 43 1 3 2 1388.76 45.7 -1 3 -2 1364.96 50.69 2 -3 2 1631.14 61.89 2 -3 2 1616.34 55.89 -2 -3 -2 1676.03 47.3 -2 -3 -2 1657.83 40.6 2 -3 2 1632.74 48.4 -2 -3 -2 1643.84 62.59 -2 -3 -2 1741.83 53.39 2 -3 2 1691.03 48.9 -2 3 -2 1563.64 58.99 2 3 2 1612.84 51.19 2 3 2 1663.23 49.6 -2 3 -2 1589.84 53.39 2 3 2 1682.03 60.99 2 3 2 1689.83 54.49 -2 3 -2 1678.93 50.89 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23.2 10 3 -3 132.69 31.2 10 3 -3 187.88 28.7 -10 3 3 87.89 34.5 9 -3 -3 456.25 40.9 -9 -3 3 469.45 43.2 9 -3 -3 468.85 37.5 9 3 -3 443.96 40.8 -9 3 3 406.66 55.59 9 3 -3 421.26 48.3 -8 -3 3 759.52 57.99 8 -3 -3 886.41 46 8 -3 -3 836.92 61.19 8 -3 -3 805.72 44.3 8 -3 -3 894.71 52.79 -8 -3 3 928.31 56.29 -8 3 3 957.6 71.49 8 3 -3 928.31 57.99 8 3 -3 891.81 55.09 7 -3 -3 2122.39 78.89 7 -3 -3 2232.28 99.69 -7 -3 3 2236.18 95.39 -7 -3 3 2334.27 77.79 7 -3 -3 2300.37 95.49 -7 -3 3 2499.35 91.39 7 -3 -3 2262.07 76.39 -7 3 3 2355.46 107.09 7 3 -3 2086.79 87.49 -7 3 3 2168.88 74.99 7 3 -3 1878.71 92.79 7 3 -3 2085.69 84.99 -6 -3 3 1971.6 80.89 6 -3 -3 1964 63.59 6 -3 -3 1966.2 69.39 6 -3 -3 2088.09 84.39 -6 -3 3 1984 81.69 6 -3 -3 1963.2 67.39 -6 -3 3 2102.69 78.49 6 -3 -3 1810.52 83.69 -6 -3 3 2083.69 68.19 6 3 -3 1931.51 75.99 -6 3 3 1929.81 80.09 6 3 -3 1990.1 78.79 -6 3 3 2097.89 67.09 6 3 -3 1753.12 81.59 -6 3 3 1995.1 66.59 -6 3 3 2040.1 91.79 -5 -3 3 4550.74 129.69 5 -3 -3 4185.58 137.19 5 -3 -3 4399.36 115.99 5 -3 -3 4543.95 118.59 -5 -3 3 4487.95 132.59 5 -3 -3 4419.16 118.29 -5 -3 3 4463.55 131.49 5 -3 -3 4554.64 135.99 -5 -3 3 4484.15 118.39 -5 3 3 4349.06 131.39 -5 3 3 4573.04 118.19 -5 3 3 4395.26 143.49 5 3 -3 3935.41 130.59 5 3 -3 4324.37 128.29 5 3 -3 4587.24 132.09 -5 3 3 4644.24 117.49 4 -3 -3 9236.08 247.48 -4 -3 3 9777.52 240.78 4 -3 -3 9666.03 225.78 -4 -3 3 9968.6 241.68 -4 3 3 9999 254.67 3 -3 -3 3108.29 93.49 3 -3 -3 3286.57 86.99 3 -3 -3 3238.28 106.79 3 -3 -3 3192.88 78.29 -3 -3 3 3176.58 91.29 -3 -3 3 3355.76 91.19 -3 -3 3 3116.89 91.59 3 -3 -3 3144.49 82.99 3 3 -3 3207.38 93.49 -3 3 3 3275.47 83.79 -3 3 3 3240.38 83.39 3 3 -3 3178.88 76.89 -3 3 3 3146.79 100.49 3 3 -3 3202.88 91.29 3 3 -3 3036.4 92.39 -3 3 3 3187.78 91.79 2 -3 -3 1394.16 36.3 2 -3 -3 1392.36 45.6 -2 -3 3 1461.15 45.5 2 -3 -3 1374.66 49.9 2 -3 -3 1418.06 48.5 2 -3 -3 1394.36 40.2 -2 -3 3 1353.86 35.2 -2 -3 3 1364.66 48.6 -2 -3 3 1420.56 46.2 2 3 -3 1355.06 46.2 2 3 -3 1382.16 49.8 -2 3 3 1437.36 40 2 3 -3 1349.36 35.1 2 3 -3 1399.56 45.9 -2 3 3 1439.76 43.6 -2 3 3 1346.17 52.19 -2 3 3 1366.86 46.1 1 -3 -3 2610.74 62.29 1 -3 -3 2536.95 70.09 -1 -3 3 2552.94 74.89 -1 -3 3 2599.34 69.39 -1 -3 3 2612.84 62.09 1 -3 -3 2563.34 66.99 -1 -3 3 2556.44 68.09 -1 -3 3 2570.64 68.29 1 -3 -3 2619.94 72.19 -1 3 3 2539.15 68.99 -1 3 3 2626.14 61.49 1 3 -3 2568.44 68.29 1 3 -3 2619.34 61.59 1 3 -3 2545.95 69.49 -1 3 3 2565.74 70.29 -1 3 3 2565.24 74.79 1 3 -3 2548.25 75.59 -1 3 3 2467.15 63.89 1 -3 3 3854.31 108.49 -1 -3 -3 3897.31 102.79 1 -3 3 3775.22 100.99 1 -3 3 3949.9 95.39 1 -3 3 3886.11 96.89 -1 -3 -3 3847.22 109.39 1 3 3 3983.2 108.59 -1 3 -3 3780.82 99.29 -1 3 -3 3676.13 103.09 1 3 3 3914.41 103.39 -1 3 -3 3956.5 97.39 1 3 3 3818.82 96.19 2 -3 3 1857.21 54.89 2 -3 3 1912.91 55.39 -2 -3 -3 1901.31 58.49 -2 -3 -3 1933.91 45.1 2 -3 3 1793.12 61.09 -2 -3 -3 1846.22 70.49 2 3 3 1952.1 56.89 2 3 3 1951 70.29 2 3 3 1877.91 54.49 -2 3 -3 1847.12 54.49 2 3 3 1810.92 61.19 2 3 3 1938.31 46.4 -2 3 -3 1763.42 58.49 -2 3 -3 1812.02 62.69 3 -3 3 5438.46 147.79 3 -3 3 5385.56 137.69 3 -3 3 5712.63 162.08 -3 -3 -3 5658.63 162.98 -3 -3 -3 5615.74 127.09 -3 -3 -3 5595.54 145.79 3 -3 3 5517.05 137.29 3 -3 3 5413.86 154.88 3 3 3 5549.04 140.49 -3 3 -3 5298.97 144.09 3 3 3 5560.94 158.58 3 3 3 5510.45 147.29 -3 3 -3 5314.27 147.29 3 3 3 5561.54 142.29 -3 3 -3 5395.86 136.19 3 3 3 5624.34 129.09 4 -3 3 1731.73 59.29 -4 -3 -3 1762.02 68.09 4 -3 3 1831.72 58.39 -4 -3 -3 1729.53 49.2 4 -3 3 1738.33 77.79 -4 -3 -3 1897.51 82.69 4 -3 3 1817.72 70.29 -4 -3 -3 1827.12 54.89 4 -3 3 1708.43 73.89 4 3 3 1832.92 52.19 4 3 3 1806.32 77.89 4 3 3 1775.12 64.09 -4 3 -3 1656.83 64.59 4 3 3 1805.52 67.39 4 3 3 1702.23 63.79 -4 3 -3 1769.92 56.49 -4 3 -3 1767.02 68.99 5 -3 3 200.98 29.6 5 -3 3 228.88 31.3 -5 -3 -3 213.88 16.7 -5 -3 -3 217.88 37 -5 -3 -3 214.08 31.6 5 -3 3 196.68 19 -5 -3 -3 211.98 14.6 5 -3 3 172.38 20.1 5 -3 3 179.88 33 5 3 3 182.38 22.5 -5 3 -3 208.78 23.4 -5 3 -3 186.68 16.5 -5 3 -3 211.28 30.8 5 3 3 180.68 32.8 5 3 3 160.88 26.6 5 3 3 201.58 18 -6 -3 -3 102.29 13.7 6 -3 3 115.29 28.1 6 -3 3 146.39 30 6 -3 3 114.69 34.8 -6 -3 -3 94.99 11.8 6 -3 3 112.89 18.7 6 3 3 100.29 32.4 6 3 3 76.99 23.1 6 3 3 121.99 20.8 -6 3 -3 88.69 21.9 6 3 3 102.39 15.4 -7 -3 -3 827.62 40.5 7 -3 3 811.62 43.5 7 -3 3 787.32 56.79 7 3 3 769.62 37.8 -7 3 -3 743.23 51.19 7 3 3 776.12 58.69 7 3 3 702.23 57.59 8 -3 3 347.67 41.6 8 -3 3 323.97 48 -8 -3 -3 427.26 41 8 -3 3 299.07 29.6 8 3 3 380.66 38.2 8 3 3 350.06 27.9 -8 3 -3 332.27 38.3 8 3 3 335.07 44.2 9 -3 3 7.4 13.7 9 -3 3 13.1 19.9 -9 -3 -3 32.3 11.3 9 -3 3 36.1 29.8 9 3 3 45.9 25.8 -9 3 -3 33.5 17.8 9 3 3 12.4 13.9 9 3 3 25.5 15.1 -10 -3 -3 166.58 22.9 10 -3 3 144.39 36.6 10 3 3 197.58 26.3 -10 3 -3 129.69 28.1 10 3 3 253.57 40.8 10 3 3 149.59 31.4 -12 -4 3 3.8 13 12 -4 -3 24.7 20.6 12 -4 -3 -39.5 27.4 12 4 -3 -13.4 15.8 12 4 -3 -11.4 12.3 -11 -4 3 -12.1 8.6 11 -4 -3 -22.5 15.5 11 -4 -3 -34.2 21.5 11 4 -3 54.69 20.1 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4 -3 364.96 27.5 4 4 3 416.86 28.2 -4 4 -3 377.66 22.5 4 4 3 382.06 19.7 4 4 3 345.67 27.7 4 4 3 400.76 38 -4 4 -3 423.76 38.1 -5 -4 -3 171.28 17.7 -5 -4 -3 155.48 12.6 5 -4 3 150.68 28 5 -4 3 179.08 37.8 5 -4 3 153.08 18.1 -5 -4 -3 147.19 38.1 5 -4 3 122.29 17.2 -5 -4 -3 174.08 29.6 5 -4 3 125.39 29.8 5 4 3 152.68 16.4 5 4 3 164.28 21.9 5 4 3 180.98 35.5 -5 4 -3 154.88 20.7 5 4 3 159.68 25 -5 4 -3 124.09 25.7 -5 4 -3 141.29 14.9 5 4 3 148.29 20.5 6 -4 3 173.98 38.8 -6 -4 -3 134.99 13.6 6 -4 3 145.39 30.5 6 -4 3 138.09 19.5 -6 -4 -3 167.28 16.7 6 4 3 164.18 35.8 6 4 3 152.58 22 6 4 3 92.79 22.6 6 4 3 141.49 22.2 -6 4 -3 140.09 27.6 6 4 3 140.99 17.9 -7 -4 -3 253.67 19.4 7 -4 3 276.37 40.6 -7 -4 -3 251.07 22.2 7 -4 3 274.57 41.8 7 -4 3 251.57 27.3 7 4 3 223.38 29.4 7 4 3 286.47 24 7 4 3 237.98 37.1 -7 4 -3 253.47 39.2 7 4 3 195.18 28 8 -4 3 76.79 34.7 8 -4 3 86.09 29 -8 -4 -3 90.39 15.1 8 -4 3 78.89 20.1 -8 -4 -3 76.09 14.2 8 4 3 123.89 33.7 8 4 3 99.09 23.5 8 4 3 81.89 22.4 8 4 3 67.99 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3456.95 93.69 1 -7 -3 3356.36 103.59 1 -7 -3 3420.96 83.09 1 -7 -3 3446.06 102.39 1 -7 -3 3274.87 101.99 -1 7 3 3338.67 81.59 1 7 -3 3219.28 90.79 -1 7 3 3404.66 99.49 1 7 -3 3583.14 120.19 -1 7 3 3301.87 115.99 1 7 -3 3285.17 97.59 -1 7 3 3255.37 95.99 0 -7 3 3101.69 96.99 0 -7 -3 3219.38 97.59 0 -7 -3 3167.08 99.89 0 -7 3 3144.69 101.59 0 -7 -3 3094.59 102.89 0 -7 -3 3180.98 99.69 0 -7 3 3339.47 91.49 0 -7 3 3293.17 89.59 0 -7 -3 3266.47 75.89 0 -7 3 3126.19 103.69 0 7 -3 3164.28 93.29 0 7 3 3178.68 93.99 0 7 3 3363.76 113.89 0 7 3 3151.68 96.89 0 7 3 3152.68 97.79 0 7 -3 3203.38 114.89 1 -7 3 1979.6 78.39 1 -7 3 2048.59 77.29 1 -7 3 2135.59 89.39 -1 -7 -3 2052.49 75.79 1 -7 3 2111.29 64.69 1 -7 3 2024.7 65.49 -1 -7 -3 2141.69 81.59 -1 -7 -3 2039.3 72.89 1 -7 3 2099.09 72.59 -1 -7 -3 2007.9 47 -1 -7 -3 1980.2 81.29 -1 7 -3 2127.79 66.79 -1 7 -3 1944.91 63.99 1 7 3 1971 71.29 1 7 3 2087.99 74.19 -1 7 -3 2091.69 67.59 1 7 3 2018.8 67.89 -1 7 -3 1983.5 86.39 -2 -7 -3 1288.57 54.49 -2 -7 -3 1297.07 67.19 2 -7 3 1294.27 48 2 -7 3 1295.97 48.8 -2 -7 -3 1299.77 54.09 2 -7 3 1311.97 60.09 -2 7 -3 1287.57 49.6 2 7 3 1225.58 58.49 2 7 3 1252.97 50.49 -2 7 -3 1371.16 52.59 2 7 3 1261.87 54.99 -2 7 -3 1239.78 54.79 -2 7 -3 1225.38 69.09 -2 7 -3 1262.37 47.5 3 -7 3 876.11 51.79 -3 -7 -3 891.21 23 3 -7 3 927.91 40.7 -3 -7 -3 949.01 23.7 3 -7 3 970.3 62.69 3 -7 3 905.31 40.4 -3 -7 -3 919.81 63.39 -3 -7 -3 927.21 47 3 7 3 934.31 47.9 -3 7 -3 862.81 60.89 -3 7 -3 882.91 40.6 -3 7 -3 1025.4 47.5 -3 7 -3 834.92 45.7 3 7 3 932.31 44.4 3 7 3 881.51 44.5 3 7 3 986 55.69 -3 7 -3 876.21 39 4 -7 3 796.92 39.3 4 -7 3 738.33 50.19 -4 -7 -3 838.22 24.7 -4 7 -3 806.32 59.99 4 7 3 813.02 44.5 4 7 3 729.33 42.7 4 7 3 775.82 52.59 -4 7 -3 831.42 46.2 4 7 3 763.82 45.2 -5 -7 -3 450.35 28.6 -5 -7 -3 425.36 18.5 5 -7 3 414.76 44.8 -5 7 -3 381.36 47.7 5 7 3 449.16 39.2 5 7 3 408.96 34.4 5 7 3 415.26 41.7 6 -7 3 399.66 32.2 6 -7 3 328.27 44.5 -6 -7 -3 417.36 20.8 -6 -7 -3 419.76 29 6 -7 3 431.06 45.6 6 7 3 388.26 34.9 -6 7 -3 379.46 51.39 6 7 3 418.26 35.6 6 7 3 405.36 43.1 -7 -7 -3 319.17 26.1 7 -7 3 281.17 30.4 -7 -7 -3 301.07 19.7 7 -7 3 291.97 44.5 7 -7 3 244.58 41.1 7 7 3 266.07 31 7 7 3 262.17 31.6 7 7 3 265.67 37.4 -8 -7 -3 199.48 22.2 8 -7 3 203.38 29.7 8 -7 3 118.59 40.2 8 -7 3 205.28 41.5 8 7 3 222.48 33.7 8 7 3 177.68 27.2 8 7 3 213.18 28 -9 -7 -3 93.79 17.6 9 -7 3 86.89 23.3 9 -7 3 84.39 34.2 9 7 3 72.99 21.9 9 7 3 114.59 30.4 9 7 3 106.59 25.5 10 -8 -3 -7.6 14.7 10 -8 -3 -10.5 28.1 10 -8 -3 -3.8 23.6 -10 -8 3 1.2 8.5 -10 8 3 -17.5 29.6 10 8 -3 10.3 9.9 9 -8 -3 14.4 16.9 9 -8 -3 18.9 22.9 -9 -8 3 22.5 12 9 -8 -3 29.5 27.3 9 8 -3 39.6 13.3 -9 8 3 20.1 23.7 9 8 -3 29.6 17.1 9 8 -3 45.7 17.3 -9 8 3 39.8 32.6 8 -8 -3 11.2 13.5 8 -8 -3 17.3 19.8 -8 -8 3 22.4 11.7 8 -8 -3 10.9 23.5 8 8 -3 22.8 9.7 8 8 -3 38.2 17.4 -8 8 3 9.5 17.1 8 8 -3 23.1 13.9 -8 8 3 27.2 26.3 -7 -8 3 58.19 15.6 7 -8 -3 100.09 26.2 7 -8 -3 56.79 15.7 7 8 -3 67.89 21.3 7 8 -3 74.89 25.3 7 8 -3 52.09 14 -7 8 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11.8 2 -8 -3 590.84 26.4 -2 -8 3 583.14 28.9 -2 -8 3 584.74 34.4 -2 -8 3 621.94 30.6 2 -8 -3 585.44 36.1 -2 -8 3 556.94 39.6 2 -8 -3 590.84 36.6 2 -8 -3 566.74 40.5 -2 -8 3 574.04 36.1 -2 -8 3 603.54 38.3 -2 8 3 537.05 47.2 -2 8 3 590.64 33.1 2 8 -3 585.34 29.3 2 8 -3 588.34 48.2 2 8 -3 620.64 39.5 -2 8 3 573.54 23.7 -2 8 3 631.94 38.3 -1 -8 3 155.68 21.9 1 -8 -3 126.79 22.4 -1 -8 3 153.78 16.1 -1 -8 3 168.08 19.2 1 -8 -3 175.08 13 1 -8 -3 171.28 18.5 1 -8 -3 183.88 23.5 -1 -8 3 140.99 20.9 -1 -8 3 141.99 14.1 1 -8 -3 172.58 19.7 -1 8 3 158.28 29.2 -1 8 3 161.28 10.8 1 8 -3 156.58 15.4 -1 8 3 171.88 18.3 -1 8 3 169.88 19.4 1 8 -3 176.08 18.1 1 8 -3 153.68 31.4 0 -8 -3 8.7 7.5 0 -8 3 0.7 5.3 0 -8 3 8.5 10.7 0 -8 -3 5.3 7.4 0 -8 -3 13.6 4.8 0 -8 3 14.6 7.5 0 -8 3 -5.3 9.2 0 -8 -3 19.1 17 0 -8 3 8.4 6.1 0 8 -3 -13.2 14.2 0 8 -3 8.2 5.7 0 8 3 10.3 6.7 0 8 3 2.5 12.2 0 8 -3 13.9 7.2 0 8 3 -1.5 8.1 -1 -8 -3 61.99 14.8 1 -8 3 57.49 18.4 1 -8 3 50.49 10.8 -1 -8 -3 60.39 26.3 1 -8 3 55.79 13.7 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67.89 2 -9 -3 680.43 42.8 -2 -9 3 693.33 44.9 -2 -9 3 693.43 32.6 -2 -9 3 697.93 40 -2 -9 3 705.93 35.6 2 -9 -3 714.33 48.3 2 -9 -3 744.33 31 -2 -9 3 718.13 47.7 2 9 -3 718.63 58.29 -2 9 3 678.53 58.79 -2 9 3 732.33 28.5 -2 9 3 716.13 38.8 2 9 -3 739.93 35.1 2 9 -3 670.43 39.7 -1 -9 3 318.27 28 1 -9 -3 347.67 33.3 1 -9 -3 384.86 19.5 -1 -9 3 397.36 33.7 1 -9 -3 344.57 33.5 -1 -9 3 409.76 27 -1 -9 3 396.26 24.3 1 9 -3 369.66 24.2 1 9 -3 353.06 26.9 -1 9 3 389.16 28.8 -1 9 3 353.66 29.1 -1 9 3 376.16 18 -1 9 3 365.96 43.9 1 9 -3 389.06 43 0 -9 3 1084.19 56.99 0 -9 3 1121.09 47.8 0 -9 -3 1086.69 55.49 0 -9 3 1048.5 42.8 0 -9 -3 1070.99 59.19 0 -9 3 1055.99 52.09 0 -9 -3 1108.19 33.2 0 9 3 1027.7 50.69 0 9 3 1080.59 50.19 0 9 3 1078.89 66.89 0 9 3 1022 48.6 0 9 -3 1034.2 48 0 9 -3 1037.8 44.9 0 9 -3 1084.99 69.19 1 -9 3 929.41 43.6 1 -9 3 895.21 53.19 1 -9 3 894.61 48.1 -1 -9 -3 939.11 26.8 -1 -9 -3 1001.3 61.09 1 -9 3 936.41 40.6 -1 -9 -3 953.3 50.99 1 9 3 931.51 47.7 -1 9 -3 934.61 44 1 9 3 887.71 61.79 -1 9 -3 914.81 41.2 -1 9 -3 857.91 43.3 1 9 3 918.71 49.3 -1 9 -3 935.31 66.29 2 -9 3 342.17 30 2 -9 3 335.07 25.1 2 -9 3 360.06 36.2 -2 -9 -3 300.17 42 2 -9 3 374.76 27.5 -2 -9 -3 347.37 30.5 -2 9 -3 336.07 25.9 -2 9 -3 382.76 29.8 2 9 3 330.77 33.3 2 9 3 341.97 29.6 -2 9 -3 406.16 48.7 -3 -9 -3 382.96 33.4 3 -9 3 434.76 29 3 -9 3 403.56 62.99 -3 9 -3 427.66 48.2 3 9 3 385.76 32.4 -3 9 -3 376.56 32.8 3 9 3 368.16 36.5 -4 -9 -3 554.74 16.6 4 -9 3 613.04 36.9 4 -9 3 537.15 46.1 4 9 3 576.74 39.8 -4 9 -3 448.06 46 4 9 3 584.34 41.5 4 9 3 636.34 56.59 -4 9 -3 572.04 55.69 5 -9 3 391.66 31 -5 -9 -3 392.46 14.8 -5 -9 -3 420.66 16 5 -9 3 399.06 41.9 -5 9 -3 400.86 52.59 5 9 3 390.06 35.6 5 9 3 409.36 35.2 5 9 3 437.46 42.9 6 -9 3 163.68 23.3 6 -9 3 195.08 34 6 -9 3 184.28 41.5 6 9 3 212.28 32.1 6 9 3 232.78 27.7 -6 9 -3 114.79 33.6 6 9 3 173.68 25.6 7 -9 3 147.49 25.1 7 -9 3 197.58 46.6 -7 -9 -3 136.59 13.9 7 -9 3 215.68 36.4 7 9 3 200.18 30.4 7 9 3 219.38 28.6 7 9 3 156.38 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7 191.08 28.9 7 -7 7 223.28 40.5 7 -7 7 237.88 75.49 7 7 7 248.28 28.7 10 -8 -7 -14.1 25.3 -10 -8 7 6.7 10.6 10 8 -7 -3.4 12.7 -10 8 7 -20.2 27.4 9 -8 -7 -10.9 24.1 9 -8 -7 16.3 15.7 -9 8 7 7.4 17.1 9 8 -7 17.9 16 9 8 -7 52.79 19.3 9 8 -7 18.3 6 -9 8 7 53.19 33.7 8 -8 -7 48.9 17 -8 -8 7 47.2 15.4 8 -8 -7 37.2 26.7 -8 8 7 19.9 15.3 8 8 -7 72.19 21.5 8 8 -7 36.8 6.1 -8 8 7 71.09 29.8 8 8 -7 70.79 21.9 7 -8 -7 100.99 29.2 -7 -8 7 63.79 16.8 7 -8 -7 61.09 17.2 -7 8 7 76.79 25.7 7 8 -7 64.49 21.4 7 8 -7 56.39 5.6 -7 8 7 85.19 18.1 7 8 -7 61.49 19.9 -6 -8 7 13.9 10.3 -6 -8 7 -10.5 14.9 6 -8 -7 13.5 11.5 6 -8 -7 28.9 17.7 6 8 -7 19 11.9 -6 8 7 45.1 19.5 -6 8 7 21 11.3 -6 8 7 16.9 9 -5 -8 7 76.99 22.4 -5 -8 7 97.39 17.7 5 -8 -7 100.69 25 -5 -8 7 120.99 19.7 -5 8 7 124.69 17.3 5 8 -7 113.09 22.8 5 8 -7 142.09 34.6 5 8 -7 80.89 7.6 -5 8 7 108.29 31.9 -5 8 7 94.09 12.8 5 8 -7 64.39 23.1 -4 -8 7 177.68 24.5 -4 -8 7 204.88 22.3 -4 -8 7 221.48 22.2 -4 8 7 172.08 14.2 4 8 -7 129.69 39.7 4 8 -7 177.28 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690.53 33.3 3 -3 -9 674.63 32.1 -3 3 9 646.24 31.5 -3 3 9 639.94 32.1 -3 3 9 620.44 24.8 -3 3 9 629.94 25.6 -3 3 9 672.83 40.8 -2 -3 9 1549.34 52.29 -2 -3 9 1647.04 44.1 2 -3 -9 1571.44 41.5 2 -3 -9 1646.34 44.7 -2 -3 9 1665.53 59.19 -2 -3 9 1583.74 45.6 -2 -3 9 1702.03 52.59 -2 -3 9 1542.05 48 -2 3 9 1597.54 58.19 -2 3 9 1618.24 57.49 -2 3 9 1573.94 57.29 -2 3 9 1580.24 52.79 -1 -3 9 804.52 30.3 -1 -3 9 779.32 29 -1 -3 9 761.42 29.8 -1 -3 9 813.72 32.6 -1 -3 9 768.82 30.5 -1 -3 9 806.32 37.8 -1 3 9 784.82 45.8 -1 3 9 809.72 29.5 -1 3 9 794.72 39.3 0 -3 9 460.25 27.4 0 -3 9 384.66 25.5 0 -3 9 471.55 18 0 3 9 407.36 29.7 0 3 9 435.86 19.7 0 3 9 445.86 38.9 1 -3 9 1058.09 67.99 1 -3 9 1180.18 47.4 1 -3 9 1102.09 46.7 1 -3 9 1055.79 35.2 1 -3 9 1209.28 33.6 1 3 9 1091.39 35.4 1 3 9 1168.28 36.6 1 3 9 1070.39 52.99 1 3 9 1086.59 62.79 2 -3 9 986.9 43.6 2 -3 9 815.72 43.7 2 -3 9 889.11 35.1 2 -3 9 978.7 31.6 2 3 9 960.7 51.49 2 3 9 864.41 35.5 2 3 9 928.31 62.99 2 3 9 935.01 32.8 3 -3 9 107.79 38.9 3 -3 9 113.89 21 3 -3 9 114.49 18.1 3 3 9 119.09 41.9 3 3 9 116.89 20.3 3 3 9 109.49 22.4 3 3 9 98.39 16.9 4 -3 9 195.48 44.7 4 -3 9 220.18 23.1 4 -3 9 185.98 23.2 4 3 9 173.78 27.2 4 3 9 215.88 39.4 4 3 9 189.48 17.5 5 -3 9 430.06 55.69 5 -3 9 429.96 33.7 5 -3 9 496.75 35.2 5 3 9 438.56 26.9 5 3 9 461.35 52.79 5 3 9 467.05 42.3 6 -3 9 398.86 61.49 6 -3 9 380.86 33.8 6 -3 9 324.47 33.1 6 3 9 300.07 25.7 6 3 9 340.47 38.9 6 3 9 373.96 25.9 -11 -4 9 -15 10.5 -11 4 9 -42.7 29.6 11 4 -9 -28.6 14.6 -10 -4 9 5.3 13.4 10 -4 -9 17.3 24.8 10 4 -9 55.59 18.4 10 4 -9 -11.4 16.2 -10 4 9 -20 28.8 -7 -4 9 33.7 14.1 7 -4 -9 16.8 10.4 7 -4 -9 1.5 17.2 -7 4 9 -4.4 18.7 -6 -4 9 108.59 21.5 6 -4 -9 117.29 26.5 -6 -4 9 87.79 25.7 -6 4 9 100.99 25.9 -6 4 9 116.79 14.5 6 4 -9 131.79 24.9 -6 4 9 80.59 16.5 6 4 -9 114.89 19.9 -5 -4 9 395.46 37.8 -5 -4 9 459.15 33.4 5 -4 -9 444.76 30.7 -5 -4 9 507.15 39.6 5 -4 -9 402.46 35.7 5 4 -9 415.46 29.6 -5 4 9 458.55 42.4 -5 4 9 439.46 25.7 -5 4 9 502.85 31.2 -4 -4 9 205.28 27.9 4 -4 -9 184.38 24.1 -4 -4 9 136.09 24.3 4 -4 -9 161.98 19.5 -4 -4 9 175.28 20.1 -4 4 9 192.98 18.4 -4 4 9 163.28 31.3 4 4 -9 181.98 18 -4 4 9 181.68 19.9 -4 4 9 150.88 15.5 3 -4 -9 328.77 26.8 -3 -4 9 291.77 24 -3 -4 9 343.57 23.5 -3 -4 9 286.77 21.3 -3 -4 9 337.37 28.9 -3 -4 9 297.87 26 -3 4 9 305.37 22.7 -3 4 9 316.67 32.3 -3 4 9 284.17 22.1 2 -4 -9 814.02 33.8 -2 -4 9 829.12 25.5 -2 -4 9 792.62 33.7 -2 -4 9 872.21 40.3 -2 -4 9 778.62 26.5 -2 -4 9 808.72 45.4 2 -4 -9 799.62 28.9 -2 -4 9 829.72 37.1 -2 -4 9 797.62 48.1 2 -4 -9 755.52 42.3 -2 4 9 817.12 33.1 -2 4 9 766.92 34.6 -2 4 9 810.32 42.3 -2 4 9 805.92 39.2 -1 -4 9 706.33 30.9 -1 -4 9 711.33 31.2 1 -4 -9 712.13 24.1 -1 -4 9 746.83 31.6 -1 -4 9 752.92 37 1 -4 -9 737.03 26.5 -1 -4 9 728.83 27.7 -1 4 9 706.93 37.3 -1 4 9 726.33 25.8 -1 4 9 683.93 39.9 -1 4 9 725.03 39.1 0 -4 9 447.56 32.4 0 -4 9 440.56 27.5 0 -4 9 362.96 22 0 -4 9 389.96 20.5 0 -4 9 372.56 22.2 0 4 9 349.47 34 0 4 9 361.86 29.2 0 4 9 375.76 16.4 1 -4 9 136.49 18.1 -1 -4 -9 168.28 11.2 1 -4 9 191.48 39.2 1 -4 9 206.88 20.6 1 -4 9 183.98 13.8 1 -4 9 173.88 18.2 1 4 9 176.58 13.2 1 4 9 196.58 33.1 1 4 9 186.38 22.4 1 4 9 189.18 11.3 -2 -4 -9 171.98 14.4 2 -4 9 129.29 17.4 2 -4 9 185.58 40.9 2 -4 9 188.28 21.8 2 -4 9 121.69 20.1 2 -4 9 154.98 13.5 2 4 9 154.18 11.4 2 4 9 193.58 34.8 2 4 9 139.29 21.1 2 4 9 152.58 15.1 3 -4 9 403.86 29.3 -3 -4 -9 396.96 20.2 3 -4 9 351.36 29.6 3 -4 9 390.56 48.2 -3 -4 -9 390.66 23.7 3 4 9 386.16 35.2 3 4 9 304.47 26.1 3 4 9 341.57 18.1 5 -4 9 -13.5 7.7 5 -4 9 -16.9 13.5 5 -4 9 -31.5 23.2 5 4 9 5.6 6.1 5 4 9 12.8 12.9 5 4 9 18.2 24.5 6 -4 9 78.49 44.2 6 -4 9 31.2 19.6 6 -4 9 44.4 17 6 4 9 61.59 13.2 6 4 9 89.39 37.6 6 4 9 72.39 21.9 11 5 -9 29 20.7 10 -5 -9 379.36 53.79 -10 5 9 369.26 67.19 10 5 -9 460.35 41 10 5 -9 434.56 46.9 -9 -5 9 374.46 40.2 9 -5 -9 295.17 49.7 -9 5 9 374.26 60.99 9 5 -9 393.96 42.1 -9 5 9 368.16 34.6 8 -5 -9 555.34 53.49 -8 -5 9 594.84 45.7 -8 5 9 583.14 63.19 8 5 -9 693.83 46.9 -8 5 9 500.75 34.6 8 5 -9 516.75 43 -7 -5 9 764.22 48.8 -7 -5 9 644.34 54.99 7 5 -9 781.92 49.99 -7 5 9 729.63 37.4 7 5 -9 795.72 49.3 -6 -5 9 1116.79 63.69 6 -5 -9 1152.98 62.89 -6 -5 9 1211.38 59.59 6 -5 -9 1155.08 56.39 6 5 -9 1186.58 58.69 -6 5 9 1143.39 70.99 -6 5 9 984.2 48.7 6 5 -9 1177.68 55.69 6 5 -9 1327.47 67.99 -6 5 9 1217.08 48 -5 -5 9 1182.98 56.29 -5 -5 9 1208.28 55.79 -5 -5 9 1130.19 60.49 5 -5 -9 1163.28 59.39 5 5 -9 1205.48 48.7 5 5 -9 1109.39 52.99 -5 5 9 1116.39 46.7 -5 5 9 1205.48 52.09 -5 5 9 1236.08 69.59 5 5 -9 1245.88 47.1 -5 5 9 1021.5 50.69 -4 -5 9 873.21 48.4 -4 -5 9 896.71 47.7 4 -5 -9 802.92 45 -4 -5 9 892.71 43.7 4 -5 -9 827.62 46.3 4 5 -9 855.71 42.1 -4 5 9 879.51 40.4 -4 5 9 880.11 39.9 -4 5 9 950.2 55.89 -4 5 9 824.62 37.2 -3 -5 9 579.74 32 -3 -5 9 601.14 35.2 3 -5 -9 552.64 36.8 -3 -5 9 586.64 35.7 -3 -5 9 634.54 33.7 -3 -5 9 625.34 40.7 -3 5 9 555.34 27.7 -3 5 9 539.85 32.1 -3 5 9 682.93 44.2 2 -5 -9 2031.6 64.89 -2 -5 9 2004.5 51.09 2 -5 -9 1877.41 74.99 -2 -5 9 1941.81 64.79 2 -5 -9 1618.54 71.19 -2 -5 9 1988.8 66.69 -2 -5 9 2031.3 65.79 -2 -5 9 1986.8 70.09 -2 5 9 1880.41 69.69 -2 5 9 1871.61 95.79 -2 5 9 1980.8 58.79 1 -5 -9 480.55 24.6 -1 -5 9 489.15 26.9 -1 -5 9 454.15 20.8 -1 -5 9 438.46 27.2 -1 -5 9 453.25 29.1 1 -5 -9 425.26 21.7 -1 -5 9 455.85 26 -1 5 9 429.36 18.9 -1 5 9 443.16 30.2 -1 5 9 437.66 16.7 -1 5 9 415.16 33.4 -1 5 9 438.76 30.8 0 -5 -9 314.17 17.8 0 -5 9 285.37 22.7 0 -5 9 276.37 18.5 0 -5 9 314.77 20.3 0 5 9 282.17 29.5 0 5 9 290.37 10.7 0 5 9 262.17 11.8 0 5 9 270.07 17.3 0 5 9 278.37 26.2 -1 -5 -9 416.06 20 1 -5 9 357.36 26.1 1 -5 9 354.06 26.5 1 -5 9 349.17 24.1 1 -5 9 387.26 22.7 1 5 9 381.16 37.6 1 5 9 353.46 21 2 -5 9 275.07 19.5 2 -5 9 206.68 24.1 2 -5 9 258.47 25.4 2 -5 9 285.57 43.1 2 -5 9 245.38 23.1 -2 -5 -9 205.48 23 2 5 9 268.07 29 2 5 9 241.48 19.3 2 5 9 213.48 34.1 4 -5 9 57.99 15.9 4 -5 9 79.39 32.4 4 -5 9 43 18.4 4 5 9 69.69 20.5 4 5 9 97.49 32.3 4 5 9 28.1 15.8 5 -5 9 38.8 20.4 5 -5 9 54.19 16.6 5 5 9 67.19 27.9 6 -5 9 48.6 37.9 6 -5 9 50.89 22.9 6 -5 9 70.89 19.3 6 5 9 68.89 21.4 6 5 9 103.49 33.2 6 5 9 104.89 15.4 -10 -6 9 -6.9 9.5 10 -6 -9 -19 23.7 10 6 -9 -3.7 14.7 -10 6 9 8.7 31.9 10 6 -9 44.2 16.8 9 -6 -9 55.79 31.5 -9 -6 9 12.7 11.2 -9 6 9 -4.9 16.3 -9 6 9 12.9 25.7 9 6 -9 29.9 18.4 7 -6 -9 35.8 23.3 -7 6 9 72.39 25.5 6 -6 -9 26.3 19.5 -6 6 9 31.3 18.6 -6 6 9 22.5 10.7 -6 6 9 6.1 11 6 6 -9 17.8 14.2 6 6 -9 24.6 11.7 -5 -6 9 23.7 10 -5 -6 9 -0.8 16.5 5 -6 -9 46.4 19.9 -5 6 9 15.1 7.3 -5 6 9 53.79 13.1 5 6 -9 37.6 12.8 -5 6 9 67.59 21.1 5 6 -9 28.8 13.6 -5 6 9 23.4 10.5 -4 -6 9 113.39 22.3 -4 -6 9 122.29 17.9 4 -6 -9 128.69 23.1 -4 -6 9 116.89 17.9 -4 6 9 184.38 32.9 4 6 -9 121.59 17.5 -4 6 9 117.39 15.9 -4 6 9 137.59 18.6 4 6 -9 139.79 14.2 -3 -6 9 290.47 25.6 -3 -6 9 264.87 26.8 3 -6 -9 324.07 27.7 -3 -6 9 269.07 23.9 -3 -6 9 279.47 23 -3 6 9 262.47 22.9 -3 6 9 344.57 35.9 -3 6 9 251.37 17.7 -2 -6 9 147.79 18.2 -2 -6 9 115.39 9.1 2 -6 -9 115.79 13.9 -2 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7 -9 125.59 29.5 -9 7 9 63.89 21.2 8 -7 -9 94.59 31.7 -8 7 9 100.99 30.1 8 7 -9 121.99 26.3 -8 7 9 88.39 19 7 -7 -9 214.78 38 -7 -7 9 139.09 38.5 -7 -7 9 188.98 25.1 -7 7 9 235.58 40.1 -7 7 9 182.78 22 7 7 -9 154.88 30.9 7 7 -9 160.48 26.1 -6 -7 9 289.87 28.9 -6 -7 9 211.18 36.4 -6 7 9 245.88 22.1 -6 7 9 202.28 22.5 6 7 -9 223.58 35.7 6 7 -9 245.88 28.3 5 -7 -9 391.76 37.1 -5 -7 9 411.26 31.6 -5 -7 9 343.07 36.6 5 7 -9 324.97 35.4 -5 7 9 335.37 24.1 -5 7 9 453.35 46.4 5 7 -9 392.16 37.5 -4 -7 9 261.97 30.3 4 -7 -9 293.47 30.7 -4 -7 9 259.77 26.2 -4 -7 9 276.77 25.8 -4 -7 9 285.77 25.9 -4 7 9 303.57 25.4 -4 7 9 247.18 18.4 -4 7 9 366.46 40.1 4 7 -9 199.38 33.6 -4 7 9 266.77 26.9 -3 -7 9 308.97 29.6 -3 -7 9 369.46 27.7 3 -7 -9 379.46 31.2 -3 -7 9 312.87 28.4 -3 -7 9 315.27 26.4 -3 7 9 305.87 30.5 -3 7 9 312.27 17 3 7 -9 310.67 16.6 -2 -7 9 278.57 26 -2 -7 9 298.97 29.6 -2 -7 9 289.47 24.4 2 -7 -9 320.47 25.7 -2 -7 9 291.07 15.2 -2 -7 9 268.87 24.3 -2 7 9 292.37 17.7 -2 7 9 260.47 30.7 -2 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-4 5 13 361.16 23.5 -4 5 13 395.16 29.1 -3 -5 13 691.93 42.7 -3 -5 13 661.83 36.3 -3 5 13 609.84 37.7 -3 5 13 603.84 27.9 -2 -5 13 409.86 17.7 -2 -5 13 456.65 28.4 -2 -5 13 382.06 32.4 -2 5 13 404.66 32.3 -2 5 13 423.86 20.5 -1 -5 13 429.56 37.7 -1 -5 13 445.66 24.5 -1 -5 13 440.76 49.7 -1 5 13 514.35 33.3 -1 5 13 367.06 32.4 -1 5 13 344.27 17.4 0 -5 13 399.66 50.39 0 -5 13 353.06 37.2 0 -5 13 418.66 29 0 5 13 449.86 37.2 -6 -6 13 117.49 16.9 -5 -6 13 160.88 15.8 -4 -6 13 12.8 10.1 -4 -6 13 15.8 9.8 -4 6 13 12.8 6.4 -4 6 13 24.8 10.7 -4 -7 13 199.38 23.1 -4 7 13 177.08 17.9 -4 7 13 212.28 22.8 -3 -7 13 816.92 31.6 -2 -7 13 158.98 22.8 -2 7 13 188.38 25.2 -7 0 14 -1.6 22.3 -6 0 14 10.8 21 -5 0 14 66.39 15.5 -5 0 14 56.99 19.7 -4 0 14 66.09 16.8 -4 0 14 66.69 27.1 -4 0 14 63.59 13.9 -3 0 14 236.68 19.7 -3 0 14 280.27 24.6 -3 0 14 247.08 43 -3 0 14 268.87 18.8 -2 0 14 189.58 42.3 -2 0 14 274.97 22.1 -2 0 14 283.27 24.1 -1 0 14 156.98 43.1 -1 0 14 219.48 22.5 -1 0 14 224.48 22.5 0 0 14 292.07 52.49 0 0 14 403.06 32.4 0 0 14 306.17 25.8 -6 -1 14 -5.2 14.9 -6 -1 14 34.3 19.1 -6 1 14 -30 19.9 -5 -1 14 59.19 24.8 -5 -1 14 43.3 15.5 -5 -1 14 65.79 16.4 -5 1 14 38.8 13.1 -5 1 14 48.6 17.2 -4 -1 14 54.09 13.2 -4 -1 14 83.99 29 -4 -1 14 75.29 16.5 -4 1 14 63.69 13.1 -3 -1 14 80.59 11.7 -3 -1 14 94.49 33.8 -3 -1 14 78.39 15.1 -3 1 14 76.49 14.2 -3 1 14 69.39 28 -3 1 14 103.49 14.4 -2 -1 14 51.99 13.4 -2 -1 14 61.79 29.9 -2 -1 14 54.99 7.7 -2 -1 14 59.89 10.8 -2 1 14 57.99 30.5 -2 1 14 51.89 12.4 -2 1 14 75.69 14.9 -1 -1 14 53.09 35.7 -1 -1 14 113.39 16.7 -1 -1 14 67.99 14 -1 1 14 83.49 16.3 -1 1 14 93.69 40.1 -1 1 14 71.09 13.8 0 -1 14 39 12.3 0 -1 14 30 34 0 1 14 55.29 14.9 0 1 14 15.5 32.1 -7 -2 14 136.09 27.7 -7 2 14 60.69 32.2 -6 -2 14 235.38 30.8 -6 2 14 115.89 32.7 -6 2 14 167.38 15.5 -5 -2 14 84.79 17.4 -5 -2 14 137.19 20.4 -5 2 14 35.7 23.1 -5 2 14 130.19 13.8 -5 2 14 84.49 16.6 -4 -2 14 183.48 19.8 -4 -2 14 208.38 36.4 -4 -2 14 197.58 23.9 -4 2 14 211.48 18 -4 2 14 191.48 21.2 -4 2 14 161.78 18.2 -3 -2 14 325.57 20.6 -3 -2 14 359.96 29.9 -3 -2 14 281.07 20 -3 2 14 353.66 25.5 -3 2 14 316.07 32.4 -3 2 14 336.17 24.6 -2 -2 14 213.08 23.3 -2 -2 14 210.88 43.4 -2 -2 14 232.98 17.3 -2 -2 14 192.38 14.2 -2 2 14 191.98 36.4 -1 -2 14 133.89 19.4 -1 -2 14 169.68 17.4 -1 -2 14 110.19 41 -1 2 14 136.69 37.9 -1 2 14 114.39 16.6 -1 2 14 176.98 21.4 -6 -3 14 4.2 10.4 -6 3 14 0.1 7.5 -5 -3 14 30.9 11.6 -5 3 14 34.5 9.9 -5 3 14 0.7 19.3 -5 3 14 61.99 15.4 -4 -3 14 14.1 10.3 -4 -3 14 23.9 21.1 -4 3 14 -7.4 13.3 -4 3 14 -3.3 6.8 -4 3 14 13.2 8.4 -3 -3 14 56.29 25.5 -3 -3 14 19.2 11.7 -3 3 14 26.6 9.4 -3 3 14 103.79 21.1 -2 -3 14 31.1 28.2 -2 -3 14 36.6 8.2 -2 -3 14 47.3 14.1 -2 3 14 41 18.3 -2 3 14 33.4 8.5 -2 3 14 43.8 13.1 -1 -3 14 1.7 27.8 -1 -3 14 17.7 10.4 -1 3 14 -3.9 6 -1 3 14 8 9.1 -1 3 14 16.5 21 -5 -4 14 61.79 16.6 -5 -4 14 82.69 17.3 -5 4 14 63.69 13.2 -5 4 14 60.59 13.9 -5 4 14 75.69 21.9 -4 -4 14 157.28 21.7 -4 -4 14 165.78 19.3 -4 4 14 167.48 17.8 -4 4 14 176.58 19.6 -3 -4 14 190.98 18.2 -3 -4 14 123.79 23.8 -3 4 14 178.58 16.2 -3 4 14 192.18 21.6 -2 -4 14 140.69 35.4 -2 4 14 208.78 23.5 -2 4 14 237.48 25.7 -2 4 14 185.28 15.8 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl02 Sn01 Cl02 180.0 . 3_565 ? Cl02 Sn01 Cl03 89.54(3) . . ? Cl02 Sn01 Cl03 90.46(3) 3_565 . ? Cl02 Sn01 Cl03 89.55(3) 3_565 3_565 ? Cl02 Sn01 Cl03 90.46(3) . 3_565 ? Cl03 Sn01 Cl03 180.0 3_565 . ? Cl04 Sn01 Cl02 90.31(4) . . ? Cl04 Sn01 Cl02 90.31(4) 3_565 3_565 ? Cl04 Sn01 Cl02 89.69(4) . 3_565 ? Cl04 Sn01 Cl02 89.69(4) 3_565 . ? Cl04 Sn01 Cl03 90.94(5) 3_565 3_565 ? Cl04 Sn01 Cl03 90.94(5) . . ? Cl04 Sn01 Cl03 89.06(5) . 3_565 ? Cl04 Sn01 Cl03 89.06(5) 3_565 . ? Cl04 Sn01 Cl04 180.0 3_565 . ? H00A N006 H00B 109.5 . . ? H00A N006 H00C 109.5 . . ? H00B N006 H00C 109.5 . . ? C009 N006 H00A 109.5 . . ? C009 N006 H00B 109.5 . . ? C009 N006 H00C 109.5 . . ? C008 C007 C009 116.8(3) . . ? C008 C007 C00B 121.2(3) . . ? C009 C007 C00B 122.0(3) . . ? C007 C008 H008 119.3 . . ? C00D C008 C007 121.5(4) . . ? C00D C008 H008 119.3 . . ? C007 C009 N006 120.7(3) . . ? C00A C009 N006 117.4(3) . . ? C00A C009 C007 121.8(4) . . ? C009 C00A H00D 120.2 . . ? C009 C00A C00C 119.6(4) . . ? C00C C00A H00D 120.2 . . ? O005 C00B C007 120.1(4) . . ? O005 C00B C00E 119.4(4) . . ? C00E C00B C007 120.4(4) . . ? C00A C00C H00E 119.8 . . ? C00D C00C C00A 120.3(4) . . ? C00D C00C H00E 119.8 . . ? C008 C00D H00F 120.0 . . ? C00C C00D C008 119.9(4) . . ? C00C C00D H00F 120.0 . . ? C00B C00E H00G 109.5 . . ? C00B C00E H00H 109.5 . . ? C00B C00E H00I 109.5 . . ? H00G C00E H00H 109.5 . . ? H00G C00E H00I 109.5 . . ? H00H C00E H00I 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sn01 Cl02 2.4292(9) . ? Sn01 Cl02 2.4293(9) 3_565 ? Sn01 Cl03 2.4311(10) . ? Sn01 Cl03 2.4311(10) 3_565 ? Sn01 Cl04 2.3960(11) 3_565 ? Sn01 Cl04 2.3960(11) . ? O005 C00B 1.209(5) . ? N006 H00A 0.8900 . ? N006 H00B 0.8900 . ? N006 H00C 0.8900 . ? N006 C009 1.469(5) . ? C007 C008 1.396(5) . ? C007 C009 1.398(5) . ? C007 C00B 1.490(5) . ? C008 H008 0.9300 . ? C008 C00D 1.369(6) . ? C009 C00A 1.357(5) . ? C00A H00D 0.9300 . ? C00A C00C 1.383(6) . ? C00B C00E 1.489(6) . ? C00C H00E 0.9300 . ? C00C C00D 1.363(6) . ? C00D H00F 0.9300 . ? C00E H00G 0.9600 . ? C00E H00H 0.9600 . ? C00E H00I 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N006 C009 C00A C00C -177.6(4) . . . . ? C007 C008 C00D C00C 0.2(6) . . . . ? C007 C009 C00A C00C 0.4(6) . . . . ? C008 C007 C009 N006 177.2(3) . . . . ? C008 C007 C009 C00A -0.8(5) . . . . ? C008 C007 C00B O005 164.3(4) . . . . ? C008 C007 C00B C00E -13.2(6) . . . . ? C009 C007 C008 C00D 0.4(5) . . . . ? C009 C007 C00B O005 -12.3(6) . . . . ? C009 C007 C00B C00E 170.2(4) . . . . ? C009 C00A C00C C00D 0.3(7) . . . . ? C00A C00C C00D C008 -0.6(7) . . . . ? C00B C007 C008 C00D -176.3(4) . . . . ? C00B C007 C009 N006 -6.1(5) . . . . ? C00B C007 C009 C00A 176.0(4) . . . . ?