#------------------------------------------------------------------------------
#$Date: 2021-06-12 08:05:06 +0300 (Sat, 12 Jun 2021) $
#$Revision: 266414 $
#$URL: file:///home/coder/svn-repositories/cod/cif/1/56/33/1563373.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_1563373
loop_
_publ_author_name
'Mila\<sinovi\'c, Valentina'
'Mol\<canov, Kre\<simir'
'Krawczuk, Anna'
'Bogdanov, Nikita E.'
'Zakharov, Boris A.'
'Boldyreva, Elena V.'
'Jelsch, Christian'
'Koji\'c-Prodi\'c, Biserka'
_publ_section_title
;
 Charge density studies of multicentre two-electron bonding of an anion
 radical at non-ambient temperature and pressure
;
_journal_issue                   4
_journal_name_full               IUCrJ
_journal_page_first
;
;
_journal_paper_doi               10.1107/S2052252521005273
_journal_volume                  8
_journal_year                    2021
_chemical_formula_moiety         'C15 H7 Cl2 N4 O2'
_chemical_formula_sum            'C15 H7 Cl2 N4 O2'
_chemical_formula_weight         346.132
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_atom_sites_solution_hydrogens   difmap
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           'MoPro v20.01             '
_cell_angle_alpha                90.
_cell_angle_beta                 95.781(5)
_cell_angle_gamma                90.
_cell_formula_units_Z            4
_cell_length_a                   6.2058(3)
_cell_length_b                   9.82990(10)
_cell_length_c                   19.77390(10)
_cell_volume                     1200.12(6)
_computing_structure_refinement  'MoPro (J. Appl. Cryst. 2005, 38, 38-54)'
_diffrn_measured_fraction_theta_full 0.582
_diffrn_measured_fraction_theta_max 0.505
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_sigmaI/netI    0.08065
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       8
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_theta_full        25.96
_diffrn_reflns_theta_max         28.24
_diffrn_reflns_theta_min         2.07
_exptl_crystal_density_diffrn    1.916
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             700
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.623
_refine_ls_hydrogen_treatment    refxyz
_refine_ls_matrix_type           full
_refine_ls_number_parameters     233
_refine_ls_number_reflns         1502
_refine_ls_number_restraints     40
_refine_ls_restrained_S_all      12.054
_refine_ls_R_factor_all          0.1030
_refine_ls_R_factor_gt           0.1030
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_scheme      sigma
_refine_ls_wR_factor_gt          0.0663
_refine_ls_wR_factor_ref         0.0790
_reflns_number_gt                1502
_reflns_number_total             1502
_reflns_threshold_expression     >2.0sigma(I)
_iucr_refine_instructions_details
;
! MoPro v20.01 16/04/2020 09:50:05
! molecular file: F:\kreso\rukopisi\DDQ_VT_transfer\3.95GPa\3_10.par
! reflections hkl file : F:\kreso\rukopisi\DDQ_VT_transfer\3.95GPa\OBS_NOEXTINC
#T.hkl refin. vs. F^2
! atomic table file : D:\kristalografija\MoProSuite\LibMoPro\mopro.tab
! wave functions file : D:\kristalografija\MoProSuite\LibMoPro\WAVEF
! anomalous scattering file : D:\kristalografija\MoProSuite\LibMoPro\asf_Kissel
#.dat
! Constraints file : F:\kreso\rukopisi\DDQ_VT_transfer\3.95GPa\CONSTRAIN.txt
! Restraints file : F:\kreso\rukopisi\DDQ_VT_transfer\3.95GPa\RESTRAIN.txt
! RF factor = 10.300 % RI factor = 8.132%
! wR2F factor = 4.148 % wR2I factor = 7.899%
! g.o.f.(F**2) = 1.705 Nvar= 233 Nref= 1502 Nfree= 0 0.05<sinT/l< 0.67

! P00 Dip Qua Oct Hex l=5 l=6
! Cl nl = 4 4 4 6 8 8 8
! Cl zeta= 4.259 4.259 4.259 4.259 4.259 4.259 4.259
! O nl = 2 2 2 3 4 4 4
! O zeta= 4.466 4.466 4.466 4.466 4.466 4.466 4.466
! N nl = 2 2 2 3 4 4 4
! N zeta= 3.839 3.839 3.839 3.839 3.839 3.839 3.839
! C nl = 2 2 2 3 4 4 4
! C zeta= 3.176 3.176 3.176 3.176 3.176 3.176 3.176
! H nl = 1 1 2 2 2 2 2
! H zeta= 2.000 2.000 2.000 2.000 2.000 2.000 2.000

WSIG 1.00000 ! weighting scheme
 ! SPACE GROUP P ?

CELL 6.2058 9.8299 19.7739 90.0000 95.7810 90.0000 0.71073
ZERR 0.0003 0.0001 0.0001 0.0000 0.0050 0.0000

SYMM 4 P
 X , Y, Z
 -X+1/2 , Y+1/2, -Z+1/2
 -X , -Y, -Z
 X-1/2 , -Y-1/2, Z-1/2

SCALE 4 0.737121 0.000000 -0.424850 0.787107 POLI

FMULT 1.00000

UOVER 0.00000 0.00000 0.00000 0.00000 0.00000 0.00000 ANI

SOLVT 0.00000 50.00000

EXTIN 0.00000 GAUSSIAN ISOT TYP1 ! G*10^4


DUMMY 0

KAPPA 13
 1.000820 0.716620 ! # 1 1 3.9 Cl1 2X Cl
 0.985060 0.831850 ! # 2 1 3.9 O1 2X O
 0.992600 0.989600 ! # 3 1 3.9 N1 3X N
 0.998820 0.885400 ! # 4 1 3.9 N3 1X N
 1.000420 0.906460 ! # 5 1 3.9 C1 2X C
 0.995610 0.880830 ! # 6 1 3.9 C2 3X C
 0.993650 0.930290 ! # 7 1 3.9 C5 2X C
 1.006250 0.865030 ! # 8 1 3.9 C7 3X C
 0.994380 0.817630 ! # 9 1 3.9 C9 2X C
 1.092390 1.157310 ! # 10 1 3.9 H9 5X H
 0.999600 0.921690 ! # 11 1 3.9 C10 2X C
 1.146270 1.179100 ! # 12 1 3.9 H10 2X H
 0.996960 0.907780 ! # 13 1 3.9 C14 1X C


ATOMS 30

ATOM 1 Cl1 3.9 1 0.232519 0.115470 -0.003778 1.0000 1 Cl
 ZX C5 C6 HEX K1 V0 M0 Q0
UANI 0.024591 0.012571 0.023196 -.000538 0.003279 0.000447
 7.20785 0. 0. 0. -.043 -.167 0. 0. -.010 0.
 0.133 0. 0. -.008 0. 0. 0.
 0.028 0. 0. -.011 0. 0. 0. -.020 0.

ATOM 2 Cl2 3.9 1 0.140106 0.286559 0.124748 1.0000 1 Cl
 ZX C6 C5 HEX K1 V1_Cl1 M1_Cl1 Q0
UANI 0.025531 0.021560 0.018701 -.002420 0.006463 0.002363
 7.20785 0. 0. 0. -.043 -.167 0. 0. -.010 0.
 0.133 0. 0. -.008 0. 0. 0.
 0.028 0. 0. -.011 0. 0. 0. -.020 0.

ATOM 3 O1 3.9 1 0.167826 0.578261 0.102108 1.0000 1 O
 XY C1 C6 OCT K2 V0 M0 Q0
UANI 0.029862 0.022461 0.016422 0.000051 0.011108 -.001783
 6.20498 0. -.051 0. 0. -.086 0. 0. -.080 0.
 0. -.029 0. 0. 0. 0.028 0.

ATOM 4 O2 3.9 1 0.325966 0.281605 -0.117018 1.0000 1 O
 XY C4 C5 OCT K2 V1_O1 M1_O1 Q0
UANI 0.044306 0.021315 0.005274 0.005133 0.004106 -.001602
 6.20498 0. -.051 0. 0. -.086 0. 0. -.080 0.
 0. -.029 0. 0. 0. 0.028 0.

ATOM 5 N1 3.9 1 0.264928 0.832547 -0.009162 1.0000 1 N
 ZX C7 C13 OCT K3 V0 M0 Q0
UANI 0.028579 0.025077 0.033995 -.003190 0.005765 -.006579
 5.01385 0. 0. 0. -.038 0.192 0. 0. 0. 0.
 0.056 0. 0. 0. 0. 0. 0.

ATOM 6 N2 3.9 1 0.399754 0.605086 -0.178186 1.0000 1 N
 ZX C8 C4 OCT K3 V1_N1 M1_N1 Q0
UANI 0.027563 0.028991 0.015047 -.003135 -.000032 -.000200
 5.01385 0. 0. 0. -.038 0.192 0. 0. 0. 0.
 0.056 0. 0. 0. 0. 0. 0.

ATOM 7 N3 3.9 1 0.304003 0.959133 0.178707 1.0000 1 N
bXY C9 C13 OCT K4 V0 M0 Q0
UANI 0.025234 0.028176 0.010694 0.007876 -.004883 0.000523
 4.99371 0. 0.007 0. 0. -.140 0. 0. -.012 0.
 0. 0.035 0. 0. 0. -.220 0.

ATOM 8 N4 3.9 1 1.031274 1.222590 0.256172 1.0000 1 N
 ZX C15 C12 OCT K3 V0 M0 Q0
UANI 0.028345 0.041780 0.026508 -.008398 0.005889 0.001164
 5.01385 0. 0. 0. -.038 0.192 0. 0. 0. 0.
 0.056 0. 0. 0. 0. 0. 0.

ATOM 9 C1 3.9 1 0.214831 0.510794 0.052412 1.0000 1 C
bXY C6 C2 OCT K5 V0 M0 Q0
UANI 0.017944 0.019257 0.007048 0.000323 0.003110 -.002459
 3.90971 0. -.092 0. 0. -.252 0. 0. 0.081 0.
 0. -.011 0. 0. 0. -.347 0.

ATOM 10 C2 3.9 1 0.271615 0.570004 -0.009220 1.0000 1 C
bXY C7 C3 OCT K6 V0 M0 Q0
UANI 0.025481 0.019222 0.013023 -.002531 0.004697 -.004921
 4.00185 0. -.013 0. 0. -.179 0. 0. 0.018 0.
 0. -.015 0. 0. 0. -.336 0.

ATOM 11 C3 3.9 1 0.314167 0.497181 -0.065043 1.0000 1 C
bXY C4 C8 OCT K6 V1_C2 M1_C2 Q0
UANI 0.017675 0.020360 0.012395 0.001004 -.000822 -.001781
 4.00185 0. -.013 0. 0. -.179 0. 0. 0.018 0.
 0. -.015 0. 0. 0. -.336 0.

ATOM 12 C4 3.9 1 0.300032 0.350556 -0.066127 1.0000 1 C
bXY C5 C3 OCT K5 V1_C1 M1_C1 Q0
UANI 0.018152 0.016661 0.004307 0.000045 -.000284 -.002413
 3.90971 0. -.092 0. 0. -.252 0. 0. 0.081 0.
 0. -.011 0. 0. 0. -.347 0.

ATOM 13 C5 3.9 1 0.245708 0.288595 -0.002944 1.0000 1 C
bXY C6 C4 OCT K7 V0 M0 Q0
UISO 0.014482
 4.01738 0. 0.066 -.006 0. -.164 0. 0. -.060 -.037
 0. 0.037 -.012 0. 0. -.280 -.030

ATOM 14 C6 3.9 1 0.208023 0.359663 0.052502 1.0000 1 C
bXY C5 C1 OCT K7 V1_C5 M1_C5 Q0
UANI 0.018308 0.009312 0.012930 0.000070 0.005307 -.000963
 4.01738 0. 0.066 -.006 0. -.164 0. 0. -.060 -.037
 0. 0.037 -.012 0. 0. -.280 -.030

ATOM 15 C7 3.9 1 0.270571 0.714047 -0.010375 1.0000 1 C
 ZX N1 C1 OCT K8 V0 M0 Q0
UANI 0.015287 0.051017 0.012584 -.003241 0.000537 -.005242
 4.15185 0. 0. 0. 0.258 0.409 0. 0. 0. 0.
 -.012 0. 0. 0. 0. 0. 0.

ATOM 16 C8 3.9 1 0.358092 0.558705 -0.126392 1.0000 1 C
 ZX N2 C4 OCT K8 V1_C7 M1_C7 Q0
UANI 0.022389 0.023025 0.011427 0.003888 0.004489 0.002883
 4.15185 0. 0. 0. 0.258 0.409 0. 0. 0. 0.
 -.012 0. 0. 0. 0. 0. 0.

ATOM 17 C9 3.9 1 0.333674 1.008202 0.242449 1.0000 1 C
bXY N3 C10 OCT K9 V0 M0 Q0
UANI 0.020449 0.044295 0.017655 -.004302 0.002750 -.001407
 4.12571 0. 0. 0.066 0. -.291 0. 0. 0.025 0.086
 0. -.005 -.011 0. 0. -.369 0.001

ATOM 18 H9 3.9 1 0.210753 0.990858 0.276671 1.0000 1 H
 ZX C9 N3 DIP K10 V0 M0 Q0
UISO 0.032892
 0.83502 0. 0. 0. 0.173

ATOM 19 C10 3.9 1 0.517571 1.080886 0.264569 1.0000 1 C
bXY C9 C11 OCT K11 V0 M0 Q0
UANI 0.021415 0.040353 0.020292 0.002572 0.003903 0.001684
 3.92371 0. -.048 0. 0. -.241 0. 0. 0.026 0.
 0. 0.034 0. 0. 0. -.303 0.

ATOM 20 H10 3.9 1 0.543214 1.116670 0.316557 1.0000 1 H
 ZX C10 C9 DIP K12 V0 M0 Q0
UISO 0.032677
 0.75915 0. 0. 0. 0.125

ATOM 21 C11 3.9 1 0.668022 1.103503 0.218822 1.0000 1 C
bXY C10 C12 OCT K6 V0 M0 Q0
UANI 0.020078 0.024614 0.017094 0.001479 0.000845 0.001106
 4.00185 0. -.013 0. 0. -.179 0. 0. 0.018 0.
 0. -.015 0. 0. 0. -.336 0.

ATOM 22 C12 3.9 1 0.634279 1.054574 0.153003 1.0000 1 C
bXY C13 C11 OCT K11 V1_C10 M1_C10 Q0
UANI 0.026960 0.029419 0.021072 0.002849 -.000584 -.000942
 3.92371 0. -.048 0. 0. -.241 0. 0. 0.026 0.
 0. 0.034 0. 0. 0. -.303 0.

ATOM 23 H12 3.9 1 0.751385 1.073218 0.116997 1.0000 1 H
 ZX C12 C13 DIP K12 V1_H10 M1_H10 Q0
UISO 0.031225
 0.75915 0. 0. 0. 0.125

ATOM 24 C13 3.9 1 0.452097 0.981100 0.134947 1.0000 1 C
bXY N3 C12 OCT K9 V1_C9 M1_C9 Q0
UANI 0.030261 0.028205 0.015713 0.005982 0.001221 -.002438
 4.12571 0. 0. 0.066 0. -.291 0. 0. 0.025 0.086
 0. -.005 -.011 0. 0. -.369 0.001

ATOM 25 H13 3.9 1 0.425310 0.939639 0.084051 1.0000 1 H
 ZX C13 N3 DIP K10 V1_H9 M1_H9 Q0
UISO 0.029761
 0.83502 0. 0. 0. 0.173

ATOM 26 C14 3.9 1 0.115087 0.878468 0.156312 1.0000 1 C
 ZX N3 H14C OCT K13 V0 M0 Q0
UANI 0.030053 0.043330 0.040185 -.013665 -.016079 -.004130
 4.03158 0. 0. 0. -.090 -.094 0. 0. 0. 0.
 0.257 0. 0. 0. 0. 0.106 0.

ATOM 27 H14A 3.9 1 0.120575 0.849347 0.104007 1.0000 1 H
 ZX C14 N3 DIP K10 V0 M1_H9 Q0
UISO 0.058780
 0.83502 0. 0. 0. 0.173

ATOM 28 H14B 3.9 1 0.112395 0.788618 0.187385 1.0000 1 H
 ZX C14 N3 DIP K10 V1_H14A M1_H9 Q0
UISO 0.058780
 0.83502 0. 0. 0. 0.173

ATOM 29 H14C 3.9 1 -0.028680 0.937725 0.160913 1.0000 1 H
 ZX C14 N3 DIP K10 V1_H14A M1_H9 Q0
UISO 0.058780
 0.83502 0. 0. 0. 0.173

ATOM 30 C15 3.9 1 0.865936 1.173510 0.240970 1.0000 1 C
 ZX N4 C10 OCT K8 V0 M1_C7 Q0
UANI 0.020682 0.029143 0.013252 -.006235 0.000966 0.007616
 4.15185 0. 0. 0. 0.258 0.409 0. 0. 0. 0.
 -.012 0. 0. 0. 0. 0. 0.

ANHAR 0 3 ! number_of_anharmonic_atoms max_order
! 1 ! atom number
! 0.00E+00 0.00E+00 0.00E+00 0.00E+00 0.00E+00 0.00E+00 0.00E+00 0.00E+00
! 0.00E+00 0.00E+00


STOP
;
_cod_data_source_file            lq5037.cif
_cod_data_source_block           3.95GPa
_cod_original_sg_symbol_Hall     'P ?'
_cod_database_code               1563373
_symmetry_space_group_name_h-m_alt 'P ?'
_shelx_hkl_file
; 
   0   0   4  1581.45   53.6427
   0   0   6  2137.96   76.0811
   0   1   1  1228.25   36.9655
   0   1   2  323.559    8.0305
   0   1   3  578.897    7.8401
   0   1   4  143.776    4.1102
   0   1   5  6513.85   59.5642
   0   2   3  1681.95   57.5995
   0   2   4  54.1201    5.2482
  -1   0   5  2648.70   62.9353
  -1   0   3  883.939   37.2613
  -1   0   1  42.2216    1.8008
   1   0   1  339.357    6.6135
   1   0   3  37.7810    5.6102
  -1   1   5  3434.76   41.1382
  -1   1   4  628.242   17.7100
  -1   1   3  40.7122    4.3522
  -1   1   2  990.886   19.4204
  -1   1   1  645.425   12.0907
   1   1   0  837.369   18.9860
   1   1   1  4658.31   90.4425
   1   1   2  124.511    3.9904
   1   1   3  1025.86   14.8644
   1   1   4  1036.38   20.6259
  -1   2   3  679.225   17.9535
  -1   2   2  3471.55   93.8028
   1   2   2  1827.24   70.6939
   1   2   3  3436.03   44.4079
   0   0   2  3239.80   53.3345
   0   1   6   9.2388    1.9016
   0   1   7  4155.92   36.4151
   0   2   5  4863.27   35.2620
   0   2   6   3.8875    2.9682
   0   3   4  430.210   37.4980
  -1   0   7  621.193   46.1588
   1   0   5  118.491   13.0318
  -1   1   7  5128.74   54.5475
  -1   1   6  314.808    8.8316
   1   1   5  758.958   15.4215
   1   1   6  466.815   12.7441
  -1   2   6  804.854   14.6323
  -1   2   5  2242.41   27.0500
  -1   2   4  2118.36   31.3925
   1   2   4  794.530   18.4726
   1   2   5  475.165   13.8264
   1   3   3  9908.60  190.0120
  -2   0   4  1783.92   32.7765
  -2   0   2  167.681    8.4245
   2   0   0  24495.8  246.1330
  -2   1   4  159.068    7.7257
  -2   1   3  1863.94   19.6424
  -2   1   2   4.6473    1.7166
  -2   1   1  702.570   12.0907
   2   1   0  1925.35   21.8366
   2   1   1  4630.90   40.9030
   2   1   2  16.7538    2.4725
   2   1   3  1775.43   29.4047
  -2   2   2   8.3948    5.8397
  -2   2   1  14.5002    4.7667
   2   2   0   7.3177    3.7824
   2   2   1   9.5148    9.9688
   0   0   8  21134.5  278.0030
   0   1   8  514.471   17.7854
   0   2   7  4029.23   41.8299
   0   3   5  1918.42   52.7400
   0   3   6  533.996   14.1640
   1   0   7  775.287   37.8359
  -1   1   8  59.2121    7.7803
   1   1   7  507.633   14.0760
  -1   2   7  560.054   14.3356
   1   2   6  2358.43   34.8278
  -1   3   5  1278.65   33.0244
  -1   3   4  410.082   27.3563
   1   3   4  71.8273   13.1143
   1   3   5  3388.96   64.1142
   2   0   4  5735.37   74.7417
  -2   1   6  2343.85   51.9487
  -2   1   5  6227.11   45.5532
   2   1   4   5.7727    2.6230
   2   1   5  2334.29   28.6708
  -2   2   5  393.589   16.8822
  -2   2   4  51.9633    4.8514
  -2   2   3  2017.25   40.3853
   2   2   2  2531.46   43.1535
   2   2   3  61.5260    7.7376
  -2   0   6  14424.5  131.3850
   0   1   9  350.867   17.7579
   0   2   8  4990.43   55.1250
   0   3   7  93.1867    6.2303
  -1   0   9  204.131   29.9400
   1   1   8  859.067   19.5560
  -1   2   8  2017.70   32.4920
   1   2   7  1115.98   25.3646
  -1   3   7  2432.43   44.3658
  -1   3   6  14.2080    5.2395
   1   3   6  11.0667    3.8628
   2   0   6  94.8132   14.0248
  -2   1   7   3.7527    8.6635
  -2   2   6  4410.21   52.3958
   2   2   4  580.334   16.0037
   2   2   5  83.8432   12.4217
  -2   3   4  239.810   14.1613
  -2   3   3  1483.92  218.7900
   2   3   2  171.565   29.0229
   2   3   3  47.4210    9.0543
  -3   0   1  14.1947    8.3991
   2   1   6  95.1151   15.2797
   0   1  10  1195.67   34.6475
   0   2   9  123.144   21.7198
   0   3   8  14.6171   11.1969
   0   4   6  2012.34   63.1011
  -1   1  10  478.365   25.2866
   1   1   9  2261.95   54.9040
  -1   3   8  91.5983    6.8193
   1   3   7  340.789   17.1383
  -1   4   6  394.091   20.8591
  -1   4   5  80.8887   29.3043
   1   4   5  102.610   22.2194
  -2   0   8  1039.76   48.6069
   2   1   7  1152.78   30.3046
   2   2   6  33.5317    9.1580
  -2   3   6  755.674   27.8291
   2   3   4  540.615   27.3389
   2   3   5  859.198   28.6890
  -3   0   5  1021.56   28.8259
  -3   0   3  412.970   49.9146
   3   0   3  1571.99   49.9627
  -3   1   4  56.4039    4.8323
  -3   1   3  558.251   17.8033
   3   1   1  957.224   25.7034
   3   1   2  1193.04   24.1157
  -3   2   2  1175.77   25.3860
  -3   2   1  142.252    8.7494
   3   2   0  540.634   17.5644
  -3   1   1  210.108   24.6774
  -3   1   2  177.258   35.6080
   3   0   1  344.539   57.0145
   3   1   0  218.338   24.1862
  -2   3   5  145.933   19.9583
   1   2   8  631.251   31.9068
  -2   1   8  722.597   28.5336
  -1   2   9   6.4194    8.8326
  -2   2   7  873.558   44.0537
   0   2  10  671.464   25.2495
   0   3   9  86.7042    9.9796
   0   4   7  522.307   21.8932
   1   1  10  1262.81   38.4145
  -1   2  10  4000.97   56.7820
   1   2   9  101.595    7.9997
  -1   3   9  143.864    8.5147
   1   3   8  22.1324    6.6278
  -1   4   7  11.6955    6.7111
   1   4   6  645.881   39.7379
   2   0   8  1775.63   53.4200
  -2   1   9  895.978   32.6273
   2   1   8  278.770   15.0707
  -2   2   8  1256.13   32.4133
   2   2   7  47.7438    5.6191
  -2   3   7   8.2044    5.6204
   2   3   6  769.325   21.1343
  -3   1   6  36.8840    5.8188
  -3   1   5  1003.45   18.1626
   3   1   3  1283.59   21.0801
   3   1   4  52.9381    5.5210
  -3   2   5  157.662    9.6201
  -3   2   4  452.396   15.7665
  -3   2   3  1511.33   30.2836
   3   2   1  1207.09   22.8419
   3   2   2  13.0329    4.1792
   3   2   3  518.089   29.1194
   0   1  11  413.979   24.8736
   0   3  10  58.2865   10.7305
   0   4   8  343.677   13.6389
  -1   1  11  337.185   15.9811
   1   2  10  1910.11   37.2480
   1   3   9  1567.34   42.0781
  -1   4   8  4580.76   63.2776
   1   4   7  10.2496   10.6681
  -2   0  10  1064.23   51.8240
  -2   1  10  670.345   39.2218
  -2   2   9  32.4207    8.4957
   2   2   8  918.960   28.6102
  -2   3   8  535.583   20.8812
   2   3   7  912.747   23.3522
  -2   4   6  99.2127   18.1688
  -2   4   5  214.121   35.4230
   2   4   4  50.3822   19.0581
   2   4   5  16.8054    7.9796
   3   0   5  997.565   24.4410
  -3   1   7  322.100   14.7543
   3   1   5  42.4380    4.5781
  -3   2   6  956.758   33.8405
   3   2   4  194.645   18.9747
  -3   3   4  844.550   27.3716
  -3   3   3  1434.68   45.1775
  -3   3   2  11.7931   12.0292
  -3   3   1  3887.86  270.9770
   3   3   0  36.4957    9.0892
   3   3   1  48.3580   11.3450
   3   3   2  244.025   21.2844
  -3   0   7  1971.42   39.6880
   0   1  12  23.7183    9.2570
   0   2  11  245.279   11.5016
   0   4   9   6.8257    6.7281
   1   1  11  37.8056    8.4927
  -1   2  11  228.786   12.9591
  -1   3  10  1626.16   29.8015
   1   4   8  2163.50   55.7136
   2   1   9  649.583   22.8421
  -2   2  10  134.159   12.5014
  -2   3   9  821.835   26.3574
  -2   4   7  41.0022    9.8584
   2   4   6  1592.66   57.8782
  -3   1   8   7.9983    8.5771
   3   1   6  72.5198    6.3266
  -3   2   7   4.1373   11.0834
   3   2   5  29.3029    8.2464
  -3   3   5  1087.86   25.2040
   3   3   3  2125.84   60.1293
   0   2  12  330.405   15.2871
   0   3  11  407.014   23.3005
   0   5   7  1501.59   91.6834
  -1   1  12  72.3989    9.4985
   1   2  11  303.007   17.9587
  -1   3  11  590.514   19.9914
   1   3  10  40.8388    8.9274
  -1   4   9  162.970   12.6505
   1   4   9  324.108   20.3463
  -1   5   7  19.8187   11.2033
   2   0  10  5804.43  134.8644
  -2   1  11  1147.98   44.5654
   2   1  10  185.808   14.2384
   2   2   9  915.220   29.6230
   2   3   8  104.275    8.7417
  -2   4   8  588.920   29.9237
  -3   0   9  207.711   24.9941
   3   0   7  114.330   10.5402
  -3   1   9  386.417   15.6705
   3   1   7  427.572   14.6267
  -3   2   8  2751.45   53.7757
   3   2   6  335.111   17.3511
  -3   3   6  114.573    9.2876
   3   3   4  70.7215   16.4851
   0   1  13  1339.49   85.1938
   0   4  10  1218.32   30.1742
   0   5   8  284.555   20.3426
   1   1  12  52.9867   14.4297
  -1   2  12  488.544   19.2773
  -1   4  10  16.6138    8.0313
  -1   5   8  431.518   28.4874
  -2   2  11  321.622   21.0994
   2   2  10  2189.87   56.2150
  -2   3  10  196.619   15.0051
   2   3   9  36.4830    9.3787
   2   4   7  343.295   29.6735
  -3   2   9  74.7399   14.4771
   3   2   7  21.4282    5.7327
  -3   3   7   6.1028   11.7688
   3   3   5  1778.09   55.5976
  -3   4   5   9.0245   15.5263
  -3   4   4  185.384   37.4737
   3   4   2  4499.11  639.6500
   3   4   3  231.428   21.6381
  -4   0   4  3157.37   50.3501
  -4   0   2  304.600   16.9030
   4   0   0  75.2725    9.2453
   4   0   2  11543.7  104.2880
  -4   1   4  631.349   15.6064
  -4   1   3  620.320   15.2406
  -4   1   2  33.2788    4.9044
  -4   1   1  1380.19   23.2403
   4   1   0  51.1880    6.5050
   4   1   1  39.1445    5.7122
  -2   0  12  157.654   30.5120
   0   3  12  157.969   15.4463
   0   5   9  1493.47   38.4185
  -1   1  13  26.8304    7.6527
   1   2  12  1973.63   52.0930
  -1   3  12  528.582   22.5654
   1   3  11  140.583   13.0586
   1   4  10  1706.64   48.8771
   1   5   8  95.6542   14.2194
  -2   1  12  927.160   41.4480
   2   1  11  456.285   22.8591
  -2   3  11  433.100   22.8370
  -2   4   9  183.437   15.4703
   2   4   8  858.111   28.6248
  -2   5   7  2446.56  134.5539
  -3   1  10  66.9226   10.9200
   3   1   8  338.022   15.4617
  -3   3   8  374.336   19.5056
   3   3   6  344.989   20.0238
  -3   4   6  2187.65   49.3791
   3   4   4  1849.28   59.0906
  -4   0   6  1896.52   37.8095
  -4   1   5  419.620   13.0423
   4   1   2  1558.50   28.9307
   4   1   3  282.724   12.6747
  -4   2   4  1654.40   30.6242
  -4   2   3  21.4752    9.1529
  -4   2   2   8.1757    6.9074
  -4   2   1  955.441   24.1196
   4   2   0  24.5102    6.8671
   4   2   1  59.2861    8.5932
   0   2  13  41.2394    7.9677
   0   4  11  85.0850   11.5997
   1   1  13  610.109   43.9391
  -1   2  13  1513.56   42.4201
  -1   4  11  102.589   11.0698
  -1   5   9  200.444   17.3438
  -2   2  12  554.263   32.8965
   2   2  11  309.135   22.9589
   2   3  10  129.307   14.5103
  -2   4  10  1611.29   34.8540
  -2   5   8  94.5044   13.5225
   2   5   6  198.081   40.6841
  -3   0  11  1448.45   56.5139
   3   0   9  1716.27   59.3675
  -3   1  11   2.2866   15.3262
   3   1   9  16.9633    8.2901
  -3   2  10  1085.40   40.2455
   3   2   8  1517.89   34.0248
  -3   3   9  479.696   23.1311
   3   3   7  2865.69   50.9238
  -3   4   7  137.665   11.7127
   3   4   5  143.197   18.7694
   4   0   4  16045.0  246.8570
  -4   1   6  1928.12   30.4821
   4   1   4  18.9978    7.5444
  -4   2   5  47.5729    8.8839
   4   2   2  70.4701    9.5080
   4   2   3  99.3667   13.1303
   0   1  14  398.799   33.9051
   0   3  13  991.728   33.9294
   0   5  10  35.6199    7.9506
  -1   1  14  12.3825    6.6350
   1   2  13  602.844   30.4996
   1   3  12  494.975   24.4314
   1   4  11  20.7579   12.0449
  -1   5  10  12.4776   11.4223
   1   5   9  182.657   16.8675
  -2   1  13  668.060   36.9655
   2   1  12  88.1300   17.9132
  -2   3  12  18.7392    8.4144
   2   4   9  147.670   17.7539
   2   5   7   2.8949   17.9981
   3   2   9  158.784   15.2167
  -3   4   8  96.1775   12.8420
   3   4   6  367.965   35.0626
  -4   0   8  418.148   22.5025
  -4   1   7  688.988   19.9466
   4   1   5  558.408   17.8020
  -4   2   6  299.400   20.0716
   4   2   4  36.4884    9.8258
  -4   3   4  929.915   33.6437
  -4   3   3  295.967   19.3766
  -4   3   2  17.9137    6.0863
  -4   3   1  402.005   17.3220
   4   3   0  68.8408   11.3147
   4   3   1  319.529   33.3139
   0   2  14  11.1370    8.0592
   0   4  12  1528.15   47.8058
  -1   2  14   8.7662    8.9229
  -1   3  13  1796.64   42.3963
  -1   4  12  236.958   19.1479
  -2   2  13  13.2468   13.4383
   2   2  12  18.3328   13.9819
   2   3  11  82.5224   10.2933
  -2   4  11  192.005   13.2295
  -2   5   9  11.6415    8.7604
   2   5   8  183.319   25.5419
  -3   1  12  18.0552   12.1162
   3   1  10  50.7266    9.9429
  -3   2  11  829.004   35.6213
  -3   3  10  262.139   17.3703
   3   3   8  19.4092   11.3246
   4   0   6  418.369   22.0330
  -4   1   8  271.999   13.7610
  -4   2   7  77.3572   18.6825
   4   2   5  932.058   40.2281
  -4   3   5  22.7049    7.4332
   4   3   2  21.9929   17.8842
   4   3   3  48.9534   13.7618
  -3   5   6  88.0037   80.7022
   0   6   9  12.6058   17.8539
   1   1  14  34.8320   14.3959
   1   3  13  803.634   29.2620
   1   4  12  25.3621   14.8478
  -1   5  11  497.769   26.2770
   1   5  10  13.0089   15.4521
  -2   1  14  291.566   26.1631
   2   4  10  17.7000   12.1511
   3   2  10  18.2608   14.0146
   3   3   9  54.3957   12.2932
  -3   4   9   5.2815   18.1978
   3   4   7  288.704   24.4982
   3   5   5  818.073   79.8946
  -4   1   9  439.681   20.5795
   4   1   6  154.380   11.3124
  -4   2   8  51.6573   10.1976
  -4   3   6  44.9353    9.1357
   4   3   4  23.5109   11.5275
   0   5  11  16.6796   18.7995
   0   1  15  26.4489   26.9810
   0   3  14  10.3913    8.8780
   0   4  13  464.078   27.7404
  -1   1  15  3060.65  463.4610
   1   2  14  191.413   16.3424
  -1   3  14  43.1606   12.7666
  -1   4  13  167.660   21.5875
   2   1  13  221.810   21.1527
  -2   2  14  1575.95   56.3620
  -2   3  13  86.5100   13.3913
   2   3  12  622.743   26.9424
  -2   4  12  488.098   27.0797
  -2   5  10  38.3161   10.5470
   2   5   9  2632.39   97.8897
   3   0  11  203.571   20.1555
  -3   2  12  36.6507   10.7023
  -3   3  11  1676.69   46.6869
  -3   4  10  21.2899    9.2200
   3   4   8  85.6025   14.7297
  -3   5   7   3.9211   19.7661
   4   1   7  527.679   19.7090
  -4   2   9  180.220   18.5193
   4   2   6   8.5880   10.0521
  -4   3   7  114.188   13.2457
   4   3   5  162.205   21.6137
  -4   4   4  95.1823   14.5965
  -4   4   3  529.743  126.0430
   4   4   1  187.205   28.2029
   4   4   2  152.822   21.5830
   0   2  15  82.0372   19.4831
   0   5  12  56.5023   11.3636
   0   6  10  1386.31   48.2929
  -1   2  15  678.341   36.3044
   1   5  11  68.2396   15.2384
   1   6   9  392.391   55.5419
   2   2  13  354.756   23.4911
   2   4  11  47.7162   11.5628
  -3   1  13  2200.18   88.4407
   3   1  11  435.317   29.2023
  -3   5   8  424.253   42.1876
   3   5   6  111.323   18.1988
  -4   0  10  28.1150   14.3380
  -4   1  10  149.087   17.3347
   4   2   7  20.8873   11.8331
  -4   3   8  12.0156   12.3005
  -4   4   5  323.315   21.0998
   4   4   3  30.5409   15.5469
   1   1  15  140.026   23.2007
   1   3  14  69.9348   10.9213
   1   4  13  349.229   25.6514
  -1   5  12  473.718   28.4818
  -1   6  10  406.037   23.3069
  -2   1  15  1711.83   62.2078
  -2   3  14   8.4386   18.7865
  -2   5  11   6.3664   20.1096
   2   5  10  712.209   48.6823
  -2   6   9  628.235   69.1238
  -3   2  13  25.6079    9.9636
   3   2  11  131.629   17.5530
  -3   3  12  203.962   19.3011
  -3   4  11  527.175   25.4421
   3   4   9  50.0030   27.9659
  -3   5   9  48.0254   28.1207
   3   5   7  41.8587   28.2307
   4   0   8  29.2265   15.6868
   4   1   8  18.6052   11.9946
  -4   2  10  29.8534   10.5250
   4   3   6  849.090   45.1203
  -4   4   6  26.0499   16.5124
   4   4   4  30.2760   21.9732
  -5   0   3  16.6352   10.5717
  -5   0   1  20.7146   19.7153
  -5   1   2  959.060   24.7379
  -5   1   1  85.6581    9.2451
   0   1  16  39.4631   27.4049
   0   3  15  12.1914   23.2517
   0   4  14  517.433   29.7209
   0   6  11  564.101   31.2453
  -1   1  16  116.182   33.2145
   1   2  15  181.656   22.2234
  -1   3  15  23.9607   28.6877
  -1   4  14  362.906   30.5788
   1   5  12  14.7783   10.0215
   1   6  10  1584.04  111.2050
   2   1  14  16.7073   18.8339
  -2   2  15  17.5776   23.2061
   2   3  13  475.534   24.2380
  -2   4  13  102.886   15.6832
   2   4  12  161.972   17.8482
   2   6   8  210.166   47.7520
  -3   1  14  692.439   52.5978
   3   1  12  28.1366   13.0688
  -4   1  11  183.831   19.2718
   4   2   8  26.7855   10.2267
  -4   3   9  747.984   30.1943
  -4   4   7  15.2326   17.7190
   4   4   5  36.5922   13.0938
  -5   0   5  182.995   28.8989
   5   0   1  16.4112    9.3096
  -5   1   4  38.4903   13.1532
  -5   1   3  131.741   11.0811
   5   1   0  134.304   10.2740
   5   1   1   8.2647    8.0777
   0   2  16  468.106   41.7754
   0   5  13  79.6330   13.8980
  -1   2  16  289.845   50.5997
  -1   5  13  90.3085   16.4353
  -1   6  11  51.9866   11.5975
   2   2  14  36.7030   10.4384
  -2   5  12  108.548   19.5265
  -2   6  10  115.210   20.5639
   3   2  12  1395.53   45.9002
  -3   3  13  30.8865   12.5588
   3   3  11  586.260   30.0383
  -3   5  10  237.600   26.4752
   3   5   8  594.668   74.3062
   4   1   9  355.852   33.8677
  -4   2  11  233.194   21.6336
  -4   3  10  103.357   35.4981
   4   3   7  793.419   44.0724
  -4   4   8  1405.31   47.4261
   5   0   3  578.849   25.4571
  -5   1   6  14.0990   10.0827
  -5   1   5  550.434   29.2915
   5   1   2  252.817   14.8716
  -5   2   4  544.953   27.3199
  -5   2   3  607.165   24.5933
  -5   2   2  57.7101   13.5331
  -5   2   1  346.091   16.4028
   5   2   0  605.957   21.6612
   5   2   1   5.9487   16.0305
   1   1  16  61.2486   29.7227
   1   3  15  728.348   33.4387
   1   4  14  172.226   20.5688
   1   6  11  26.3107   22.6577
  -2   1  16  569.913   39.3537
  -2   3  15  60.7921   24.7554
  -2   4  14  46.0914   25.4231
   2   5  11  174.003   48.2163
   2   6   9  1337.17  107.1450
  -3   2  14  193.219   39.2183
  -3   4  12  16.4990   21.0304
   3   4  10  218.973   32.0978
  -4   0  12  4108.24  177.6080
  -4   1  12  38.7331   17.8783
   4   2   9  78.8810   20.1542
   4   3   8  100.693   22.0080
   4   4   6  578.951   39.4005
  -4   5   6  236.936   50.1294
  -5   0   7  30.7793   13.5855
   5   1   3  412.180   17.7059
  -5   2   5  951.191   33.5058
   5   2   2  62.8045   12.1221
   0   3  16  19.3304   14.4570
   0   4  15  30.3151   25.3848
   0   6  12  40.5699   17.4877
   1   2  16  16.7659   25.9311
  -1   3  16   9.7657   25.4838
  -1   4  15  24.3340   17.6041
   1   5  13  117.728   18.5511
  -1   6  12  31.6999   14.3556
   2   1  15  447.873   43.0553
  -2   2  16  36.2506   22.0665
   2   3  14  58.8391   11.6879
   2   4  13  45.2863   13.0100
  -2   6  11  465.182   37.2933
  -3   1  15  983.704   64.1114
   3   1  13  29.4947   16.5045
  -3   5  11  527.992   35.5532
   4   0  10  2618.69   74.2980
   4   1  10  623.712   45.2192
  -4   2  12  244.270   23.5979
  -4   3  11  126.488   15.9808
  -4   4   9  92.8011   15.4977
   4   5   4  92.7206   23.7278
  -5   1   7  428.003   25.7372
   5   1   4  162.429   13.2417
  -5   2   6  979.486   30.9080
   5   2   3  688.172   27.9871
  -5   3   3  413.768   20.2642
  -5   3   2  168.223   16.9039
  -5   3   1  829.626   47.6650
   5   3   0  107.226   11.5643
   0   5  14  25.5997   12.7063
  -1   5  14  151.768   24.4019
   2   2  15  16.2457   13.5533
  -2   5  13  1906.30   61.5705
   2   5  12  50.8844   13.7088
   2   6  10  1906.55  128.7740
   3   2  13  60.6024   13.0215
  -3   3  14  643.490   35.5718
   3   3  12  1230.78   46.1712
  -3   4  13  34.5177   22.3102
   3   4  11  248.061   26.4697
  -3   6   9  25.5846   21.7764
  -4   4  10  600.665   29.1873
   4   4   7  20.7892   16.3781
  -4   5   7  47.7312   26.3887
   4   5   5  1461.96   75.8351
   5   0   5   8.7878   13.8941
  -5   1   8  24.7988    9.5195
   5   1   5  355.443   16.9325
  -5   2   7  172.447   19.9231
   5   2   4  71.8611   18.8017
  -5   3   5  78.2639   25.2913
  -5   3   4   5.3118   12.9785
   5   3   1  1092.94   54.7166
   5   3   2  24.3419   14.8502
   0   2  17  316.146   64.2585
  -1   2  17  182.206   66.9975
   1   4  15  78.1615   15.9054
   1   6  12  185.272   22.4984
  -3   2  15  242.276   23.1385
  -4   1  13  47.5086   17.9350
   4   2  10  102.059   20.8173
   4   3   9  30.7219   29.6064
  -4   5   8  263.237   53.2679
  -5   0   9  226.494   31.4881
  -5   1   9  23.2649   17.1695
  -5   2   8  478.323   35.7230
  -5   3   6  31.5225   19.3169
   5   3   3  46.7913   17.9321
   0   6  13  705.026   45.2786
   1   3  16  15.7078   19.6086
   1   5  14  570.757   49.6383
  -1   6  13  26.7473   12.1054
  -2   3  16  44.3709   20.1820
  -2   4  15  51.8632   18.6784
   2   4  14  1857.88   66.4250
  -2   6  12  104.764   20.8921
   3   1  14  208.320   22.1670
  -3   5  12  18.7989   15.7109
   3   5  10  59.4862   32.8433
  -3   6  10  42.9355   31.3849
   3   6   8  132.458   44.4634
   4   1  11  883.398   54.3321
  -4   2  13   9.1260   19.5575
  -4   3  12  44.7097   13.5671
   4   4   8  318.484   60.7763
   4   5   6  41.4768   19.6705
   5   1   6  150.254   13.0119
   5   2   5  128.355   32.5610
  -5   3   7 0.047700   27.8453
   5   3   4  13.2367   16.7398
  -5   4   3  34.9379   23.7091
  -5   4   2  16.1351   28.2971
   0   3  17  12.7547   26.4609
   0   4  16  257.301   28.7490
   0   5  15  1931.08   79.0912
  -1   3  17  15.1049   17.8374
  -1   4  16  1721.98   88.5008
  -1   5  15  41.6446   21.5499
  -2   2  17  478.803   72.1427
   2   3  15  361.839   37.2164
  -2   5  14  194.610   26.2286
   2   5  13  40.4238   13.4979
   2   6  11  36.2300   24.5889
  -3   1  16  344.305   40.7315
  -3   3  15  241.503   23.6889
   3   3  13  313.382   28.3976
  -3   4  14  2418.08   69.3485
   3   4  12  1434.63   63.1223
  -4   1  14  992.142   54.5938
   4   3  10  25.3201   20.7511
  -4   4  11  55.5096   11.4385
  -4   5   9   3.5867   28.8946
   5   0   7  26.4221   27.5620
  -5   1  10  342.461   24.9367
  -5   2   9  572.148   40.3544
  -5   4   5  44.3528   21.3022
  -5   4   4  715.873   48.6040
   5   4   1  146.665   28.4648
   2   1  16  10.1831   21.2907
   1   6  13   7.5145   21.5240
   2   2  16  16.0433   14.1516
  -3   2  16  177.965   21.2431
   3   2  14  683.872   41.0292
  -3   5  13  48.5732   15.3121
   3   5  11  61.6519   33.0201
  -3   6  11  141.925   31.5152
   3   6   9  30.9422   33.1044
   4   2  11  330.122   36.1260
  -4   3  13  118.936   18.8764
   4   4   9  78.3475   40.9555
   4   5   7  25.9505   27.2186
   5   1   7  27.9118   18.0515
  -5   3   8  28.3793   11.8364
   5   3   5  368.386   34.3082
  -5   4   6  263.030   29.4644
   5   4   2  446.837   40.4830
   0   2  18   7.5503   24.3248
   0   6  14  18.7062   31.6127
   0   7  12  18.8387   23.3175
  -1   2  18  129.778   56.2142
   1   4  16  643.323   43.4565
  -1   6  14  291.013   31.8174
  -1   7  12  281.094   47.7375
  -2   4  16  143.476   29.8727
  -2   6  13  48.4878   28.0709
   4   1  12  72.8845   20.2565
  -4   2  14  32.8919   12.6436
  -4   4  12  29.3295   14.4601
  -4   5  10  80.8811   17.0942
  -5   0  11  530.724   48.8794
  -5   1  11  1026.01   55.2838
  -5   2  10  18.0123   16.7883
   5   2   7  26.8838   18.5679
  -5   3   9  1152.23   46.1636
   5   4   3  60.1338   21.6603
   4   0  12  39.5863   26.7094
   1   3  17  60.2227   13.7501
   1   5  15  201.350   28.3314
  -2   3  17  148.909   30.4337
   2   4  15  22.7656   18.6329
  -2   5  15  1719.24   91.7973
   2   6  12  43.1756   16.3334
   3   1  15  500.646   70.9539
   3   3  14  17.3557   14.2765
  -3   4  15  524.152   50.0408
   3   4  13  174.096   30.4705
   4   3  11  14.6385   32.3632
   4   5   8  25.7051   30.3255
   5   1   8  165.693   35.3636
   5   3   6   7.5892   28.2465
  -5   4   7  19.2407   15.6844
   5   4   4  1028.83   55.4049
   0   4  17  403.937   35.8167
   0   5  16  672.531   45.7461
  -1   3  18  820.387   64.9828
  -1   4  17  383.261   43.8882
  -1   5  16  117.766   27.7853
   1   6  14  41.5672   14.3980
  -2   2  18  529.597   74.5829
   2   3  16  16.4756   14.5510
   2   5  14  44.0017   33.6520
  -3   3  16  27.9405   18.6956
   3   5  12  122.352   29.0154
  -3   6  12  652.466   40.4114
   3   6  10  1230.79  112.7560
  -4   1  15  26.8474   17.1010
   4   2  12  1272.39   68.0159
  -4   3  14  40.8653   15.1212
   4   4  10  98.8402   39.9325
  -4   5  11  1443.86   47.8418
  -5   2  11  35.5346   25.2217
   5   2   8  399.397   31.7288
  -5   3  10  181.339   26.1246
  -5   4   8  326.896   30.5128
   5   4   5  130.211   23.3068
   0   3  18  198.561   33.3221
   0   7  13  38.5755   26.1101
   1   2  18  491.843  149.8338
  -1   7  13  288.187   38.4081
   2   2  17  51.2230   32.7552
  -2   6  14  20.9819   14.5784
  -2   7  12  35.6421   30.5137
  -3   2  17  201.465   28.7858
   3   2  15  28.6375   13.5533
  -3   5  14  27.1334   16.2093
  -4   2  15  262.031   26.5625
  -4   4  13  20.8711   25.8005
   4   5   9  23.9515   30.9188
  -4   6   9  28.3371   27.5458
   5   0   9  25.2690   14.5695
  -5   1  12  55.6763   23.5987
   5   1   9  146.317   26.3104
   5   3   7  1076.44   57.0710
  -6   0   4  30.1087   23.7433
  -6   0   2  3185.04  123.3548
   6   0   0  50.9574   18.6802
  -6   1   3  534.419   34.2717
  -6   1   2  28.7106   18.6767
  -6   1   1  369.103   24.0838
   0   6  15  42.2440   19.1635
  -1   2  19  41.8946   26.6238
   1   4  17  306.554   29.0347
  -1   6  15  37.6296   35.5119
  -2   4  17  40.4650   24.4602
   2   6  13  75.6401   27.4876
   4   1  13  318.043   39.9391
  -5   3  11  27.0115   22.8242
  -5   4   9  153.310   19.8468
   5   4   6  956.849   55.0168
  -6   1   5  23.6032   18.0353
  -6   1   4  1766.83   67.4355
   6   1   0  48.9800   12.5893
   6   1   1  124.599   13.7726
  -5   5   6  465.416   88.4550
  -5   2  12  117.406   27.0429
   0   2  19  210.531   53.2880
   1   3  18  320.808   28.4063
   1   5  16  362.751   32.5712
  -2   3  18  17.7047   30.9078
   2   4  16  40.3636   18.0003
  -2   5  16  470.396   51.7379
   3   3  15  305.101   29.6684
   3   4  14  113.410   31.1447
  -3   6  13  23.3247   17.5610
   3   6  11  312.305   64.4580
  -4   1  16  112.742   21.6973
   4   2  13  407.736   40.7149
   4   4  11  258.810   57.1233
  -4   5  12  150.959   18.3872
  -4   6  10  254.471   59.7776
  -5   0  13  359.177   44.3421
   5   2   9  12.5947   23.7498
   5   3   8  340.685   96.6764
  -5   5   7  43.5788   40.5147
   5   5   4  333.463   33.9283
  -6   0   6  194.070   53.1758
   6   0   2  278.491   29.7797
  -6   1   6  184.571   26.5780
   6   1   2  95.4910   12.6947
  -6   2   4  697.877   36.1054
  -6   2   3  26.4866   15.5400
  -6   2   2  50.9614   13.6372
  -6   2   1  42.7855   11.9215
   6   2   0  31.9595   10.8841
   3   1  16   1.6405   20.2427
   0   4  18  449.098   39.6535
   0   5  17  643.034   48.5608
  -1   4  18  60.3142   23.9726
  -1   5  17  111.253   27.9895
   1   7  13  95.8414   26.8858
   2   3  17  24.5684   31.1897
   2   5  15  247.521   42.3144
  -2   6  15  348.703   36.7064
  -2   7  13  88.5593   38.2137
  -3   3  17  108.884   26.2380
  -3   5  15  30.2336   20.4744
   3   5  13  32.2696   36.0069
  -4   3  15  199.440   23.7689
  -4   4  14  28.1474   17.0280
   4   5  10  70.2746   33.5389
  -5   1  13  841.696   53.4290
   5   1  10  79.3387   27.5330
  -5   4  10  141.174   18.6548
   5   4   7  213.452   54.7698
   6   1   3  34.8453   10.2135
  -6   2   5  39.1754   19.6208
   6   2   1  825.763   30.9195
   0   3  19  627.696   57.9994
   0   7  14  336.363   34.9238
  -1   3  19  500.933   52.7357
  -2   2  19  294.006   80.7960
   2   6  14  168.836   36.1730
   2   7  12  173.145   63.3255
  -3   2  18  276.744   39.9179
   3   2  16  13.3063   24.7172
   4   1  14  153.409   68.9296
  -4   2  16  82.2429   19.1693
  -4   5  13  809.751   36.9987
  -5   2  13  920.683   55.3124
  -5   3  12  64.9626   19.2267
  -5   5   8  48.4388   18.3130
   5   5   5  212.373   35.6236
  -6   0   8  34.5248   33.9367
   6   0   4  3275.90   82.3933
  -6   1   7  695.574   52.8838
  -6   2   6  25.0491   24.3071
   6   2   2  18.6552   11.1543
  -6   3   2  211.586   19.4144
  -6   3   1  27.8652   10.5922
   0   6  16  53.1209   19.9382
   1   2  19  336.316   41.1419
  -1   6  16  1379.10   86.1991
   2   2  18  487.710   40.9887
  -2   4  18  398.436   67.6655
  -3   6  14  754.973   45.1614
   3   6  12  779.323   96.0430
   4   3  13  62.3431   40.2024
   4   4  12  12.9519   31.9808
  -4   6  11  191.459   35.5560
   5   2  10  129.169   40.2325
   5   3   9  490.196   74.7499
  -5   4  11  202.780   27.7359
  -5   5   9  125.216   24.5738
  -6   1   8  38.7546   28.0340
   6   1   4  961.443   31.6474
  -6   2   7  196.669   32.0400
   6   2   3  56.2216   12.9322
  -6   3   4  25.5738   32.8525
  -6   3   3  18.6564   13.5901
   6   3   0  207.131   18.1774
   6   3   1  552.500   44.8130
  -1   2  20  1009.34  106.2790
   1   4  18  983.174   56.8916
   1   5  17  28.0112   27.0134
   1   7  14  138.971   26.3307
  -2   3  19  288.760   43.3509
  -2   5  17  136.840   30.5607
  -3   4  17  30.7942   22.1412
   3   4  15  111.269   30.9533
  -4   1  17  230.266   38.3479
   4   2  14  53.1054   21.5199
  -4   3  16  45.8811   37.0392
  -4   4  15  150.689   20.1968
   4   5  11  612.664   88.7994
   4   6   9  868.651  101.4140
   5   0  11  545.555   56.5649
  -5   1  14  808.644   53.7088
   5   4   8  346.005   67.9153
   5   5   6  67.0439   33.4172
   6   1   5  156.399   16.1588
   6   2   4  31.2080   12.3256
  -6   3   5  90.1144   24.0823
   6   3   2  22.3478   16.5377
   0   7  15  102.948   22.4427
   1   3  19  38.8835   16.2461
   1   6  16  654.306   47.3405
   2   4  17  131.068   25.5501
   2   5  16  13.2699   32.5650
  -2   6  16  26.8026   22.6181
  -2   7  14  108.254   30.5129
  -3   3  18  124.408   29.5624
  -3   5  16  638.823   61.0632
   3   5  14  26.2273   32.8006
  -4   6  12  77.3174   20.9967
   5   1  11   6.8297   34.3857
  -5   2  14  60.2814   23.2477
  -5   3  13  47.6574   18.4224
  -6   1   9  78.5332   18.1787
  -6   2   8  74.9711   32.6609
  -6   3   6  43.3465   20.3128
   0   4  19  27.6964   31.6672
   0   5  18  30.0239   18.8019
  -1   4  19  122.669   33.5340
  -1   5  18  30.4485   30.0856
  -1   7  15  268.538   44.6803
   2   3  18  124.095   23.5784
   2   7  13   3.0109   30.1522
  -4   2  17  225.405   25.2153
  -4   5  14  153.961   22.2973
   5   2  11  418.928   42.4598
  -5   4  12  611.399   46.8513
   5   4   9  47.4804   32.8440
  -5   5  10  80.1750   21.5531
   5   5   7  67.5667   48.8053
  -6   0  10  1704.41  142.4610
   6   0   6  4720.44  124.4214
   6   1   6  30.9662   17.6912
  -6   2   9  215.863   56.5687
   6   2   5  69.4685   20.9791
  -6   3   7  381.645   34.4336
   6   3   3  10.2631   31.4658
  -6   4   3  12.6084   23.3855
   0   6  17  280.880   42.2312
  -1   3  20  281.043   41.3795
  -1   6  17  26.1566   31.7153
  -2   2  20  82.9799   55.0800
   2   6  15  393.492   65.8774
  -3   2  19  1421.45  125.0837
   3   2  17  441.146   41.7264
  -3   6  15  25.2807   20.2952
   3   6  13  38.3680   33.4921
  -3   7  13  278.258   79.6535
   4   3  14  246.234   40.6498
   4   4  13  49.1052   38.8479
   4   6  10  294.677   62.6033
  -5   1  15  54.0884   38.1670
  -6   1  10  27.0901   17.0548
  -6   3   8  97.7303   26.4912
   6   3   4  35.0756   23.4913
  -6   4   5  54.2090   19.6146
  -6   4   4  33.7421   23.0373
   6   4   1  29.8979   21.1685
   4   1  15  467.724  175.4950
   0   3  20 0.640300   28.0226
   1   7  15  299.302   43.3529
  -2   4  19  284.352   44.8280
  -2   5  18  42.0959   37.4714
  -2   7  15  536.186   46.6086
   3   4  16  53.6408   29.6972
   4   2  15  95.0701   28.4391
  -4   4  16  744.233   63.8607
   4   5  12  85.8465   42.9913
  -4   6  13  722.760   79.8390
   5   1  12  27.7540   27.7365
  -5   3  14  85.5690   21.8914
  -5   5  11  13.6850   17.1050
  -6   2  10  49.7536   35.7137
   6   2   6  37.4380   26.2777
  -6   4   6  390.669   35.7056
   6   4   2  186.603   26.5322
   2   2  19  125.613   50.8601
   1   4  19  174.132   33.2770
   1   5  18   9.0016   24.1743
   3   3  17  80.0364   20.4960
  -3   4  18  39.3928   22.1353
  -3   5  17  317.687   46.3962
   3   5  15  80.6341   30.0153
  -4   3  17  261.249   40.0195
  -4   5  15  321.771   44.8939
  -5   2  15  16.9594   16.6526
   5   3  11  115.606   33.0759
  -5   4  13  50.3644   21.7282
   5   4  10  55.2670   43.3616
   5   5   8  235.048   59.1391
  -6   1  11  38.5312   19.0534
   6   1   7  80.9625   15.2907
  -6   3   9  28.0433   31.7311
   6   4   3  49.0227   19.1726
   0   7  16  77.3768   29.1947
   1   6  17   7.9673   32.8589
  -1   7  16  39.0097   26.2754
  -2   3  20  20.6121   34.6578
   2   4  18  36.0930   32.3913
   2   5  17  1093.53   77.2528
  -2   6  17  322.706   48.2869
   2   7  14  55.5463   37.6519
  -3   3  19  381.127   50.2498
  -3   7  14  44.5595   25.5737
   3   7  12  15.6449   30.8502
  -4   2  18  279.374   45.5456
   4   6  11  351.833   95.2886
   5   2  12  105.731   25.1518
   6   2   7  175.938   29.3617
  -6   4   7  32.5966   16.7826
   0   4  20  459.491   58.6426
   0   5  19  473.349   53.9288
   1   3  20  44.8782   30.7944
  -1   4  20  22.4950   25.4429
  -1   5  19  302.946   44.6026
   2   3  19  43.4545   36.1877
   2   6  16  141.652   27.2949
  -3   6  16  43.0786   26.1404
   3   6  14  44.9704   39.6937
   4   3  15  154.899   39.0891
   4   4  14  375.397   71.8542
  -5   1  16  39.5014   33.7856
  -5   5  12  53.2583   22.4571
   5   5   9  125.102   51.8579
  -6   0  12  1105.26  118.7350
   6   0   8  28.2669   24.5134
   6   1   8  31.1105   20.9538
  -6   2  11  65.0913   27.9980
  -6   3  10  26.6478   23.9853
   6   3   6  206.112   38.5300
  -6   4   8  317.061   33.4099
   6   4   4   8.6798   24.4185
   0   6  18  145.024   37.5295
  -1   6  18  67.5671   26.2233
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   3   2  18   8.5309   29.4779
   4   5  13  156.398   48.2734
  -4   6  14  150.709   26.0574
   5   1  13  299.483   39.1102
  -5   3  15  192.941   29.9876
  -5   4  14  141.765   27.3043
  -5   6  10  170.548   38.3550
  -6   1  12  1056.52  108.6151
   0   3  21  121.125   45.9086
  -1   3  21  297.178   42.8283
   1   7  16  60.6853   27.8864
  -2   5  19   7.6505   29.3470
  -2   7  16  36.6421   24.1219
   3   4  17  43.9204   26.7000
   3   5  16  287.386   42.7498
   4   2  16  292.677   38.9776
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  -4   5  16  42.3466   26.3341
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   5   3  12  55.2723   46.4802
   5   4  11  14.6931   38.0317
   6   2   8  18.8792   33.7123
   6   3   7  68.7884   45.3216
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   6   4   5  66.7788   30.6440
  -6   5   6  10.8412   26.6349
   0   7  17  796.832   71.5776
   1   5  19  58.1357   22.6039
  -1   7  17  475.818   57.6572
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   2   7  15   8.1021   31.6268
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  -3   7  15  158.164   28.4956
   3   7  13  15.9115   33.2275
   4   6  12  718.381   98.3503
   5   2  13  337.494   41.5192
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   6   1   9  102.860   26.7897
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   1   4  20  32.0224   21.6153
   1   6  18  462.453   42.8806
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   2   4  19  122.569   25.8568
   2   5  18  281.320   45.8920
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   3   3  18  40.6260   25.7127
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   3   6  15  20.0392   33.7368
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   4   4  15  18.3794   31.7931
   5   6   8  41.4312   38.1353
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   6   4   6  28.3302   30.8924
   5   5  10  501.445   83.6801
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   2   6  17  73.9731   24.2258
   4   3  16  87.3996   45.8380
   4   5  14  17.1480   31.4298
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   5   1  14  163.674   47.0470
  -5   3  16  34.9213   25.0690
  -5   4  15  27.8204   18.5384
   6   2   9  94.5895   42.7623
   6   3   8  248.035   66.5862
  -6   5   8  236.292   41.5494
   6   5   4  22.7606   28.2057
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  -7   1   3  85.0913   20.6824
  -7   1   2  20.1560   18.8455
  -7   1   1  31.7521   17.8409
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   0   4  21  10.4660   27.5121
   0   5  20  181.097   37.3736
   0   6  19  185.345   39.5107
   1   3  21  422.470   71.6801
  -1   4  21  363.963   50.8457
   2   3  20  13.0692   16.6528
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  -4   4  18  369.630   47.3310
  -5   2  17  365.935   40.4694
   5   3  13  59.3309   41.8534
   5   4  12  238.801   62.8448
  -5   5  14  376.797   40.7222
  -5   6  12  474.446   58.2069
   6   0  10  79.5102   43.3517
  -6   2  13  64.5284   38.2070
   6   4   7  34.0976   36.8850
  -7   0   5  76.4807   62.5453
   7   0   1  15.8269   30.3805
  -7   1   5  28.0248   24.2391
  -7   1   4  83.4897   27.1149
   7   1   0  69.4329   17.5955
   0   8  16  20.9423   24.3742
   1   7  17  302.797   37.2119
  -1   8  16  31.5841   35.5550
   3   7  14  52.9128   36.7438
   4   2  17  32.7651   38.7387
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  -4   5  17  27.1607   22.6337
   4   6  13  49.3727   50.2989
   5   2  14  391.253   45.3367
   5   5  11  59.0366   48.2485
   5   6   9  62.8431   37.5333
  -6   1  14  122.185   45.9772
   6   1  10  99.0792   32.5751
  -6   4  11  38.1019   37.7103
  -6   5   9  496.250   47.6117
   6   5   5  407.823   76.9483
  -7   1   6  18.6413   21.3930
   7   1   1  56.2807   18.4521
  -7   2   4  462.327   40.6151
  -7   2   3  105.410   22.3673
  -7   2   2  47.5938   23.8856
  -7   2   1  98.2237   19.8243
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   2   7  16  282.941   47.8397
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   3   4  18  371.599   54.7771
  -3   5  19  263.544   46.0264
  -3   7  16  32.5227   35.5970
  -4   7  14  72.0520   32.6154
   6   3   9  244.737   63.5976
  -7   0   7  39.8445   38.0276
  -7   1   7  50.9170   23.3528
   7   1   2  78.1369   28.9432
  -7   2   5  35.7826   20.5022
   7   2   0  154.857   21.5121
   7   2   1  283.485   24.8658
   3   5  17  21.1121   56.7217
   0   3  22  97.4832   46.9437
   0   7  18  37.1364   28.7607
   1   5  20  42.1352   26.5762
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   3   3  19  62.2338   23.0291
  -3   6  18  17.0684   20.4645
   3   6  16  13.0028   29.8846
   4   4  16  141.251   46.9029
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  -5   4  16  32.3839   19.3225
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   6   2  10  74.4030   53.8327
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   6   4   8  98.3598   44.2728
   6   5   6  43.6157   35.1884
   7   0   3  94.7388   34.2989
   7   1   3  63.3940   24.5391
  -7   2   6  279.531   38.3125
   1   4  21  46.2473   43.9485
   1   6  19   9.1809   28.1959
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   2   4  20  62.7213   23.0199
   2   5  19  521.765   57.1616
   2   6  18  50.5396   28.3276
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   4   3  17  65.1469   29.1847
   4   5  15  147.193   52.4221
   5   3  14  35.6416   34.8928
   5   4  13  20.8591   34.7682
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   5   6  10  278.252   67.0855
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  -6   5  10   3.4439   39.1320
  -7   1   8  123.125   28.5078
  -7   2   7  197.333   64.5230
   7   2   2  76.3253   15.8100
  -7   3   4  178.039   34.1290
  -7   3   3  45.3090   31.0165
  -7   3   2  157.457   21.4375
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   1   8  16  12.5946   28.9601
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   4   7  12  95.7578   45.4554
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   5   5  12  190.770   61.4562
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   6   1  11  134.395   31.7167
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   7   1   4  158.960   20.9228
   7   2   3  37.2457   23.1723
  -7   3   5  53.6325   40.7019
   7   3   0  76.6438   29.4993
   7   3   1  474.799   46.0163
   4   6  14  281.417   71.6419
   0   5  21  175.687   38.8070
   0   6  20  17.8207   26.8438
   0   8  17  376.202   75.1838
   1   3  22   2.2086   24.8897
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   1   7  18  40.4471   23.4223
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   2   3  21  127.124   26.2430
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   3   7  15  92.8491   44.7350
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  -4   7  15  19.9475   30.4460
   5   2  15  35.5768   26.2254
   6   2  11  35.7056   24.7499
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   6   3  10  143.790   71.2699
   6   4   9  11.3844   36.9460
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   6   5   7  348.378   74.0826
   7   0   5  127.715   29.7582
  -7   1   9  579.811   54.3086
  -7   2   8  13.3183   36.1010
  -7   3   6  174.161   53.2882
   0   4  22  239.120   63.1356
   2   7  17  125.187   51.6237
   3   5  18  221.577   65.7595
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   7   1   5  129.453   20.7806
   7   2   4  46.2505   27.9024
  -7   3   7  258.556   70.2824
   7   3   2  42.1864   24.4124
   4   2  18   5.3005   33.7529
   0   7  19  176.751   40.7747
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  -2   5  21  193.954   43.5971
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   3   4  19  150.825   38.9203
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   3   6  17  61.1194   45.8133
  -5   3  18  161.656   54.9655
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   5   6  11  141.708   57.1971
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  -7   2   9  55.4620   33.2973
   7   3   3  132.751   25.7122
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  -2   6  20  35.8859   27.7757
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   4   4  17  107.103   47.1556
   4   5  16  58.0741   38.6003
   4   7  13  1294.45  139.8810
   5   3  15  27.1900   36.2235
   5   4  14  421.297   82.5336
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   5   5  13  16.3531   37.5819
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   6   1  12  320.909   43.7409
   6   3  11  60.7491   48.5342
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   6   5   8  53.5870   40.5452
   7   1   6  63.3378   31.7673
   7   2   5  262.318   35.8102
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  -7   4   5  56.4867   32.4807
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  -7   4   4  79.7552   46.6683
   1   6  20  52.9326   39.3912
   1   8  17   7.7337   35.8444
   2   5  20  70.3009   40.3251
   2   6  19  156.951   56.2317
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   3   3  20  245.034   43.1714
   4   3  18  145.395   39.5225
   4   6  15  82.0571   57.4287
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   6   4  10  140.117   60.7805
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  -7   2  10  21.2532   41.0129
   7   3   4  70.0575   46.8775
  -7   4   6  78.4430   27.8080
   7   4   1  53.2284   35.4766
   1   4  22  37.9516   41.5240
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   2   8  16  64.6406   46.6969
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   3   7  16  92.6279   55.8302
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   5   2  16  152.973   42.6347
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   6   2  12  259.886   49.3241
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   7   2   6 0.068100   31.2535
  -7   3   9  11.2628   37.0893
   7   4   2  56.7329   26.1732
   0   8  18  271.725   71.7705
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   1   7  19   3.9311   30.1001
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   5   6  12  172.764   60.0526
   6   5   9   4.8668   37.0801
   7   0   7  25.0277   40.1510
   7   1   7  142.169   54.6631
   7   3   5  89.3354   53.9634
  -7   4   7  90.3329   27.9446
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   0   6  21  864.338   78.3884
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   2   7  18  164.628   59.6493
   3   5  19  17.0132   32.8699
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  -4   6  18  37.1002   30.4278
  -5   3  19  29.1649   33.1013
  -5   4  18  120.964   54.4007
  -5   5  17  312.750   73.8946
   6   1  13  83.2530   32.9387
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  -7   2  11  372.672   83.4643
  -7   4   8  25.8506   44.6047
   7   4   3  169.203   41.7497
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   0   4  23  47.2821   36.9635
   0   7  20  38.6349   30.1595
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   3   4  20  598.140   95.4325
  -3   5  21  54.1800   27.9052
   3   6  18  165.241   41.7232
   4   5  17  141.555   54.6063
   4   7  14  410.941   84.7178
   5   4  15  109.910   53.1758
   5   5  14  47.2849   45.0966
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   6   3  12  95.0953   58.1297
   6   4  11  167.790   61.1393
  -7   1  12  452.401   86.8794
   7   2   7  40.4938   43.8863
   7   4   4  119.250   75.0653
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  -2   8  18  377.682   58.5103
  -3   4  22  413.971   59.6250
  -3   6  20  290.262   68.9614
   5   3  16  403.479   60.3325
  -5   7  14  41.4913   36.8109
   6   2  13  169.319   44.8613
  -6   4  15  49.2309   27.7596
   7   1   8  157.691   64.0202
   7   3   6  31.4007   41.0985
  -7   4   9  335.104   77.5024
   1   5  22  432.443   84.5484
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   2   8  17  80.0356   49.6573
   4   3  19  59.1283   44.6148
  -4   7  17  69.3670   41.0253
  -5   6  16  32.9491   38.6868
   5   6  13  120.301   60.5335
  -6   2  17  200.931   65.3311
  -6   5  14  34.9558   24.1429
   6   5  10  19.7270   43.1143
  -6   6  12  47.8054   30.8624
  -7   2  12  24.1773   44.0444
  -7   3  11  59.9921   43.0744
   1   6  21  75.2703   44.8465
   2   6  20  66.0226   44.6044
  -2   7  20  41.7574   29.3986
   3   3  21  96.7902   52.2860
  -3   7  19  316.581   75.5351
   3   7  17  171.851   81.9094
  -4   4  21  14.5602   36.6154
  -4   5  20  40.7043   32.3535
   5   2  17  58.4366   40.9965
  -7   1  13  66.1499   44.8038
   7   2   8  29.1178   40.9547
   7   3   7  93.8851   53.3827
   7   4   5  44.5982   37.4716
   0   8  19  190.008   55.8793
   1   4  23  45.8937   40.4868
   1   7  20  45.3396   46.2312
  -1   8  19  48.8565   51.3578
   2   4  22  215.141   63.6005
  -4   6  19  189.764   62.7699
  -5   4  19  26.3474   31.4379
  -5   5  18  216.474   60.9612
   6   3  13  54.0741   51.6736
   7   0   9  16.5001   40.7451
  -7   4  10  356.180   80.8687
  -1   5  23  35.7272   31.2982
  -1   6  22  379.259   80.6639
   2   7  19  387.737   86.1745
  -4   3  22  68.2226   51.7146
   4   7  15  25.7420   41.2003
  -5   3  20  32.1518   33.9875
   5   4  16  263.523   73.5299
   5   5  15  93.7859   51.4525
  -5   7  15  315.986   72.9912
  -6   3  17  38.5508   29.5255
  -6   4  16  410.412   57.7365
   7   1   9  48.3162   43.5155
  -7   2  13  87.5259   50.1633
  -7   3  12  209.137   65.8839
   7   4   6  524.379   93.8246
   0   5  23  321.911   72.1032
   0   6  22  57.4501   43.0059
   3   5  20  49.4968   36.6885
  -5   6  17  35.3149   42.0622
  -6   5  15  50.5109   44.4425
  -6   6  13  811.505  113.6900
   0   7  21  63.0192   46.6301
  -1   7  21  82.4243   43.3301
   3   4  21  443.573   88.8444
   3   6  19  39.1117   52.1892
   4   4  19  101.927   46.2260
  -6   2  18  38.2610   37.1413
  -7   1  14  116.220   60.0808
   7   2   9  78.0910   50.4073
   0   4  24 0.505900   32.5579
   2   8  18  80.8928   45.5400
   4   6  17  110.994   51.4773
  -7   3  13  47.5770   46.7290
   7   4   7  284.281   73.5672
   3   7  18  176.542   68.9793
   4   3  20  71.7902   54.9780
  -4   5  21  637.771   95.6532
  -7   2  14  148.231   60.9419
   0   8  20  181.338   54.0980
   1   5  23  92.8264   47.3425
   1   6  22  20.2138   39.0330
  -1   8  20  223.306   66.0692
   2   5  22  59.3085   43.6652
   2   6  21  44.8168   48.2246
  -4   4  22   9.8847   30.9350
  -4   6  20  101.816   52.8438
  -5   4  20  255.195   63.3375
  -6   3  18  147.367   59.7778
  -6   4  17   1.6540   44.5823
   7   3   9  242.431   65.1282
   8   1   0  64.5699   52.2446
   1   7  21  419.148   89.1015
   2   7  20  17.5317   44.3165
   8   1   1  59.5074   37.5354
   2   4  23  47.1227   44.8655
   8   1   2  37.4303   31.4102
   8   2   0  141.378   53.8793
   4   5  19  468.600   99.1010
   8   2   1  34.3846   30.4859
   4   6  18  41.6262   38.8909
   8   1   3  98.9720   35.9439
   8   2   2  22.4837   36.1402
   8   0   4  82.9232   37.6720
;
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_disorder_assembly
_atom_site_disorder_group
Cl Cl1 0.23252(19) 0.1155(2) -0.00378(6) 0.0201(8) Uani 1 d . . . .
Cl Cl2 0.14011(18) 0.2866(2) 0.12475(6) 0.0216(8) Uani 1 d . . . .
O O1 0.1678(5) 0.5783(5) 0.10211(16) 0.0223(11) Uani 1 d . . . .
O O2 0.3260(5) 0.2816(5) -0.11702(15) 0.0235(11) Uani 1 d . . . .
N N1 0.2649(7) 0.8325(7) -0.0092(2) 0.0290(15) Uani 1 d . . . .
N N2 0.3998(6) 0.6051(6) -0.1782(2) 0.0240(12) Uani 1 d . . . .
N N3 0.3040(6) 0.9591(6) 0.17871(19) 0.0218(11) Uani 1 d . . . .
N N4 1.0313(6) 1.2226(7) 0.2562(2) 0.0320(12) Uani 1 d . . . .
C C1 0.2148(7) 0.5108(8) 0.0524(2) 0.0146(11) Uani 1 d . . . .
C C2 0.2716(7) 0.5700(9) -0.0092(2) 0.0191(12) Uani 1 d . . . .
C C3 0.3142(7) 0.4972(8) -0.0650(2) 0.0170(12) Uani 1 d . . . .
C C4 0.3000(7) 0.3506(8) -0.0661(2) 0.0131(12) Uani 1 d . . . .
C C5 0.2457(7) 0.2886(8) -0.0029(2) 0.014(3) Uiso 1 d . . . .
C C6 0.2080(7) 0.3597(7) 0.0525(2) 0.0133(12) Uani 1 d . . . .
C C7 0.2706(8) 0.7140(10) -0.0104(2) 0.0264(18) Uani 1 d . . . .
C C8 0.3581(7) 0.5587(8) -0.1264(3) 0.0188(12) Uani 1 d . . . .
C C9 0.3337(7) 1.0082(8) 0.2424(3) 0.0274(12) Uani 1 d . . . .
H H9 0.211(6) 0.991(7) 0.277(17) 0.03289 Uiso 1 d D U . .
C C10 0.5176(7) 1.0809(8) 0.2646(2) 0.0272(12) Uani 1 d . . . .
H H10 0.543(8) 1.117(7) 0.317(17) 0.03268 Uiso 1 d D U . .
C C11 0.6680(7) 1.1035(7) 0.2188(2) 0.0207(11) Uani 1 d . . . .
C C12 0.6343(8) 1.0546(8) 0.1530(3) 0.0260(12) Uani 1 d . . . .
H H12 0.751(6) 1.073(8) 0.117(17) 0.03122 Uiso 1 d D U . .
C C13 0.4521(8) 0.9811(7) 0.1349(2) 0.0248(12) Uani 1 d . . . .
H H13 0.425(8) 0.940(7) 0.084(17) 0.02976 Uiso 1 d D U . .
C C14 0.1151(10) 0.8785(11) 0.1563(3) 0.0392(13) Uani 1 d . . . .
H H14A 0.121(10) 0.849(9) 0.104(17) 0.05878 Uiso 1 calc D U . .
H H14B 0.112(11) 0.789(5) 0.187(17) 0.05878 Uiso 1 calc D U . .
H H14C -0.029(7) 0.938(17) 0.161(3) 0.05878 Uiso 1 calc D U . .
C C15 0.8659(7) 1.1735(7) 0.2410(2) 0.0211(12) Uani 1 d . . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Cl1 0.025(2) 0.013(3) 0.023(3) -0.0005(8) 0.0033(6) 0.0004(7)
Cl2 0.026(2) 0.022(3) 0.019(3) -0.0024(8) 0.0065(6) 0.0024(7)
O1 0.030(3) 0.022(5) 0.016(3) 0.000(2) 0.0111(14) -0.0018(18)
O2 0.044(3) 0.021(5) 0.005(3) 0.005(2) 0.0041(15) -0.0016(18)
N1 0.029(3) 0.025(9) 0.034(4) -0.003(2) 0.006(2) -0.007(2)
N2 0.028(3) 0.029(6) 0.015(4) -0.003(3) 0.0000(17) 0.000(2)
N3 0.025(3) 0.028(5) 0.011(3) 0.008(2) -0.0049(16) 0.0005(18)
N4 0.028(3) 0.042(6) 0.027(4) -0.008(3) 0.0059(19) 0.001(2)
C1 0.018(3) 0.019(5) 0.007(4) 0.000(2) 0.0031(17) -0.0025(18)
C2 0.025(3) 0.019(5) 0.013(4) -0.003(2) 0.0047(17) -0.005(2)
C3 0.018(3) 0.020(5) 0.012(4) 0.001(2) -0.0008(16) -0.0018(19)
C4 0.018(3) 0.017(6) 0.004(4) 0.000(2) -0.0003(18) -0.002(2)
C6 0.018(3) 0.009(5) 0.013(3) 0.000(2) 0.0053(17) -0.0010(18)
C7 0.015(4) 0.051(13) 0.013(4) -0.003(2) 0.001(2) -0.005(2)
C8 0.022(3) 0.023(6) 0.011(4) 0.004(3) 0.0045(18) 0.003(3)
C9 0.020(3) 0.044(5) 0.018(4) -0.004(3) 0.0027(17) -0.001(2)
C10 0.021(3) 0.040(6) 0.020(4) 0.003(3) 0.004(2) 0.002(2)
C11 0.020(3) 0.025(5) 0.017(4) 0.001(3) 0.0008(17) 0.001(2)
C12 0.027(3) 0.029(5) 0.021(4) 0.003(3) -0.0006(17) -0.001(2)
C13 0.030(3) 0.028(6) 0.016(4) 0.006(3) 0.001(2) -0.002(2)
C14 0.030(3) 0.043(6) 0.040(5) -0.014(4) -0.016(3) -0.004(4)
C15 0.021(3) 0.029(5) 0.013(4) -0.006(3) 0.001(2) 0.008(2)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016
'Clementi & Roetti 1974. Atomic Data & Nuclear Data Tables. 14, 177'
H H 0.0000 0.0000
'Clementi & Roetti 1974. Atomic Data & Nuclear Data Tables. 14, 177'
N N 0.0061 0.0033
'Clementi & Roetti 1974. Atomic Data & Nuclear Data Tables. 14, 177'
O O 0.0106 0.0060
'Clementi & Roetti 1974. Atomic Data & Nuclear Data Tables. 14, 177'
Cl Cl 0.1484 0.1585
'Clementi & Roetti 1974. Atomic Data & Nuclear Data Tables. 14, 177'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C13 N3 C9 120.6(4) . . . ?
C13 N3 C14 118.5(4) . . . ?
C9 N3 C14 120.9(5) . . . ?
O1 C1 C6 121.5(5) . . . ?
O1 C1 C2 123.7(4) . . . ?
C6 C1 C2 114.7(6) . . . ?
C1 C2 C7 114.9(6) . . . ?
C1 C2 C3 124.2(5) . . . ?
C7 C2 C3 120.9(6) . . . ?
C4 C3 C8 115.7(5) . . . ?
C4 C3 C2 121.3(6) . . . ?
C8 C3 C2 122.9(5) . . . ?
O2 C4 C5 121.9(4) . . . ?
O2 C4 C3 123.1(5) . . . ?
C5 C4 C3 115.0(5) . . . ?
Cl1 C5 C6 121.1(5) . . . ?
Cl1 C5 C4 115.1(5) . . . ?
C6 C5 C4 123.9(4) . . . ?
Cl2 C6 C5 123.3(4) . . . ?
Cl2 C6 C1 115.8(4) . . . ?
C5 C6 C1 120.8(6) . . . ?
N1 C7 C2 177.32(11) . . . ?
N2 C8 C3 177.09(15) . . . ?
N3 C9 C10 120.9(4) . . . ?
N3 C9 H9 119.(16) . . . ?
C10 C9 H9 120.(5) . . . ?
C9 C10 C11 117.9(4) . . . ?
C9 C10 H10 120.(5) . . . ?
C11 C10 H10 122.(13) . . . ?
C15 C11 C10 119.4(4) . . . ?
C15 C11 C12 119.8(4) . . . ?
C10 C11 C12 120.8(4) . . . ?
C13 C12 C11 118.4(5) . . . ?
C13 C12 H12 121.(4) . . . ?
C11 C12 H12 121.(16) . . . ?
N3 C13 C12 121.5(4) . . . ?
N3 C13 H13 119.(13) . . . ?
C12 C13 H13 119.(4) . . . ?
N3 C14 H14A 110.(5) . . . ?
N3 C14 H14B 109.(5) . . . ?
N3 C14 H14C 109.(5) . . . ?
H14A C14 H14B 109.(20) . . . ?
H14A C14 H14C 109.(6) . . . ?
H14B C14 H14C 110.(9) . . . ?
N4 C15 C11 175.15(19) . . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cl1 C5 1.704(7) . ?
Cl2 C6 1.690(5) . ?
O1 C1 1.244(6) . ?
O2 C4 1.237(6) . ?
N1 C7 1.166(10) . ?
N2 C8 1.173(6) . ?
N3 C13 1.342(6) . ?
N3 C9 1.345(6) . ?
N3 C14 1.447(8) . ?
N4 C15 1.146(6) . ?
C1 C6 1.486(9) . ?
C1 C2 1.426(8) . ?
C2 C7 1.416(10) . ?
C2 C3 1.364(8) . ?
C3 C4 1.444(9) . ?
C3 C8 1.407(7) . ?
C4 C5 1.460(7) . ?
C5 C6 1.340(7) . ?
C9 C10 1.380(8) . ?
C9 H9 1.1(2) . ?
C10 C11 1.382(6) . ?
C10 H10 1.1(3) . ?
C11 C15 1.437(7) . ?
C11 C12 1.384(7) . ?
C12 C13 1.359(8) . ?
C12 H12 1.1(2) . ?
C13 H13 1.1(3) . ?
C14 H14A 1.1(3) . ?
C14 H14B 1.08(19) . ?
C14 H14C 1.08(9) . ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
C14 H14C C12 1.08(9) 2.38(9) 3.445(10) 171.(1) 1_455
C14 H14B C10 1.08(19) 2.42(15) 3.456(11) 160.(4) 2_545
C13 H13 N1 1.1(3) 2.3(3) 3.307(7) 161.(4) 1
C14 H14A N1 1.1(3) 2.5(3) 3.520(8) 158.(2) 1
C9 H9 Cl2 1.1(2) 2.9(2) 3.403(7) 109.(12) 2
C9 H9 O1 1.1(2) 2.6(3) 3.151(6) 112.(17) 2
C10 H10 O1 1.1(3) 2.2(3) 2.981(6) 127.(16) 2
C13 H13 Cl1 1.1(3) 2.6(2) 3.221(5) 112.(13) 1_565
C14 H14A Cl1 1.1(3) 2.8(2) 3.528(6) 123.(13) 3_565
C9 H9 N2 1.1(2) 2.40(15) 3.436(6) 160.(6) 4_576
C14 H14B N4 1.08(19) 2.46(14) 3.065(9) 114.(9) 2_645
C12 H12 Cl1 1.1(2) 2.9(3) 3.560(6) 118.(15) 3_665
C13 H13 Cl1 1.1(3) 2.8(2) 3.533(5) 123.(13) 3_665
C12 H12 N1 1.1(2) 2.3(3) 3.173(8) 135.(17) 3_675
C10 H10 O2 1.1(3) 2.31(17) 3.173(6) 135.(12) 4_676
C10 H10 C8 1.1(3) 2.76(13) 3.175(7) 102.(9) 4_676
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Cl1 C5 C6 Cl2 . . . . -1.3(3) ?
Cl1 C5 C6 C1 . . . . -178.6(3) ?
Cl1 C5 C4 O2 . . . . 2.7(3) ?
Cl1 C5 C4 C3 . . . . -179.2(3) ?
Cl2 C6 C5 C4 . . . . 178.7(3) ?
Cl2 C6 C1 O1 . . . . -1.7(3) ?
Cl2 C6 C1 C2 . . . . -179.7(3) ?
O1 C1 C6 C5 . . . . 175.7(3) ?
O1 C1 C2 C7 . . . . -0.2(3) ?
O1 C1 C2 C3 . . . . -177.0(3) ?
O2 C4 C5 C6 . . . . -177.3(4) ?
O2 C4 C3 C8 . . . . 0.5(3) ?
O2 C4 C3 C2 . . . . 176.0(3) ?
N3 C13 C12 C11 . . . . 2.0(6) ?
N3 C13 C12 H12 . . . . -179.(5) ?
N3 C9 C10 C11 . . . . 1.1(6) ?
N3 C9 C10 H10 . . . . -178.(5) ?
C1 C6 C5 C4 . . . . 1.4(3) ?
C1 C2 C3 C4 . . . . 1.3(4) ?
C1 C2 C3 C8 . . . . 176.4(4) ?
C2 C1 C6 C5 . . . . -2.3(4) ?
C2 C3 C4 C5 . . . . -2.2(4) ?
C3 C4 C5 C6 . . . . 0.8(3) ?
C3 C2 C1 C6 . . . . 1.0(3) ?
C4 C3 C2 C7 . . . . -175.4(3) ?
C5 C4 C3 C8 . . . . -177.6(4) ?
C6 C1 C2 C7 . . . . 177.8(3) ?
C7 C2 C3 C8 . . . . -0.3(4) ?
C9 N3 C13 C12 . . . . -0.9(6) ?
C9 N3 C13 H13 . . . . 179.(4) ?
C9 N3 C14 H14A . . . . 180.(4) ?
C9 N3 C14 H14B . . . . -60.(4) ?
C9 N3 C14 H14C . . . . 60.(5) ?
C9 C10 C11 C15 . . . . -177.2(6) ?
C9 C10 C11 C12 . . . . 0.0(6) ?
H9 C9 N3 C13 . . . . 179.(6) ?
H9 C9 N3 C14 . . . . -3.(6) ?
H9 C9 C10 C11 . . . . -178.(6) ?
H9 C9 C10 H10 . . . . 3.(8) ?
C10 C9 N3 C13 . . . . -0.7(6) ?
C10 C9 N3 C14 . . . . 177.6(6) ?
C10 C11 C12 C13 . . . . -1.5(6) ?
C10 C11 C12 H12 . . . . 179.(5) ?
H10 C10 C11 C15 . . . . 1.(5) ?
H10 C10 C11 C12 . . . . 179.(5) ?
C11 C12 C13 H13 . . . . -178.(4) ?
C12 C13 N3 C14 . . . . -179.2(6) ?
H12 C12 C13 H13 . . . . 1.(7) ?
H12 C12 C11 C15 . . . . -3.(6) ?
C13 N3 C14 H14A . . . . -2.(5) ?
C13 N3 C14 H14B . . . . 118.(4) ?
C13 N3 C14 H14C . . . . -122.(5) ?
C13 C12 C11 C15 . . . . 175.7(6) ?
H13 C13 N3 C14 . . . . 1.(6) ?