#------------------------------------------------------------------------------ #$Date: 2021-02-23 10:23:55 +0200 (Tue, 23 Feb 2021) $ #$Revision: 262152 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/56/05/1560568.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1560568 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6875 _cell_length_b 20.7157 _cell_length_c 23.6214 _exptl_crystal_F_000 2564.00 _reflns_d_resolution_high 0.8204 _cod_data_source_file 1-D.fcf _cod_data_source_block 1-D _shelx_title ' a in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 540.47 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 292111.91 332500.91 2946.78 o 4 0 0 63271.36 67480.95 1478.99 o 6 0 0 16504.08 15492.08 832.87 o 8 0 0 19.15 168.07 130.72 o 10 0 0 1170.99 1068.16 201.68 o 12 0 0 191.67 168.07 119.51 o 1 1 0 15869.45 15710.24 252.10 o 2 1 0 27954.19 33911.06 678.34 o 3 1 0 110372.70 125395.32 2257.71 o 4 1 0 41125.57 46153.89 1031.95 o 5 1 0 85733.78 98270.00 1668.56 o 6 1 0 8136.65 8071.59 524.22 o 7 1 0 10640.46 10408.35 646.23 o 8 1 0 4088.37 3850.61 631.19 o 9 1 0 1747.64 1759.81 168.46 o 10 1 0 491.05 491.81 99.42 o 11 1 0 38.19 29.00 65.46 o 12 1 0 137.35 110.35 69.95 o 13 1 0 7.44 26.14 85.90 o 0 2 0 7053.43 9706.83 112.04 o 1 2 0 31442.83 26895.95 528.48 o 2 2 0 4462.18 4702.15 168.07 o 3 2 0 8367.23 9726.19 311.86 o 4 2 0 32627.83 38466.64 1022.95 o 5 2 0 38967.76 40981.89 1336.69 o 6 2 0 1065.24 841.46 157.81 o 7 2 0 19259.21 18610.67 1344.54 o 8 2 0 5939.37 6461.26 791.78 o 9 2 0 9070.55 8876.99 440.71 o 10 2 0 274.14 295.48 89.71 o 11 2 0 3454.59 3611.41 287.58 o 12 2 0 2485.01 2562.00 207.30 o 13 2 0 403.88 489.26 164.33 o 1 3 0 232.65 178.63 49.26 o 2 3 0 19434.34 20283.88 362.28 o 3 3 0 6142.63 5516.35 261.44 o 4 3 0 198.89 247.40 73.10 o 5 3 0 173.72 282.19 70.96 o 6 3 0 693.97 489.26 295.05 o 7 3 0 13428.65 13422.99 1098.04 o 8 3 0 2746.81 2323.07 537.82 o 9 3 0 17274.76 16754.27 598.65 o 10 3 0 7420.07 7514.39 363.12 o 11 3 0 30885.50 31690.62 736.82 o 12 3 0 4836.43 5307.20 414.57 o 13 3 0 11521.98 14349.22 616.25 o 0 4 0 32520.99 34674.18 791.78 o 1 4 0 2582.55 3743.02 295.64 o 2 4 0 2122.35 1825.93 43.75 o 3 4 0 228.70 168.07 112.04 o 4 4 0 18415.48 14980.41 481.79 o 5 4 0 30221.04 29426.74 1419.24 o 6 4 0 32938.39 30431.41 1736.70 o 7 4 0 2114.86 1561.16 414.57 o 8 4 0 39697.10 38509.86 2054.16 o 9 4 0 292.31 411.57 83.05 o 10 4 0 19190.61 19093.81 576.93 o 11 4 0 53.05 157.45 203.55 o 12 4 0 1344.14 1792.72 235.29 o 13 4 0 95.37 257.70 115.78 o 1 5 0 9239.12 9381.17 403.41 o 2 5 0 24666.96 26364.18 847.81 o 3 5 0 6658.34 5871.16 231.56 o 4 5 0 12083.78 10502.35 336.13 o 5 5 0 13973.67 13718.04 1090.57 o 6 5 0 16287.62 15566.78 1176.47 o 7 5 0 2546.89 3208.22 657.33 o 8 5 0 1.69 21.04 84.08 o 9 5 0 38.65 169.28 80.20 o 10 5 0 1323.46 1247.66 159.76 o 11 5 0 5868.82 6065.37 470.59 o 12 5 0 1374.82 1408.03 224.09 o 13 5 0 1914.63 1938.38 227.82 o 0 6 0 92912.70 111103.79 1830.07 o 1 6 0 100815.38 109234.01 1353.28 o 2 6 0 38949.90 38489.18 773.79 o 3 6 0 27855.31 27701.25 1000.94 o 4 6 0 25301.74 24795.55 1098.04 o 5 6 0 14664.34 13378.17 1098.04 o 6 6 0 14012.51 13247.45 1206.35 o 7 6 0 2979.78 2726.43 586.37 o 8 6 0 1017.89 958.10 119.82 o 9 6 0 7155.85 7041.35 311.77 o 10 6 0 1517.64 1863.68 276.38 o 11 6 0 925.68 1180.21 212.89 o 12 6 0 1921.98 2207.29 265.17 o 13 6 0 34.67 149.39 97.11 o 1 7 0 895.02 1172.85 205.94 o 2 7 0 115.76 170.89 126.52 o 3 7 0 30305.25 31473.43 1083.10 o 4 7 0 8150.01 8582.64 832.87 o 5 7 0 43286.82 43424.89 1732.96 o 6 7 0 22.14 57.05 114.68 o 7 7 0 31119.35 28559.19 1322.13 o 8 7 0 1249.60 1189.11 153.42 o 9 7 0 5921.08 5927.49 415.58 o 10 7 0 4714.10 4638.66 433.24 o 11 7 0 1288.13 1381.89 220.36 o 12 7 0 5824.34 6259.58 444.45 o 13 7 0 624.74 623.72 126.98 o 0 8 0 7371.82 10065.37 556.49 o 1 8 0 637.69 687.64 117.65 o 2 8 0 13888.30 16052.22 613.96 o 3 8 0 26215.78 28668.57 1314.66 o 4 8 0 7377.86 7604.12 653.60 o 5 8 0 11864.10 11555.57 986.00 o 6 8 0 525.83 777.91 185.05 o 7 8 0 1009.82 677.07 226.71 o 8 8 0 992.05 1034.89 171.65 o 9 8 0 316.45 407.10 156.86 o 10 8 0 458.31 328.67 119.51 o 11 8 0 46.53 141.92 126.98 o 12 8 0 681.65 623.72 149.39 o 13 8 0 2.20 0.00 56.02 o 1 9 0 890.28 1274.51 300.75 o 2 9 0 1876.73 2379.50 338.43 o 3 9 0 480.77 227.82 257.70 o 4 9 0 4721.41 4683.48 440.71 o 5 9 0 12095.46 11667.62 1004.67 o 6 9 0 2326.06 1703.08 341.83 o 7 9 0 6876.88 5834.28 358.45 o 8 9 0 309.26 256.47 78.70 o 9 9 0 318.31 534.08 197.95 o 10 9 0 4242.93 4474.33 429.51 o 11 9 0 39.43 67.23 89.64 o 12 9 0 6039.88 7383.76 448.18 o 13 9 0 1.01 18.67 59.76 o 0 10 0 84413.47 118095.39 3021.48 o 1 10 0 73927.18 90616.34 2965.46 o 2 10 0 116363.60 128952.84 2126.71 o 3 10 0 860.19 575.16 235.29 o 4 10 0 67057.48 65561.25 2001.87 o 5 10 0 2882.95 2774.98 545.29 o 6 10 0 32789.47 31271.66 1284.06 o 7 10 0 4777.62 4446.09 454.73 o 8 10 0 17851.00 17446.55 667.44 o 9 10 0 8614.01 9512.62 597.57 o 10 10 0 5461.20 6218.50 519.14 o 11 10 0 1096.28 1239.96 212.89 o 12 10 0 2420.83 2595.71 261.44 o 13 10 0 115.23 156.86 63.49 o 1 11 0 7477.97 9316.42 1288.52 o 2 11 0 37724.56 43650.54 1665.74 o 3 11 0 4192.28 3704.95 451.91 o 4 11 0 25741.67 24806.76 1422.97 o 5 11 0 126.85 444.45 220.36 o 6 11 0 11192.79 10663.36 458.62 o 7 11 0 32.62 143.79 107.38 o 8 11 0 3064.22 3380.02 377.22 o 9 11 0 6436.37 7925.31 578.90 o 10 11 0 50.18 309.99 141.92 o 11 11 0 5142.44 6763.78 463.12 o 12 11 0 62.75 93.37 67.23 o 0 12 0 1996.25 1651.42 372.84 o 1 12 0 2189.27 2678.30 292.55 o 2 12 0 1747.00 1826.39 293.53 o 3 12 0 1193.89 1090.57 276.38 o 4 12 0 5571.43 4552.76 709.62 o 5 12 0 317.85 403.36 339.87 o 6 12 0 20559.26 20793.79 961.76 o 7 12 0 2858.43 2877.86 268.59 o 8 12 0 2059.30 2162.47 302.52 o 9 12 0 2395.08 2819.80 343.60 o 10 12 0 13142.29 16067.25 739.50 o 11 12 0 0.92 164.33 119.51 o 12 12 0 1380.35 1740.43 179.27 o 1 13 0 531.24 620.44 192.03 o 2 13 0 4507.04 5152.25 446.63 o 3 13 0 1130.85 1019.61 250.23 o 4 13 0 9927.71 8993.48 937.44 o 5 13 0 4.07 3.73 78.05 o 6 13 0 4390.29 4454.91 307.51 o 7 13 0 4826.96 4900.10 466.85 o 8 13 0 342.70 358.54 156.86 o 9 13 0 14717.75 16929.99 784.31 o 10 13 0 18.20 59.76 100.84 o 11 13 0 12022.94 13445.40 567.69 o 12 13 0 430.03 549.02 89.64 o 0 14 0 29987.25 35372.60 1815.13 o 1 14 0 142.30 74.42 122.70 o 2 14 0 19800.44 21423.00 1411.77 o 3 14 0 759.64 1239.96 444.45 o 4 14 0 11151.26 11425.84 963.59 o 5 14 0 5473.85 5506.39 999.07 o 6 14 0 11281.25 12557.04 1006.32 o 7 14 0 11796.68 12728.31 694.68 o 8 14 0 1518.53 1493.93 261.44 o 9 14 0 9302.52 10278.26 578.90 o 10 14 0 4410.24 4795.52 362.28 o 11 14 0 510.44 556.49 126.98 o 1 15 0 1403.60 1873.63 298.72 o 2 15 0 2815.61 3235.26 214.45 o 3 15 0 3646.92 4289.76 519.14 o 4 15 0 3640.71 3728.32 295.22 o 5 15 0 3107.86 3480.22 963.59 o 6 15 0 3187.69 3357.61 332.40 o 7 15 0 148.82 224.09 130.72 o 8 15 0 229.76 149.39 108.31 o 9 15 0 5.90 44.82 85.90 o 10 15 0 1108.15 1284.78 186.74 o 11 15 0 338.57 313.73 82.17 o 0 16 0 49573.98 56138.27 2491.13 o 1 16 0 5042.04 5439.32 297.24 o 2 16 0 31478.16 38685.24 1312.79 o 3 16 0 3328.59 3449.94 390.29 o 4 16 0 8662.43 9389.42 655.46 o 5 16 0 3070.68 3324.00 369.75 o 6 16 0 315.78 362.28 149.39 o 7 16 0 2744.15 2707.75 309.99 o 8 16 0 290.92 324.93 85.90 o 9 16 0 1052.69 941.18 168.07 o 10 16 0 5.71 0.00 52.29 o 1 17 0 3309.82 3415.65 227.60 o 2 17 0 4676.67 5171.44 290.56 o 3 17 0 3668.86 4084.92 498.60 o 4 17 0 8192.84 8866.49 496.73 o 5 17 0 11203.41 10700.29 586.37 o 6 17 0 8461.52 8866.49 549.02 o 7 17 0 5650.03 5535.02 436.98 o 8 17 0 279.10 179.27 78.43 o 9 17 0 3363.29 3790.85 291.32 o 10 17 0 442.78 422.04 93.37 o 0 18 0 5543.44 5624.66 328.67 o 1 18 0 20069.76 20967.35 702.15 o 2 18 0 836.29 918.77 168.07 o 3 18 0 4327.54 3805.79 347.34 o 4 18 0 922.73 1195.15 201.68 o 5 18 0 225.45 212.89 78.43 o 6 18 0 2427.84 2476.19 291.32 o 7 18 0 3202.18 3320.27 295.05 o 8 18 0 1892.96 2024.28 227.82 o 9 18 0 3314.71 3193.28 239.03 o 1 19 0 385.93 235.29 119.51 o 2 19 0 934.57 926.24 126.98 o 3 19 0 1590.73 1852.48 216.62 o 4 19 0 2468.79 2450.05 250.23 o 5 19 0 44.66 11.20 67.23 o 6 19 0 213.89 317.46 112.04 o 7 19 0 77.62 179.27 67.23 o 8 19 0 250.03 194.21 74.70 o 9 19 0 2557.33 2009.34 164.33 o 0 20 0 7685.93 8104.59 440.71 o 1 20 0 21.73 23.51 44.66 o 2 20 0 6185.59 5986.94 403.36 o 3 20 0 693.30 690.94 138.19 o 4 20 0 17441.75 17774.07 649.86 o 5 20 0 8.17 3.73 74.70 o 6 20 0 14514.30 14412.72 578.90 o 7 20 0 11.73 63.49 63.49 o 8 20 0 9471.51 9774.06 373.48 o 1 21 0 17.03 42.46 49.97 o 2 21 0 532.08 556.34 77.87 o 3 21 0 718.28 668.53 130.72 o 4 21 0 974.07 1019.61 156.86 o 5 21 0 906.11 829.13 130.72 o 6 21 0 726.89 668.53 123.25 o 7 21 0 108.04 56.02 37.35 o 0 22 0 667.89 694.68 119.51 o 1 22 0 4915.91 5246.30 371.62 o 2 22 0 1747.10 1869.25 153.13 o 3 22 0 2130.72 2144.49 222.22 o 4 22 0 316.53 384.57 64.66 o 5 22 0 163.48 239.03 63.49 o 6 22 0 21.45 0.00 41.08 o 1 23 0 1058.14 961.77 96.37 o 2 23 0 230.44 293.03 60.57 o 3 23 0 4389.42 4151.99 248.37 o 4 23 0 962.53 965.14 100.84 o 5 23 0 6190.81 5530.97 339.87 o 0 24 0 14734.57 14677.89 470.59 o 1 24 0 1860.76 1808.65 117.50 o 2 24 0 8705.59 8314.76 242.79 o 3 24 0 897.36 786.76 75.23 o 4 24 0 4003.27 3803.15 377.22 o 1 25 0 16.70 10.55 22.33 o 2 25 0 224.94 148.16 72.83 o 1 0 1 59664.47 67731.75 651.40 o 2 0 1 44182.08 49963.89 661.86 o 3 0 1 210277.86 232166.84 4965.46 o 4 0 1 107308.98 120431.42 1677.83 o 5 0 1 104449.64 113057.99 1770.15 o 6 0 1 8393.11 8128.46 562.44 o 7 0 1 14441.76 13405.26 724.84 o 8 0 1 2556.59 2625.59 500.47 o 9 0 1 6510.35 5726.53 294.38 o 10 0 1 596.81 517.29 109.57 o 11 0 1 2001.95 2094.79 193.45 o 12 0 1 1042.46 1519.46 161.12 o 13 0 1 53.00 85.90 70.96 o -13 1 1 2705.64 3200.75 309.99 o -12 1 1 780.36 748.86 147.53 o -11 1 1 4049.46 4257.30 273.10 o -10 1 1 5477.30 5771.53 328.67 o -9 1 1 2519.89 2458.92 262.88 o -8 1 1 17594.96 17180.23 1381.89 o -7 1 1 3405.17 3682.54 515.41 o -6 1 1 11691.06 11347.28 418.98 o -5 1 1 27294.09 31280.37 1064.43 o -4 1 1 2333.29 2066.06 160.51 o -3 1 1 101797.11 118392.23 6937.45 o -2 1 1 12766.44 15667.62 422.04 o -1 1 1 176352.05 186267.31 978.53 o 1 1 1 169172.56 181837.78 1183.94 o 2 1 1 11856.93 13537.95 294.03 o 3 1 1 90235.82 100548.73 1305.94 o 4 1 1 1502.42 1114.39 77.95 o 5 1 1 24991.27 28984.06 1039.20 o 6 1 1 13874.44 14830.32 673.37 o 7 1 1 4058.50 4415.68 402.58 o 8 1 1 20164.37 19260.53 1411.77 o 9 1 1 2447.75 2620.20 199.38 o 10 1 1 5722.46 6132.65 320.86 o 11 1 1 4057.02 4461.54 279.94 o 12 1 1 1041.98 1099.88 142.54 o 13 1 1 2840.87 3368.82 302.52 o -13 2 1 1885.76 2110.18 250.23 o -12 2 1 3966.46 4686.37 275.97 o -11 2 1 7900.14 7647.03 368.35 o -10 2 1 6757.33 6666.46 341.93 o -9 2 1 559.55 433.29 94.86 o -8 2 1 14154.90 13998.15 1191.41 o -7 2 1 5947.21 5826.34 732.03 o -6 2 1 9372.47 8844.36 442.77 o -5 2 1 56904.80 57583.35 2903.83 o -4 2 1 26209.40 25939.79 1060.69 o -3 2 1 29906.83 32276.42 676.00 o -2 2 1 43937.81 45874.95 638.66 o -1 2 1 7243.84 7982.51 276.38 o 0 2 1 18812.85 19351.42 234.83 o 2 2 1 45989.43 37818.91 369.75 o 3 2 1 23908.33 25746.84 619.25 o 4 2 1 28039.23 30659.45 1381.89 o 5 2 1 60498.79 65592.50 1392.26 o 6 2 1 8003.92 8300.17 523.82 o 7 2 1 7076.10 7447.26 806.72 o 8 2 1 13028.52 14192.36 1165.27 o 9 2 1 747.56 725.43 138.00 o 10 2 1 6824.21 6410.44 332.73 o 11 2 1 7673.63 7819.84 368.35 o 12 2 1 3710.34 4555.31 433.24 o 13 2 1 1919.69 2255.84 250.23 o -13 3 1 182.45 239.03 138.19 o -12 3 1 2453.53 2771.25 309.99 o -11 3 1 5344.49 5134.10 310.30 o -10 3 1 3522.52 3504.76 250.85 o -9 3 1 12298.15 12212.80 423.03 o -8 3 1 8699.38 8093.38 989.73 o -7 3 1 34089.67 32112.09 1796.45 o -6 3 1 6190.31 5594.78 802.99 o -5 3 1 33863.56 31286.22 2485.53 o -4 3 1 18310.25 17094.11 1938.38 o -3 3 1 5380.17 6009.35 272.64 o -2 3 1 17406.75 17598.53 358.54 o -1 3 1 26878.16 25785.55 301.99 o 0 3 1 65137.04 68512.11 900.09 o 1 3 1 25486.38 23990.98 493.00 o 3 3 1 7316.34 6987.87 197.95 o 4 3 1 16725.85 15181.76 1880.49 o 5 3 1 33023.13 35413.68 1359.48 o 6 3 1 8288.30 7992.54 888.89 o 7 3 1 30499.81 30031.79 1684.41 o 8 3 1 7969.79 7170.88 903.83 o 9 3 1 11420.70 11649.74 408.73 o 10 3 1 3655.16 3563.60 249.56 o 11 3 1 5422.68 5371.21 308.95 o 12 3 1 2279.76 2901.94 272.64 o 13 3 1 86.95 358.54 138.19 o -13 4 1 1195.98 1576.10 209.15 o -12 4 1 9435.76 10341.75 582.63 o -11 4 1 1743.81 1937.68 195.21 o -10 4 1 9744.22 10154.66 430.45 o -9 4 1 921.64 945.92 190.79 o -8 4 1 1751.88 1587.30 410.83 o -7 4 1 4041.03 3185.81 590.10 o -6 4 1 3342.28 3630.26 601.31 o -5 4 1 20222.96 18769.96 1133.52 o -4 4 1 26252.21 23551.85 571.43 o -3 4 1 16672.05 15376.30 444.45 o -2 4 1 28847.79 29087.45 1094.31 o -1 4 1 31691.02 33825.14 445.04 o 0 4 1 1224.39 2046.73 238.99 o 1 4 1 35884.57 39445.18 900.09 o 4 4 1 26395.06 21929.08 2521.01 o 5 4 1 21508.36 23077.53 1236.23 o 6 4 1 1383.51 1557.43 395.89 o 7 4 1 4541.52 4500.47 676.00 o 8 4 1 1508.34 1751.64 418.30 o 9 4 1 747.97 844.19 128.50 o 10 4 1 9258.06 8823.32 521.01 o 11 4 1 1901.99 1998.57 195.21 o 12 4 1 9214.18 10412.71 567.69 o 13 4 1 1302.35 1635.86 201.68 o -13 5 1 631.85 724.56 164.33 o -12 5 1 1145.17 1493.93 239.03 o -11 5 1 9135.23 10005.62 605.04 o -10 5 1 2512.27 3034.89 245.56 o -9 5 1 22980.69 22923.23 582.60 o -8 5 1 4053.10 3851.99 240.04 o -7 5 1 17954.50 18001.89 1396.83 o -6 5 1 2451.32 2696.55 455.65 o -5 5 1 49320.14 45449.17 1994.40 o -4 5 1 1534.73 1912.23 242.76 o -3 5 1 14610.60 14028.03 455.65 o -2 5 1 16586.63 17171.87 775.76 o -1 5 1 27013.59 30767.62 663.61 o 0 5 1 50513.74 63360.58 1277.31 o 1 5 1 27018.51 29220.25 621.93 o 2 5 1 15497.46 15365.10 661.07 o 5 5 1 51686.62 50692.88 2020.54 o 6 5 1 3105.19 2662.94 444.45 o 7 5 1 18960.71 18487.42 1359.48 o 8 5 1 3454.05 3111.85 403.36 o 9 5 1 21136.96 20772.57 545.83 o 10 5 1 2323.77 2307.10 209.64 o 11 5 1 9043.94 9400.57 571.43 o 12 5 1 1062.87 1389.36 227.82 o 13 5 1 491.56 791.78 149.39 o -13 6 1 5236.02 6222.23 392.16 o -12 6 1 578.31 676.00 171.80 o -11 6 1 8924.46 9579.84 586.37 o -10 6 1 3999.47 3932.78 380.95 o -9 6 1 4612.97 4402.51 246.74 o -8 6 1 3474.94 3121.52 221.38 o -7 6 1 1570.51 1676.94 489.26 o -6 6 1 7199.10 6442.59 806.72 o -4 6 1 15907.52 14542.54 1656.40 o -3 6 1 26742.64 24766.85 1927.17 o -2 6 1 7954.51 8933.94 521.11 o -1 6 1 6411.95 6685.83 291.86 o 0 6 1 3759.89 5085.34 369.75 o 1 6 1 5661.63 5951.98 262.68 o 2 6 1 8232.86 8888.90 690.94 o 3 6 1 21916.65 21456.61 948.65 o 4 6 1 15134.40 15671.36 978.53 o 5 6 1 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