#------------------------------------------------------------------------------ #$Date: 2019-04-26 05:47:55 +0300 (Fri, 26 Apr 2019) $ #$Revision: 214796 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/09/1550945.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1550945 loop_ _publ_author_name 'Peloquin, Andrew J.' 'Smith, Madelyn B.' 'Balaich, Gary J.' 'Iacono, Scott T.' _publ_section_title ; 1,1'-Bis(4-bromophenyl)-3,3'-diphenylferrocene ; _journal_coeditor_code HB4292 _journal_issue 4 _journal_name_full IUCrData _journal_page_first x190487 _journal_paper_doi 10.1107/S2414314619004875 _journal_volume 4 _journal_year 2019 _chemical_formula_iupac '[Fe (C17 H12 Br1)2]' _chemical_formula_moiety 'C34 H24 Br2 Fe' _chemical_formula_sum 'C34 H24 Br2 Fe' _chemical_formula_weight 648.20 _chemical_name_common ; 1,1'-Bis(4-bromophenyl)-3,3'-diphenylferrocene ; _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_Hall 'P 2c -2n' _space_group_name_H-M_alt 'P n a 21' _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 24.2914(17) _cell_length_b 14.3317(10) _cell_length_c 7.5014(5) _cell_measurement_reflns_used 7252 _cell_measurement_temperature 100.(2) _cell_measurement_theta_max 22.8933 _cell_measurement_theta_min 2.1980 _cell_volume 2611.5(3) _computing_cell_refinement ; SAINT (Bruker, 2017) ; _computing_data_collection ; APEX3 (Bruker, 2017) ; _computing_data_reduction ; SAINT (Bruker, 2017) ; _computing_molecular_graphics ; ORTEP-3 for Windows (Farrugia, 2012) and Mercury (Macrae, et al., 2008) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100.(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker SMART APEX CCD' _diffrn_measurement_method \w _diffrn_radiation_monochromator graphite _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0750 _diffrn_reflns_av_unetI/netI 0.0505 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 53974 _diffrn_reflns_theta_full 28.32 _diffrn_reflns_theta_max 28.32 _diffrn_reflns_theta_min 2.20 _diffrn_source 'fine focus sealed tube' _exptl_absorpt_coefficient_mu 3.660 _exptl_absorpt_correction_T_max 0.75 _exptl_absorpt_correction_T_min 0.50 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2017) ; _exptl_crystal_colour 'translucent orange' _exptl_crystal_density_diffrn 1.649 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 1296 _exptl_crystal_size_max 0.19 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.083 _refine_diff_density_max 1.444 _refine_diff_density_min -0.766 _refine_ls_abs_structure_details ; Flack x determined using 2036 quotients [(I^+^)-(I^-^)]/[(I^+^)+(I^-^)] (Parsons et al., 2013) ; _refine_ls_abs_structure_Flack 0.052(6) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.067 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 344 _refine_ls_number_reflns 6454 _refine_ls_number_restraints 6 _refine_ls_restrained_S_all 1.088 _refine_ls_R_factor_all 0.0637 _refine_ls_R_factor_gt 0.0461 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0333P)^2^+3.9647P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0954 _refine_ls_wR_factor_ref 0.1033 _reflns_number_gt 5283 _reflns_number_total 6454 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb4292sup1.cif _cod_data_source_block I _cod_database_code 1550945 _shelx_hkl_file ; 0 0 -1 7.40 1.60 0 0 -1 9.50 2.00 0 0 -1 9.90 1.80 0 0 -3 -3.20 1.50 0 0 -3 5.20 3.80 0 0 -3 -2.50 3.00 0 0 -3 -1.20 1.50 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4.70 -1 2 -1 61.19 6.80 1 -2 -1 53.99 5.80 1 2 1 36.50 5.30 1 -2 1 37.50 5.20 -1 2 1 42.60 5.60 -1 -2 -1 49.80 6.10 -1 2 1 35.20 4.60 1 2 -1 49.20 6.20 -1 -2 -1 65.69 7.40 1 2 -1 54.49 5.50 1 -2 1 40.00 4.20 1 2 -1 38.10 5.60 -1 -2 -1 54.09 4.80 1 2 2 2069.79 118.89 -1 2 -2 1849.42 120.69 1 -2 -2 1994.50 120.79 1 2 2 1985.90 119.39 -1 -2 2 2011.60 117.99 -1 -2 2 1994.50 119.39 1 -2 -2 1856.41 119.69 -1 2 -2 1698.73 118.99 -1 2 -2 1969.70 117.99 1 -2 -2 1920.71 118.29 -1 -2 2 2066.29 118.89 1 2 2 2040.30 119.69 -1 2 -2 1907.61 120.29 1 2 -2 1880.71 119.89 -1 -2 -2 1860.91 118.49 -1 2 2 2028.40 119.39 -1 -2 -2 1977.90 119.69 1 -2 2 2114.89 119.29 1 2 -2 2050.59 118.99 1 2 -2 1918.01 117.89 -1 -2 -2 1821.52 119.49 -1 -2 -2 1930.11 118.79 -1 2 2 2090.89 118.39 -1 -2 -2 1969.00 120.69 1 -2 2 2069.89 118.09 1 2 -2 1954.70 119.39 1 2 -2 1930.41 120.99 -1 2 2 2005.20 118.79 -1 2 -3 154.98 17.10 1 2 3 186.38 15.30 -1 -2 3 187.48 15.10 1 -2 -3 151.38 15.00 -1 2 -3 169.28 13.80 1 -2 -3 165.38 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99.49 23.80 7 8 -7 81.89 27.30 -7 -8 -7 74.29 21.10 7 -8 7 84.19 21.50 7 8 8 2.60 12.60 -7 8 -8 13.30 17.90 7 -8 -8 21.00 13.20 -7 8 -8 4.50 22.30 -7 -8 8 18.80 13.50 7 -8 -8 -2.60 18.60 7 -8 -8 -6.10 15.80 -7 8 -8 -8.40 11.40 7 8 8 12.10 13.30 -7 8 8 16.00 17.10 7 -8 8 -0.70 14.20 7 8 -8 -1.10 18.80 -7 -8 -8 8.20 17.60 -7 -8 -8 16.10 10.30 7 8 -8 2.30 11.30 7 -9 0 22.90 10.00 7 9 0 35.60 10.10 -7 9 0 38.40 7.80 -7 9 0 28.30 8.80 -7 9 0 52.89 13.70 -7 9 0 36.00 9.90 -7 -9 0 37.40 10.90 -7 -9 0 30.80 11.30 -7 -9 0 32.60 8.50 7 9 0 36.20 12.70 7 -9 0 30.50 6.80 7 -9 0 27.70 8.20 7 -9 0 50.19 12.50 -7 9 -1 322.17 23.80 -7 -9 1 313.97 29.20 -7 -9 1 286.47 27.60 -7 9 -1 332.47 28.00 7 -9 -1 285.77 26.80 -7 9 -1 305.47 25.60 7 9 1 283.67 25.90 7 9 1 326.47 35.70 7 9 1 281.67 30.20 7 -9 -1 336.67 26.80 -7 9 -1 289.97 31.30 7 -9 -1 314.47 26.50 7 -9 -1 282.17 30.30 7 -9 1 257.77 24.10 -7 9 1 278.77 31.40 7 9 -1 306.37 28.20 -7 9 1 259.57 25.30 -7 -9 -1 280.67 27.20 7 -9 1 312.77 28.40 -7 -9 -1 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8 62.19 17.30 -10 2 -8 44.30 20.60 10 2 -8 86.39 21.70 10 -2 8 62.99 19.70 -10 2 8 52.09 16.30 -10 2 8 35.30 16.00 10 2 -8 10.40 9.70 -10 -2 -8 76.69 21.60 10 2 9 13.30 13.70 -10 2 -9 29.90 17.90 10 2 9 5.10 13.20 -10 2 -9 15.70 17.90 10 -2 -9 16.40 14.10 -10 -2 9 7.20 13.90 10 2 9 20.90 11.80 -10 -2 9 3.50 13.10 10 2 -9 39.30 18.90 10 -2 9 32.10 16.10 -10 2 9 14.50 14.90 -10 -2 -9 1.00 15.60 -10 2 9 31.50 16.30 -10 3 0 1127.39 71.49 10 3 0 1135.99 73.99 10 -3 0 1118.39 70.99 10 3 0 1135.59 69.99 -10 -3 0 1111.89 70.29 -10 -3 0 1062.59 72.39 -10 -3 0 1148.29 73.19 -10 3 0 1134.99 70.39 -10 -3 0 1170.58 70.19 -10 3 0 1148.09 70.19 10 -3 0 1101.29 71.69 10 -3 0 1138.09 73.39 10 3 0 1141.59 71.09 10 -3 0 1130.39 70.29 -10 3 0 1114.49 72.89 -10 3 -1 16.20 5.60 10 -3 -1 29.00 6.80 -10 -3 1 22.50 6.70 -10 3 -1 17.10 3.90 -10 -3 1 32.70 8.00 10 3 1 35.20 8.20 -10 -3 1 35.50 6.50 -10 3 -1 11.20 4.60 10 -3 -1 24.70 5.90 -10 3 -1 15.10 6.00 10 -3 -1 21.00 6.70 10 -3 -1 26.90 6.40 10 3 1 40.70 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481.75 30.40 -10 -3 3 439.26 34.00 10 3 3 439.56 34.80 -10 -3 3 484.05 35.10 10 -3 3 464.15 31.00 10 3 -3 428.26 33.00 -10 3 3 444.06 35.00 -10 -3 -3 445.76 34.20 10 3 -3 450.95 37.60 10 3 -3 449.46 34.40 -10 -3 -3 379.26 34.00 10 -3 3 468.85 35.50 -10 3 3 485.45 32.40 -10 -3 -3 433.96 36.10 -10 -3 4 215.68 23.10 10 -3 -4 170.88 22.20 -10 3 -4 158.58 19.90 -10 3 -4 163.68 24.40 10 3 4 202.58 22.80 -10 3 -4 154.48 21.70 -10 -3 4 194.18 18.30 -10 -3 4 172.48 21.20 10 -3 -4 181.68 22.10 10 3 4 224.28 23.40 10 -3 -4 173.88 16.80 10 -3 -4 168.28 21.30 -10 3 -4 142.39 22.40 10 3 -4 179.68 21.90 -10 3 4 193.38 17.10 10 3 -4 149.79 23.40 -10 -3 -4 177.08 20.50 -10 -3 -4 187.58 25.30 -10 -3 -4 189.98 22.90 10 3 -4 185.78 18.10 10 -3 4 198.08 23.70 -10 3 4 256.17 26.60 10 -3 4 238.68 18.10 10 -3 -5 249.88 27.20 -10 -3 5 221.58 27.20 -10 -3 5 235.08 24.70 -10 3 -5 230.48 30.10 -10 3 -5 221.68 28.40 -10 3 -5 253.27 23.80 -10 -3 5 251.17 27.10 10 3 5 218.18 26.90 10 -3 -5 221.98 27.10 10 3 5 241.38 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349.47 26.40 -10 4 -1 362.86 28.30 -10 4 -1 360.26 27.30 -10 4 -1 349.67 28.00 -10 -4 -1 349.17 27.10 10 4 -1 349.17 30.20 -10 -4 -1 342.17 29.20 -10 4 1 421.16 30.00 -10 -4 -1 371.06 26.10 10 -4 1 402.86 24.60 -10 4 1 437.06 28.30 10 -4 1 417.36 27.40 -10 -4 -1 355.76 29.50 10 4 -1 335.77 25.30 10 -4 1 421.76 30.60 -10 4 1 394.76 24.40 10 4 -1 374.26 30.30 10 -4 -2 134.89 13.00 10 4 2 126.09 10.90 -10 -4 2 153.88 16.70 10 -4 -2 161.68 17.80 10 -4 -2 153.48 16.90 -10 4 -2 133.29 17.10 10 -4 -2 162.98 18.80 -10 -4 2 128.59 16.10 -10 4 -2 147.19 16.70 10 4 2 144.99 18.20 -10 4 -2 181.78 19.70 10 4 2 144.99 16.30 10 4 2 113.49 16.10 -10 -4 2 172.88 19.30 -10 4 2 139.29 18.60 10 4 -2 182.58 20.60 10 -4 2 123.69 16.80 -10 -4 -2 133.09 11.30 10 4 -2 163.18 10.50 10 4 -2 144.79 19.90 10 4 -2 173.48 17.70 10 -4 2 157.78 13.90 -10 4 2 156.78 17.00 -10 -4 -2 150.38 17.60 -10 -4 -2 160.18 19.90 -10 4 -3 359.86 29.20 -10 -4 3 299.07 25.60 -10 -4 3 300.37 27.40 -10 -4 3 314.47 27.70 -10 4 -3 373.46 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438.96 34.40 -10 -5 5 386.56 34.00 10 -5 -5 395.26 34.90 10 5 -5 388.76 42.50 -10 -5 -5 329.37 32.90 -10 -5 -5 336.07 37.00 10 5 -5 371.96 33.30 10 -5 5 370.86 39.10 -10 5 5 457.05 38.10 -10 -5 -5 419.46 43.40 10 5 6 168.28 24.60 10 -5 -6 182.98 27.60 10 5 6 143.79 24.20 10 -5 -6 143.29 25.40 10 -5 -6 183.18 25.30 10 5 6 182.68 23.70 -10 5 -6 146.49 24.90 -10 -5 6 142.19 23.10 -10 5 -6 98.99 24.50 -10 5 -6 127.59 26.50 -10 -5 6 167.68 23.70 -10 -5 -6 163.08 28.30 -10 -5 -6 155.68 22.40 10 -5 6 206.18 28.20 10 5 -6 125.89 22.40 10 5 -6 194.68 31.10 -10 -5 -6 149.69 25.30 -10 5 6 173.18 26.30 10 5 7 107.99 22.50 -10 -5 7 95.49 21.10 -10 5 -7 126.89 24.90 -10 -5 7 114.49 21.10 10 -5 -7 72.09 21.70 10 5 7 90.89 20.20 10 -5 -7 98.69 20.80 10 5 7 116.29 20.10 -10 5 -7 108.89 26.00 -10 5 -7 100.89 24.90 10 -5 -7 109.99 23.40 10 -5 7 98.49 22.50 -10 -5 -7 127.99 24.00 -10 -5 -7 69.69 20.30 10 5 -7 104.99 26.10 -10 5 7 75.59 19.50 -10 5 -8 50.99 22.70 -10 5 -8 52.89 16.90 10 -5 -8 91.69 26.60 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189.78 22.90 -10 8 3 190.58 26.20 -10 8 3 180.48 23.70 -10 -8 4 64.39 15.00 10 -8 -4 72.69 16.90 10 8 4 47.20 14.30 10 8 4 67.79 13.90 -10 8 -4 58.89 17.00 -10 8 -4 57.79 16.30 -10 -8 4 56.39 15.90 10 -8 -4 49.20 15.70 10 8 4 72.79 16.00 10 -8 -4 82.99 15.70 10 -8 -4 45.10 14.30 -10 8 -4 63.69 17.80 -10 8 4 74.49 15.10 10 8 -4 76.89 17.00 10 -8 4 57.39 13.10 -10 -8 -4 66.29 18.30 -10 8 4 81.69 17.90 10 -8 4 63.39 16.50 10 8 -4 64.29 19.20 -10 -8 -4 79.19 18.50 10 -8 -5 16.60 11.90 -10 -8 5 27.30 13.70 -10 8 -5 7.50 15.70 10 8 5 30.90 13.70 -10 8 -5 25.50 17.10 -10 8 -5 6.60 12.60 10 -8 -5 -17.50 11.10 10 -8 -5 11.30 12.80 10 -8 -5 33.10 13.30 -10 -8 5 28.90 12.80 10 8 5 20.50 12.50 10 8 -5 -10.70 13.30 10 8 -5 4.50 7.80 -10 8 5 31.90 14.30 -10 -8 -5 37.60 13.90 10 -8 5 13.30 13.80 -10 8 5 23.70 10.40 10 -8 5 29.40 14.30 -10 -8 -5 6.10 15.10 10 -8 -6 90.59 20.50 10 -8 -6 85.89 22.20 10 -8 -6 124.39 24.90 -10 -8 6 138.19 21.80 -10 8 -6 154.48 30.00 -10 8 -6 107.19 24.90 10 8 6 129.69 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10.60 -10 -14 -5 29.00 18.40 10 -14 5 10.80 12.00 -10 -14 -5 -18.90 14.20 -10 -14 6 -1.50 14.10 10 14 6 26.20 14.20 -10 14 -6 6.00 13.10 10 -14 -6 20.90 15.60 10 -14 -6 -9.40 14.40 -10 14 -6 -8.50 16.30 10 14 6 19.10 12.70 -10 14 -6 14.20 16.20 10 14 -6 5.10 11.80 -10 14 6 21.90 14.70 10 -14 6 15.20 12.50 10 14 -6 11.20 19.20 -10 14 6 6.50 12.60 -10 -14 -6 -34.60 11.40 -10 -14 -6 -7.90 14.30 -10 -15 0 16.70 13.80 -10 15 0 -14.70 11.80 10 15 0 8.50 6.90 -10 -15 0 -17.60 12.80 10 -15 0 -6.70 5.90 10 -15 0 -1.80 12.40 10 15 0 -12.70 11.80 10 -15 -1 128.69 26.20 -10 -15 1 174.08 28.50 -10 -15 1 146.09 29.30 -10 15 -1 108.99 26.90 -10 15 -1 139.19 25.70 10 15 1 145.69 30.10 10 15 1 153.28 26.90 -10 -15 -1 148.19 30.00 -10 15 1 107.89 25.40 10 -15 1 132.99 25.00 10 -15 1 180.98 29.10 10 15 -1 211.68 35.30 10 15 -1 199.08 30.80 -10 -15 2 26.70 14.70 -10 -15 2 -1.50 15.30 10 -15 -2 9.80 14.20 -10 15 -2 34.60 18.20 -10 15 -2 34.50 15.10 10 15 2 13.50 11.30 10 -15 -2 39.00 17.20 10 15 2 15.50 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1789.52 121.19 -11 3 0 1991.40 118.49 -11 3 0 1970.20 118.99 -11 -3 0 1895.21 121.69 11 -3 0 1913.21 120.59 -11 3 0 1985.50 119.99 11 3 0 1905.81 118.29 -11 -3 0 1922.81 121.29 -11 -3 0 2029.90 118.59 11 -3 0 1965.30 122.39 11 3 0 1892.51 119.49 11 3 0 1962.90 122.79 -11 -3 1 288.87 21.50 -11 3 -1 261.87 21.30 11 -3 -1 284.17 17.90 -11 3 -1 286.27 22.30 -11 -3 1 223.88 22.00 11 -3 -1 258.27 21.50 -11 -3 1 288.07 22.90 11 -3 -1 266.97 23.20 -11 3 -1 258.07 18.90 11 3 1 297.37 23.20 11 -3 -1 243.98 21.40 11 3 1 294.87 24.00 11 3 1 283.87 20.20 11 -3 -1 280.27 21.70 11 3 -1 270.27 18.40 11 -3 1 280.97 23.70 -11 -3 -1 273.47 23.70 -11 -3 -1 263.47 21.10 -11 3 1 312.57 21.30 11 -3 1 267.47 22.40 11 -3 1 279.37 20.20 11 3 -1 264.77 24.70 11 3 -1 270.57 23.30 11 3 -1 258.27 21.80 -11 -3 -1 281.97 19.30 11 3 -1 276.17 21.50 -11 3 1 278.77 23.30 -11 -3 2 459.35 33.50 11 3 2 489.85 35.00 11 -3 -2 424.66 33.00 11 3 2 453.55 34.70 -11 -3 2 462.35 33.90 11 3 2 462.55 30.60 11 -3 -2 469.65 33.80 11 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56.29 14.20 -11 -12 -3 -0.90 13.70 -11 12 3 40.40 16.90 -11 -12 -3 30.40 16.80 11 12 -3 -2.20 13.40 11 -12 3 10.50 11.90 11 12 -3 20.80 15.10 -11 -12 4 15.90 14.20 11 12 4 8.10 12.60 11 -12 -4 32.30 16.40 11 -12 -4 15.30 14.40 -11 12 -4 15.30 15.50 -11 -12 4 12.60 14.70 11 -12 -4 24.90 16.30 -11 12 -4 12.20 13.60 11 12 4 4.40 11.60 -11 12 -4 20.10 14.50 11 12 -4 12.40 16.00 11 -12 4 5.60 12.30 -11 12 4 26.30 13.60 11 12 -4 2.40 14.30 -11 12 4 7.30 12.20 11 -12 4 4.60 10.90 -11 -12 -4 5.10 14.10 11 -12 -5 19.10 16.60 11 12 5 29.80 14.60 -11 12 -5 21.20 16.70 11 -12 -5 13.90 14.40 -11 -12 5 23.90 16.50 -11 12 -5 42.20 18.60 11 -12 -5 24.60 17.50 11 12 5 42.40 16.70 -11 12 -5 16.10 15.10 -11 -12 5 29.70 16.10 -11 12 5 22.70 13.80 11 -12 5 -1.80 11.50 11 -12 5 35.60 15.00 11 12 -5 15.80 17.10 -11 12 5 22.80 16.20 11 12 -5 9.70 14.70 -11 -12 -5 59.69 20.40 -11 -12 -5 11.00 16.60 -11 12 -6 9.00 16.40 11 12 6 34.80 18.10 11 -12 -6 14.00 14.60 11 -12 -6 40.40 20.20 -11 -12 6 17.60 13.30 -11 12 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2 50.89 19.20 -11 -13 -2 85.09 23.50 -11 -13 -2 36.80 16.80 11 -13 2 67.39 18.20 11 13 -2 72.19 20.50 11 13 -2 64.99 22.50 -11 13 2 68.59 19.60 -11 13 2 37.50 13.90 -11 -13 3 87.89 20.40 11 13 3 64.79 21.30 -11 -13 3 76.49 21.90 11 13 3 52.59 18.00 11 -13 -3 75.49 19.80 -11 13 -3 54.89 17.60 -11 13 -3 70.29 22.40 11 -13 -3 50.89 19.50 -11 -13 -3 62.79 20.50 11 13 -3 73.59 24.40 -11 13 3 58.09 18.70 11 -13 3 68.29 18.00 -11 13 3 82.39 20.10 -11 -13 -3 54.49 19.80 11 13 -3 126.99 27.00 11 -13 -4 44.10 18.20 11 -13 -4 33.80 17.20 -11 13 -4 34.00 15.20 -11 -13 4 45.90 17.80 -11 13 -4 40.20 18.40 11 13 4 52.69 19.00 -11 13 -4 51.19 20.70 11 13 4 51.59 17.30 -11 -13 4 53.29 19.40 11 -13 4 44.70 15.20 11 13 -4 23.60 18.70 -11 13 4 52.79 18.10 -11 13 4 48.20 17.20 -11 -13 -4 28.00 17.80 -11 -13 -4 44.60 22.20 11 13 -4 51.59 21.50 11 -13 -5 34.50 18.30 11 -13 -5 21.80 14.80 -11 13 -5 21.00 17.10 11 -13 -5 43.10 19.30 -11 -13 5 34.10 16.90 11 13 5 49.99 18.20 -11 13 -5 20.10 17.80 -11 -13 5 48.40 19.70 -11 13 -5 14.90 15.90 11 13 5 43.50 17.60 11 13 -5 11.90 15.80 11 13 -5 44.80 20.70 -11 -13 -5 35.20 22.00 11 -13 5 48.70 15.40 11 -13 5 82.09 20.70 -11 13 5 34.10 15.80 -11 13 5 59.89 19.40 -11 -13 -5 52.79 21.30 11 13 6 33.00 15.80 -11 13 -6 23.10 14.40 -11 13 -6 -1.50 15.00 -11 -13 6 35.50 16.10 11 -13 -6 -25.70 11.50 -11 13 -6 5.40 18.40 11 13 6 50.79 18.80 11 -13 -6 12.10 11.10 11 -13 -6 -2.70 13.70 -11 13 6 11.20 11.10 11 -13 6 -2.50 12.00 11 13 -6 -12.40 12.50 -11 -13 -6 12.50 16.80 11 13 -6 45.00 23.30 -11 -13 -6 26.30 19.80 -11 13 6 -1.00 14.90 11 14 0 58.29 16.80 -11 -14 0 54.89 16.90 -11 14 0 76.49 21.60 11 -14 0 40.90 15.10 11 14 0 70.09 17.30 -11 -14 0 56.09 21.70 11 14 0 68.89 23.60 -11 -14 1 102.89 21.70 11 -14 -1 75.59 19.80 -11 14 -1 119.29 21.60 -11 -14 1 115.09 26.10 11 14 1 127.39 24.40 -11 14 -1 72.39 23.80 11 -14 -1 94.79 22.40 11 -14 1 91.49 21.00 -11 14 1 102.79 24.30 11 -14 1 98.49 22.30 -11 -14 -1 112.49 26.90 11 14 -1 86.29 25.20 -11 -14 -1 112.39 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103.49 26.90 -11 -16 0 93.09 21.00 -11 16 0 67.89 22.30 11 -16 0 55.39 20.40 -11 -16 0 93.09 26.40 -11 -16 1 124.59 24.90 11 -16 -1 81.79 23.20 -11 -16 1 109.99 27.40 -11 16 -1 106.89 26.70 11 16 1 126.79 23.50 11 16 1 147.79 31.90 11 16 -1 91.59 26.10 -11 -16 -1 158.48 31.10 11 -16 1 86.09 23.20 11 -16 1 97.89 21.40 -11 16 1 97.09 25.30 11 -16 -2 58.69 20.20 11 16 2 57.39 21.60 -11 16 -2 56.19 21.30 -11 -16 2 43.80 20.10 -11 16 -2 66.19 19.40 -11 -16 2 55.29 20.20 11 16 2 73.69 19.50 11 -16 2 59.69 19.10 -11 -16 -2 80.19 23.70 11 16 -2 68.79 20.00 11 16 -2 84.59 26.40 11 -16 2 42.70 17.40 -11 16 2 73.49 22.60 11 16 3 106.99 26.50 -11 -16 3 60.89 21.60 11 -16 -3 99.49 21.90 -11 16 -3 47.30 22.50 -11 -16 3 111.69 28.30 -11 16 -3 48.10 19.80 11 16 3 76.69 20.40 11 -16 -3 64.59 21.20 11 16 -3 56.59 21.30 11 -16 3 50.19 18.70 -11 -16 -3 68.39 20.10 11 16 -3 100.99 28.40 -11 16 3 83.69 23.40 -11 -16 -3 90.59 25.30 -11 16 -4 30.90 16.50 11 -16 -4 47.90 18.90 11 16 4 60.19 20.80 -11 -16 4 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19.50 12.50 12 -8 -5 22.50 13.70 -12 -8 -5 14.60 14.40 12 8 -5 44.20 19.50 12 8 -5 33.10 14.20 -12 8 5 26.90 12.00 -12 -8 -5 35.90 15.60 12 -8 5 35.70 14.90 -12 8 5 4.70 13.80 -12 8 -6 -10.90 16.40 -12 8 -6 16.90 16.50 12 -8 -6 9.70 14.80 -12 -8 6 8.80 13.40 12 -8 -6 1.50 11.70 12 8 6 -4.40 10.70 -12 -8 6 7.90 12.60 12 8 6 3.10 12.30 -12 8 -6 15.90 14.40 -12 -8 -6 -12.70 13.90 12 -8 6 33.40 17.30 12 8 -6 -12.80 17.20 12 8 -6 32.10 15.30 -12 8 6 5.70 15.20 -12 -8 -6 2.90 7.00 -12 -8 7 20.20 14.70 12 8 7 15.30 13.00 12 8 7 12.60 14.10 -12 8 -7 46.30 26.20 12 -8 -7 20.80 15.70 -12 -8 7 2.80 12.60 -12 8 -7 8.80 15.40 12 -8 -7 29.80 19.30 -12 8 -7 -0.30 15.80 12 -8 7 8.80 15.20 12 8 -7 -41.40 14.30 -12 -8 -7 1.90 17.10 -12 8 7 12.20 13.60 12 8 8 -3.50 10.20 12 8 8 -1.00 11.90 -12 8 -8 14.40 18.80 -12 8 -8 13.30 12.70 12 -8 -8 -5.80 10.80 12 -8 -8 27.90 15.90 -12 8 -8 20.40 21.30 -12 -8 8 16.90 14.60 -12 8 8 14.60 15.50 12 8 -8 17.70 18.70 -12 -8 -8 3.40 16.70 12 -8 8 4.60 13.60 12 -9 0 112.19 15.00 12 -9 0 100.79 18.90 12 9 0 114.49 22.70 -12 -9 0 98.59 17.00 -12 -9 0 125.89 21.60 -12 -9 0 113.09 18.20 -12 9 0 85.59 15.60 12 9 0 116.59 20.10 -12 9 0 113.29 20.00 12 9 0 95.39 16.20 -12 9 0 110.89 16.50 12 -9 0 95.49 16.60 12 9 1 241.98 27.30 12 -9 -1 247.78 30.40 12 -9 -1 262.07 24.00 -12 -9 1 193.28 26.00 -12 9 -1 227.98 25.30 12 -9 -1 224.58 26.90 -12 -9 1 194.18 27.40 -12 9 -1 182.78 27.30 12 9 1 237.48 31.70 12 9 1 276.67 30.70 -12 9 -1 217.68 25.60 -12 -9 1 242.08 23.00 12 9 -1 284.07 35.60 12 -9 1 228.78 26.90 -12 9 1 286.87 31.80 -12 -9 -1 194.28 28.40 12 -9 1 238.08 22.40 -12 -9 -1 248.78 28.00 12 9 -1 219.78 29.00 12 -9 1 256.87 30.70 -12 -9 -1 254.07 28.70 12 9 -1 272.07 23.80 -12 9 -2 49.99 14.70 -12 9 -2 45.40 13.60 12 9 2 39.00 12.40 -12 -9 2 48.60 11.20 12 -9 -2 44.20 13.70 12 9 2 42.40 11.90 12 -9 -2 40.90 12.60 -12 -9 2 55.49 14.30 -12 9 -2 30.30 11.80 12 -9 -2 45.00 12.50 12 9 2 81.89 18.30 -12 -9 2 62.69 15.90 -12 9 2 39.20 12.40 -12 -9 -2 60.39 17.80 12 9 -2 38.60 16.00 12 -9 2 52.19 13.70 -12 -9 -2 48.00 15.00 -12 9 2 21.60 11.40 12 -9 2 44.90 12.00 12 9 -2 35.10 14.30 12 -9 -3 94.19 19.20 12 9 3 120.59 18.90 12 9 3 91.19 17.80 -12 -9 3 91.49 17.50 -12 9 -3 86.19 17.70 -12 9 -3 95.69 20.50 12 -9 -3 123.79 19.80 -12 -9 3 83.99 18.50 12 9 3 94.19 19.90 -12 9 -3 46.30 14.10 12 9 -3 95.79 21.20 12 -9 3 104.69 17.90 12 9 -3 104.19 23.10 -12 -9 -3 123.99 22.70 12 -9 3 58.19 13.40 -12 9 3 99.29 18.20 -12 9 3 90.59 18.40 -12 -9 -3 88.29 20.90 12 -9 -4 46.20 15.40 -12 9 -4 31.60 15.40 -12 9 -4 34.80 14.80 12 -9 -4 28.80 14.30 -12 9 -4 49.30 16.90 12 9 4 39.40 12.40 12 9 4 51.19 15.80 12 -9 -4 69.49 15.40 -12 -9 4 39.30 15.10 -12 -9 4 55.79 15.90 12 9 4 50.79 15.00 12 9 -4 40.80 18.00 -12 -9 -4 39.20 15.50 12 9 -4 20.20 13.60 -12 9 4 42.60 12.50 12 -9 4 26.10 10.50 12 -9 4 34.70 14.60 -12 9 4 19.80 13.60 -12 -9 -4 10.60 14.70 -12 9 -5 168.08 29.50 -12 -9 5 156.08 25.70 -12 9 -5 155.58 27.00 -12 -9 5 165.38 25.70 -12 9 -5 153.08 27.40 12 -9 -5 190.18 26.70 12 9 5 128.39 24.70 12 -9 -5 137.89 23.50 12 9 5 137.79 23.70 12 -9 -5 155.38 27.00 -12 9 5 150.88 22.80 -12 -9 -5 108.59 25.70 -12 -9 -5 135.39 26.30 12 9 -5 153.38 32.70 12 -9 5 94.09 22.50 -12 9 5 150.78 27.70 12 -9 -6 41.10 16.20 -12 9 -6 48.70 20.00 -12 9 -6 50.69 22.50 12 9 6 29.20 14.40 -12 -9 6 42.10 16.70 12 9 6 48.50 16.30 -12 -9 6 68.79 19.40 12 -9 -6 29.60 17.20 -12 9 -6 60.89 21.20 -12 9 6 34.50 17.80 12 9 -6 93.89 19.90 12 9 -6 64.79 23.30 -12 -9 -6 11.30 18.30 12 -9 6 43.70 17.90 -12 -9 -6 47.50 18.60 -12 9 -7 56.39 24.20 12 -9 -7 39.90 20.80 12 9 7 91.39 21.50 -12 9 -7 42.00 19.20 -12 9 -7 80.39 27.80 -12 -9 7 35.60 17.00 12 -9 -7 57.89 19.50 12 9 7 91.99 22.40 -12 -9 7 56.29 18.40 -12 9 7 80.89 25.30 -12 -9 -7 59.99 21.60 12 -9 7 32.80 18.50 12 9 -7 41.30 21.30 -12 9 -8 21.80 14.30 -12 -9 -8 -16.40 12.00 12 -10 0 117.79 19.60 -12 10 0 114.99 21.00 12 10 0 124.69 19.60 -12 -10 0 141.69 21.40 12 -10 0 144.49 20.00 -12 -10 0 92.89 18.00 12 -10 0 150.88 23.30 -12 -10 0 135.49 23.90 -12 10 0 137.99 19.80 12 10 0 120.69 22.00 12 10 0 100.09 22.80 -12 10 0 163.98 21.50 12 -10 -1 33.10 13.50 12 10 1 57.69 15.00 12 10 1 57.69 13.70 12 -10 -1 53.59 14.70 12 -10 -1 63.19 12.70 -12 -10 1 55.59 14.10 -12 -10 1 31.60 13.40 -12 10 -1 37.40 12.90 -12 10 -1 69.19 18.10 -12 -10 1 61.19 12.50 12 10 1 48.00 16.80 12 -10 1 51.59 14.00 -12 -10 -1 32.70 13.40 -12 10 1 53.19 15.10 -12 -10 -1 54.89 17.00 12 -10 1 44.90 15.00 -12 10 1 54.89 14.00 12 10 -1 67.79 16.80 -12 -10 -1 51.39 12.70 12 10 -1 68.59 19.70 12 -10 -2 15.90 9.60 12 10 2 21.70 12.20 12 -10 -2 25.90 11.30 -12 10 -2 14.20 12.20 12 10 2 5.50 8.70 -12 10 -2 6.60 10.40 12 10 2 13.30 9.50 12 -10 -2 0.00 9.40 -12 -10 2 -6.90 7.80 -12 10 -2 14.30 10.50 -12 -10 2 15.60 10.90 12 -10 2 6.00 9.80 12 10 -2 -0.60 12.50 -12 -10 -2 14.60 12.20 -12 10 2 7.70 8.30 -12 -10 -2 5.30 12.50 -12 10 2 12.00 11.00 12 10 -2 7.20 10.10 12 -10 2 15.10 9.20 -12 -10 3 43.20 16.60 12 10 3 22.80 9.80 12 -10 -3 16.70 12.10 -12 10 -3 23.30 14.30 12 -10 -3 4.10 10.50 -12 10 -3 8.90 11.00 -12 -10 3 41.30 14.20 12 10 3 9.60 11.50 12 -10 -3 13.30 10.50 -12 10 -3 28.10 12.10 12 10 3 16.00 10.00 -12 -10 -3 21.90 13.90 -12 10 3 42.90 14.30 -12 -10 -3 40.60 17.00 12 10 -3 19.30 15.10 12 10 -3 6.70 13.20 -12 10 3 29.60 13.00 12 -10 3 20.80 9.20 12 -10 3 15.80 11.00 -12 10 -4 96.29 21.30 12 -10 -4 69.69 17.10 -12 -10 4 61.59 18.00 -12 10 -4 56.19 18.90 12 10 4 72.99 18.10 -12 10 -4 37.70 17.00 12 -10 -4 70.09 18.80 12 10 4 71.29 18.60 -12 -10 4 81.39 19.30 12 -10 -4 67.99 17.80 -12 -10 -4 89.09 22.20 12 10 -4 80.09 23.00 -12 -10 -4 43.10 18.00 12 -10 4 64.79 16.90 12 10 -4 23.40 17.10 -12 10 4 69.09 19.10 -12 10 4 60.39 16.40 12 -10 4 79.19 17.10 -12 10 -5 21.50 16.00 -12 10 -5 29.30 15.60 -12 -10 5 29.90 15.80 12 10 5 10.90 11.90 12 -10 -5 11.50 13.20 -12 10 -5 17.20 16.40 -12 -10 5 27.20 15.50 12 10 -5 32.60 18.20 12 10 -5 34.00 14.40 12 -10 5 50.09 17.20 -12 -10 -5 28.20 17.00 -12 -10 -5 11.60 15.50 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81.59 18.20 12 -11 -1 95.29 19.20 -12 11 -1 77.09 20.10 12 11 1 90.29 21.80 12 11 1 93.39 17.60 12 11 -1 89.99 22.60 -12 11 1 83.39 17.50 -12 -11 -1 112.99 19.40 -12 -11 -1 98.59 22.20 -12 -11 -1 77.49 17.40 12 -11 1 107.59 19.70 12 -11 1 83.09 19.30 -12 11 1 78.99 19.50 12 11 -1 95.49 19.80 -12 11 -2 276.47 32.90 -12 11 -2 282.97 33.50 -12 -11 2 218.38 32.10 -12 -11 2 268.37 34.10 -12 11 -2 308.17 37.70 12 11 2 300.67 38.00 12 -11 -2 311.07 32.30 12 -11 -2 233.68 31.50 12 11 2 269.17 32.30 12 11 2 280.87 32.70 -12 11 2 241.38 31.00 12 -11 2 207.48 29.40 12 -11 2 231.98 34.40 -12 -11 -2 279.07 34.60 12 11 -2 329.77 42.60 12 11 -2 314.47 37.30 -12 -11 -2 319.07 40.10 12 11 3 69.79 19.60 -12 11 -3 100.49 20.20 -12 11 -3 51.59 18.80 12 -11 -3 54.69 17.50 -12 -11 3 75.89 18.60 12 11 3 88.19 20.80 -12 -11 3 83.59 20.70 -12 11 -3 69.49 19.10 12 -11 -3 51.49 14.30 12 -11 -3 67.79 18.30 -12 11 3 93.89 20.60 -12 -11 -3 60.69 20.90 12 -11 3 78.69 17.50 -12 11 3 104.79 21.50 12 11 -3 80.89 21.90 12 -11 3 67.09 16.20 -12 -11 -3 61.19 19.90 12 -11 -4 90.29 20.30 12 11 4 85.09 19.20 -12 11 -4 98.49 22.70 12 11 4 63.29 19.70 -12 11 -4 53.09 18.30 12 -11 -4 80.99 21.00 -12 11 -4 68.99 20.50 -12 -11 4 80.19 19.80 -12 -11 4 83.39 20.30 -12 11 4 73.79 20.00 12 -11 4 48.40 17.00 12 -11 4 82.69 18.50 12 11 -4 96.19 24.80 -12 -11 -4 70.49 22.80 -12 11 4 80.59 19.60 -12 -11 -4 111.19 24.80 12 11 -4 112.89 27.50 12 11 5 8.80 13.10 -12 11 -5 2.60 15.40 12 -11 -5 9.40 14.00 -12 -11 5 1.40 12.30 12 11 5 14.80 12.70 -12 11 -5 -2.00 14.40 12 -11 -5 28.00 15.90 -12 11 -5 16.50 16.60 -12 -11 5 4.20 15.20 12 11 -5 2.00 13.20 12 11 -5 -5.70 16.90 -12 11 5 -2.60 13.40 -12 11 5 12.70 11.30 -12 -11 -5 33.00 16.80 12 -11 5 22.40 13.90 -12 -11 -5 -12.90 13.40 12 11 6 66.89 21.80 -12 -11 6 40.00 18.70 -12 11 -6 25.80 19.80 12 -11 -6 63.79 18.90 -12 -11 6 77.09 21.10 -12 11 -6 25.40 16.40 -12 11 -6 5.60 18.20 12 11 6 35.20 16.60 12 -11 -6 20.20 18.70 12 -11 6 25.50 15.60 -12 -11 -6 59.09 20.50 -12 11 6 23.30 17.00 12 11 -6 46.80 22.20 -12 -11 -6 18.70 20.60 12 11 -6 20.50 14.80 12 11 7 19.30 15.10 -12 11 -7 32.00 23.30 -12 11 -7 13.50 12.50 12 -11 -7 9.80 15.80 12 11 7 8.50 13.30 -12 11 -7 14.50 17.00 -12 -11 7 1.20 12.20 12 -11 -7 6.90 11.80 12 -11 7 17.60 12.60 -12 -11 -7 -3.60 16.90 12 11 -7 9.40 17.50 -12 11 7 2.80 14.80 -12 -11 -7 -2.70 13.10 -12 -12 0 87.79 19.70 -12 -12 0 67.49 20.70 -12 12 0 69.09 18.90 12 -12 0 72.09 17.80 12 12 0 62.59 16.00 -12 -12 0 90.69 17.00 12 12 0 74.69 16.90 12 12 0 59.69 19.50 12 -12 0 55.89 17.30 -12 -12 1 72.49 20.40 -12 12 -1 91.09 17.90 12 12 1 56.49 20.60 12 -12 -1 65.79 14.90 12 12 1 106.89 19.60 -12 -12 1 86.89 19.70 12 -12 -1 73.69 18.40 12 -12 -1 74.49 18.10 -12 12 -1 64.49 17.20 -12 12 1 67.39 19.10 -12 -12 -1 86.29 18.60 12 -12 1 85.79 19.50 -12 12 1 68.99 16.30 12 -12 1 72.79 19.80 12 12 -1 62.59 17.30 12 12 -1 35.40 17.60 -12 -12 -1 40.00 15.30 -12 -12 -1 83.29 23.00 -12 12 -2 74.19 17.90 12 -12 -2 100.69 19.10 12 -12 -2 104.69 21.20 12 12 2 62.89 20.00 12 -12 -2 88.79 19.70 12 12 2 74.69 16.80 12 12 2 69.29 18.40 -12 -12 2 98.99 22.00 -12 12 -2 78.19 20.50 -12 -12 -2 77.49 21.90 -12 12 2 105.29 22.30 -12 -12 -2 61.39 18.60 12 -12 2 86.49 19.90 12 12 -2 66.39 19.90 12 12 -2 126.69 26.80 -12 12 -3 90.99 19.20 12 -12 -3 110.09 20.30 -12 -12 3 83.69 20.00 12 12 3 92.59 22.60 -12 12 -3 82.59 20.00 12 -12 -3 123.29 23.60 12 -12 -3 113.79 22.50 -12 -12 3 100.09 22.60 -12 12 -3 98.19 23.20 12 12 3 107.19 23.20 -12 -12 -3 84.49 22.70 12 12 -3 128.79 27.40 -12 -12 -3 110.09 25.60 12 -12 3 99.89 20.60 12 -12 3 133.99 21.40 -12 12 3 119.19 22.30 12 12 -3 96.49 25.10 -12 12 3 77.29 20.50 -12 -12 4 124.49 25.70 12 -12 -4 104.99 22.60 -12 -12 4 106.29 23.80 -12 12 -4 94.19 23.10 12 -12 -4 83.99 21.60 12 12 4 130.39 24.90 12 12 4 128.89 24.40 -12 12 -4 64.79 19.70 -12 12 -4 109.69 26.10 12 12 -4 116.49 28.60 -12 -12 -4 105.59 25.50 12 12 -4 85.39 27.10 12 -12 4 82.99 18.80 -12 12 4 124.29 23.90 12 -12 4 107.69 21.50 -12 12 4 147.49 25.80 -12 -12 5 85.69 22.00 12 -12 -5 94.79 24.10 12 12 5 38.60 18.60 -12 12 -5 73.09 23.10 -12 -12 5 52.19 19.40 -12 12 -5 48.70 20.30 12 -12 -5 75.09 21.40 12 12 5 75.89 20.10 -12 -12 -5 56.49 21.70 -12 12 5 65.09 18.50 -12 12 5 88.89 21.50 -12 -12 -5 112.49 26.00 12 -12 5 73.39 19.50 12 12 -5 72.49 21.90 12 12 -5 80.19 26.20 12 12 6 22.90 16.00 12 -12 -6 27.00 15.90 -12 12 -6 2.90 19.40 -12 12 -6 42.80 17.00 -12 -12 6 40.20 17.50 -12 12 -6 25.00 16.20 12 12 6 29.60 15.70 -12 -12 6 25.70 15.00 12 -12 -6 5.20 15.70 12 12 -6 48.50 16.60 12 12 -6 -10.60 16.80 12 -12 6 16.80 13.80 -12 -12 -6 11.30 15.70 -12 -12 -6 24.80 19.30 -12 12 6 14.50 16.40 -12 13 0 43.10 18.10 12 13 0 55.79 14.80 -12 -13 0 51.39 19.60 12 13 0 55.29 20.80 12 13 0 49.20 14.70 12 -13 0 51.59 17.00 12 -13 0 44.00 15.70 12 -13 -1 14.20 9.80 -12 -13 1 57.19 19.60 -12 13 -1 20.60 15.00 -12 -13 1 58.29 18.70 12 -13 -1 35.00 16.30 12 13 1 72.59 21.00 -12 13 -1 46.90 13.00 12 13 1 50.39 14.50 -12 -13 -1 30.50 14.60 -12 -13 -1 46.00 14.10 12 -13 1 51.09 16.80 -12 -13 -1 17.20 16.50 12 13 -1 54.09 20.90 -12 13 1 55.69 18.40 12 13 -1 37.50 15.80 12 -13 1 41.50 16.30 12 -13 -2 54.79 18.10 -12 -13 2 35.60 17.10 12 13 2 29.70 17.00 12 -13 -2 29.80 14.50 12 -13 -2 43.60 15.60 -12 13 -2 42.70 17.00 -12 -13 2 49.30 17.50 12 13 2 51.09 15.60 -12 13 2 45.60 14.70 12 13 -2 57.29 17.80 12 -13 2 56.39 17.90 12 13 -2 59.39 21.40 12 -13 2 61.89 18.30 -12 -13 -2 85.09 24.20 -12 13 2 63.49 20.70 -12 -13 -2 62.69 19.00 12 13 3 11.40 13.10 -12 13 -3 10.40 16.70 12 -13 -3 16.00 14.60 -12 13 -3 23.70 14.60 12 -13 -3 26.90 14.70 -12 -13 3 11.60 12.60 -12 -13 3 43.20 18.10 12 13 3 41.20 17.50 12 -13 3 27.50 14.40 -12 13 3 18.70 12.70 -12 13 3 28.70 14.80 -12 -13 -3 26.00 16.20 12 13 -3 24.70 17.40 12 13 -3 16.50 15.70 -12 -13 -3 10.80 13.60 -12 -13 4 7.90 13.20 12 13 4 24.10 15.30 -12 13 -4 29.00 13.70 -12 -13 4 -9.60 14.30 -12 13 -4 4.10 13.60 12 13 4 15.20 14.10 -12 13 -4 56.49 20.40 12 -13 -4 -13.50 15.90 12 -13 -4 21.10 15.50 12 13 -4 8.80 15.40 12 13 -4 5.00 16.80 -12 13 4 21.80 16.10 -12 13 4 0.10 11.10 12 -13 4 10.10 12.10 12 -13 4 1.20 7.50 -12 -13 -4 2.70 15.90 -12 -13 -4 16.30 17.20 -12 -13 5 47.50 18.70 -12 -13 5 9.30 14.30 12 -13 -5 13.40 14.20 12 13 5 4.60 12.40 12 -13 -5 37.50 17.80 -12 13 -5 29.90 17.10 -12 13 -5 -1.40 14.30 12 13 5 15.80 16.10 -12 13 -5 7.20 17.70 -12 13 5 5.40 13.00 -12 -13 -5 -12.00 18.40 12 -13 5 4.40 11.80 12 13 -5 26.70 21.80 -12 -13 -5 -0.10 16.70 12 13 -5 10.20 16.10 -12 13 5 -10.00 11.80 12 13 6 21.40 13.10 -12 13 -6 23.80 21.20 -12 -13 6 -9.20 12.20 -12 -13 6 11.60 16.40 12 -13 -6 -5.00 14.40 12 13 6 26.80 13.40 -12 13 -6 40.30 15.20 12 -13 -6 33.50 14.20 -12 13 -6 -6.20 13.90 -12 -13 -6 15.70 16.60 -12 -13 -6 9.30 19.20 12 13 -6 21.00 19.40 -12 13 6 34.00 14.50 12 13 -6 -8.80 13.20 12 -13 6 14.50 11.90 -12 -14 0 51.19 19.80 12 -14 0 64.19 20.00 12 14 0 46.70 15.50 -12 -14 0 22.00 9.90 12 -14 0 31.40 15.00 -12 14 0 43.30 18.40 12 14 0 47.70 20.40 12 14 0 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11 -5 168.08 30.40 -13 -11 5 105.39 24.10 -13 11 -5 91.09 24.30 13 11 5 122.29 25.70 13 11 5 125.49 24.80 -13 11 -5 143.19 29.20 13 -11 -5 133.29 26.00 13 -11 -5 130.69 24.90 13 11 -5 119.99 26.60 -13 -11 -5 104.49 25.00 13 -11 5 110.39 22.90 -13 11 5 82.19 19.00 -13 -11 -5 87.19 23.60 -13 11 5 124.09 24.30 13 11 -5 122.19 29.20 -13 11 -6 33.70 19.20 -13 11 -6 8.30 18.70 -13 -11 6 72.59 20.30 13 11 6 1.80 14.20 13 -11 -6 25.20 17.70 -13 -11 6 31.00 17.10 13 -11 -6 12.30 14.70 -13 11 -6 36.40 18.90 13 11 6 7.70 13.90 -13 -11 -6 49.90 20.50 13 11 -6 42.70 24.60 -13 11 6 47.20 17.60 13 -11 6 -4.90 13.30 13 11 -6 41.00 17.00 -13 -11 -6 17.70 18.60 -13 -11 7 79.79 20.40 13 11 7 64.39 20.50 -13 11 -7 10.20 22.40 -13 11 -7 49.50 22.30 13 -11 -7 50.99 17.30 -13 11 -7 27.50 15.50 -13 -11 7 104.29 25.20 13 11 7 93.69 21.60 13 -11 -7 43.50 19.20 -13 -11 -7 53.59 21.80 -13 11 7 66.79 20.80 13 11 -7 69.39 25.60 -13 -11 -7 34.20 14.80 13 12 0 303.67 37.50 -13 -12 0 279.77 38.10 -13 -12 0 245.88 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176.48 25.20 14 -8 3 131.19 21.90 14 8 -3 191.58 30.70 -14 -8 -3 225.08 31.30 -14 -8 -3 195.78 28.50 -14 -8 4 5.70 11.90 14 -8 -4 18.20 11.60 14 8 4 12.20 10.60 14 -8 -4 19.20 13.60 14 -8 -4 40.50 15.60 -14 -8 4 17.40 11.50 -14 8 -4 9.80 11.40 14 8 4 14.80 11.20 -14 8 -4 3.70 11.50 14 8 4 16.90 11.60 14 8 -4 10.20 11.00 -14 8 4 6.50 11.90 14 8 -4 5.70 14.60 -14 -8 -4 12.10 15.40 14 -8 4 28.80 13.30 -14 8 4 13.30 7.90 -14 -8 -4 -7.10 9.90 14 8 5 290.87 32.60 -14 -8 5 254.07 32.80 14 8 5 250.47 34.00 -14 8 -5 320.47 40.80 -14 8 -5 290.77 38.30 -14 -8 5 258.17 33.40 14 -8 -5 223.38 32.50 -14 8 -5 241.88 35.20 14 8 5 289.17 34.10 -14 8 5 237.48 33.30 14 8 -5 284.17 35.50 14 8 -5 340.77 45.20 -14 -8 -5 244.98 35.70 14 -8 5 285.27 36.40 -14 8 -6 24.50 20.80 14 8 6 37.30 16.40 -14 8 -6 21.60 16.30 -14 -8 6 26.50 14.00 14 8 6 42.90 16.80 -14 -8 6 23.00 14.90 14 -8 -6 68.29 16.70 -14 8 -6 31.00 18.10 14 -8 -6 60.09 19.50 14 -8 -6 38.70 18.00 14 -8 6 30.10 16.90 -14 -8 -6 29.20 19.50 -14 -8 -6 28.80 15.00 -14 8 6 61.09 20.80 14 8 -6 71.79 25.70 14 8 7 194.28 30.90 -14 8 -7 128.59 27.20 14 -8 -7 175.38 28.40 -14 -8 7 149.39 27.60 -14 8 -7 181.18 36.50 -14 8 -7 125.39 29.70 14 -8 -7 191.58 32.40 14 8 7 183.18 30.70 -14 -8 7 182.38 29.20 -14 8 7 147.29 30.70 14 -8 7 160.18 29.90 14 8 -7 176.68 37.00 -14 -8 -7 166.18 32.90 -14 8 -8 -10.20 10.30 -14 9 0 183.08 25.50 -14 9 0 155.98 22.70 14 -9 0 133.89 23.90 14 9 0 202.18 28.10 14 9 0 185.58 23.30 14 9 0 244.98 32.50 14 -9 0 194.58 24.30 -14 -9 0 172.28 26.50 -14 -9 0 169.28 22.60 -14 -9 0 189.18 25.20 14 -9 -1 -10.40 5.20 14 9 1 4.80 9.80 14 9 1 -4.40 5.70 -14 -9 1 13.00 8.80 -14 9 -1 1.70 10.10 14 -9 -1 -10.50 7.00 14 -9 -1 -3.70 9.10 14 9 1 -2.40 8.20 -14 -9 1 -1.60 8.40 -14 9 -1 -5.10 6.30 -14 -9 1 7.00 7.90 -14 9 -1 -0.90 6.80 -14 -9 -1 0.20 10.10 -14 9 1 -1.80 8.30 14 -9 1 8.70 8.30 14 9 -1 -8.60 9.60 14 -9 1 2.90 10.20 -14 -9 -1 -11.40 8.50 14 -9 1 4.70 6.90 14 9 -1 -5.80 9.00 -14 9 1 -4.50 3.70 14 -9 -2 186.68 23.00 14 9 2 192.38 28.10 -14 -9 2 227.38 24.30 -14 9 -2 209.28 26.80 -14 -9 2 175.38 25.70 14 -9 -2 194.68 25.60 -14 -9 2 152.08 23.10 -14 9 -2 170.08 25.90 14 -9 -2 157.38 25.30 14 9 2 178.38 25.60 -14 9 2 222.38 27.70 -14 -9 -2 220.18 32.10 14 -9 2 213.48 25.30 14 -9 2 160.28 22.50 14 9 -2 190.88 29.40 -14 -9 -2 179.68 27.20 14 -9 2 135.59 23.70 -14 9 2 245.18 29.50 14 9 -2 208.28 31.00 -14 -9 3 28.10 13.10 14 -9 -3 35.10 14.30 -14 -9 3 50.39 17.00 14 -9 -3 49.80 15.80 14 9 3 30.80 12.50 14 9 3 44.10 13.00 -14 9 -3 41.00 13.80 14 9 3 27.60 14.30 14 -9 -3 53.19 14.40 -14 9 -3 44.00 15.00 -14 9 -3 26.50 15.20 14 -9 3 9.20 5.40 -14 -9 -3 40.80 15.70 -14 9 3 40.10 14.90 -14 9 3 38.90 12.90 -14 -9 -3 55.79 17.50 14 -9 3 23.90 10.00 14 9 -3 54.99 17.90 14 9 -3 57.79 17.30 -14 -9 4 57.49 17.50 14 9 4 62.69 15.90 14 -9 -4 61.49 16.80 14 -9 -4 60.09 17.50 14 9 4 78.09 19.20 -14 9 -4 37.90 17.40 -14 -9 4 58.29 16.10 -14 9 -4 43.20 16.40 14 9 4 58.59 16.20 -14 9 -4 62.59 19.90 -14 -9 -4 59.39 19.20 -14 9 4 58.99 14.60 14 9 -4 47.10 20.30 14 -9 4 77.29 18.50 -14 9 4 44.20 16.90 -14 -9 -4 44.90 18.30 14 9 5 9.40 11.40 14 9 5 37.90 14.60 -14 -9 5 34.50 16.20 -14 9 -5 21.20 17.40 14 -9 -5 18.10 12.90 -14 -9 5 40.70 16.40 14 -9 -5 33.70 16.40 -14 9 -5 9.00 14.10 14 -9 -5 40.70 15.70 14 9 -5 22.80 19.00 14 9 -5 17.70 12.90 -14 9 5 45.90 18.00 14 -9 5 35.50 15.30 -14 -9 -5 21.40 15.80 14 9 6 19.20 14.20 14 -9 -6 -1.10 13.60 -14 -9 6 27.90 16.00 -14 -9 6 19.40 13.70 -14 9 -6 41.80 23.20 14 9 6 28.70 15.70 -14 9 -6 26.60 17.70 14 -9 -6 23.30 18.00 -14 9 -6 33.30 17.50 -14 -9 -6 19.40 19.50 -14 9 6 36.80 18.70 14 -9 6 8.40 14.20 -14 -9 -6 6.30 7.00 14 9 -6 24.70 18.90 -14 9 -7 9.30 15.30 -14 9 -7 18.40 18.60 -14 9 -7 -6.90 19.20 14 9 7 -0.40 11.60 14 -9 -7 0.50 12.60 14 9 7 12.60 14.40 -14 -9 7 -0.50 14.40 -14 -9 7 -14.90 10.90 14 -9 -7 28.60 16.80 14 9 -7 2.40 18.70 14 -9 7 19.70 15.00 -14 -9 -7 -25.60 14.90 -14 9 7 18.30 16.80 -14 10 0 90.19 20.50 -14 -10 0 132.29 24.60 -14 10 0 108.19 18.70 14 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372.66 44.30 14 -10 -3 446.06 40.90 -14 10 -3 428.36 40.50 14 -10 -3 443.66 40.10 14 10 3 424.36 39.10 14 10 3 437.46 42.60 -14 -10 3 413.96 45.40 14 10 3 441.86 40.20 -14 10 -3 468.65 42.60 14 10 -3 508.15 55.69 14 -10 3 438.86 38.40 -14 10 3 421.56 39.70 14 10 -3 533.35 55.29 -14 10 3 420.56 40.80 -14 -10 -3 556.24 48.90 14 -10 3 431.76 39.40 -14 -10 -3 448.86 49.20 14 -10 -4 56.29 17.40 -14 -10 4 32.40 16.20 -14 -10 4 16.50 13.00 14 -10 -4 24.60 11.40 14 10 4 14.60 13.40 14 -10 -4 24.40 14.10 14 10 4 36.90 15.80 -14 10 -4 38.80 17.00 -14 10 -4 48.30 17.40 14 10 4 22.50 10.90 -14 10 -4 41.90 18.00 -14 -10 -4 31.60 17.40 14 10 -4 63.49 22.90 -14 -10 -4 30.30 18.10 14 -10 4 24.00 14.30 14 10 -4 20.80 14.30 -14 10 4 41.50 13.80 -14 10 4 29.30 14.20 14 -10 -5 133.79 25.10 -14 10 -5 217.28 33.40 14 10 5 172.68 27.80 -14 10 -5 166.48 31.90 14 -10 -5 201.18 32.00 14 10 5 175.08 29.20 -14 -10 5 183.38 28.90 -14 10 -5 181.78 32.60 -14 -10 5 184.18 29.10 14 10 -5 230.88 39.70 -14 10 5 181.08 31.00 14 -10 5 195.28 30.20 -14 -10 -5 146.69 30.30 -14 -10 -5 212.68 33.80 14 -10 -6 34.90 18.20 -14 -10 6 64.99 19.80 -14 10 -6 43.90 18.40 -14 10 -6 92.29 27.60 14 10 6 30.00 16.90 14 -10 -6 50.99 18.90 -14 10 -6 22.30 22.50 14 10 6 37.90 17.00 -14 -10 6 58.79 19.90 14 10 -6 66.89 25.40 -14 -10 -6 40.90 23.20 -14 10 6 46.30 19.50 -14 -10 -6 59.49 19.30 14 -10 6 46.30 18.10 -14 10 -7 2.10 12.40 14 -10 -7 39.80 15.10 14 10 7 37.90 15.60 -14 -10 7 2.20 13.70 14 -10 -7 47.80 18.90 -14 10 -7 49.40 21.20 14 10 7 19.80 13.80 -14 -10 7 12.20 14.00 -14 10 -7 37.50 23.00 -14 -10 -7 7.90 17.90 14 -10 7 25.80 15.00 -14 10 7 42.40 20.30 14 10 -7 37.70 23.80 14 -11 0 250.47 33.40 -14 11 0 210.58 30.40 14 11 0 228.18 32.40 -14 -11 0 248.68 30.30 -14 -11 0 249.18 34.50 -14 -11 0 307.47 33.90 14 -11 0 219.78 29.80 14 11 0 276.67 37.40 14 -11 -1 98.19 21.80 -14 -11 1 57.19 18.50 -14 11 -1 63.19 19.10 14 11 1 74.09 20.40 14 11 1 66.09 16.10 14 11 1 76.19 17.70 14 -11 -1 59.89 13.00 14 -11 -1 58.39 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28.90 12.30 -15 10 -2 27.30 15.40 15 10 2 38.70 14.40 15 -10 -2 51.79 15.30 -15 -10 2 49.99 16.70 15 10 2 44.10 15.90 -15 10 2 49.70 15.10 15 10 -2 50.89 19.00 15 -10 2 20.60 13.20 15 -10 2 50.99 13.90 15 10 -2 44.10 17.60 15 -10 2 28.10 11.80 -15 -10 -2 27.70 16.50 -15 10 2 45.40 14.40 15 -10 -3 114.19 22.70 15 -10 -3 102.49 21.70 15 10 3 114.09 24.00 15 -10 -3 154.78 23.90 -15 -10 3 136.79 25.00 -15 10 -3 111.49 25.20 15 10 3 129.79 22.60 -15 10 -3 118.79 23.30 15 10 3 94.69 19.70 15 -10 3 108.89 17.90 -15 -10 -3 127.59 25.90 15 10 -3 97.49 24.90 -15 10 3 111.49 21.00 15 -10 3 101.49 20.00 15 10 -3 186.18 32.60 -15 -10 -3 119.29 24.40 -15 10 3 126.29 22.10 15 10 4 24.30 11.10 -15 -10 4 25.10 14.20 -15 -10 4 18.30 15.00 15 10 4 29.60 14.00 -15 10 -4 46.10 17.00 15 -10 -4 17.30 13.80 15 -10 -4 33.30 15.90 -15 10 -4 24.90 17.00 -15 -10 -4 30.10 17.60 -15 10 4 36.70 13.10 -15 10 4 19.40 14.80 15 10 -4 13.80 12.90 15 10 -4 31.40 18.30 15 -10 4 29.30 14.00 -15 -10 -4 32.50 16.10 15 -10 -5 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3.60 13.80 20 5 6 2.50 10.80 -20 5 6 23.10 15.10 20 5 -6 12.90 18.10 20 -5 6 4.20 15.20 20 -5 6 31.60 14.40 -20 -5 -6 17.90 17.50 -20 -5 -6 -4.30 12.80 20 5 -6 -2.00 12.30 -20 5 6 12.10 15.20 -20 -5 7 -3.20 9.90 -20 -5 7 28.70 16.10 20 5 7 7.60 11.80 20 5 7 10.50 12.80 -20 5 -7 23.50 15.90 20 -5 -7 4.40 12.30 20 5 7 0.30 12.00 -20 5 -7 -18.30 12.60 -20 -5 -7 11.80 14.30 -20 -5 -7 14.50 20.00 20 5 -7 -14.30 14.70 -20 5 7 -28.00 11.70 20 -5 7 -15.10 11.70 -20 5 7 -15.00 11.50 20 -6 0 2.90 7.50 20 6 0 -1.60 8.40 20 -6 0 7.40 10.50 -20 6 0 16.40 12.00 -20 -6 0 11.80 11.60 -20 6 0 10.10 8.60 20 6 0 3.70 10.70 20 -6 0 6.10 7.30 -20 -6 0 21.80 13.60 -20 6 -1 205.88 27.40 20 -6 -1 294.57 29.60 20 6 1 252.27 34.30 -20 -6 1 251.67 35.80 -20 6 -1 249.18 32.00 20 6 1 240.78 31.60 -20 -6 1 303.07 34.90 -20 -6 1 228.08 30.80 20 -6 -1 209.78 30.00 -20 -6 -1 291.57 35.50 -20 6 1 224.78 28.90 20 6 -1 250.57 32.40 -20 6 1 205.88 29.60 -20 -6 -1 263.57 34.30 -20 6 1 269.87 31.00 20 -6 1 278.57 31.70 20 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3.50 12.70 20 6 -7 -5.50 13.90 20 -6 7 2.20 13.40 -20 -7 0 -11.40 9.80 20 -7 0 7.10 11.70 -20 7 0 23.90 11.80 -20 7 0 13.00 9.70 20 7 0 -1.10 10.80 20 7 0 1.80 6.60 -20 -7 0 1.00 11.50 20 -7 0 3.10 7.20 20 -7 -1 16.50 10.10 -20 -7 1 21.60 13.40 20 7 1 10.80 13.10 20 -7 -1 11.20 11.70 20 7 1 31.40 14.10 -20 -7 1 40.90 16.20 -20 7 -1 16.10 8.40 -20 7 -1 6.90 10.90 20 -7 1 9.00 11.80 -20 7 1 20.60 10.20 -20 -7 -1 25.30 14.60 20 7 -1 11.90 13.40 20 -7 1 8.10 9.60 -20 -7 -1 15.20 13.50 -20 7 1 17.70 12.40 20 7 -1 40.40 14.40 -20 -7 2 3.40 8.90 -20 -7 2 4.80 12.40 20 -7 -2 5.10 10.40 20 7 2 9.30 8.90 -20 -7 2 13.50 11.80 20 -7 -2 20.20 12.20 -20 7 -2 -13.30 8.00 20 7 2 16.00 13.00 -20 7 -2 -0.50 10.40 20 -7 -2 -1.40 8.00 20 -7 2 2.40 11.40 -20 -7 -2 4.90 12.00 -20 7 2 1.70 10.10 20 7 -2 5.70 11.50 -20 7 2 4.40 7.80 20 7 -2 -3.30 14.20 20 -7 2 -12.40 6.20 -20 -7 -2 -0.60 13.60 20 -7 -3 0.20 10.50 -20 -7 3 10.40 9.90 -20 7 -3 5.00 10.60 -20 7 -3 19.40 13.40 -20 -7 3 12.50 11.30 20 7 3 17.30 12.70 20 7 3 19.60 13.70 20 -7 -3 14.20 13.20 -20 -7 3 33.00 15.10 20 -7 -3 4.40 10.50 20 7 3 5.60 7.70 20 -7 3 14.60 12.70 -20 -7 -3 30.40 15.70 -20 -7 -3 5.10 15.40 -20 7 3 20.90 10.70 -20 7 3 26.00 15.90 20 -7 3 16.30 13.00 20 7 -3 -0.80 15.50 20 -7 -4 1.30 11.10 -20 -7 4 23.50 16.00 20 7 4 29.00 14.80 -20 7 -4 18.20 13.80 -20 7 -4 16.50 13.10 20 7 4 28.80 15.20 -20 -7 4 41.10 15.00 20 -7 -4 8.80 12.40 20 7 4 40.10 13.50 20 -7 -4 0.60 10.90 -20 -7 -4 17.90 18.10 20 -7 4 15.90 14.80 20 -7 4 20.60 14.30 -20 7 4 24.70 12.80 -20 7 4 35.00 15.70 20 7 -4 7.90 16.40 -20 7 -5 23.40 16.80 20 -7 -5 15.10 15.60 20 7 5 25.90 12.30 -20 7 -5 11.00 13.60 20 -7 -5 19.20 14.20 -20 -7 5 21.50 17.10 20 7 5 27.70 16.50 20 -7 -5 10.00 13.40 20 7 5 21.90 14.90 -20 -7 5 15.70 13.40 -20 7 5 19.20 16.50 -20 -7 -5 25.50 18.50 20 -7 5 34.70 16.20 -20 7 5 28.90 14.20 20 7 -5 0.00 18.40 20 -7 5 36.70 17.30 20 -7 -6 3.20 14.20 -20 7 -6 2.50 16.20 -20 7 -6 15.70 15.50 20 7 6 17.60 16.50 20 7 6 28.60 13.40 -20 -7 6 20.00 14.60 -20 -7 6 -2.20 14.80 20 -7 -6 22.20 15.00 20 7 6 3.20 12.70 20 -7 -6 -7.90 11.40 20 -7 6 -14.20 11.10 -20 7 6 6.80 13.00 20 -7 6 -3.80 11.30 -20 -7 -6 38.00 20.50 -20 7 6 12.60 15.90 20 7 -6 -0.20 17.70 20 -8 0 137.39 21.10 -20 8 0 168.48 26.30 20 8 0 157.48 28.40 -20 8 0 132.69 22.30 -20 -8 0 182.98 28.00 20 -8 0 149.09 25.00 20 8 0 179.28 28.80 -20 -8 1 66.49 17.50 -20 -8 1 65.49 18.80 20 -8 -1 53.19 18.10 -20 8 -1 66.19 17.00 20 8 1 64.89 18.90 20 -8 -1 29.40 12.10 20 8 1 46.90 17.40 -20 8 -1 50.79 14.80 20 -8 1 44.10 17.50 20 -8 1 52.29 17.40 -20 8 1 64.89 19.00 -20 -8 -1 26.40 15.90 -20 8 1 56.69 14.10 20 8 -1 22.40 16.60 -20 -8 2 274.67 35.90 -20 -8 2 268.37 31.40 20 -8 -2 265.67 33.00 20 8 2 262.27 36.80 -20 8 -2 277.37 34.60 20 -8 -2 298.27 31.50 20 8 2 302.67 38.20 20 -8 -2 287.97 37.40 -20 -8 2 255.37 32.80 20 -8 2 222.78 33.40 -20 -8 -2 311.17 39.10 -20 8 2 260.37 30.90 -20 -8 -2 281.17 37.60 20 -8 2 246.88 31.50 20 8 -2 367.46 47.50 20 8 -2 307.07 40.40 -20 8 2 237.78 34.30 20 -8 -3 55.79 18.60 20 8 3 76.29 20.20 20 -8 -3 43.10 15.20 -20 8 -3 55.89 15.00 -20 -8 3 56.79 18.20 20 8 3 74.29 19.50 20 -8 -3 64.49 16.70 -20 -8 3 58.39 15.80 20 8 3 59.79 14.40 -20 8 -3 31.90 15.70 -20 -8 -3 112.89 26.50 -20 -8 -3 57.49 18.90 20 8 -3 81.59 24.30 20 -8 3 45.60 15.00 -20 8 3 29.40 12.10 20 -8 3 25.60 15.10 -20 8 3 77.39 21.00 -20 -8 4 77.09 21.10 -20 8 -4 87.39 21.30 20 -8 -4 80.09 19.30 -20 -8 4 65.79 17.70 20 -8 -4 109.79 21.50 20 8 4 59.59 18.20 -20 8 -4 48.80 19.80 20 8 4 81.49 21.80 20 8 4 58.09 16.90 20 -8 -4 74.79 20.10 20 -8 4 58.49 18.80 -20 8 4 72.79 20.70 -20 -8 -4 83.59 20.40 -20 -8 -4 140.29 30.50 20 8 -4 69.09 24.70 -20 8 4 77.79 18.50 20 -8 4 80.59 20.40 -20 8 -5 27.30 15.40 -20 -8 5 1.30 11.80 -20 8 -5 7.60 15.10 20 -8 -5 34.80 15.90 20 8 5 9.10 14.70 -20 -8 5 13.80 15.80 20 -8 -5 11.60 15.30 20 -8 -5 35.60 16.10 20 8 5 38.90 14.70 -20 8 5 12.30 12.70 20 -8 5 -11.90 11.10 -20 -8 -5 7.60 17.50 20 -8 5 22.50 14.30 20 8 -5 16.80 20.10 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18.00 -20 9 5 23.70 17.30 20 -9 5 -13.00 11.80 -20 -9 6 12.20 15.20 20 -9 -6 7.50 12.00 -20 9 -6 -15.40 12.20 20 9 6 13.40 12.30 -20 -9 6 6.40 12.10 20 -9 -6 12.20 13.20 20 -9 -6 -14.10 13.80 20 9 6 34.50 14.60 -20 9 -6 10.80 14.70 20 -9 6 17.50 15.30 -20 -9 -6 19.50 18.50 20 9 -6 -15.20 13.70 20 -9 6 2.80 11.50 -20 9 6 4.30 11.00 -20 9 6 1.80 14.20 -20 10 0 146.89 24.30 20 10 0 170.28 31.70 -20 10 0 176.78 27.60 20 -10 0 129.29 22.80 20 10 0 220.18 34.10 -20 -10 0 136.19 26.10 -20 -10 0 179.38 32.10 20 -10 0 163.58 29.10 -20 -10 1 67.89 18.20 20 10 1 58.49 20.90 -20 10 -1 50.79 17.10 -20 -10 1 62.49 21.30 20 10 1 101.29 22.90 20 -10 -1 40.30 15.90 20 -10 -1 53.99 16.40 -20 10 1 56.79 18.70 -20 10 1 75.99 18.40 20 10 -1 42.90 19.50 20 -10 1 62.09 19.60 -20 -10 -1 27.00 17.20 20 -10 1 49.70 14.00 20 10 -1 46.80 20.20 -20 -10 -1 76.09 22.60 20 -10 -2 204.18 31.90 -20 -10 2 180.18 31.20 -20 10 -2 183.78 28.70 20 10 2 231.28 35.40 20 10 2 176.88 30.20 20 -10 -2 156.08 26.60 -20 -10 2 227.48 30.00 20 -10 2 212.88 33.60 -20 10 2 180.88 29.60 20 10 -2 146.79 28.40 -20 -10 -2 204.38 34.20 -20 -10 -2 169.38 29.80 20 10 -2 225.28 36.30 20 -10 -3 32.90 15.40 -20 -10 3 28.40 17.30 20 10 3 8.70 8.30 20 10 3 53.49 20.00 20 -10 -3 25.30 15.60 -20 -10 3 43.80 15.50 -20 10 -3 39.40 16.60 20 10 3 31.70 15.30 20 -10 -3 16.20 12.90 20 10 -3 46.00 22.40 -20 -10 -3 21.30 18.50 20 -10 3 16.00 13.00 -20 10 3 40.00 16.50 -20 -10 -3 13.10 16.60 20 10 4 109.19 25.00 -20 10 -4 40.80 19.30 20 10 4 74.19 19.90 -20 -10 4 111.69 26.60 20 10 4 72.09 17.90 20 -10 -4 118.69 24.20 20 -10 -4 126.29 26.50 -20 10 -4 100.99 21.60 -20 -10 4 77.09 19.90 -20 -10 -4 75.89 22.70 20 -10 4 87.49 20.40 20 10 -4 129.59 32.90 -20 -10 -4 118.79 25.50 -20 10 4 96.29 22.80 20 -10 4 74.99 21.10 -20 10 -5 6.90 14.20 20 10 5 39.30 15.40 -20 10 -5 -6.90 14.60 20 -10 -5 15.90 13.70 20 10 5 5.50 10.80 20 -10 -5 16.90 16.40 -20 -10 5 25.10 18.80 -20 -10 5 18.40 13.50 20 10 5 33.00 15.40 20 -10 -5 19.70 14.70 -20 10 5 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28.10 22 5 3 192.48 28.90 -22 5 -3 181.58 28.30 22 -5 -3 192.68 26.20 -22 5 -3 159.38 27.20 -22 -5 3 187.78 28.20 22 -5 3 210.38 30.50 22 5 -3 226.58 36.40 -22 5 3 234.58 33.00 -22 -5 -3 204.58 33.20 22 -5 3 204.58 27.00 -22 5 3 225.68 29.10 22 -5 3 176.88 28.10 -22 -5 -3 203.68 27.40 22 5 4 1.80 13.10 -22 -5 4 17.50 12.10 -22 -5 4 -2.80 10.30 22 5 4 21.50 11.60 22 -5 -4 -1.30 11.80 -22 5 -4 17.80 14.30 22 -5 -4 25.40 14.60 -22 5 -4 15.50 13.90 22 5 4 14.20 14.00 -22 -5 4 10.40 14.00 22 -5 4 35.40 15.60 -22 -5 -4 21.60 13.60 22 -5 4 6.60 13.00 -22 5 4 5.90 10.60 22 5 -4 26.10 15.80 -22 5 4 -11.90 12.90 -22 -5 -4 42.50 20.90 22 5 5 207.28 32.50 -22 -5 5 200.78 30.20 -22 5 -5 153.88 28.40 22 -5 -5 241.38 31.50 22 5 5 245.78 31.20 -22 5 -5 219.78 34.50 22 5 5 230.78 32.20 22 -5 -5 183.08 31.30 -22 -5 5 231.68 32.90 -22 5 5 207.68 30.20 22 5 -5 240.58 39.00 -22 -5 -5 224.68 35.90 22 -5 5 202.58 29.10 -22 -5 -5 155.58 28.10 -22 5 5 213.78 33.90 22 5 -5 222.58 30.70 22 -5 5 222.18 31.60 22 5 6 6.90 13.60 22 5 6 17.60 12.30 22 5 6 12.00 15.60 22 -5 -6 6.10 13.00 -22 5 -6 -4.50 13.80 -22 -5 6 1.40 12.40 -22 -5 6 8.50 14.40 -22 5 -6 5.40 15.60 -22 5 6 18.70 14.00 -22 -5 -6 -11.20 14.40 22 -5 6 14.00 11.90 22 -5 6 1.10 11.90 -22 5 6 -10.90 11.20 22 5 -6 9.50 13.80 22 -5 6 -2.70 13.70 -22 -5 -6 11.40 14.20 22 6 0 38.50 17.40 -22 -6 0 20.20 15.50 22 6 0 30.40 11.70 -22 6 0 12.10 8.40 -22 -6 0 13.90 14.60 -22 6 0 13.60 12.90 22 -6 0 22.80 13.90 22 -6 -1 79.59 16.90 -22 6 -1 63.09 15.90 22 6 1 89.99 23.60 22 6 1 92.19 19.20 -22 -6 1 84.89 21.30 -22 -6 1 77.29 20.60 -22 6 -1 81.59 19.20 22 -6 -1 67.89 19.70 22 -6 1 83.89 19.60 -22 6 1 53.69 17.70 -22 -6 -1 98.19 21.80 22 6 -1 136.39 27.80 22 -6 1 76.19 17.60 -22 -6 -1 81.69 22.50 -22 6 -2 42.60 14.80 22 -6 -2 58.89 17.10 -22 -6 2 38.90 15.40 -22 -6 2 33.20 15.70 22 6 2 78.19 20.90 22 -6 -2 41.10 13.30 -22 6 -2 20.30 13.70 -22 -6 2 50.69 13.50 22 6 2 105.09 21.20 22 6 -2 59.09 21.60 -22 6 2 43.40 18.00 -22 6 2 44.50 13.50 -22 -6 -2 73.99 20.70 22 -6 2 53.19 15.00 -22 -6 -2 37.00 18.00 22 -6 2 39.60 16.20 -22 -6 3 2.80 12.80 22 6 3 -12.60 10.70 -22 -6 3 9.50 12.70 22 -6 -3 -0.70 10.60 22 6 3 0.60 11.70 22 -6 -3 6.30 12.40 -22 -6 3 4.20 6.70 22 6 3 -7.60 7.40 -22 6 -3 -1.20 12.80 -22 6 3 4.70 12.60 22 -6 3 2.30 11.60 -22 -6 -3 14.00 12.40 -22 6 3 8.30 9.60 22 6 -3 -9.40 14.00 22 6 4 73.79 20.70 -22 -6 4 59.19 16.60 -22 6 -4 60.69 17.90 -22 -6 4 83.89 21.30 22 -6 -4 47.10 16.20 22 6 4 84.99 20.30 22 6 4 79.69 16.70 -22 6 -4 31.50 16.80 22 -6 -4 66.19 21.60 22 -6 4 52.29 17.50 -22 6 4 52.99 15.20 22 -6 4 32.70 16.10 -22 6 4 72.49 21.40 -22 -6 -4 37.60 19.90 22 6 -4 80.29 26.00 -22 -6 -4 23.60 13.30 -22 -6 5 6.70 12.90 -22 6 -5 1.50 15.10 22 6 5 24.50 16.70 -22 -6 5 13.50 15.60 -22 6 -5 -9.70 11.80 22 6 5 4.20 9.90 22 6 5 -4.10 12.20 22 -6 -5 2.90 13.60 22 -6 -5 13.70 14.30 22 -6 5 13.40 12.60 -22 -6 -5 -11.80 11.40 22 -6 5 16.00 14.40 22 6 -5 10.60 18.20 -22 6 5 9.40 16.20 -22 6 5 1.50 10.00 -22 -6 -5 11.50 20.40 -22 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87.29 24.50 22 -7 2 33.10 10.80 -22 -7 -2 45.60 17.70 22 -7 2 31.00 16.40 -22 -7 -2 16.00 15.20 -22 -7 3 241.58 32.60 -22 7 -3 210.58 32.20 22 7 3 285.37 37.50 -22 -7 3 296.57 37.70 22 -7 -3 228.78 30.90 22 -7 -3 256.67 35.60 22 7 3 289.57 36.40 22 7 3 268.57 30.90 22 -7 3 224.08 33.80 -22 -7 -3 261.47 36.50 -22 -7 -3 208.98 33.80 22 7 -3 279.17 42.40 22 -7 3 244.28 32.60 -22 7 3 269.27 37.90 22 7 4 -22.10 10.80 22 7 4 -10.70 12.10 22 -7 -4 10.60 11.20 -22 -7 4 -6.80 9.60 22 -7 -4 21.30 13.70 -22 7 -4 5.00 10.60 -22 -7 4 -1.30 14.20 -22 7 -4 13.60 13.30 22 7 4 -1.40 9.20 22 7 -4 0.20 17.30 22 -7 4 16.10 12.60 -22 -7 -4 7.60 17.20 -22 7 4 0.20 9.50 -22 7 4 -1.50 13.20 22 -7 4 3.30 12.40 -22 -7 5 126.49 25.60 22 -7 -5 83.09 22.50 -22 7 -5 111.79 25.70 22 7 5 101.89 23.60 -22 -7 5 66.09 19.90 22 7 5 125.29 25.80 -22 7 -5 115.69 26.40 22 -7 -5 134.29 24.60 22 7 5 103.29 20.70 -22 7 5 85.29 21.80 -22 7 5 105.29 27.00 22 7 -5 151.58 35.00 22 -7 5 78.29 19.90 22 -7 5 70.89 20.80 -22 -7 -5 138.09 30.50 -22 7 -6 19.00 16.60 22 -7 -6 30.80 14.10 22 -7 -6 57.39 19.30 -22 -7 6 60.99 20.10 -22 -7 6 41.80 16.70 22 7 6 65.89 18.50 22 7 6 59.99 19.70 22 7 6 76.89 19.90 -22 7 -6 49.70 20.90 22 7 -6 85.59 28.30 -22 7 6 73.39 23.10 22 -7 6 23.00 14.40 -22 -7 -6 60.99 22.20 -22 7 6 64.89 17.00 22 -7 6 34.70 15.90 22 -8 0 46.70 18.80 -22 8 0 60.29 18.80 22 8 0 54.49 20.30 -22 -8 0 82.29 22.60 22 8 0 64.29 20.30 -22 8 0 53.49 15.20 22 -8 0 30.00 12.30 -22 -8 0 73.89 20.60 22 -8 -1 13.70 11.00 22 8 1 5.40 11.70 -22 8 -1 -2.50 10.10 -22 -8 1 -2.60 11.70 -22 -8 1 -21.80 12.70 -22 8 -1 -14.60 9.30 22 -8 -1 9.90 13.90 22 8 1 4.10 13.20 22 8 -1 11.00 13.40 22 8 -1 -8.70 11.80 22 -8 1 1.30 10.50 -22 -8 -1 -9.50 11.60 -22 8 1 11.40 12.20 -22 -8 2 35.60 15.30 22 -8 -2 24.70 13.00 -22 -8 2 19.80 16.30 22 -8 -2 2.00 12.70 -22 8 -2 13.00 14.30 22 8 2 36.00 16.90 22 8 2 31.60 15.90 -22 -8 -2 15.40 16.10 22 -8 2 24.90 14.30 -22 -8 -2 18.30 15.10 22 8 -2 2.60 16.10 22 -8 2 32.60 13.20 -22 8 2 28.00 15.10 22 8 3 2.70 14.50 22 -8 -3 -3.20 10.60 22 8 3 7.50 13.60 -22 -8 3 29.10 15.90 -22 -8 3 -2.50 7.40 22 -8 -3 -7.40 10.10 22 -8 -3 16.40 12.90 -22 8 -3 9.10 12.40 -22 8 3 2.80 12.80 22 8 -3 -17.70 15.20 -22 -8 -3 16.40 17.40 -22 -8 -3 -11.50 7.00 -22 8 3 0.20 5.50 22 -8 3 -8.40 11.00 22 -8 3 5.30 10.80 22 8 4 38.00 16.60 22 -8 -4 35.40 16.00 -22 8 -4 6.70 11.50 22 -8 -4 39.20 16.20 22 8 4 50.39 15.10 -22 8 -4 17.90 15.90 -22 -8 4 34.00 17.40 -22 -8 4 13.70 13.00 22 8 4 49.80 18.00 22 -8 4 48.10 16.20 -22 -8 -4 16.70 17.80 -22 8 4 49.10 19.80 -22 8 4 31.50 12.90 22 -8 4 39.10 16.70 22 8 -4 46.30 26.20 22 8 5 -8.80 12.00 22 8 5 19.70 11.90 -22 -8 5 -2.90 16.00 22 -8 -5 7.70 12.70 22 -8 -5 9.30 14.50 -22 8 -5 -6.90 12.50 22 -8 -5 1.10 13.60 22 8 5 -13.00 11.10 -22 8 -5 20.20 16.70 -22 -8 5 10.40 11.00 22 8 -5 -6.90 16.40 -22 -8 -5 10.10 18.80 22 -8 5 0.70 11.20 -22 8 5 13.60 12.10 22 -8 5 3.60 12.10 -22 8 5 -14.70 11.70 22 8 6 0.70 8.70 22 -8 -6 -17.70 9.90 22 -8 -6 -1.30 12.20 -22 -8 6 -1.60 14.60 22 8 6 13.00 12.10 22 -8 -6 8.80 15.10 22 8 6 -2.10 13.90 -22 8 -6 -0.10 13.20 -22 8 -6 24.60 17.50 -22 -8 -6 -34.10 13.20 22 -8 6 11.50 11.00 22 -8 6 6.70 12.80 -22 8 6 14.90 9.70 22 -9 0 33.10 12.80 -22 9 0 11.50 11.60 22 -9 0 38.90 16.40 -22 -9 0 22.10 17.70 -22 9 0 -6.20 8.20 22 9 0 55.69 19.20 -22 -9 0 34.60 17.30 22 9 0 40.60 18.50 -22 -9 1 84.79 24.20 22 -9 -1 143.89 27.70 -22 9 -1 97.39 20.40 -22 -9 1 102.49 23.30 22 -9 -1 115.39 20.80 22 9 1 85.39 22.50 22 9 1 115.59 27.20 -22 -9 -1 119.99 26.90 -22 -9 -1 98.79 23.10 22 9 -1 124.59 29.60 -22 9 1 127.69 25.10 22 -9 1 96.19 22.20 22 9 2 60.49 20.60 22 -9 -2 15.90 12.70 22 -9 -2 34.50 16.80 -22 9 -2 23.90 15.10 22 9 2 34.90 15.70 -22 -9 2 61.99 20.90 -22 -9 -2 21.20 16.20 -22 9 2 34.80 16.10 22 -9 2 3.40 12.90 -22 -9 -2 36.40 18.80 22 9 -2 79.29 26.70 22 9 3 56.19 19.40 -22 -9 3 61.69 22.30 -22 9 -3 37.50 16.60 22 -9 -3 44.90 16.90 22 -9 -3 47.20 15.30 -22 -9 3 31.20 12.80 22 -9 -3 44.30 16.90 22 -9 3 39.90 16.70 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16.50 17.70 -22 11 -3 50.29 19.20 22 -11 -3 21.20 14.40 22 -11 -3 80.19 22.10 22 11 3 106.59 23.80 22 11 3 65.59 19.60 -22 -11 3 69.99 18.70 -22 -11 3 72.59 22.80 22 -11 3 33.20 16.70 -22 11 3 28.30 14.80 -22 -11 -3 44.30 20.60 -22 -11 -3 47.90 23.20 22 11 -3 64.09 25.20 22 11 4 -2.50 11.70 -22 -11 4 15.90 11.40 22 -11 -4 -8.00 10.50 22 -11 -4 -10.30 10.50 22 11 4 1.10 12.10 22 -11 -4 -28.80 10.00 -22 -11 4 33.00 18.80 -22 11 -4 1.10 14.10 22 11 -4 2.90 15.10 22 -11 4 14.80 13.00 -22 11 4 13.90 10.00 -22 11 4 28.30 16.30 -22 -11 -4 29.80 19.80 -22 -11 -4 -25.70 14.00 -22 12 0 172.88 29.00 22 -12 0 171.68 32.20 22 -12 0 185.48 28.60 22 12 0 210.88 37.40 -22 -12 0 183.88 30.50 22 12 0 233.88 38.60 -22 -12 0 213.98 37.60 22 12 1 3.90 15.00 22 12 1 18.50 15.90 22 -12 -1 28.70 14.20 -22 -12 1 20.50 19.90 22 -12 -1 4.00 12.10 -22 12 -1 -6.60 12.10 -22 -12 -1 -7.00 13.30 22 -12 1 10.70 14.20 -22 -12 -1 12.50 16.90 22 12 -1 1.90 16.50 22 12 -1 7.90 15.20 -22 12 1 5.20 10.90 22 -12 -2 97.29 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8.60 12.80 23 0 -5 2.20 12.00 -23 0 -5 4.30 14.50 -23 0 5 5.10 13.10 -23 0 5 13.70 13.50 -23 0 -6 -31.10 11.80 -23 0 6 6.50 14.20 23 0 6 -11.30 12.30 -23 0 -6 8.10 14.90 23 0 6 -8.30 11.80 23 0 -6 7.70 12.90 -23 0 6 16.90 13.60 -23 0 -7 28.40 15.00 23 0 7 -6.90 11.90 -23 0 7 18.90 15.20 -23 0 7 -11.30 10.20 -23 0 7 -15.30 9.90 23 0 7 -8.00 11.30 23 0 -7 -4.60 11.20 23 1 0 148.69 25.90 -23 -1 0 142.99 25.60 -23 -1 0 139.69 21.80 -23 1 0 111.79 22.00 23 -1 0 142.89 24.60 23 1 0 113.49 19.90 23 -1 -1 99.29 21.00 -23 -1 1 102.79 22.40 23 1 1 122.99 23.50 23 -1 -1 109.09 20.60 -23 1 -1 95.59 21.40 23 1 1 101.49 17.40 -23 -1 -1 68.09 20.10 -23 1 1 114.09 19.20 23 -1 1 100.29 18.30 23 -1 1 114.59 22.30 -23 1 1 83.89 21.40 23 1 -1 87.79 20.40 23 -1 -2 144.79 19.60 -23 -1 2 108.59 23.20 23 -1 -2 78.39 19.50 -23 1 -2 129.59 24.60 23 1 2 128.29 19.60 -23 1 -2 128.69 21.10 -23 -1 2 125.79 21.90 23 1 2 119.69 22.80 23 1 2 132.19 19.50 23 -1 -2 98.59 20.80 23 1 -2 121.69 24.90 -23 -1 -2 124.59 19.30 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169.88 25.00 24 -3 4 40.90 14.70 -24 -3 -4 96.69 24.90 24 -3 4 102.09 21.10 24 3 5 32.40 17.70 24 -3 -5 12.80 13.70 24 -3 -5 37.40 18.40 24 3 5 23.30 14.80 -24 -3 5 45.30 16.80 -24 3 -5 11.40 14.20 -24 -3 5 21.80 13.40 -24 -3 5 31.60 16.90 24 3 -5 67.09 19.50 -24 -3 -5 31.90 19.60 -24 3 5 18.60 14.50 -24 -3 -5 33.90 16.40 -24 3 5 50.19 17.10 24 -3 5 -3.00 13.00 24 -3 5 83.39 19.00 24 3 -5 41.10 17.30 24 -3 -6 27.20 14.40 -24 -3 6 42.60 17.90 -24 3 -6 34.10 17.00 24 3 6 28.40 17.90 -24 -3 6 51.59 16.90 -24 -3 6 20.20 14.90 24 3 6 69.99 22.00 24 3 -6 9.30 15.80 -24 3 6 65.09 18.10 -24 -3 -6 46.70 17.40 24 -3 6 76.09 19.80 24 -3 6 35.20 14.90 -24 -3 -6 60.79 23.60 -24 3 6 73.99 21.70 24 3 -6 67.99 20.20 -24 -4 0 183.38 28.00 -24 4 0 135.69 25.30 24 -4 0 136.79 23.90 -24 -4 0 163.88 27.90 24 -4 0 109.99 22.50 24 4 0 157.88 27.70 24 4 0 166.18 22.90 24 -4 -1 1.60 11.00 -24 -4 1 2.50 12.30 -24 4 -1 3.30 13.10 24 4 1 10.70 10.30 -24 -4 1 -7.30 10.90 24 4 1 26.40 16.20 -24 -4 -1 0.70 12.40 -24 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260.67 37.00 -25 6 -1 31.80 15.70 25 6 1 45.50 19.70 -25 -6 1 28.20 15.80 -25 -6 1 37.40 17.00 25 6 1 74.49 17.60 25 -6 -1 35.20 16.00 -25 -6 -1 3.90 13.00 -25 6 1 57.29 18.90 25 -6 1 37.10 14.60 25 -6 1 44.30 16.80 25 6 -1 58.49 21.30 -25 -6 -1 23.90 18.20 25 -6 -2 175.08 28.90 25 -6 -2 138.69 22.70 25 6 2 155.98 30.10 -25 -6 2 141.69 27.70 -25 -6 2 139.09 27.00 25 6 2 96.29 22.60 -25 6 -2 131.89 25.80 -25 6 -2 136.49 23.50 -25 6 2 107.19 23.90 -25 -6 -2 173.78 31.90 25 -6 2 105.59 24.30 25 6 -2 242.98 40.20 25 -6 2 153.28 27.20 -25 -6 3 54.89 18.80 25 -6 -3 84.39 18.30 25 6 3 66.69 21.20 -25 -6 3 71.99 20.20 25 -6 -3 64.09 21.50 25 6 3 55.99 17.90 -25 6 -3 27.50 14.60 25 -6 3 41.00 16.20 25 6 -3 76.79 26.00 -25 -6 -3 68.39 24.00 25 -6 3 65.39 19.40 -25 6 3 58.19 20.20 25 6 4 239.88 38.00 -25 -6 4 206.38 29.30 -25 6 -4 114.09 25.50 25 -6 -4 187.78 28.10 -25 -6 4 202.58 29.90 25 -6 -4 181.78 31.50 25 6 4 261.47 35.80 -25 -6 4 241.18 36.00 -25 6 4 203.38 33.50 25 -6 4 174.58 30.50 25 6 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24.90 13.10 30 2 -1 1.70 10.30 -30 2 1 5.40 14.10 30 -2 -2 -4.40 13.70 30 2 2 11.70 16.70 -30 -2 2 19.70 12.80 -30 -2 2 16.20 15.60 -30 2 -2 -11.00 13.80 30 2 -2 27.90 13.90 30 -2 2 19.90 12.60 -30 2 2 0.90 14.90 30 2 -2 4.40 15.90 30 -2 2 0.60 15.40 -30 -2 -2 28.70 19.30 -30 -2 3 10.40 14.00 -30 -2 3 36.20 14.50 -30 2 -3 23.90 18.10 30 -2 -3 11.90 13.60 30 2 3 16.10 14.20 30 -2 3 30.10 16.00 -30 2 3 33.30 17.50 30 2 -3 -13.00 11.70 -30 -2 -3 22.10 16.60 -30 2 3 30.60 17.40 30 -3 0 19.20 12.60 -30 -3 0 17.30 19.10 30 -3 0 22.80 12.40 30 3 0 62.99 23.30 -30 3 0 37.30 19.20 30 -3 -1 2.80 12.30 -30 3 -1 5.60 17.50 -30 -3 1 0.10 17.10 30 3 1 14.30 17.40 -30 -3 1 -1.00 12.80 30 -3 1 0.60 11.60 -30 -3 -1 12.30 18.30 -30 3 1 27.40 18.60 30 -3 1 17.40 12.50 30 3 -1 8.40 10.20 30 3 -1 2.90 15.60 30 -3 -2 69.49 21.10 -30 -3 2 88.29 23.10 -30 3 -2 40.60 20.40 30 3 2 78.09 23.70 -30 -3 2 38.70 15.80 -30 3 2 73.59 22.50 -30 -3 -2 56.29 20.90 30 -3 2 73.79 18.60 30 3 -2 60.49 21.70 30 -3 2 50.89 19.20 -30 3 -3 4.10 16.00 30 -3 -3 -4.50 11.70 -30 -3 3 -0.30 11.20 -30 -3 3 -14.00 12.30 30 3 3 5.40 15.60 -30 3 3 -3.50 13.30 30 3 -3 2.80 12.70 30 -3 3 1.00 10.30 30 -3 3 -30.40 11.50 -30 -3 -3 -12.10 17.30 -30 4 0 -4.30 13.50 30 4 0 29.70 20.40 -30 -4 0 3.60 17.10 30 -4 0 -1.80 12.60 -30 4 -1 102.89 25.30 -30 -4 1 167.48 28.90 -30 -4 1 132.39 28.90 30 -4 -1 132.49 26.10 30 4 1 188.18 35.60 -30 4 1 132.89 28.60 30 -4 1 84.09 22.50 -30 -4 -1 92.79 26.10 30 4 -1 170.48 35.50 30 -4 1 78.79 18.50 30 -4 -2 4.50 12.70 30 4 2 24.10 18.20 -30 4 -2 -1.00 13.70 -30 -4 2 41.70 16.20 -30 -4 2 5.90 15.30 -30 4 2 5.90 15.60 30 4 -2 -14.70 16.70 30 -4 2 6.60 11.30 30 -4 2 16.90 14.10 -30 -4 -2 6.80 15.40 -30 4 -3 37.10 17.20 -30 -4 3 25.50 17.20 30 -4 -3 33.70 16.70 -30 -4 3 45.40 16.40 30 4 3 107.79 25.20 30 -4 3 17.80 13.80 -30 4 3 14.40 15.00 30 -4 3 43.70 18.70 30 4 -3 66.39 24.00 -30 -4 -3 49.20 19.60 -30 5 0 5.30 15.40 -30 -5 0 -6.70 16.50 30 5 0 -5.60 15.00 30 -5 0 4.50 12.60 -30 5 -1 2.10 14.80 30 5 1 34.70 17.10 -30 -5 1 4.60 15.90 30 -5 -1 14.20 14.20 -30 -5 1 58.99 17.40 -30 5 1 19.70 15.50 30 -5 1 18.60 14.00 -30 -5 -1 -4.80 16.90 30 5 -1 22.80 19.30 30 5 2 39.80 17.60 30 -5 -2 18.60 14.10 -30 -5 2 0.20 15.90 -30 5 -2 46.90 19.00 -30 -5 2 -3.20 11.00 -30 5 2 16.10 16.60 -30 -5 -2 -3.70 15.80 30 -5 2 -0.80 9.60 30 5 -2 26.40 17.10 30 -5 2 7.60 12.10 -30 6 0 0.40 15.40 30 6 0 -27.10 14.20 30 -6 0 8.50 14.50 -30 -6 0 -3.20 12.20 -30 -6 0 17.70 17.90 30 -6 -1 70.99 19.90 30 6 1 101.89 24.70 -30 -6 1 68.69 24.40 -30 6 -1 57.29 19.10 -30 -6 1 88.49 23.80 30 -6 1 52.49 16.80 -30 -6 -1 72.59 24.10 30 6 -1 64.69 23.80 -30 6 1 62.09 21.40 -30 -6 2 -1.50 9.80 30 -6 -2 9.00 13.80 30 -6 2 3.00 11.90 30 6 -2 18.30 17.70 30 -7 0 -12.10 10.90 30 7 0 1.50 12.20 -30 7 0 29.20 14.80 -30 -7 0 -13.00 9.90 -30 -7 0 -20.30 14.90 -31 0 0 -9.50 14.80 31 0 0 -8.30 10.50 31 0 0 -11.50 12.90 -31 0 -1 12.90 15.10 31 0 -1 3.70 11.60 31 0 1 7.80 14.00 -31 0 1 -19.10 14.50 31 0 -1 -7.60 12.50 31 0 1 -0.40 13.60 -31 0 -2 -5.60 15.40 31 0 2 20.90 16.30 31 0 -2 2.60 11.30 -31 0 2 -9.80 15.00 31 0 -2 14.60 11.50 31 -1 0 85.19 24.20 31 1 0 57.99 17.80 -31 1 0 89.89 24.00 -31 -1 0 86.79 26.20 31 -1 0 62.89 18.70 31 1 0 80.49 23.00 -31 1 -1 19.60 17.70 -31 -1 1 16.50 17.10 31 -1 -1 -1.20 10.80 31 -1 -1 18.40 13.50 31 1 1 19.30 15.80 31 1 -1 12.30 12.10 31 -1 1 1.40 13.20 -31 -1 -1 -5.40 15.70 -31 1 1 7.80 14.70 31 1 -1 14.80 18.50 31 -1 1 12.90 12.00 31 -1 -2 55.89 19.90 31 1 2 134.29 27.10 -31 1 -2 77.79 23.30 -31 -1 2 69.49 23.60 31 1 -2 97.79 26.30 -31 -1 -2 88.39 24.20 31 1 -2 91.79 21.60 -31 1 2 99.89 24.70 31 -1 2 105.99 23.80 31 -2 0 11.30 10.60 31 -2 0 -1.90 12.50 -31 -2 0 19.20 18.00 -31 2 0 -2.20 14.20 31 2 0 -15.60 14.50 -31 -2 1 110.89 27.40 31 -2 -1 97.59 22.90 31 2 1 147.39 31.40 -31 2 -1 104.89 25.30 31 2 -1 94.79 20.90 -31 2 1 122.99 28.50 31 2 -1 174.08 33.60 -31 -2 -1 145.59 31.20 31 -2 1 105.59 22.60 31 -2 1 107.69 25.30 -31 2 -2 6.50 14.60 -31 -2 2 -3.50 9.40 -31 -2 2 7.90 15.40 31 -2 -2 15.10 13.60 31 2 2 9.10 14.10 -31 2 2 25.80 17.80 31 -2 2 8.70 9.30 -31 -2 -2 -6.90 16.00 31 2 -2 4.60 10.80 31 -2 2 -11.70 10.70 31 2 -2 -11.30 12.70 -31 -3 0 10.80 16.30 31 -3 0 6.60 10.90 31 3 0 4.00 15.70 -31 3 0 3.50 12.70 -31 -3 1 36.30 19.70 31 -3 -1 27.80 14.10 31 3 1 41.20 18.00 -31 3 -1 -15.20 12.60 31 -3 1 -10.80 10.20 31 -3 1 21.80 13.20 -31 3 1 3.40 14.70 31 3 -1 8.30 15.70 -31 -3 -1 14.20 18.00 -31 3 -2 30.40 16.50 31 3 2 24.10 15.10 -31 -3 2 3.10 11.60 -31 -3 2 -0.90 15.70 31 -3 -2 2.20 10.80 -31 3 2 2.30 13.30 -31 -3 -2 -4.40 18.40 31 -3 2 7.00 11.30 31 3 -2 -21.00 12.90 31 -3 2 -4.00 14.10 -31 4 0 -10.90 12.30 31 -4 0 4.00 12.50 31 4 0 -0.30 14.70 -31 -4 0 -3.20 15.10 31 4 1 22.20 15.80 -31 -4 1 25.60 18.60 -31 4 -1 2.80 14.70 31 -4 -1 11.70 12.30 31 4 -1 10.40 15.00 31 -4 1 6.60 12.00 31 -4 1 10.30 14.10 -31 4 1 15.30 15.30 -31 -4 -1 9.30 16.30 31 5 0 13.20 16.30 -31 5 0 -11.90 11.80 31 -5 0 8.10 11.80 -31 -5 0 31.40 19.80 31 5 1 19.40 13.70 31 -5 -1 -21.30 8.90 -31 -5 1 42.70 17.00 31 -5 1 -7.30 11.20 -31 -5 -1 20.70 17.40 31 5 -1 3.70 14.50 32 0 0 23.80 12.30 32 0 0 -3.50 11.50 -32 0 0 -10.40 15.60 32 0 -1 63.89 16.20 -32 0 1 76.69 24.20 32 0 1 78.49 22.10 32 0 -1 56.79 18.00 -32 0 -1 97.59 26.70 32 1 0 24.90 15.80 32 1 0 7.50 13.80 -32 1 0 -13.70 14.00 32 -1 0 24.60 13.60 32 -1 0 -3.40 14.30 -32 -1 0 16.80 19.00 32 1 1 -26.90 10.90 -32 -1 1 2.40 17.00 32 -1 -1 3.70 11.30 -32 1 -1 -3.70 14.70 32 -1 -1 -9.40 11.60 32 -1 1 14.00 11.30 32 -1 1 -14.30 12.10 32 1 -1 5.90 15.50 32 1 -1 6.30 12.10 -32 -1 -1 -4.50 13.40 -32 1 1 2.00 13.60 32 2 0 31.20 16.90 32 -2 0 24.30 13.50 32 -2 0 18.50 13.30 -32 2 0 42.20 17.80 -32 -2 0 36.50 19.00 32 -2 -1 -10.10 10.60 32 2 -1 9.10 11.70 32 -2 1 4.20 10.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 78409 _shelx_res_file ; TITL 21Sep17_AP1_a.res in Pna2(1) 21Sep17_AP1_a.res created by SHELXL-2016/6 at 04:58:21 on 13-Jun-2018 CELL 0.71073 24.2914 14.3317 7.5014 90.000 90.000 90.000 ZERR 4.000 0.0017 0.0010 0.0005 0.000 0.000 0.000 LATT -1 SYMM -X, -Y, 1/2+Z SYMM 1/2+X, 1/2-Y, Z SYMM 1/2-X, 1/2+Y, 1/2+Z SFAC C H Br Fe UNIT 136 96 8 4 L.S. 10 ACTA BOND $H FMAP 2 DFIX 1.86 0.02 C15 BR1A FLAT C12 C13 C14 C15 C16 C17 BR1A PLAN 20 SIZE 0.083 0.14 0.19 TEMP -173 WGHT 0.033300 3.964700 FVAR 0.33722 0.83925 PART 1 21.00 BR1 3 0.660625 0.922330 0.173412 21.00000 0.05121 0.02593 = 0.05650 0.00105 0.01293 -0.00575 PART 2 -21.00 BR1A 3 0.514801 0.014898 0.144390 -21.00000 0.04212 0.04245 = 0.05848 -0.00560 -0.00503 -0.00720 PART 0 BR1' 3 0.772818 0.888889 0.612504 11.00000 0.03175 0.05007 = 0.04217 0.00744 0.00225 -0.00679 FE1 4 0.594005 0.452413 0.602722 11.00000 0.01923 0.04396 = 0.01699 0.00425 -0.00004 0.00620 C1 1 0.568607 0.547236 0.412802 11.00000 0.01989 0.05064 = 0.02003 0.00549 -0.00206 0.00862 C2 1 0.580821 0.458204 0.336607 11.00000 0.02092 0.04580 = 0.01745 0.00330 -0.00048 0.00820 AFIX 43 H2 2 0.608217 0.446759 0.248916 11.00000 -1.20000 AFIX 0 C3 1 0.545229 0.388466 0.413130 11.00000 0.02285 0.04890 = 0.02022 0.00737 -0.00211 0.00634 C4 1 0.512299 0.435922 0.543301 11.00000 0.01909 0.04495 = 0.02308 0.00621 0.00209 0.00121 AFIX 43 H4 2 0.485344 0.407651 0.617479 11.00000 -1.20000 AFIX 0 C5 1 0.526284 0.530499 0.543357 11.00000 0.01904 0.06137 = 0.02050 0.00607 0.00027 0.01444 AFIX 43 H5 2 0.510318 0.576675 0.618071 11.00000 -1.20000 AFIX 0 C6 1 0.591949 0.637041 0.364648 11.00000 0.02174 0.04466 = 0.01770 0.00169 -0.00518 0.01114 C7 1 0.641134 0.644012 0.269225 11.00000 0.02590 0.04701 = 0.02657 0.00511 0.00375 0.00287 AFIX 43 H7 2 0.660541 0.588559 0.239819 11.00000 -1.20000 AFIX 0 C8 1 0.662274 0.728068 0.216731 11.00000 0.02641 0.05462 = 0.03503 0.00611 0.00113 0.00609 AFIX 43 H8 2 0.696148 0.731057 0.153696 11.00000 -1.20000 AFIX 0 C9 1 0.633611 0.808406 0.256806 11.00000 0.03903 0.04601 = 0.03649 0.00923 -0.00161 -0.00003 PART 2 -21 AFIX 43 H9 2 0.647462 0.866911 0.217657 -21.00000 -1.20000 AFIX 0 PART 0 C10 1 0.584883 0.805377 0.353310 11.00000 0.03480 0.04412 = 0.04008 0.00223 -0.00285 0.00935 AFIX 43 H10 2 0.565861 0.861300 0.382097 11.00000 -1.20000 AFIX 0 C11 1 0.564609 0.720647 0.406453 11.00000 0.03259 0.04405 = 0.02864 0.00300 0.00345 0.00174 AFIX 43 H11 2 0.531359 0.718346 0.472983 11.00000 -1.20000 AFIX 0 C12 1 0.540293 0.290824 0.361522 11.00000 0.02963 0.04739 = 0.02214 0.00547 -0.00547 0.00450 C13 1 0.493026 0.238378 0.406998 11.00000 0.02675 0.06044 = 0.03822 0.00591 -0.00164 0.00012 AFIX 43 H13 2 0.465195 0.266712 0.477610 11.00000 -1.20000 AFIX 0 C14 1 0.486224 0.148597 0.352665 11.00000 0.03808 0.05651 = 0.06770 -0.00594 -0.00199 -0.01095 AFIX 43 H14 2 0.453349 0.115966 0.381278 11.00000 -1.20000 AFIX 0 C15 1 0.527431 0.104551 0.255153 11.00000 0.04816 0.05468 = 0.05223 -0.00985 -0.00457 -0.00992 PART 1 21 AFIX 43 H15 2 0.522978 0.041609 0.218143 21.00000 -1.20000 AFIX 0 PART 0 C16 1 0.574981 0.152936 0.212310 11.00000 0.04792 0.04481 = 0.03353 -0.00709 0.00198 0.00644 AFIX 43 H16 2 0.603479 0.122737 0.147555 11.00000 -1.20000 AFIX 0 C17 1 0.581049 0.244022 0.262893 11.00000 0.02674 0.05410 = 0.02869 0.00746 0.00302 0.00396 AFIX 43 H17 2 0.613640 0.276524 0.230570 11.00000 -1.20000 AFIX 0 C1' 1 0.661959 0.508313 0.728836 11.00000 0.02084 0.04559 = 0.02203 0.00168 -0.00473 0.00172 C2' 1 0.674954 0.421656 0.648079 11.00000 0.01819 0.05041 = 0.01736 -0.00054 -0.00143 0.00831 AFIX 43 H2' 2 0.702109 0.412482 0.558641 11.00000 -1.20000 AFIX 0 C3' 1 0.640617 0.349727 0.722640 11.00000 0.02187 0.04449 = 0.01697 0.00428 -0.00173 0.00412 C4' 1 0.605470 0.395470 0.847627 11.00000 0.02461 0.04337 = 0.01707 0.00705 -0.00198 0.00432 AFIX 43 H4' 2 0.577765 0.365716 0.916606 11.00000 -1.20000 AFIX 0 C5' 1 0.617964 0.490678 0.853237 11.00000 0.02486 0.04446 = 0.01804 0.00061 -0.00035 0.00257 AFIX 43 H5' 2 0.600468 0.535922 0.926426 11.00000 -1.20000 AFIX 0 C6' 1 0.687889 0.598815 0.695808 11.00000 0.02135 0.05072 = 0.01753 0.00449 -0.00281 0.00474 C7' 1 0.736923 0.606234 0.596444 11.00000 0.02843 0.04481 = 0.03117 0.00168 0.00165 0.00629 AFIX 43 H7' 2 0.752997 0.551791 0.546345 11.00000 -1.20000 AFIX 0 C8' 1 0.762046 0.692456 0.570928 11.00000 0.02337 0.05849 = 0.03181 0.01099 0.00082 0.00446 AFIX 43 H8' 2 0.795343 0.697049 0.505082 11.00000 -1.20000 AFIX 0 C9' 1 0.738158 0.770594 0.641949 11.00000 0.02882 0.05039 = 0.02617 0.00424 -0.00174 -0.00324 C10' 1 0.689495 0.766215 0.736473 11.00000 0.03104 0.04661 = 0.03353 -0.00496 0.00631 0.00288 AFIX 43 H10' 2 0.673468 0.821246 0.784335 11.00000 -1.20000 AFIX 0 C11' 1 0.664555 0.681017 0.760344 11.00000 0.02672 0.04589 = 0.03293 -0.00130 0.01072 -0.00176 AFIX 43 H11' 2 0.630518 0.678081 0.822461 11.00000 -1.20000 AFIX 0 C12' 1 0.642653 0.250409 0.680152 11.00000 0.02552 0.04818 = 0.01975 0.00463 -0.00362 0.00833 C13' 1 0.602106 0.188760 0.745355 11.00000 0.03963 0.04720 = 0.03406 -0.00070 0.00730 0.00466 AFIX 43 H13' 2 0.572269 0.212889 0.813014 11.00000 -1.20000 AFIX 0 C14' 1 0.604960 0.092463 0.712272 11.00000 0.05098 0.04379 = 0.06071 0.00006 0.01177 0.00156 AFIX 43 H14' 2 0.577072 0.052326 0.757026 11.00000 -1.20000 AFIX 0 C15' 1 0.648051 0.055850 0.615116 11.00000 0.05846 0.04553 = 0.04405 0.00348 0.00120 0.00633 AFIX 43 H15' 2 0.650562 -0.009517 0.595725 11.00000 -1.20000 AFIX 0 C16' 1 0.687842 0.115620 0.545720 11.00000 0.05529 0.05128 = 0.03689 -0.00678 -0.00087 0.01760 AFIX 43 H16' 2 0.717118 0.091094 0.476041 11.00000 -1.20000 AFIX 0 C17' 1 0.684937 0.210583 0.577787 11.00000 0.02841 0.05417 = 0.02541 0.00698 -0.00113 0.00357 AFIX 43 H17' 2 0.712463 0.250117 0.528919 11.00000 -1.20000 AFIX 0 HKLF 4 REM 21Sep17_AP1_a.res in Pna2(1) REM R1 = 0.0461 for 5283 Fo > 4sig(Fo) and 0.0637 for all 6454 data REM 344 parameters refined using 6 restraints END WGHT 0.0333 3.9709 REM Highest difference peak 1.444, deepest hole -0.766, 1-sigma level 0.087 Q1 1 0.6038 0.5076 0.6106 11.00000 0.05 1.44 Q2 1 0.6303 -0.0279 0.6105 11.00000 0.05 0.65 Q3 1 0.6685 0.7794 0.2426 11.00000 0.05 0.46 Q4 1 0.7755 0.9392 0.6221 11.00000 0.05 0.44 Q5 1 0.6318 0.4413 0.5483 11.00000 0.05 0.44 Q6 1 0.6578 0.9213 0.0455 11.00000 0.05 0.42 Q7 1 0.8097 0.9181 0.6721 11.00000 0.05 0.41 Q8 1 0.7355 0.8601 0.6639 11.00000 0.05 0.41 Q9 1 0.7682 0.8906 0.7402 11.00000 0.05 0.39 Q10 1 0.6543 0.9202 0.2982 11.00000 0.05 0.39 Q11 1 0.7684 0.8805 0.4864 11.00000 0.05 0.38 Q12 1 0.8120 0.8617 0.5985 11.00000 0.05 0.38 Q13 1 0.6253 0.5005 0.7358 11.00000 0.05 0.36 Q14 1 0.6733 0.9028 0.1624 11.00000 0.05 0.36 Q15 1 0.5204 0.5198 0.6721 11.00000 0.05 0.36 Q16 1 0.6367 -0.0790 0.6469 11.00000 0.05 0.36 Q17 1 0.6000 0.7191 0.6075 11.00000 0.05 0.36 Q18 1 0.5566 0.4808 0.6165 11.00000 0.05 0.35 Q19 1 0.6275 0.8834 0.1296 11.00000 0.05 0.35 Q20 1 0.5985 0.4454 0.4901 11.00000 0.05 0.35 ; _shelx_res_checksum 36803 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br Br1 0.66063(4) 0.92233(6) 0.17341(14) 0.0445(3) Uani d 0.839(2) A 1 Br Br1A 0.51480(18) 0.0149(3) 0.1444(7) 0.0477(17) Uani d 0.161(2) A 2 Br Br1' 0.77282(3) 0.88889(5) 0.61250(11) 0.04133(18) Uani d 1.0 . . Fe Fe1 0.59400(3) 0.45241(6) 0.60272(13) 0.02673(19) Uani d 1.0 . . C C1 0.5686(2) 0.5472(5) 0.4128(8) 0.0302(15) Uani d 1.0 . . C C2 0.5808(3) 0.4582(5) 0.3366(8) 0.0281(14) Uani d 1.0 . . H H2 0.608217 0.446759 0.248916 0.034 Uiso calc 1.0 . . C C3 0.5452(3) 0.3885(5) 0.4131(8) 0.0307(15) Uani d 1.0 . . C C4 0.5123(2) 0.4359(5) 0.5433(9) 0.0290(14) Uani d 1.0 . . H H4 0.485344 0.407651 0.617479 0.035 Uiso calc 1.0 . . C C5 0.5263(2) 0.5305(5) 0.5434(9) 0.0336(16) Uani d 1.0 . . H H5 0.510318 0.576675 0.618071 0.04 Uiso calc 1.0 . . C C6 0.5919(2) 0.6370(5) 0.3646(8) 0.0280(14) Uani d 1.0 . . C C7 0.6411(3) 0.6440(5) 0.2692(9) 0.0332(15) Uani d 1.0 . . H H7 0.660541 0.588559 0.239819 0.04 Uiso calc 1.0 . . C C8 0.6623(3) 0.7281(5) 0.2167(10) 0.0387(17) Uani d 1.0 . . H H8 0.696148 0.731057 0.153696 0.046 Uiso calc 1.0 . . C C9 0.6336(3) 0.8084(5) 0.2568(10) 0.0405(17) Uani d 1.0 . . H H9 0.647462 0.866911 0.217657 0.049 Uiso calc 0.161(2) A 2 C C10 0.5849(3) 0.8054(5) 0.3533(10) 0.0397(17) Uani d 1.0 . . H H10 0.565861 0.8613 0.382097 0.048 Uiso calc 1.0 . . C C11 0.5646(3) 0.7206(5) 0.4065(9) 0.0351(16) Uani d 1.0 . . H H11 0.531359 0.718346 0.472983 0.042 Uiso calc 1.0 . . C C12 0.5403(3) 0.2908(5) 0.3615(8) 0.0331(15) Uani d 1.0 . . C C13 0.4930(3) 0.2384(6) 0.4070(10) 0.0418(18) Uani d 1.0 . . H H13 0.465195 0.266712 0.47761 0.05 Uiso calc 1.0 . . C C14 0.4862(3) 0.1486(6) 0.3527(12) 0.054(2) Uani d 1.0 . . H H14 0.453349 0.115966 0.381278 0.065 Uiso calc 1.0 . . C C15 0.5274(3) 0.1046(6) 0.2552(12) 0.052(2) Uani d 1.0 . . H H15 0.522978 0.041609 0.218143 0.062 Uiso calc 0.839(2) A 1 C C16 0.5750(3) 0.1529(5) 0.2123(10) 0.0421(18) Uani d 1.0 . . H H16 0.603479 0.122737 0.147555 0.051 Uiso calc 1.0 . . C C17 0.5810(3) 0.2440(6) 0.2629(9) 0.0365(16) Uani d 1.0 . . H H17 0.61364 0.276524 0.23057 0.044 Uiso calc 1.0 . . C C1' 0.6620(3) 0.5083(5) 0.7288(8) 0.0295(14) Uani d 1.0 . . C C2' 0.6750(2) 0.4217(5) 0.6481(8) 0.0287(14) Uani d 1.0 . . H H2' 0.702109 0.412482 0.558641 0.034 Uiso calc 1.0 . . C C3' 0.6406(2) 0.3497(5) 0.7226(8) 0.0278(14) Uani d 1.0 . . C C4' 0.6055(3) 0.3955(5) 0.8476(8) 0.0284(14) Uani d 1.0 . . H H4' 0.577765 0.365716 0.916606 0.034 Uiso calc 1.0 . . C C5' 0.6180(3) 0.4907(5) 0.8532(8) 0.0291(14) Uani d 1.0 . . H H5' 0.600468 0.535922 0.926426 0.035 Uiso calc 1.0 . . C C6' 0.6879(2) 0.5988(5) 0.6958(8) 0.0299(14) Uani d 1.0 . . C C7' 0.7369(2) 0.6062(5) 0.5964(11) 0.0348(14) Uani d 1.0 . . H H7' 0.752997 0.551791 0.546345 0.042 Uiso calc 1.0 . . C C8' 0.7620(3) 0.6925(5) 0.5709(9) 0.0379(18) Uani d 1.0 . . H H8' 0.795343 0.697049 0.505082 0.045 Uiso calc 1.0 . . C C9' 0.7382(3) 0.7706(5) 0.6419(8) 0.0351(16) Uani d 1.0 . . C C10' 0.6895(3) 0.7662(5) 0.7365(9) 0.0371(16) Uani d 1.0 . . H H10' 0.673468 0.821246 0.784335 0.044 Uiso calc 1.0 . . C C11' 0.6646(3) 0.6810(5) 0.7603(9) 0.0352(16) Uani d 1.0 . . H H11' 0.630518 0.678081 0.822461 0.042 Uiso calc 1.0 . . C C12' 0.6427(2) 0.2504(5) 0.6802(8) 0.0311(14) Uani d 1.0 . . C C13' 0.6021(3) 0.1888(5) 0.7454(10) 0.0403(17) Uani d 1.0 . . H H13' 0.572269 0.212889 0.813014 0.048 Uiso calc 1.0 . . C C14' 0.6050(3) 0.0925(6) 0.7123(13) 0.052(2) Uani d 1.0 . . H H14' 0.577072 0.052326 0.757026 0.062 Uiso calc 1.0 . . C C15' 0.6481(3) 0.0558(5) 0.6151(13) 0.0493(18) Uani d 1.0 . . H H15' 0.650562 -0.009517 0.595725 0.059 Uiso calc 1.0 . . C C16' 0.6878(4) 0.1156(6) 0.5457(10) 0.048(2) Uani d 1.0 . . H H16' 0.717118 0.091094 0.476041 0.057 Uiso calc 1.0 . . C C17' 0.6849(3) 0.2106(5) 0.5778(9) 0.0360(17) Uani d 1.0 . . H H17' 0.712463 0.250117 0.528919 0.043 Uiso calc 1.0 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Br1 0.0512(5) 0.0259(4) 0.0565(6) -0.0057(4) 0.0129(4) 0.0011(4) Br1A 0.042(3) 0.042(3) 0.058(4) -0.0072(19) -0.005(2) -0.006(2) Br1' 0.0317(3) 0.0501(4) 0.0422(4) -0.0068(3) 0.0022(4) 0.0074(4) Fe1 0.0192(4) 0.0440(5) 0.0170(3) 0.0062(3) 0.0000(4) 0.0042(5) C1 0.020(3) 0.051(4) 0.020(3) 0.009(3) -0.002(2) 0.005(3) C2 0.021(3) 0.046(4) 0.017(3) 0.008(3) 0.000(2) 0.003(3) C3 0.023(3) 0.049(4) 0.020(3) 0.006(3) -0.002(2) 0.007(3) C4 0.019(3) 0.045(4) 0.023(3) 0.001(3) 0.002(2) 0.006(3) C5 0.019(3) 0.061(5) 0.021(3) 0.014(3) 0.000(2) 0.006(3) C6 0.022(3) 0.045(4) 0.018(3) 0.011(3) -0.005(2) 0.002(3) C7 0.026(3) 0.047(4) 0.027(3) 0.003(3) 0.004(3) 0.005(3) C8 0.026(3) 0.055(4) 0.035(4) 0.006(3) 0.001(3) 0.006(3) C9 0.039(4) 0.046(4) 0.036(4) 0.000(3) -0.002(3) 0.009(3) C10 0.035(4) 0.044(4) 0.040(4) 0.009(3) -0.003(3) 0.002(3) C11 0.033(4) 0.044(4) 0.029(3) 0.002(3) 0.003(3) 0.003(3) C12 0.030(4) 0.047(4) 0.022(3) 0.004(3) -0.005(3) 0.005(3) C13 0.027(3) 0.060(5) 0.038(4) 0.000(3) -0.002(3) 0.006(4) C14 0.038(4) 0.057(5) 0.068(6) -0.011(4) -0.002(4) -0.006(5) C15 0.048(5) 0.055(5) 0.052(5) -0.010(4) -0.005(4) -0.010(4) C16 0.048(4) 0.045(4) 0.034(4) 0.006(4) 0.002(3) -0.007(3) C17 0.027(3) 0.054(5) 0.029(4) 0.004(3) 0.003(3) 0.007(3) C1' 0.021(3) 0.046(4) 0.022(3) 0.002(3) -0.005(2) 0.002(3) C2' 0.018(3) 0.050(4) 0.017(3) 0.008(3) -0.001(2) -0.001(3) C3' 0.022(3) 0.044(4) 0.017(3) 0.004(3) -0.002(2) 0.004(3) C4' 0.025(3) 0.043(4) 0.017(3) 0.004(3) -0.002(2) 0.007(3) C5' 0.025(3) 0.044(4) 0.018(3) 0.003(3) 0.000(2) 0.001(3) C6' 0.021(3) 0.051(4) 0.018(3) 0.005(3) -0.003(2) 0.004(3) C7' 0.028(3) 0.045(4) 0.031(3) 0.006(3) 0.002(3) 0.002(4) C8' 0.023(3) 0.058(5) 0.032(5) 0.004(3) 0.001(3) 0.011(3) C9' 0.029(3) 0.050(4) 0.026(4) -0.003(3) -0.002(3) 0.004(3) C10' 0.031(4) 0.047(4) 0.034(4) 0.003(3) 0.006(3) -0.005(3) C11' 0.027(3) 0.046(4) 0.033(4) -0.002(3) 0.011(3) -0.001(3) C12' 0.026(3) 0.048(4) 0.020(3) 0.008(3) -0.004(3) 0.005(3) C13' 0.040(4) 0.047(4) 0.034(4) 0.005(3) 0.007(3) -0.001(3) C14' 0.051(5) 0.044(5) 0.061(6) 0.002(4) 0.012(4) 0.000(4) C15' 0.058(4) 0.046(4) 0.044(4) 0.006(4) 0.001(5) 0.003(4) C16' 0.055(5) 0.051(5) 0.037(4) 0.018(4) -0.001(4) -0.007(4) C17' 0.028(3) 0.054(4) 0.025(4) 0.004(3) -0.001(3) 0.007(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C2 Fe1 C4' 158.6(3) C2 Fe1 C5 68.5(3) C4' Fe1 C5 121.9(3) C2 Fe1 C5' 160.4(3) C4' Fe1 C5' 40.2(3) C5 Fe1 C5' 106.5(3) C2 Fe1 C2' 109.0(2) C4' Fe1 C2' 68.3(2) C5 Fe1 C2' 158.6(3) C5' Fe1 C2' 68.3(2) C2 Fe1 C4 68.7(3) C4' Fe1 C4 106.5(3) C5 Fe1 C4 40.0(3) C5' Fe1 C4 120.5(3) C2' Fe1 C4 160.7(3) C2 Fe1 C3' 123.1(3) C4' Fe1 C3' 40.8(2) C5 Fe1 C3' 158.4(3) C5' Fe1 C3' 68.5(3) C2' Fe1 C3' 41.0(3) C4 Fe1 C3' 123.0(3) C2 Fe1 C1 40.9(3) C4' Fe1 C1 158.6(3) C5 Fe1 C1 41.1(2) C5' Fe1 C1 122.9(3) C2' Fe1 C1 123.0(3) C4 Fe1 C1 68.6(3) C3' Fe1 C1 159.2(2) C2 Fe1 C1' 124.2(3) C4' Fe1 C1' 68.4(3) C5 Fe1 C1' 122.2(3) C5' Fe1 C1' 41.1(2) C2' Fe1 C1' 40.4(3) C4 Fe1 C1' 156.9(3) C3' Fe1 C1' 68.8(3) C1 Fe1 C1' 107.5(3) C2 Fe1 C3 41.2(3) C4' Fe1 C3 121.6(3) C5 Fe1 C3 68.3(3) C5' Fe1 C3 156.4(3) C2' Fe1 C3 124.8(3) C4 Fe1 C3 40.8(3) C3' Fe1 C3 107.4(3) C1 Fe1 C3 69.2(3) C1' Fe1 C3 161.2(3) C2 C1 C5 105.8(6) C2 C1 C6 127.6(6) C5 C1 C6 126.6(6) C2 C1 Fe1 68.0(4) C5 C1 Fe1 68.5(4) C6 C1 Fe1 129.7(4) C1 C2 C3 109.6(6) C1 C2 Fe1 71.0(4) C3 C2 Fe1 70.9(3) C1 C2 H2 125.2 C3 C2 H2 125.2 Fe1 C2 H2 124.4 C4 C3 C2 106.1(6) C4 C3 C12 126.2(6) C2 C3 C12 127.6(6) C4 C3 Fe1 68.9(4) C2 C3 Fe1 67.8(4) C12 C3 Fe1 131.0(5) C5 C4 C3 108.9(6) C5 C4 Fe1 69.7(4) C3 C4 Fe1 70.3(4) C5 C4 H4 125.5 C3 C4 H4 125.5 Fe1 C4 H4 126.1 C4 C5 C1 109.6(6) C4 C5 Fe1 70.4(4) C1 C5 Fe1 70.4(3) C4 C5 H5 125.2 C1 C5 H5 125.2 Fe1 C5 H5 125.7 C7 C6 C11 117.2(6) C7 C6 C1 121.7(6) C11 C6 C1 121.0(6) C8 C7 C6 122.1(7) C8 C7 H7 118.9 C6 C7 H7 118.9 C7 C8 C9 118.9(7) C7 C8 H8 120.6 C9 C8 H8 120.6 C8 C9 C10 121.2(7) C8 C9 Br1 118.7(6) C10 C9 Br1 120.1(6) C8 C9 H9 119.4 C10 C9 H9 119.4 C11 C10 C9 119.1(7) C11 C10 H10 120.5 C9 C10 H10 120.5 C10 C11 C6 121.4(6) C10 C11 H11 119.3 C6 C11 H11 119.3 C17 C12 C13 116.4(7) C17 C12 C3 122.7(6) C13 C12 C3 120.9(6) C14 C13 C12 122.0(7) C14 C13 H13 119.0 C12 C13 H13 119.0 C13 C14 C15 120.0(8) C13 C14 H14 120.0 C15 C14 H14 120.0 C16 C15 C14 119.7(8) C16 C15 Br1A 116.9(7) C14 C15 Br1A 120.8(7) C16 C15 H15 120.2 C14 C15 H15 120.2 C17 C16 C15 120.2(7) C17 C16 H16 119.9 C15 C16 H16 119.9 C16 C17 C12 121.7(7) C16 C17 H17 119.2 C12 C17 H17 119.2 C2' C1' C5' 106.8(6) C2' C1' C6' 127.5(6) C5' C1' C6' 125.8(6) C2' C1' Fe1 69.0(3) C5' C1' Fe1 68.6(4) C6' C1' Fe1 127.6(4) C1' C2' C3' 109.4(5) C1' C2' Fe1 70.6(3) C3' C2' Fe1 70.2(3) C1' C2' H2' 125.3 C3' C2' H2' 125.3 Fe1 C2' H2' 125.5 C4' C3' C2' 105.8(6) C4' C3' C12' 127.7(6) C2' C3' C12' 126.4(6) C4' C3' Fe1 68.3(3) C2' C3' Fe1 68.8(3) C12' C3' Fe1 128.2(4) C5' C4' C3' 109.8(6) C5' C4' Fe1 70.4(4) C3' C4' Fe1 70.9(3) C5' C4' H4' 125.1 C3' C4' H4' 125.1 Fe1 C4' H4' 125.2 C4' C5' C1' 108.2(6) C4' C5' Fe1 69.4(4) C1' C5' Fe1 70.3(4) C4' C5' H5' 125.9 C1' C5' H5' 125.9 Fe1 C5' H5' 126.0 C11' C6' C7' 117.6(6) C11' C6' C1' 121.0(6) C7' C6' C1' 121.4(6) C8' C7' C6' 120.7(6) C8' C7' H7' 119.7 C6' C7' H7' 119.7 C9' C8' C7' 119.1(6) C9' C8' H8' 120.4 C7' C8' H8' 120.4 C8' C9' C10' 121.7(6) C8' C9' Br1' 119.7(5) C10' C9' Br1' 118.6(5) C11' C10' C9' 119.0(7) C11' C10' H10' 120.5 C9' C10' H10' 120.5 C10' C11' C6' 121.7(6) C10' C11' H11' 119.1 C6' C11' H11' 119.1 C17' C12' C13' 116.5(7) C17' C12' C3' 122.7(6) C13' C12' C3' 120.8(6) C14' C13' C12' 121.3(7) C14' C13' H13' 119.3 C12' C13' H13' 119.3 C15' C14' C13' 120.3(8) C15' C14' H14' 119.8 C13' C14' H14' 119.8 C14' C15' C16' 119.4(8) C14' C15' H15' 120.3 C16' C15' H15' 120.3 C17' C16' C15' 120.3(7) C17' C16' H16' 119.8 C15' C16' H16' 119.8 C16' C17' C12' 122.2(7) C16' C17' H17' 118.9 C12' C17' H17' 118.9 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Br1 C9 1.868(8) Br1A C15 1.561(9) Br1' C9' 1.906(7) Fe1 C2 2.023(6) Fe1 C4' 2.029(6) Fe1 C5 2.039(6) Fe1 C5' 2.042(6) Fe1 C2' 2.044(5) Fe1 C4 2.048(6) Fe1 C3' 2.063(6) Fe1 C1 2.063(6) Fe1 C1' 2.064(6) Fe1 C3 2.066(7) C1 C2 1.429(10) C1 C5 1.440(9) C1 C6 1.452(10) C2 C3 1.441(9) C2 H2 0.95 C3 C4 1.434(9) C3 C12 1.457(10) C4 C5 1.397(10) C4 H4 0.95 C5 H5 0.95 C6 C7 1.396(9) C6 C11 1.405(9) C7 C8 1.367(10) C7 H7 0.95 C8 C9 1.379(10) C8 H8 0.95 C9 C10 1.388(10) C9 H9 0.95 C10 C11 1.370(10) C10 H10 0.95 C11 H11 0.95 C12 C17 1.406(9) C12 C13 1.414(10) C13 C14 1.360(12) C13 H13 0.95 C14 C15 1.391(12) C14 H14 0.95 C15 C16 1.385(11) C15 H15 0.95 C16 C17 1.367(11) C16 H16 0.95 C17 H17 0.95 C1' C2' 1.417(9) C1' C5' 1.441(9) C1' C6' 1.463(9) C2' C3' 1.439(9) C2' H2' 0.95 C3' C4' 1.427(9) C3' C12' 1.459(9) C4' C5' 1.398(9) C4' H4' 0.95 C5' H5' 0.95 C6' C11' 1.394(9) C6' C7' 1.409(9) C7' C8' 1.391(10) C7' H7' 0.95 C8' C9' 1.369(10) C8' H8' 0.95 C9' C10' 1.380(9) C10' C11' 1.375(10) C10' H10' 0.95 C11' H11' 0.95 C12' C17' 1.404(9) C12' C13' 1.411(10) C13' C14' 1.404(11) C13' H13' 0.95 C14' C15' 1.379(11) C14' H14' 0.95 C15' C16' 1.393(12) C15' H15' 0.95 C16' C17' 1.384(11) C16' H16' 0.95 C17' H17' 0.95 _cod_database_fobs_code 1550945