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Information card for entry 1550733
Preview
| Coordinates | 1550733.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H61 K1.5 N4 O10 Rh0.5 Sn6 |
|---|---|
| Calculated formula | C30 H61 K1.5 N4 O10 Rh0.5 Sn6 |
| Title of publication | Synthesis and Structure of a Family of Rhodium Polystannide Clusters [Rh@Sn10]3‒, [Rh@Sn12]3‒, [Rh2@Sn17]6‒ and the First Triply-Fused Stannide, [Rh3@Sn24]5‒ |
| Authors of publication | Liu, Chao; Jin, Xiao; Li, Leijiao; Xu, Jun; McGrady, John E.; Sun, Zhong-Ming |
| Journal of publication | Chemical Science |
| Year of publication | 2019 |
| a | 27.302 ± 0.005 Å |
| b | 17.503 ± 0.003 Å |
| c | 21.667 ± 0.004 Å |
| α | 90° |
| β | 97.132 ± 0.004° |
| γ | 90° |
| Cell volume | 10274 ± 3 Å3 |
| Cell temperature | 120 ± 2 K |
| Ambient diffraction temperature | 120 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0711 |
| Residual factor for significantly intense reflections | 0.0477 |
| Weighted residual factors for significantly intense reflections | 0.115 |
| Weighted residual factors for all reflections included in the refinement | 0.1254 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.057 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 214073 (current) | 2019-03-12 | cif/ Adding structures of 1550730, 1550731, 1550732, 1550733, 1550734 via cif-deposit CGI script. |
1550733.cif |
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Users of the data should acknowledge the original authors of the
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