Crystallography Open Database

Information card for entry 1517869

Preview

Coordinates	1517869.cif

Structure parameters

Formula	C12 H36 Li N Si5
Calculated formula	C12 Li N Si5
SMILES	[Si]([Si](C)(C)C)([Si](C)(C)C)([Si](C)(C)C)[N]1([Si](C)(C)C)[Li][N]([Si](C)(C)C)([Si]([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)[Li]1
Title of publication	Tris(trimethylsilyl)silylamine and the lithiated and silylated derivatives - X-ray structure of the dimeric lithium trimethylsilyl-[tris(trimethylsilyl)silyl]amide
Authors of publication	Westerhausen, Matthias; Schwarz, Wolfgang
Journal of publication	Zeitschrift fuer Anorganische und Allgemeine Chemie
Year of publication	1993
Journal volume	619
Pages of publication	1053 - 1063
a	13.867 ± 0.002 Å
b	20.402 ± 0.003 Å
c	16.096 ± 0.002 Å
α	90°
β	96.95 ± 0.01°
γ	90°
Cell volume	4520.3 ± 1.1 Å³
Ambient diffraction temperature	173 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.0496
Weighted residual factors for significantly intense reflections	0.0513
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1517869.cif
124455	2014-10-01	cif/ Adding structures of 1517869 via cif-deposit CGI script.	1517869.cif